NMR Restraints Grid |
Result table
image | mrblock_id | pdb_id | bmrb_id | cing | stage | position | program | type | subtype | subsubtype |
576478 | 2mou | 19952 | cing | 1-original | 1 | XPLOR/CNS | distance | NOE | simple |
assign ( resid 103 and name HN ) ( resid 102 and name HB# ) 3.7 1.9 1.5 volume=0.441 peak=1851 ppm1=8.451 ppm2=1.275 assign ( resid 185 and name HB1 ) ( resid 185 and name HA ) 3.2 1.5 1.3 volume=0.971 peak=2601 ppm1=2.155 ppm2=3.895 assign ( resid 199 and name HB# ) ( resid 200 and name HG2 or resid 200 and name HG1 ) 3.2 1.4 1.3 volume=1.078 peak=4974 ppm1=0.692 ppm2=1.104 assign ( resid 76 and name HE1 ) ( resid 197 and name HD1# ) 2.7 1.0 1.1 volume=2.734 peak=2917 ppm1=2.862 ppm2=0.771 assign ( resid 192 and name HD1# ) ( resid 189 and name HA ) 3.9 2.2 1.6 volume=0.301 peak=4190 ppm1=0.494 ppm2=4.679 assign ( resid 91 and name HG2# ) ( resid 116 and name HB2 ) 2.7 1.0 1.1 volume=2.659 peak=4361 ppm1=1.018 ppm2=2.862 assign ( resid 76 and name HA ) ( resid 76 and name HB1 ) 4.1 2.4 1.6 volume=0.223 peak=3394 ppm1=4.124 ppm2=2.006 assign ( resid 204 and name HB1 ) ( resid 204 and name HG2 ) 3.4 1.7 1.4 volume=0.672 peak=3800 ppm1=1.710 ppm2=1.318 assign ( resid 153 and name HB2 ) ( resid 152 and name HA2 ) 3.3 1.6 1.3 volume=0.830 peak=3765 ppm1=2.853 ppm2=3.834 assign ( resid 54 and name HG2# ) ( resid 200 and name HD1 ) 2.9 1.2 1.2 volume=1.715 peak=2762 ppm1=0.576 ppm2=1.552 assign ( resid 203 and name HA ) ( resid 204 and name HB2 ) 4.4 2.7 1.6 volume=0.143 peak=3246 ppm1=2.830 ppm2=1.622 assign ( resid 196 and name HA ) ( resid 54 and name HD1# ) 4.8 3.1 1.2 volume=0.087 peak=4935 ppm1=3.453 ppm2=0.493 assign ( resid 200 and name HG2 ) ( resid 200 and name HE1 ) 2.9 1.2 1.2 volume=1.644 peak=4578 ppm1=1.132 ppm2=2.790 assign ( resid 155 and name HB1 ) ( resid 155 and name HN ) 4.0 2.3 1.6 volume=0.270 peak=4084 ppm1=3.009 ppm2=8.985 assign ( resid 93 and name HG2# ) ( resid 93 and name HB ) 3.3 1.6 1.3 volume=0.776 peak=3657 ppm1=-0.014 ppm2=1.226 assign ( resid 72 and name HN ) ( resid 71 and name HB1 ) 3.4 1.7 1.4 volume=0.684 peak=534 ppm1=7.537 ppm2=1.531 assign ( resid 134 and name HB2 ) ( resid 134 and name HE1 or resid 134 and name HE2 ) 4.2 2.5 1.7 volume=0.190 peak=4877 ppm1=2.953 ppm2=7.140 assign ( resid 174 and name HN ) ( resid 147 and name HD1 or resid 147 and name HD2 ) 3.6 1.9 1.5 volume=0.462 peak=1569 ppm1=9.153 ppm2=6.220 assign ( resid 183 and name HA ) ( resid 183 and name HG11 ) 3.0 1.3 1.2 volume=1.519 peak=2506 ppm1=3.918 ppm2=1.268 assign ( resid 112 and name HG2# ) ( resid 134 and name HD1 or resid 134 and name HD2 ) 3.7 1.9 1.5 volume=0.441 peak=4061 ppm1=0.676 ppm2=6.859 assign ( resid 128 and name HN ) ( resid 129 and name HN ) 4.0 2.3 1.6 volume=0.245 peak=1418 ppm1=9.931 ppm2=8.722 assign ( resid 132 and name HG2# ) ( resid 93 and name HG2# ) 3.9 2.2 1.6 volume=0.298 peak=3767 ppm1=0.936 ppm2=-0.012 assign ( resid 64 and name HB2 or resid 64 and name HB1 ) ( resid 60 and name HD1 ) 4.2 2.5 1.7 volume=0.198 peak=4166 ppm1=3.019 ppm2=1.557 assign ( resid 106 and name HG2# ) ( resid 109 and name HD2 ) 3.1 1.3 1.2 volume=1.298 peak=4031 ppm1=0.897 ppm2=3.155 assign ( resid 199 and name HA ) ( resid 203 and name HG2# ) 4.4 2.7 1.6 volume=0.147 peak=4093 ppm1=2.796 ppm2=0.319 assign ( resid 130 and name HG2 ) ( resid 130 and name HB2 ) 3.5 1.8 1.4 volume=0.574 peak=2856 ppm1=1.309 ppm2=1.830 assign ( resid 34 and name HN ) ( resid 30 and name HN ) 3.7 2.0 1.5 volume=0.406 peak=1091 ppm1=8.136 ppm2=8.700 assign ( resid 98 and name HG2# ) ( resid 110 and name HN ) 4.1 2.3 1.6 volume=0.239 peak=3773 ppm1=1.321 ppm2=8.771 assign ( resid 196 and name HD1# ) ( resid 51 and name HA ) 4.3 2.6 1.7 volume=0.173 peak=2945 ppm1=0.730 ppm2=5.588 assign ( resid 201 and name HN ) ( resid 200 and name HN ) 3.1 1.4 1.2 volume=1.162 peak=2020 ppm1=7.404 ppm2=8.048 assign ( resid 98 and name HG2# ) ( resid 99 and name HG1 ) 3.9 2.2 1.6 volume=0.302 peak=2931 ppm1=1.318 ppm2=2.440 assign ( resid 140 and name HN ) ( resid 140 and name HA ) 2.9 1.2 1.2 volume=1.662 peak=1331 ppm1=9.582 ppm2=4.801 assign ( resid 199 and name HB# ) ( resid 64 and name HD1 or resid 64 and name HD2 ) 3.3 1.6 1.3 volume=0.822 peak=3083 ppm1=0.691 ppm2=5.982 assign ( resid 54 and name HD1# ) ( resid 54 and name HG12 ) 2.6 0.9 1.0 volume=3.398 peak=3077 ppm1=0.491 ppm2=1.205 assign ( resid 74 and name HN ) ( resid 73 and name HN ) 2.7 0.9 1.1 volume=3.014 peak=245 ppm1=6.491 ppm2=7.523 assign ( resid 200 and name HN ) ( resid 198 and name HA ) 3.6 1.9 1.4 volume=0.491 peak=2075 ppm1=8.085 ppm2=4.525 assign ( resid 203 and name HD1# ) ( resid 62 and name HN ) 4.2 2.5 1.7 volume=0.201 peak=3160 ppm1=-0.010 ppm2=8.128 assign ( resid 205 and name HB# ) ( resid 205 and name HA ) 4.6 2.9 1.4 volume=0.115 peak=2761 ppm1=1.300 ppm2=4.151 assign ( resid 87 and name HG11 ) ( resid 93 and name HD1# ) 4.2 2.4 1.7 volume=0.207 peak=4817 ppm1=1.265 ppm2=-0.280 assign ( resid 12 and name HN ) ( resid 12 and name HG1 ) 2.8 1.1 1.1 volume=2.185 peak=1527 ppm1=7.549 ppm2=2.449 assign ( resid 134 and name HB2 ) ( resid 112 and name HG2# ) 5.2 3.4 0.8 volume=0.057 peak=4954 ppm1=2.956 ppm2=0.596 assign ( resid 20 and name HN ) ( resid 21 and name HN ) 3.5 1.8 1.4 volume=0.597 peak=804 ppm1=7.409 ppm2=8.303 assign ( resid 51 and name HA ) ( resid 49 and name HG1 or resid 49 and name HG2 ) 4.4 2.7 1.6 volume=0.152 peak=2523 ppm1=5.622 ppm2=1.559 assign ( resid 70 and name HB1 ) ( resid 74 and name HD1 ) 4.0 2.3 1.6 volume=0.270 peak=3194 ppm1=2.588 ppm2=6.953 assign ( resid 91 and name HA ) ( resid 91 and name HG2# ) 3.9 2.1 1.5 volume=0.325 peak=4034 ppm1=5.876 ppm2=1.017 assign ( resid 21 and name HN ) ( resid 20 and name HN ) 3.9 2.2 1.6 volume=0.286 peak=278 ppm1=8.286 ppm2=7.403 assign ( resid 187 and name HN ) ( resid 184 and name HN ) 2.8 1.1 1.1 volume=2.278 peak=2173 ppm1=7.600 ppm2=7.522 assign ( resid 99 and name HN ) ( resid 99 and name HG1 ) 3.3 1.6 1.3 volume=0.855 peak=1692 ppm1=7.801 ppm2=2.441 assign ( resid 46 and name HB2 ) ( resid 45 and name HN ) 4.1 2.4 1.6 volume=0.226 peak=4328 ppm1=2.050 ppm2=6.635 assign ( resid 93 and name HN ) ( resid 93 and name HG11 ) 3.2 1.5 1.3 volume=0.955 peak=2360 ppm1=8.905 ppm2=0.623 assign ( resid 136 and name HN ) ( resid 137 and name HB1 ) 3.8 2.1 1.5 volume=0.352 peak=2175 ppm1=6.893 ppm2=2.773 assign ( resid 106 and name HD1# ) ( resid 187 and name HB ) 4.1 2.4 1.7 volume=0.216 peak=3360 ppm1=0.772 ppm2=4.143 assign ( resid 159 and name HN ) ( resid 159 and name HA ) 2.9 1.2 1.2 volume=1.732 peak=509 ppm1=9.025 ppm2=3.755 assign ( resid 109 and name HB2 ) ( resid 106 and name HG2# ) 4.0 2.3 1.6 volume=0.245 peak=5147 ppm1=1.719 ppm2=0.896 assign ( resid 191 and name HN ) ( resid 191 and name HB2 ) 2.8 1.1 1.1 volume=2.070 peak=2282 ppm1=7.651 ppm2=2.704 assign ( resid 153 and name HB1 ) ( resid 127 and name HG12 ) 2.8 1.1 1.1 volume=2.030 peak=4596 ppm1=2.853 ppm2=0.977 assign ( resid 136 and name HA ) ( resid 136 and name HB1 ) 2.8 1.0 1.1 volume=2.433 peak=3370 ppm1=3.787 ppm2=1.755 assign ( resid 194 and name HA ) ( resid 197 and name HB2 ) 3.4 1.6 1.3 volume=0.741 peak=4778 ppm1=4.323 ppm2=1.762 assign ( resid 14 and name HB ) ( resid 16 and name HN ) 3.5 1.7 1.4 volume=0.620 peak=4771 ppm1=1.713 ppm2=7.484 assign ( resid 52 and name HN ) ( resid 53 and name HN ) 3.8 2.0 1.5 volume=0.385 peak=1477 ppm1=8.620 ppm2=8.315 assign ( resid 167 and name HA ) ( resid 167 and name HG ) 3.5 1.8 1.4 volume=0.566 peak=3505 ppm1=5.218 ppm2=0.921 assign ( resid 78 and name HN ) ( resid 78 and name HG ) 2.7 1.0 1.1 volume=2.797 peak=830 ppm1=7.149 ppm2=1.258 assign ( resid 41 and name HG2 or resid 41 and name HG1 ) ( resid 42 and name HN ) 3.9 2.1 1.5 volume=0.320 peak=4495 ppm1=1.538 ppm2=8.706 assign ( resid 112 and name HD1# ) ( resid 134 and name HE1 or resid 134 and name HE2 ) 3.8 2.1 1.5 volume=0.356 peak=2892 ppm1=0.372 ppm2=7.154 assign ( resid 86 and name HB2 ) ( resid 87 and name HN ) 4.2 2.5 1.7 volume=0.183 peak=4556 ppm1=1.554 ppm2=8.070 assign ( resid 168 and name HG1# ) ( resid 168 and name HB ) 2.5 0.8 1.0 volume=4.433 peak=4339 ppm1=0.767 ppm2=1.729 assign ( resid 164 and name HN ) ( resid 163 and name HN ) 3.0 1.3 1.2 volume=1.558 peak=1901 ppm1=7.977 ppm2=7.387 assign ( resid 87 and name HA ) ( resid 87 and name HN ) 3.6 1.8 1.4 volume=0.530 peak=5096 ppm1=3.871 ppm2=8.037 assign ( resid 76 and name HE2 ) ( resid 76 and name HD2 ) 1.9 0.2 0.8 volume=20.908 peak=4072 ppm1=2.912 ppm2=1.548 assign ( resid 203 and name HG2# ) ( resid 203 and name HA ) 3.2 1.5 1.3 volume=1.033 peak=4469 ppm1=0.340 ppm2=2.838 assign ( resid 203 and name HD1# ) ( resid 202 and name HA1 ) 3.6 1.8 1.4 volume=0.521 peak=3913 ppm1=-0.011 ppm2=3.051 assign ( resid 180 and name HB2 ) ( resid 183 and name HN ) 3.5 1.8 1.4 volume=0.587 peak=4436 ppm1=3.883 ppm2=7.468 assign ( resid 68 and name HN ) ( resid 69 and name HN ) 3.5 1.8 1.4 volume=0.557 peak=2269 ppm1=8.024 ppm2=8.212 assign ( resid 130 and name HG2 ) ( resid 130 and name HD1 ) 2.7 1.0 1.1 volume=2.525 peak=5123 ppm1=1.306 ppm2=1.653 assign ( resid 179 and name HN ) ( resid 178 and name HA ) 2.6 0.9 1.1 volume=3.112 peak=1574 ppm1=7.304 ppm2=4.277 assign ( resid 73 and name HG2# ) ( resid 72 and name HN ) 3.1 1.4 1.2 volume=1.227 peak=3101 ppm1=1.217 ppm2=7.543 assign ( resid 6 and name HD1# ) ( resid 6 and name HN ) 3.2 1.5 1.3 volume=0.936 peak=3770 ppm1=0.796 ppm2=7.740 assign ( resid 74 and name HN ) ( resid 74 and name HA ) 3.0 1.3 1.2 volume=1.513 peak=2024 ppm1=6.493 ppm2=4.793 assign ( resid 114 and name HB1 ) ( resid 114 and name HB2 ) 4.5 2.8 1.5 volume=0.129 peak=3927 ppm1=1.063 ppm2=1.704 assign ( resid 112 and name HD1# ) ( resid 111 and name HB1 ) 3.6 1.8 1.4 volume=0.522 peak=2638 ppm1=0.371 ppm2=2.881 assign ( resid 124 and name HB2 or resid 124 and name HB1 ) ( resid 124 and name HA ) 4.0 2.3 1.6 volume=0.266 peak=2685 ppm1=2.048 ppm2=5.140 assign ( resid 79 and name HN ) ( resid 78 and name HD2# ) 3.4 1.7 1.4 volume=0.689 peak=2160 ppm1=8.843 ppm2=0.489 assign ( resid 42 and name HN ) ( resid 42 and name HA ) 3.7 2.0 1.5 volume=0.431 peak=1369 ppm1=8.699 ppm2=4.136 assign ( resid 87 and name HG12 ) ( resid 91 and name HB ) 4.1 2.4 1.6 volume=0.218 peak=4434 ppm1=1.049 ppm2=3.633 assign ( resid 102 and name HN ) ( resid 101 and name HA ) 3.7 2.0 1.5 volume=0.399 peak=1380 ppm1=8.523 ppm2=4.658 assign ( resid 15 and name HB2 ) ( resid 15 and name HD1# ) 4.3 2.6 1.7 volume=0.170 peak=5108 ppm1=1.368 ppm2=0.442 assign ( resid 199 and name HB# ) ( resid 54 and name HB ) 3.1 1.3 1.2 volume=1.333 peak=4184 ppm1=0.692 ppm2=1.750 assign ( resid 160 and name HN ) ( resid 160 and name HA ) 2.8 1.1 1.1 volume=2.259 peak=2028 ppm1=8.833 ppm2=4.014 assign ( resid 84 and name HG2# ) ( resid 93 and name HD1# ) 3.7 1.9 1.5 volume=0.453 peak=4582 ppm1=0.112 ppm2=-0.271 assign ( resid 106 and name HG12 ) ( resid 179 and name HG ) 2.4 0.6 0.9 volume=6.320 peak=4735 ppm1=1.412 ppm2=1.614 assign ( resid 154 and name HG2# ) ( resid 15 and name HD1# ) 3.1 1.4 1.2 volume=1.219 peak=4082 ppm1=0.840 ppm2=0.444 assign ( resid 166 and name HG1 ) ( resid 166 and name HE1 ) 4.4 2.7 1.6 volume=0.141 peak=4906 ppm1=1.208 ppm2=2.705 assign ( resid 112 and name HD1# ) ( resid 96 and name HN ) 4.0 2.3 1.6 volume=0.253 peak=3893 ppm1=0.371 ppm2=8.460 assign ( resid 184 and name HD1# ) ( resid 184 and name HN ) 3.2 1.5 1.3 volume=0.938 peak=2981 ppm1=0.894 ppm2=7.509 assign ( resid 117 and name HN ) ( resid 116 and name HN ) 4.0 2.3 1.6 volume=0.247 peak=345 ppm1=8.231 ppm2=8.829 assign ( resid 126 and name HD1# ) ( resid 126 and name HG11 or resid 126 and name HG12 ) 2.8 1.1 1.1 volume=2.076 peak=4386 ppm1=0.348 ppm2=1.024 assign ( resid 92 and name HN ) ( resid 91 and name HN ) 3.4 1.6 1.3 volume=0.738 peak=1008 ppm1=9.456 ppm2=7.217 assign ( resid 20 and name HB1 or resid 20 and name HB2 ) ( resid 19 and name HB1 ) 4.0 2.3 1.6 volume=0.266 peak=4046 ppm1=2.715 ppm2=1.745 assign ( resid 121 and name HG1 ) ( resid 121 and name HA ) 4.3 2.5 1.7 volume=0.178 peak=3491 ppm1=2.310 ppm2=4.147 assign ( resid 207 and name HN ) ( resid 206 and name HB1 ) 3.6 1.8 1.4 volume=0.536 peak=379 ppm1=7.834 ppm2=2.962 assign ( resid 5 and name HA ) ( resid 9 and name HN ) 4.5 2.7 1.5 volume=0.135 peak=3940 ppm1=4.023 ppm2=7.998 assign ( resid 127 and name HN ) ( resid 127 and name HG12 ) 3.2 1.5 1.3 volume=1.052 peak=1406 ppm1=9.380 ppm2=1.021 assign ( resid 97 and name HN ) ( resid 97 and name HG2# ) 3.1 1.4 1.3 volume=1.128 peak=950 ppm1=8.362 ppm2=0.228 assign ( resid 169 and name HB2 ) ( resid 50 and name HG1# ) 3.3 1.6 1.3 volume=0.875 peak=4640 ppm1=1.787 ppm2=0.644 assign ( resid 186 and name HN ) ( resid 185 and name HN ) 3.1 1.3 1.2 volume=1.303 peak=1617 ppm1=7.371 ppm2=8.179 assign ( resid 10 and name HN ) ( resid 12 and name HN ) 4.0 2.3 1.6 volume=0.251 peak=316 ppm1=8.316 ppm2=7.538 assign ( resid 203 and name HD1# ) ( resid 64 and name HB2 ) 3.5 1.7 1.4 volume=0.627 peak=4011 ppm1=-0.010 ppm2=2.981 assign ( resid 183 and name HA ) ( resid 183 and name HN ) 3.4 1.7 1.4 volume=0.639 peak=3313 ppm1=3.918 ppm2=7.424 assign ( resid 8 and name HA ) ( resid 7 and name HB# ) 3.2 1.5 1.3 volume=1.052 peak=3978 ppm1=3.837 ppm2=0.753 assign ( resid 184 and name HN ) ( resid 183 and name HG12 ) 3.2 1.4 1.3 volume=1.080 peak=1230 ppm1=7.500 ppm2=1.531 assign ( resid 7 and name HB# ) ( resid 6 and name HB ) 3.1 1.4 1.2 volume=1.176 peak=4057 ppm1=0.752 ppm2=1.750 assign ( resid 53 and name HN ) ( resid 53 and name HA ) 3.4 1.6 1.3 volume=0.736 peak=2438 ppm1=8.306 ppm2=4.918 assign ( resid 193 and name HN ) ( resid 189 and name HA ) 3.6 1.9 1.5 volume=0.457 peak=645 ppm1=7.621 ppm2=4.659 assign ( resid 73 and name HB ) ( resid 72 and name HG11 ) 3.0 1.3 1.2 volume=1.387 peak=4600 ppm1=4.300 ppm2=1.170 assign ( resid 93 and name HG2# ) ( resid 114 and name HG ) 3.7 2.0 1.5 volume=0.417 peak=2907 ppm1=-0.013 ppm2=0.971 assign ( resid 19 and name HN ) ( resid 20 and name HB1 ) 3.7 2.0 1.5 volume=0.423 peak=1169 ppm1=7.481 ppm2=2.705 assign ( resid 194 and name HB1 ) ( resid 194 and name HA ) 4.2 2.4 1.7 volume=0.206 peak=4502 ppm1=2.823 ppm2=4.294 assign ( resid 74 and name HN ) ( resid 73 and name HB ) 2.7 1.0 1.1 volume=2.577 peak=1494 ppm1=6.494 ppm2=4.270 assign ( resid 132 and name HG1# ) ( resid 93 and name HD1# ) 3.2 1.5 1.3 volume=0.979 peak=4401 ppm1=0.543 ppm2=-0.271 assign ( resid 203 and name HD1# ) ( resid 57 and name HN ) 4.2 2.5 1.7 volume=0.185 peak=3803 ppm1=-0.010 ppm2=9.239 assign ( resid 35 and name HN ) ( resid 29 and name HA ) 3.3 1.6 1.3 volume=0.815 peak=218 ppm1=9.428 ppm2=5.188 assign ( resid 200 and name HN ) ( resid 200 and name HD1 ) 2.9 1.1 1.1 volume=1.980 peak=1930 ppm1=8.085 ppm2=1.529 assign ( resid 72 and name HN ) ( resid 72 and name HA ) 3.4 1.7 1.4 volume=0.654 peak=2131 ppm1=7.535 ppm2=3.620 assign ( resid 93 and name HG11 ) ( resid 93 and name HB ) 3.4 1.7 1.4 volume=0.680 peak=4762 ppm1=0.688 ppm2=1.224 assign ( resid 217 and name HN ) ( resid 217 and name HB1 ) 3.3 1.6 1.3 volume=0.801 peak=1722 ppm1=8.148 ppm2=2.192 assign ( resid 40 and name HN ) ( resid 47 and name HN ) 3.5 1.8 1.4 volume=0.605 peak=584 ppm1=8.523 ppm2=8.746 assign ( resid 203 and name HD1# ) ( resid 64 and name HD1 or resid 64 and name HD2 ) 4.0 2.2 1.6 volume=0.276 peak=5084 ppm1=-0.009 ppm2=5.921 assign ( resid 166 and name HN ) ( resid 156 and name HB2 ) 3.4 1.7 1.4 volume=0.645 peak=958 ppm1=9.000 ppm2=3.176 assign ( resid 178 and name HA ) ( resid 178 and name HB2 ) 2.8 1.1 1.1 volume=2.252 peak=4041 ppm1=4.275 ppm2=1.664 assign ( resid 153 and name HN ) ( resid 127 and name HG11 or resid 127 and name HG12 ) 3.1 1.4 1.2 volume=1.278 peak=1348 ppm1=9.329 ppm2=1.012 assign ( resid 30 and name HN ) ( resid 33 and name HN ) 2.7 1.0 1.1 volume=2.752 peak=2105 ppm1=8.722 ppm2=8.175 assign ( resid 25 and name HN ) ( resid 25 and name HG1 ) 3.0 1.3 1.2 volume=1.406 peak=2215 ppm1=9.010 ppm2=1.279 assign ( resid 186 and name HG1 ) ( resid 186 and name HN ) 4.0 2.3 1.6 volume=0.274 peak=3304 ppm1=1.479 ppm2=7.381 assign ( resid 197 and name HB2 ) ( resid 197 and name HD1# ) 3.1 1.4 1.2 volume=1.191 peak=2806 ppm1=1.782 ppm2=0.751 assign ( resid 106 and name HA ) ( resid 179 and name HG ) 4.2 2.4 1.7 volume=0.209 peak=4396 ppm1=4.143 ppm2=1.495 assign ( resid 211 and name HN ) ( resid 205 and name HB# ) 3.8 2.1 1.5 volume=0.336 peak=2143 ppm1=8.308 ppm2=1.279 assign ( resid 155 and name HA ) ( resid 155 and name HB1 ) 6.0 4.3 0.0 volume=0.005 peak=4999 ppm1=5.258 ppm2=3.007 assign ( resid 53 and name HN ) ( resid 53 and name HD1# ) 2.6 0.9 1.0 volume=3.397 peak=855 ppm1=8.308 ppm2=0.759 assign ( resid 193 and name HN ) ( resid 192 and name HB2 ) 3.3 1.6 1.3 volume=0.854 peak=455 ppm1=7.622 ppm2=1.392 assign ( resid 134 and name HN ) ( resid 93 and name HD1# ) 3.9 2.1 1.5 volume=0.322 peak=2401 ppm1=8.746 ppm2=-0.279 assign ( resid 73 and name HN ) ( resid 72 and name HD1# ) 3.3 1.6 1.3 volume=0.869 peak=1244 ppm1=7.505 ppm2=0.582 assign ( resid 153 and name HA ) ( resid 127 and name HG12 ) 3.8 2.1 1.5 volume=0.337 peak=4094 ppm1=5.318 ppm2=0.966 assign ( resid 140 and name HN ) ( resid 140 and name HB2 ) 2.8 1.1 1.1 volume=2.338 peak=627 ppm1=9.582 ppm2=4.098 assign ( resid 96 and name HG2# ) ( resid 78 and name HG ) 3.3 1.5 1.3 volume=0.901 peak=2688 ppm1=1.143 ppm2=1.287 assign ( resid 84 and name HG1# ) ( resid 82 and name HB2 ) 3.2 1.5 1.3 volume=0.934 peak=3219 ppm1=0.533 ppm2=2.464 assign ( resid 119 and name HD1 ) ( resid 119 and name HB1 ) 2.8 1.0 1.1 volume=2.449 peak=4925 ppm1=2.902 ppm2=1.406 assign ( resid 88 and name HN ) ( resid 89 and name HA ) 3.4 1.7 1.4 volume=0.660 peak=1540 ppm1=8.595 ppm2=4.141 assign ( resid 137 and name HB1 ) ( resid 134 and name HZ ) 3.6 1.9 1.5 volume=0.458 peak=4169 ppm1=2.805 ppm2=6.636 assign ( resid 166 and name HG1 ) ( resid 166 and name HD2 ) 2.4 0.7 1.0 volume=5.867 peak=4562 ppm1=1.213 ppm2=1.441 assign ( resid 102 and name HB# ) ( resid 104 and name HN ) 4.0 2.3 1.6 volume=0.244 peak=3755 ppm1=1.279 ppm2=8.072 assign ( resid 6 and name HN ) ( resid 5 and name HN ) 3.3 1.6 1.3 volume=0.828 peak=1286 ppm1=7.722 ppm2=7.465 assign ( resid 176 and name HA ) ( resid 176 and name HG2 ) 3.6 1.9 1.5 volume=0.462 peak=3478 ppm1=3.996 ppm2=1.637 assign ( resid 87 and name HN ) ( resid 87 and name HA ) 4.0 2.3 1.6 volume=0.249 peak=216 ppm1=8.041 ppm2=3.874 assign ( resid 167 and name HA ) ( resid 154 and name HN ) 4.4 2.7 1.6 volume=0.150 peak=3117 ppm1=5.218 ppm2=10.022 assign ( resid 165 and name HA ) ( resid 61 and name HD1# ) 3.7 2.0 1.5 volume=0.397 peak=5135 ppm1=5.220 ppm2=0.757 assign ( resid 84 and name HG2# ) ( resid 93 and name HG11 ) 3.2 1.5 1.3 volume=0.924 peak=3530 ppm1=0.111 ppm2=0.688 assign ( resid 137 and name HN ) ( resid 134 and name HN ) 3.7 2.0 1.5 volume=0.427 peak=2385 ppm1=8.050 ppm2=8.744 assign ( resid 202 and name HN ) ( resid 200 and name HB2 ) 3.3 1.6 1.3 volume=0.827 peak=575 ppm1=8.576 ppm2=1.663 assign ( resid 106 and name HG12 ) ( resid 106 and name HA ) 3.8 2.0 1.5 volume=0.383 peak=4023 ppm1=1.408 ppm2=4.164 assign ( resid 192 and name HD1# ) ( resid 192 and name HB1 ) 3.6 1.8 1.4 volume=0.520 peak=4879 ppm1=0.492 ppm2=1.312 assign ( resid 6 and name HD1# ) ( resid 9 and name HN ) 4.3 2.6 1.7 volume=0.171 peak=4377 ppm1=0.794 ppm2=7.989 assign ( resid 143 and name HN ) ( resid 143 and name HA ) 2.5 0.8 1.0 volume=4.660 peak=2095 ppm1=6.899 ppm2=4.662 assign ( resid 10 and name HA ) ( resid 10 and name HG2# ) 3.8 2.0 1.5 volume=0.380 peak=3713 ppm1=3.625 ppm2=1.076 assign ( resid 35 and name HG2# ) ( resid 50 and name HB ) 3.3 1.6 1.3 volume=0.853 peak=2514 ppm1=0.891 ppm2=1.858 assign ( resid 129 and name HN ) ( resid 150 and name HA ) 3.3 1.6 1.3 volume=0.875 peak=948 ppm1=8.718 ppm2=3.996 assign ( resid 26 and name HA ) ( resid 37 and name HN ) 4.1 2.4 1.6 volume=0.231 peak=4581 ppm1=3.979 ppm2=9.696 assign ( resid 205 and name HN ) ( resid 205 and name HA ) 2.5 0.8 1.0 volume=3.938 peak=154 ppm1=7.180 ppm2=4.137 assign ( resid 197 and name HD1# ) ( resid 198 and name HN ) 3.1 1.4 1.2 volume=1.268 peak=4813 ppm1=0.756 ppm2=8.701 assign ( resid 61 and name HN ) ( resid 61 and name HD2# ) 2.6 0.9 1.0 volume=3.658 peak=1215 ppm1=8.716 ppm2=0.756 assign ( resid 196 and name HA ) ( resid 196 and name HB ) 5.2 3.5 0.8 volume=0.053 peak=4205 ppm1=3.454 ppm2=2.269 assign ( resid 125 and name HN ) ( resid 125 and name HA ) 3.6 1.9 1.4 volume=0.519 peak=1846 ppm1=8.773 ppm2=5.572 assign ( resid 115 and name HG1# ) ( resid 115 and name HA ) 4.1 2.4 1.6 volume=0.219 peak=2553 ppm1=0.303 ppm2=4.409 assign ( resid 111 and name HN ) ( resid 96 and name HB ) 4.2 2.5 1.7 volume=0.188 peak=1499 ppm1=8.631 ppm2=3.876 assign ( resid 135 and name HG1 ) ( resid 135 and name HA ) 4.2 2.5 1.7 volume=0.194 peak=4806 ppm1=1.787 ppm2=4.159 assign ( resid 200 and name HE1 ) ( resid 200 and name HG2 ) 2.9 1.2 1.2 volume=1.761 peak=2656 ppm1=2.803 ppm2=1.144 assign ( resid 167 and name HN ) ( resid 168 and name HN ) 2.9 1.2 1.2 volume=1.864 peak=553 ppm1=8.642 ppm2=8.702 assign ( resid 169 and name HA ) ( resid 154 and name HG1# ) 3.6 1.9 1.4 volume=0.489 peak=2641 ppm1=5.233 ppm2=0.908 assign ( resid 184 and name HN ) ( resid 185 and name HN ) 3.1 1.3 1.2 volume=1.283 peak=1820 ppm1=7.501 ppm2=8.176 assign ( resid 144 and name HG12 ) ( resid 144 and name HG2# ) 3.0 1.3 1.2 volume=1.490 peak=4691 ppm1=1.270 ppm2=0.767 assign ( resid 72 and name HA ) ( resid 72 and name HG12 ) 3.7 2.0 1.5 volume=0.434 peak=4951 ppm1=3.634 ppm2=1.039 assign ( resid 106 and name HG2# ) ( resid 100 and name HB1 ) 4.0 2.2 1.6 volume=0.278 peak=4303 ppm1=0.898 ppm2=3.644 assign ( resid 127 and name HB ) ( resid 127 and name HG11 ) 4.0 2.3 1.6 volume=0.257 peak=2736 ppm1=2.058 ppm2=1.048 assign ( resid 76 and name HE1 ) ( resid 194 and name HA ) 3.2 1.5 1.3 volume=0.965 peak=2593 ppm1=2.863 ppm2=4.303 assign ( resid 168 and name HG1# ) ( resid 167 and name HA ) 4.0 2.2 1.6 volume=0.282 peak=4489 ppm1=0.768 ppm2=5.259 assign ( resid 6 and name HA ) ( resid 5 and name HN ) 4.2 2.4 1.7 volume=0.208 peak=4788 ppm1=3.617 ppm2=7.482 assign ( resid 40 and name HA ) ( resid 47 and name HB2 ) 3.8 2.1 1.5 volume=0.362 peak=3525 ppm1=3.988 ppm2=0.827 assign ( resid 70 and name HN ) ( resid 71 and name HN ) 2.9 1.2 1.2 volume=1.657 peak=589 ppm1=8.575 ppm2=7.226 assign ( resid 124 and name HN ) ( resid 124 and name HA ) 3.1 1.4 1.2 volume=1.266 peak=1479 ppm1=6.472 ppm2=5.181 assign ( resid 188 and name HN ) ( resid 188 and name HA ) 3.1 1.3 1.2 volume=1.328 peak=421 ppm1=8.441 ppm2=4.140 assign ( resid 208 and name HG2# ) ( resid 208 and name HA ) 3.8 2.1 1.5 volume=0.374 peak=3324 ppm1=1.137 ppm2=4.405 assign ( resid 3 and name HE1 or resid 3 and name HE2 ) ( resid 132 and name HG2# ) 2.8 1.0 1.1 volume=2.422 peak=124 ppm1=7.212 ppm2=0.930 assign ( resid 110 and name HN ) ( resid 109 and name HG2 ) 3.1 1.4 1.2 volume=1.166 peak=763 ppm1=8.721 ppm2=1.522 assign ( resid 98 and name HN ) ( resid 97 and name HD1# ) 3.4 1.7 1.4 volume=0.649 peak=926 ppm1=9.354 ppm2=0.106 assign ( resid 134 and name HZ ) ( resid 112 and name HG2# ) 2.9 1.2 1.2 volume=1.873 peak=7 ppm1=6.644 ppm2=0.678 assign ( resid 187 and name HN ) ( resid 186 and name HA ) 3.0 1.3 1.2 volume=1.420 peak=1507 ppm1=7.600 ppm2=4.161 assign ( resid 48 and name HN ) ( resid 48 and name HB2 ) 3.4 1.7 1.4 volume=0.637 peak=1335 ppm1=9.287 ppm2=2.680 assign ( resid 7 and name HN ) ( resid 8 and name HN ) 3.2 1.5 1.3 volume=1.039 peak=328 ppm1=8.423 ppm2=7.635 assign ( resid 200 and name HA ) ( resid 203 and name HG2# ) 3.7 2.0 1.5 volume=0.403 peak=4938 ppm1=3.363 ppm2=0.307 assign ( resid 91 and name HN ) ( resid 91 and name HA ) 3.5 1.8 1.4 volume=0.590 peak=2229 ppm1=7.216 ppm2=5.836 assign ( resid 30 and name HN ) ( resid 29 and name HB ) 4.0 2.2 1.6 volume=0.283 peak=1859 ppm1=8.723 ppm2=3.886 assign ( resid 132 and name HB ) ( resid 3 and name HE1 or resid 3 and name HE2 ) 4.0 2.2 1.6 volume=0.275 peak=2518 ppm1=2.283 ppm2=7.211 assign ( resid 154 and name HG1# ) ( resid 154 and name HB ) 2.9 1.2 1.2 volume=1.747 peak=5057 ppm1=0.916 ppm2=2.179 assign ( resid 169 and name HA ) ( resid 154 and name HN ) 4.5 2.8 1.5 volume=0.134 peak=4132 ppm1=5.253 ppm2=10.079 assign ( resid 184 and name HG2# ) ( resid 186 and name HN ) 3.7 2.0 1.5 volume=0.407 peak=2480 ppm1=1.095 ppm2=7.369 assign ( resid 125 and name HN ) ( resid 157 and name HD1 ) 3.3 1.6 1.3 volume=0.809 peak=932 ppm1=8.772 ppm2=3.616 assign ( resid 115 and name HN ) ( resid 115 and name HG1# ) 3.3 1.6 1.3 volume=0.847 peak=238 ppm1=9.052 ppm2=0.297 assign ( resid 203 and name HG11 ) ( resid 203 and name HB ) 3.4 1.7 1.4 volume=0.638 peak=3750 ppm1=0.515 ppm2=0.126 assign ( resid 201 and name HN ) ( resid 202 and name HN ) 3.0 1.3 1.2 volume=1.441 peak=732 ppm1=7.405 ppm2=8.570 assign ( resid 103 and name HG1# ) ( resid 103 and name HA ) 3.0 1.3 1.2 volume=1.385 peak=4164 ppm1=0.878 ppm2=3.687 assign ( resid 167 and name HA ) ( resid 167 and name HD2# ) 3.6 1.8 1.4 volume=0.536 peak=4666 ppm1=5.218 ppm2=0.769 assign ( resid 127 and name HD1# ) ( resid 67 and name HG1 ) 4.1 2.4 1.6 volume=0.233 peak=2851 ppm1=0.284 ppm2=2.640 assign ( resid 65 and name HD1# ) ( resid 64 and name HN ) 4.3 2.6 1.7 volume=0.176 peak=3506 ppm1=0.175 ppm2=7.932 assign ( resid 144 and name HG2# ) ( resid 109 and name HG2 ) 2.8 1.1 1.1 volume=2.020 peak=3986 ppm1=0.766 ppm2=1.553 assign ( resid 196 and name HG2# ) ( resid 196 and name HA ) 3.8 2.0 1.5 volume=0.386 peak=2465 ppm1=0.811 ppm2=3.452 assign ( resid 10 and name HG2# ) ( resid 8 and name HN ) 3.3 1.6 1.3 volume=0.808 peak=4261 ppm1=1.084 ppm2=7.611 assign ( resid 51 and name HG1 or resid 51 and name HG2 ) ( resid 166 and name HE2 ) 3.0 1.2 1.2 volume=1.582 peak=4431 ppm1=1.971 ppm2=2.662 assign ( resid 151 and name HN ) ( resid 130 and name HA ) 4.2 2.5 1.7 volume=0.199 peak=545 ppm1=8.647 ppm2=3.878 assign ( resid 91 and name HN ) ( resid 89 and name HB2 ) 3.7 1.9 1.5 volume=0.444 peak=2238 ppm1=7.215 ppm2=3.874 assign ( resid 171 and name HN ) ( resid 151 and name HB1 ) 4.0 2.2 1.6 volume=0.280 peak=2256 ppm1=9.062 ppm2=2.964 assign ( resid 145 and name HB2 ) ( resid 145 and name HD1 ) 3.3 1.6 1.3 volume=0.811 peak=3074 ppm1=1.930 ppm2=3.458 assign ( resid 116 and name HN ) ( resid 116 and name HA ) 4.2 2.5 1.7 volume=0.186 peak=2088 ppm1=8.835 ppm2=6.147 assign ( resid 14 and name HG1# ) ( resid 14 and name HG2# ) 2.6 0.8 1.0 volume=3.876 peak=4336 ppm1=0.677 ppm2=0.757 assign ( resid 17 and name HN ) ( resid 17 and name HD1 or resid 17 and name HD2 ) 3.0 1.3 1.2 volume=1.409 peak=1635 ppm1=7.610 ppm2=6.484 assign ( resid 73 and name HN ) ( resid 73 and name HA ) 2.9 1.2 1.2 volume=1.790 peak=287 ppm1=7.500 ppm2=3.878 assign ( resid 202 and name HN ) ( resid 200 and name HN ) 3.8 2.1 1.5 volume=0.359 peak=2294 ppm1=8.577 ppm2=8.052 assign ( resid 84 and name HG2# ) ( resid 84 and name HG1# ) 2.7 1.0 1.1 volume=2.491 peak=4898 ppm1=0.109 ppm2=0.515 assign ( resid 168 and name HB ) ( resid 51 and name HG2 ) 3.2 1.5 1.3 volume=0.966 peak=2905 ppm1=1.729 ppm2=1.963 assign ( resid 170 and name HN ) ( resid 152 and name HN ) 3.9 2.1 1.5 volume=0.327 peak=1303 ppm1=9.146 ppm2=8.339 assign ( resid 42 and name HB2 ) ( resid 40 and name HB1 ) 4.0 2.3 1.6 volume=0.273 peak=3968 ppm1=1.666 ppm2=3.369 assign ( resid 54 and name HB ) ( resid 54 and name HD1# ) 3.4 1.7 1.4 volume=0.714 peak=2862 ppm1=1.770 ppm2=0.491 assign ( resid 121 and name HG1 ) ( resid 121 and name HB1 ) 3.7 2.0 1.5 volume=0.438 peak=2560 ppm1=2.310 ppm2=1.971 assign ( resid 117 and name HN ) ( resid 90 and name HA ) 3.6 1.9 1.4 volume=0.513 peak=2066 ppm1=8.233 ppm2=4.921 assign ( resid 144 and name HN ) ( resid 143 and name HB1 ) 3.7 2.0 1.5 volume=0.412 peak=1131 ppm1=7.536 ppm2=2.709 assign ( resid 76 and name HN ) ( resid 76 and name HD2 ) 2.8 1.1 1.1 volume=2.217 peak=1735 ppm1=6.699 ppm2=1.537 assign ( resid 121 and name HB1 ) ( resid 121 and name HN ) 4.3 2.6 1.7 volume=0.168 peak=3316 ppm1=2.052 ppm2=8.591 assign ( resid 168 and name HG2# ) ( resid 50 and name HG1# ) 4.3 2.5 1.7 volume=0.179 peak=3231 ppm1=0.198 ppm2=0.613 assign ( resid 11 and name HA ) ( resid 14 and name HN ) 3.9 2.2 1.6 volume=0.288 peak=4576 ppm1=3.957 ppm2=7.802 assign ( resid 185 and name HN ) ( resid 185 and name HG1 ) 2.9 1.2 1.2 volume=1.862 peak=358 ppm1=8.183 ppm2=2.338 assign ( resid 186 and name HE1 ) ( resid 102 and name HB# ) 2.6 0.9 1.0 volume=3.543 peak=3281 ppm1=2.959 ppm2=1.282 assign ( resid 179 and name HB1 ) ( resid 179 and name HD1# ) 3.3 1.6 1.3 volume=0.849 peak=5143 ppm1=2.752 ppm2=0.526 assign ( resid 167 and name HA ) ( resid 155 and name HA ) 4.6 2.9 1.4 volume=0.114 peak=3414 ppm1=5.218 ppm2=5.266 assign ( resid 137 and name HB1 ) ( resid 112 and name HG2# ) 3.6 1.9 1.5 volume=0.472 peak=4572 ppm1=2.809 ppm2=0.641 assign ( resid 183 and name HB ) ( resid 183 and name HG11 ) 3.2 1.5 1.3 volume=0.977 peak=4315 ppm1=1.977 ppm2=1.270 assign ( resid 191 and name HB2 ) ( resid 188 and name HA ) 4.4 2.7 1.6 volume=0.150 peak=4179 ppm1=2.817 ppm2=4.213 assign ( resid 168 and name HG2# ) ( resid 166 and name HE1 ) 4.4 2.7 1.6 volume=0.138 peak=4717 ppm1=0.201 ppm2=2.662 assign ( resid 39 and name HB# ) ( resid 39 and name HN ) 3.1 1.3 1.2 volume=1.309 peak=4242 ppm1=1.171 ppm2=8.259 assign ( resid 172 and name HB1 ) ( resid 172 and name HG2 ) 4.6 2.8 1.4 volume=0.119 peak=3258 ppm1=1.798 ppm2=2.317 assign ( resid 68 and name HA ) ( resid 67 and name HB1 ) 3.3 1.6 1.3 volume=0.792 peak=4567 ppm1=4.303 ppm2=2.202 assign ( resid 35 and name HN ) ( resid 35 and name HB ) 3.3 1.6 1.3 volume=0.828 peak=927 ppm1=9.430 ppm2=2.054 assign ( resid 84 and name HG1# ) ( resid 82 and name HB1 ) 3.3 1.5 1.3 volume=0.910 peak=5103 ppm1=0.533 ppm2=2.529 assign ( resid 172 and name HN ) ( resid 172 and name HA ) 4.2 2.5 1.7 volume=0.189 peak=2005 ppm1=8.855 ppm2=3.118 assign ( resid 34 and name HN ) ( resid 33 and name HA ) 3.2 1.4 1.3 volume=1.083 peak=1655 ppm1=8.136 ppm2=4.658 assign ( resid 139 and name HB1 ) ( resid 145 and name HB2 ) 2.7 1.0 1.1 volume=2.523 peak=3901 ppm1=2.198 ppm2=1.923 assign ( resid 64 and name HB2 or resid 64 and name HB1 ) ( resid 203 and name HD1# ) 4.3 2.6 1.7 volume=0.162 peak=4424 ppm1=3.022 ppm2=-0.016 assign ( resid 196 and name HB ) ( resid 196 and name HG12 ) 3.8 2.1 1.5 volume=0.340 peak=4278 ppm1=2.253 ppm2=1.477 assign ( resid 61 and name HN ) ( resid 203 and name HG11 ) 4.0 2.3 1.6 volume=0.244 peak=1844 ppm1=8.715 ppm2=0.519 assign ( resid 206 and name HA ) ( resid 206 and name HN ) 3.3 1.5 1.3 volume=0.887 peak=3402 ppm1=4.366 ppm2=7.460 assign ( resid 29 and name HB ) ( resid 30 and name HN ) 3.9 2.2 1.6 volume=0.303 peak=3678 ppm1=3.930 ppm2=8.720 assign ( resid 128 and name HN ) ( resid 126 and name HB ) 4.1 2.4 1.6 volume=0.231 peak=892 ppm1=9.932 ppm2=1.550 assign ( resid 187 and name HG2# ) ( resid 187 and name HN ) 3.6 1.9 1.5 volume=0.462 peak=2605 ppm1=1.051 ppm2=7.596 assign ( resid 9 and name HN ) ( resid 7 and name HN ) 3.5 1.8 1.4 volume=0.611 peak=532 ppm1=7.982 ppm2=8.429 assign ( resid 104 and name HN ) ( resid 103 and name HB ) 3.5 1.8 1.4 volume=0.537 peak=839 ppm1=8.051 ppm2=2.576 assign ( resid 6 and name HD1# ) ( resid 7 and name HN ) 3.6 1.9 1.4 volume=0.518 peak=2857 ppm1=0.794 ppm2=8.451 assign ( resid 20 and name HB1 or resid 20 and name HB2 ) ( resid 20 and name HN ) 3.6 1.9 1.5 volume=0.454 peak=5141 ppm1=2.715 ppm2=7.416 assign ( resid 66 and name HN ) ( resid 65 and name HB1 ) 3.4 1.7 1.4 volume=0.666 peak=857 ppm1=8.049 ppm2=1.656 assign ( resid 162 and name HB1 ) ( resid 162 and name HA ) 3.4 1.6 1.3 volume=0.759 peak=3041 ppm1=2.207 ppm2=3.646 assign ( resid 52 and name HN ) ( resid 168 and name HG2# ) 3.8 2.1 1.5 volume=0.356 peak=1273 ppm1=8.617 ppm2=0.210 assign ( resid 186 and name HE1 ) ( resid 186 and name HN ) 4.1 2.4 1.6 volume=0.232 peak=3840 ppm1=2.956 ppm2=7.368 assign ( resid 134 and name HD1 or resid 134 and name HD2 ) ( resid 134 and name HE1 or resid 134 and name HE2 ) 2.8 1.0 1.1 volume=2.440 peak=32 ppm1=6.862 ppm2=7.138 assign ( resid 204 and name HG2 ) ( resid 204 and name HN ) 3.5 1.8 1.4 volume=0.592 peak=3881 ppm1=1.295 ppm2=6.740 assign ( resid 41 and name HD2 or resid 41 and name HD1 ) ( resid 41 and name HN ) 3.5 1.8 1.4 volume=0.597 peak=4499 ppm1=3.094 ppm2=8.905 assign ( resid 161 and name HN ) ( resid 158 and name HA ) 3.3 1.6 1.3 volume=0.860 peak=1756 ppm1=6.905 ppm2=4.132 assign ( resid 61 and name HG ) ( resid 203 and name HG2# ) 3.6 1.9 1.5 volume=0.462 peak=2554 ppm1=1.717 ppm2=0.349 assign ( resid 155 and name HN ) ( resid 126 and name HA ) 3.3 1.6 1.3 volume=0.768 peak=544 ppm1=8.977 ppm2=5.385 assign ( resid 159 and name HA ) ( resid 160 and name HN ) 4.1 2.3 1.6 volume=0.242 peak=5051 ppm1=3.772 ppm2=8.848 assign ( resid 208 and name HB ) ( resid 204 and name HB2 ) 4.4 2.7 1.6 volume=0.152 peak=3331 ppm1=4.031 ppm2=1.617 assign ( resid 130 and name HB1 ) ( resid 114 and name HD2# ) 3.0 1.3 1.2 volume=1.545 peak=2989 ppm1=1.887 ppm2=0.773 assign ( resid 144 and name HN ) ( resid 109 and name HB1 ) 3.5 1.8 1.4 volume=0.606 peak=236 ppm1=7.537 ppm2=1.753 assign ( resid 170 and name HA ) ( resid 170 and name HN ) 4.1 2.3 1.6 volume=0.240 peak=2508 ppm1=5.822 ppm2=9.149 assign ( resid 42 and name HN ) ( resid 42 and name HD2 ) 3.1 1.3 1.2 volume=1.314 peak=1810 ppm1=8.699 ppm2=1.535 assign ( resid 99 and name HN ) ( resid 99 and name HA ) 3.1 1.4 1.2 volume=1.165 peak=675 ppm1=7.801 ppm2=4.276 assign ( resid 145 and name HG1 ) ( resid 147 and name HA ) 4.1 2.4 1.6 volume=0.220 peak=4909 ppm1=1.409 ppm2=4.226 assign ( resid 64 and name HB2 or resid 64 and name HB1 ) ( resid 203 and name HG12 ) 4.1 2.3 1.6 volume=0.243 peak=4747 ppm1=3.020 ppm2=0.518 assign ( resid 26 and name HG1# ) ( resid 36 and name HN ) 4.3 2.5 1.7 volume=0.181 peak=3247 ppm1=0.780 ppm2=9.949 assign ( resid 196 and name HG11 ) ( resid 193 and name HA ) 3.5 1.8 1.4 volume=0.559 peak=2716 ppm1=1.808 ppm2=3.448 assign ( resid 151 and name HN ) ( resid 148 and name HA ) 4.9 3.2 1.1 volume=0.077 peak=1580 ppm1=8.646 ppm2=4.986 assign ( resid 54 and name HN ) ( resid 167 and name HN ) 3.7 1.9 1.5 volume=0.445 peak=658 ppm1=9.020 ppm2=8.642 assign ( resid 173 and name HG2# ) ( resid 149 and name HN ) 3.7 2.0 1.5 volume=0.430 peak=4116 ppm1=1.027 ppm2=7.795 assign ( resid 71 and name HB2 ) ( resid 70 and name HN ) 4.1 2.4 1.7 volume=0.213 peak=3285 ppm1=1.528 ppm2=8.582 assign ( resid 87 and name HD1# ) ( resid 87 and name HG12 ) 2.7 1.0 1.1 volume=2.701 peak=4681 ppm1=0.440 ppm2=1.032 assign ( resid 43 and name HN ) ( resid 44 and name HA ) 3.1 1.3 1.2 volume=1.289 peak=1063 ppm1=7.303 ppm2=4.663 assign ( resid 105 and name HN ) ( resid 106 and name HD1# ) 3.7 2.0 1.5 volume=0.425 peak=2426 ppm1=7.943 ppm2=0.771 assign ( resid 170 and name HN ) ( resid 169 and name HG2 ) 3.3 1.5 1.3 volume=0.878 peak=1386 ppm1=9.146 ppm2=1.926 assign ( resid 73 and name HN ) ( resid 73 and name HB ) 2.9 1.2 1.2 volume=1.821 peak=2138 ppm1=7.501 ppm2=4.268 assign ( resid 33 and name HD1# ) ( resid 197 and name HG ) 3.7 2.0 1.5 volume=0.433 peak=2699 ppm1=0.360 ppm2=1.267 assign ( resid 161 and name HN ) ( resid 160 and name HB2 ) 2.7 1.0 1.1 volume=2.751 peak=1597 ppm1=6.904 ppm2=2.056 assign ( resid 70 and name HN ) ( resid 68 and name HA ) 3.4 1.6 1.3 volume=0.750 peak=487 ppm1=8.573 ppm2=4.276 assign ( resid 88 and name HN ) ( resid 91 and name HB ) 3.4 1.7 1.4 volume=0.717 peak=2364 ppm1=8.596 ppm2=3.620 assign ( resid 114 and name HD1# ) ( resid 130 and name HN ) 4.7 3.0 1.3 volume=0.100 peak=2663 ppm1=0.536 ppm2=7.617 assign ( resid 71 and name HN ) ( resid 72 and name HN ) 3.2 1.4 1.3 volume=1.091 peak=565 ppm1=7.218 ppm2=7.522 assign ( resid 64 and name HN ) ( resid 64 and name HB2 ) 3.1 1.4 1.2 volume=1.173 peak=1902 ppm1=7.878 ppm2=2.967 assign ( resid 36 and name HN ) ( resid 35 and name HB ) 3.6 1.9 1.5 volume=0.458 peak=1854 ppm1=9.880 ppm2=2.058 assign ( resid 70 and name HN ) ( resid 69 and name HA1 ) 2.8 1.1 1.1 volume=2.012 peak=1853 ppm1=8.576 ppm2=3.755 assign ( resid 80 and name HA ) ( resid 72 and name HG12 ) 3.6 1.9 1.4 volume=0.513 peak=2483 ppm1=3.986 ppm2=1.027 assign ( resid 155 and name HN ) ( resid 126 and name HN ) 3.3 1.6 1.3 volume=0.805 peak=308 ppm1=8.976 ppm2=9.088 assign ( resid 199 and name HB# ) ( resid 203 and name HB ) 3.6 1.9 1.5 volume=0.468 peak=4165 ppm1=0.692 ppm2=0.123 assign ( resid 165 and name HA ) ( resid 166 and name HN ) 4.3 2.5 1.7 volume=0.178 peak=4968 ppm1=5.238 ppm2=9.045 assign ( resid 112 and name HG2# ) ( resid 84 and name HG1# ) 2.5 0.8 1.0 volume=4.431 peak=2967 ppm1=0.679 ppm2=0.536 assign ( resid 6 and name HN ) ( resid 4 and name HA ) 3.4 1.7 1.4 volume=0.680 peak=1550 ppm1=7.722 ppm2=3.838 assign ( resid 26 and name HN ) ( resid 25 and name HE1 ) 3.3 1.6 1.3 volume=0.786 peak=2169 ppm1=8.862 ppm2=2.833 assign ( resid 64 and name HD1 or resid 64 and name HD2 ) ( resid 64 and name HZ ) 4.0 2.2 1.6 volume=0.280 peak=45 ppm1=5.970 ppm2=7.050 assign ( resid 184 and name HG12 ) ( resid 179 and name HD2# ) 3.0 1.3 1.2 volume=1.417 peak=4248 ppm1=1.095 ppm2=0.753 assign ( resid 156 and name HN ) ( resid 166 and name HN ) 3.3 1.6 1.3 volume=0.837 peak=1661 ppm1=8.551 ppm2=9.098 assign ( resid 124 and name HA ) ( resid 124 and name HN ) 4.8 3.0 1.2 volume=0.092 peak=3318 ppm1=5.181 ppm2=6.484 assign ( resid 194 and name HN ) ( resid 194 and name HB2 ) 2.7 1.0 1.1 volume=2.548 peak=1774 ppm1=7.774 ppm2=2.800 assign ( resid 64 and name HZ ) ( resid 199 and name HB# ) 3.3 1.6 1.3 volume=0.801 peak=15 ppm1=7.051 ppm2=0.699 assign ( resid 160 and name HB2 ) ( resid 164 and name HN ) 3.5 1.7 1.4 volume=0.636 peak=3475 ppm1=2.035 ppm2=8.004 assign ( resid 146 and name HN ) ( resid 147 and name HN ) 3.8 2.1 1.5 volume=0.341 peak=899 ppm1=8.400 ppm2=8.794 assign ( resid 106 and name HD1# ) ( resid 179 and name HB1 ) 4.0 2.3 1.6 volume=0.254 peak=4195 ppm1=0.770 ppm2=2.804 assign ( resid 186 and name HN ) ( resid 184 and name HA ) 3.7 1.9 1.5 volume=0.452 peak=537 ppm1=7.370 ppm2=3.624 assign ( resid 105 and name HN ) ( resid 102 and name HB# ) 3.7 2.0 1.5 volume=0.424 peak=2262 ppm1=7.944 ppm2=1.279 assign ( resid 39 and name HB# ) ( resid 39 and name HA ) 4.2 2.5 1.7 volume=0.188 peak=3844 ppm1=1.169 ppm2=4.137 assign ( resid 191 and name HB1 ) ( resid 171 and name HG1# ) 4.0 2.2 1.6 volume=0.281 peak=3726 ppm1=2.816 ppm2=0.776 assign ( resid 130 and name HN ) ( resid 150 and name HA ) 3.5 1.8 1.4 volume=0.602 peak=723 ppm1=7.617 ppm2=4.008 assign ( resid 6 and name HA ) ( resid 9 and name HB1 ) 3.3 1.6 1.3 volume=0.783 peak=3751 ppm1=3.617 ppm2=2.331 assign ( resid 116 and name HA ) ( resid 116 and name HB2 or resid 116 and name HB1 ) 4.9 3.1 1.1 volume=0.082 peak=3337 ppm1=6.165 ppm2=2.846 assign ( resid 169 and name HG1 ) ( resid 169 and name HN ) 4.4 2.6 1.6 volume=0.156 peak=3204 ppm1=1.934 ppm2=9.257 assign ( resid 170 and name HA ) ( resid 50 and name HG1# ) 4.0 2.3 1.6 volume=0.247 peak=3875 ppm1=5.821 ppm2=0.708 assign ( resid 117 and name HD1# ) ( resid 117 and name HB ) 2.9 1.2 1.2 volume=1.796 peak=2526 ppm1=0.243 ppm2=1.040 assign ( resid 49 and name HN ) ( resid 48 and name HA ) 3.3 1.6 1.3 volume=0.786 peak=430 ppm1=8.909 ppm2=5.310 assign ( resid 112 and name HN ) ( resid 111 and name HA ) 2.8 1.1 1.1 volume=2.212 peak=1148 ppm1=8.136 ppm2=4.777 assign ( resid 115 and name HG1# ) ( resid 92 and name HN ) 4.2 2.5 1.7 volume=0.203 peak=4962 ppm1=0.303 ppm2=9.440 assign ( resid 167 and name HB2 ) ( resid 167 and name HG ) 3.4 1.7 1.4 volume=0.710 peak=5064 ppm1=1.679 ppm2=0.923 assign ( resid 191 and name HN ) ( resid 191 and name HB1 ) 2.9 1.2 1.2 volume=1.880 peak=915 ppm1=7.651 ppm2=2.835 assign ( resid 51 and name HN ) ( resid 35 and name HG1# ) 2.9 1.1 1.1 volume=1.933 peak=1948 ppm1=8.432 ppm2=0.928 assign ( resid 203 and name HG2# ) ( resid 64 and name HD1 or resid 64 and name HD2 ) 4.3 2.6 1.7 volume=0.171 peak=3921 ppm1=0.340 ppm2=5.918 assign ( resid 119 and name HN ) ( resid 125 and name HA ) 4.3 2.5 1.7 volume=0.181 peak=846 ppm1=8.055 ppm2=5.575 assign ( resid 71 and name HN ) ( resid 67 and name HN ) 3.7 2.0 1.5 volume=0.403 peak=1564 ppm1=7.220 ppm2=7.607 assign ( resid 65 and name HD2# ) ( resid 66 and name HN ) 3.9 2.2 1.6 volume=0.307 peak=3860 ppm1=0.319 ppm2=8.061 assign ( resid 127 and name HG12 ) ( resid 127 and name HN ) 4.8 3.1 1.2 volume=0.089 peak=5126 ppm1=1.045 ppm2=9.386 assign ( resid 7 and name HN ) ( resid 7 and name HA ) 3.1 1.4 1.3 volume=1.133 peak=248 ppm1=8.428 ppm2=3.703 assign ( resid 203 and name HN ) ( resid 64 and name HE1 or resid 64 and name HE2 ) 3.8 2.1 1.5 volume=0.367 peak=1284 ppm1=7.684 ppm2=6.483 assign ( resid 115 and name HN ) ( resid 93 and name HG2# ) 3.8 2.0 1.5 volume=0.377 peak=1791 ppm1=9.052 ppm2=-0.008 assign ( resid 160 and name HN ) ( resid 160 and name HG1 ) 2.7 1.0 1.1 volume=2.643 peak=1680 ppm1=8.833 ppm2=2.143 assign ( resid 76 and name HG1 ) ( resid 76 and name HE2 ) 3.0 1.2 1.2 volume=1.615 peak=4387 ppm1=1.384 ppm2=2.912 assign ( resid 173 and name HG2# ) ( resid 175 and name HG2 or resid 175 and name HG1 ) 3.2 1.5 1.3 volume=1.001 peak=4700 ppm1=1.032 ppm2=2.530 assign ( resid 6 and name HA ) ( resid 5 and name HB# ) 4.1 2.4 1.6 volume=0.232 peak=3196 ppm1=3.616 ppm2=1.335 assign ( resid 25 and name HN ) ( resid 25 and name HE1 ) 3.7 2.0 1.5 volume=0.426 peak=1116 ppm1=9.011 ppm2=2.847 assign ( resid 132 and name HB ) ( resid 112 and name HG2# ) 3.5 1.8 1.4 volume=0.539 peak=4857 ppm1=2.283 ppm2=0.697 assign ( resid 98 and name HN ) ( resid 97 and name HN ) 4.1 2.4 1.7 volume=0.213 peak=340 ppm1=9.354 ppm2=8.376 assign ( resid 133 and name HN ) ( resid 134 and name HA ) 3.8 2.1 1.5 volume=0.371 peak=802 ppm1=8.119 ppm2=5.182 assign ( resid 93 and name HG2# ) ( resid 84 and name HG1# ) 2.9 1.2 1.2 volume=1.770 peak=3094 ppm1=-0.013 ppm2=0.511 assign ( resid 38 and name HN ) ( resid 37 and name HA ) 3.1 1.3 1.2 volume=1.305 peak=2342 ppm1=8.466 ppm2=5.825 assign ( resid 39 and name HA ) ( resid 39 and name HB# ) 2.6 0.8 1.0 volume=3.841 peak=4369 ppm1=4.141 ppm2=1.159 assign ( resid 171 and name HN ) ( resid 49 and name HN ) 3.5 1.8 1.4 volume=0.589 peak=1775 ppm1=9.062 ppm2=8.915 assign ( resid 202 and name HA1 ) ( resid 202 and name HN ) 4.3 2.6 1.7 volume=0.174 peak=3791 ppm1=3.069 ppm2=8.573 assign ( resid 117 and name HN ) ( resid 90 and name HB1 or resid 90 and name HB2 ) 3.6 1.9 1.5 volume=0.458 peak=2386 ppm1=8.232 ppm2=3.362 assign ( resid 131 and name HN ) ( resid 113 and name HA ) 3.9 2.1 1.5 volume=0.323 peak=472 ppm1=9.293 ppm2=5.304 assign ( resid 170 and name HA ) ( resid 49 and name HG1 ) 4.0 2.3 1.6 volume=0.262 peak=4866 ppm1=5.822 ppm2=1.606 assign ( resid 34 and name HG2# ) ( resid 34 and name HB ) 3.0 1.3 1.2 volume=1.453 peak=3366 ppm1=1.101 ppm2=3.830 assign ( resid 183 and name HD1# ) ( resid 180 and name HB2 or resid 180 and name HB1 ) 3.0 1.3 1.2 volume=1.456 peak=3949 ppm1=0.870 ppm2=3.896 assign ( resid 37 and name HN ) ( resid 36 and name HA ) 2.9 1.2 1.2 volume=1.751 peak=1436 ppm1=9.660 ppm2=5.869 assign ( resid 112 and name HG2# ) ( resid 112 and name HG12 ) 2.8 1.1 1.1 volume=2.150 peak=2693 ppm1=0.682 ppm2=1.245 assign ( resid 71 and name HG2 ) ( resid 69 and name HN ) 4.5 2.8 1.5 volume=0.122 peak=5125 ppm1=0.316 ppm2=8.235 assign ( resid 14 and name HN ) ( resid 13 and name HG2 ) 3.0 1.3 1.2 volume=1.356 peak=2086 ppm1=7.791 ppm2=2.041 assign ( resid 193 and name HA ) ( resid 193 and name HB ) 4.4 2.7 1.6 volume=0.146 peak=3865 ppm1=3.461 ppm2=2.055 assign ( resid 11 and name HN ) ( resid 11 and name HA ) 3.1 1.4 1.3 volume=1.123 peak=1035 ppm1=8.179 ppm2=3.955 assign ( resid 17 and name HN ) ( resid 17 and name HA ) 3.1 1.4 1.2 volume=1.252 peak=1288 ppm1=7.610 ppm2=4.542 assign ( resid 190 and name HA ) ( resid 190 and name HB2 ) 3.7 1.9 1.5 volume=0.451 peak=3780 ppm1=3.978 ppm2=3.845 assign ( resid 154 and name HG1# ) ( resid 168 and name HN ) 3.9 2.2 1.6 volume=0.296 peak=4903 ppm1=0.911 ppm2=8.719 assign ( resid 203 and name HB ) ( resid 203 and name HD1# ) 3.4 1.7 1.4 volume=0.710 peak=2893 ppm1=0.123 ppm2=-0.012 assign ( resid 133 and name HB2 or resid 133 and name HB1 ) ( resid 133 and name HN ) 3.8 2.1 1.5 volume=0.372 peak=3538 ppm1=2.559 ppm2=8.116 assign ( resid 114 and name HD2# ) ( resid 114 and name HB1 ) 2.6 0.8 1.0 volume=3.818 peak=4427 ppm1=0.782 ppm2=1.054 assign ( resid 25 and name HN ) ( resid 24 and name HD1 ) 2.9 1.1 1.1 volume=1.938 peak=880 ppm1=9.011 ppm2=6.773 assign ( resid 142 and name HN ) ( resid 142 and name HA ) 3.1 1.4 1.2 volume=1.158 peak=902 ppm1=7.897 ppm2=4.137 assign ( resid 186 and name HD2 ) ( resid 102 and name HB# ) 2.7 1.0 1.1 volume=2.525 peak=3566 ppm1=1.675 ppm2=1.296 assign ( resid 200 and name HA ) ( resid 199 and name HB# ) 3.8 2.1 1.5 volume=0.356 peak=3589 ppm1=3.362 ppm2=0.671 assign ( resid 68 and name HN ) ( resid 68 and name HA ) 3.5 1.8 1.4 volume=0.594 peak=2265 ppm1=8.024 ppm2=4.277 assign ( resid 61 and name HG ) ( resid 165 and name HB1 ) 3.8 2.1 1.5 volume=0.330 peak=3349 ppm1=1.716 ppm2=2.997 assign ( resid 205 and name HN ) ( resid 201 and name HA ) 2.7 1.0 1.1 volume=2.580 peak=367 ppm1=7.181 ppm2=4.308 assign ( resid 14 and name HG2# ) ( resid 14 and name HN ) 3.5 1.8 1.4 volume=0.602 peak=4239 ppm1=0.758 ppm2=7.795 assign ( resid 10 and name HB ) ( resid 13 and name HB2 or resid 13 and name HB1 ) 3.7 2.0 1.5 volume=0.402 peak=2501 ppm1=3.687 ppm2=2.003 assign ( resid 204 and name HG1 ) ( resid 204 and name HB2 ) 2.4 0.7 1.0 volume=5.743 peak=3339 ppm1=1.444 ppm2=1.714 assign ( resid 3 and name HZ ) ( resid 3 and name HN ) 4.2 2.5 1.7 volume=0.201 peak=139 ppm1=6.203 ppm2=7.989 assign ( resid 132 and name HG1# ) ( resid 130 and name HD2 or resid 130 and name HD1 ) 3.5 1.8 1.4 volume=0.595 peak=3987 ppm1=0.544 ppm2=1.630 assign ( resid 203 and name HB ) ( resid 203 and name HA ) 4.4 2.7 1.6 volume=0.142 peak=3874 ppm1=0.122 ppm2=2.832 assign ( resid 61 and name HN ) ( resid 61 and name HB2 ) 2.7 1.0 1.1 volume=2.563 peak=1666 ppm1=8.714 ppm2=1.652 assign ( resid 106 and name HN ) ( resid 106 and name HD1# ) 2.8 1.1 1.1 volume=2.129 peak=919 ppm1=7.941 ppm2=0.766 assign ( resid 200 and name HN ) ( resid 200 and name HG2 ) 3.2 1.5 1.3 volume=0.981 peak=854 ppm1=8.085 ppm2=1.137 assign ( resid 76 and name HG1 ) ( resid 76 and name HE1 ) 3.2 1.4 1.3 volume=1.091 peak=4141 ppm1=1.385 ppm2=2.860 assign ( resid 114 and name HD2# ) ( resid 3 and name HE1 or resid 3 and name HE2 ) 4.5 2.8 1.5 volume=0.133 peak=4733 ppm1=0.781 ppm2=7.214 assign ( resid 6 and name HD1# ) ( resid 6 and name HB ) 3.1 1.4 1.3 volume=1.135 peak=3187 ppm1=0.794 ppm2=1.761 assign ( resid 7 and name HB# ) ( resid 116 and name HB2 or resid 116 and name HB1 ) 3.4 1.7 1.4 volume=0.638 peak=4936 ppm1=0.751 ppm2=2.849 assign ( resid 34 and name HB ) ( resid 26 and name HG1# ) 3.5 1.7 1.4 volume=0.633 peak=3347 ppm1=3.827 ppm2=0.771 assign ( resid 62 and name HN ) ( resid 62 and name HA ) 3.3 1.5 1.3 volume=0.907 peak=676 ppm1=8.134 ppm2=3.963 assign ( resid 144 and name HA ) ( resid 145 and name HN ) 4.2 2.5 1.7 volume=0.200 peak=3195 ppm1=3.986 ppm2=8.337 assign ( resid 47 and name HN ) ( resid 47 and name HB1 ) 3.7 1.9 1.5 volume=0.442 peak=1943 ppm1=8.702 ppm2=0.757 assign ( resid 137 and name HB1 ) ( resid 137 and name HN ) 4.0 2.3 1.6 volume=0.256 peak=4073 ppm1=2.808 ppm2=8.055 assign ( resid 86 and name HD2 ) ( resid 86 and name HG1 ) 2.5 0.8 1.0 volume=3.914 peak=4583 ppm1=2.928 ppm2=1.459 assign ( resid 145 and name HG1 ) ( resid 112 and name HG11 ) 2.4 0.7 1.0 volume=5.223 peak=2821 ppm1=1.408 ppm2=1.618 assign ( resid 154 and name HN ) ( resid 169 and name HA ) 3.3 1.6 1.3 volume=0.856 peak=2404 ppm1=10.006 ppm2=5.177 assign ( resid 2 and name HA ) ( resid 2 and name HN ) 4.4 2.7 1.6 volume=0.139 peak=2720 ppm1=4.147 ppm2=8.191 assign ( resid 192 and name HG ) ( resid 171 and name HG2# ) 2.8 1.0 1.1 volume=2.443 peak=4056 ppm1=1.756 ppm2=0.773 assign ( resid 167 and name HD1# ) ( resid 51 and name HA ) 4.0 2.3 1.6 volume=0.271 peak=4565 ppm1=0.764 ppm2=5.597 assign ( resid 196 and name HG2# ) ( resid 196 and name HG12 ) 2.9 1.2 1.2 volume=1.798 peak=4262 ppm1=0.812 ppm2=1.468 assign ( resid 46 and name HN ) ( resid 46 and name HB2 ) 3.0 1.3 1.2 volume=1.506 peak=2092 ppm1=8.558 ppm2=2.047 assign ( resid 137 and name HB2 ) ( resid 112 and name HD1# ) 4.3 2.6 1.7 volume=0.170 peak=3054 ppm1=2.576 ppm2=0.379 assign ( resid 163 and name HN ) ( resid 163 and name HA ) 2.7 1.0 1.1 volume=2.833 peak=211 ppm1=7.326 ppm2=4.141 assign ( resid 154 and name HN ) ( resid 168 and name HN ) 3.6 1.8 1.4 volume=0.527 peak=1014 ppm1=10.005 ppm2=8.698 assign ( resid 112 and name HG2# ) ( resid 95 and name HB1 ) 3.2 1.4 1.3 volume=1.095 peak=4228 ppm1=0.680 ppm2=2.594 assign ( resid 190 and name HA ) ( resid 193 and name HG1# ) 4.4 2.7 1.6 volume=0.146 peak=4622 ppm1=3.980 ppm2=0.772 assign ( resid 158 and name HB2 ) ( resid 165 and name HN ) 4.4 2.7 1.6 volume=0.147 peak=3129 ppm1=2.218 ppm2=8.466 assign ( resid 71 and name HB2 ) ( resid 67 and name HN ) 4.6 2.9 1.4 volume=0.117 peak=4117 ppm1=1.528 ppm2=7.673 assign ( resid 69 and name HA2 ) ( resid 72 and name HN ) 4.1 2.4 1.6 volume=0.225 peak=4979 ppm1=3.778 ppm2=7.531 assign ( resid 184 and name HG2# ) ( resid 185 and name HN ) 3.5 1.8 1.4 volume=0.603 peak=3068 ppm1=1.094 ppm2=8.198 assign ( resid 11 and name HB# ) ( resid 12 and name HN ) 3.4 1.6 1.3 volume=0.748 peak=3975 ppm1=1.632 ppm2=7.602 assign ( resid 150 and name HB2 ) ( resid 13 and name HB2 ) 3.9 2.2 1.6 volume=0.316 peak=3734 ppm1=2.329 ppm2=1.900 assign ( resid 173 and name HN ) ( resid 47 and name HG ) 3.3 1.6 1.3 volume=0.854 peak=2046 ppm1=8.519 ppm2=0.618 assign ( resid 164 and name HN ) ( resid 162 and name HA ) 3.4 1.7 1.4 volume=0.667 peak=2439 ppm1=7.977 ppm2=3.736 assign ( resid 6 and name HG11 ) ( resid 6 and name HN ) 4.1 2.4 1.6 volume=0.229 peak=3423 ppm1=1.038 ppm2=7.731 assign ( resid 203 and name HG2# ) ( resid 203 and name HB ) 2.8 1.1 1.1 volume=2.327 peak=4514 ppm1=0.341 ppm2=0.124 assign ( resid 112 and name HB ) ( resid 112 and name HD1# ) 4.2 2.4 1.7 volume=0.209 peak=3741 ppm1=2.169 ppm2=0.374 assign ( resid 206 and name HN ) ( resid 203 and name HA ) 3.3 1.6 1.3 volume=0.850 peak=859 ppm1=7.463 ppm2=2.839 assign ( resid 99 and name HN ) ( resid 98 and name HG2# ) 3.0 1.3 1.2 volume=1.375 peak=1842 ppm1=7.801 ppm2=1.337 assign ( resid 201 and name HN ) ( resid 197 and name HD2# ) 3.1 1.4 1.3 volume=1.119 peak=1516 ppm1=7.405 ppm2=0.752 assign ( resid 10 and name HG2# ) ( resid 9 and name HN ) 3.9 2.2 1.6 volume=0.301 peak=2520 ppm1=1.084 ppm2=8.002 assign ( resid 129 and name HB1 ) ( resid 115 and name HN ) 4.5 2.8 1.5 volume=0.128 peak=5154 ppm1=3.366 ppm2=9.012 assign ( resid 127 and name HN ) ( resid 126 and name HN ) 4.1 2.4 1.6 volume=0.224 peak=1360 ppm1=9.384 ppm2=9.085 assign ( resid 119 and name HN ) ( resid 120 and name HN ) 4.2 2.5 1.7 volume=0.202 peak=1814 ppm1=8.060 ppm2=8.916 assign ( resid 198 and name HN ) ( resid 198 and name HB2 ) 3.1 1.4 1.2 volume=1.210 peak=1949 ppm1=8.717 ppm2=3.100 assign ( resid 144 and name HN ) ( resid 144 and name HD1# ) 3.3 1.6 1.3 volume=0.869 peak=2196 ppm1=7.536 ppm2=0.625 assign ( resid 40 and name HA ) ( resid 40 and name HN ) 3.9 2.2 1.6 volume=0.290 peak=4888 ppm1=3.988 ppm2=8.509 assign ( resid 129 and name HA ) ( resid 115 and name HG2# ) 4.4 2.6 1.6 volume=0.155 peak=3635 ppm1=5.705 ppm2=0.703 assign ( resid 6 and name HG11 ) ( resid 6 and name HB ) 3.4 1.7 1.4 volume=0.699 peak=4563 ppm1=1.059 ppm2=1.726 assign ( resid 171 and name HN ) ( resid 171 and name HG1# ) 4.3 2.5 1.7 volume=0.178 peak=357 ppm1=9.062 ppm2=0.875 assign ( resid 144 and name HG2# ) ( resid 142 and name HA ) 4.3 2.6 1.7 volume=0.175 peak=2902 ppm1=0.767 ppm2=4.147 assign ( resid 194 and name HA ) ( resid 76 and name HE1 ) 3.5 1.8 1.4 volume=0.610 peak=4409 ppm1=4.324 ppm2=2.829 assign ( resid 96 and name HG2# ) ( resid 78 and name HD2# ) 3.2 1.5 1.3 volume=0.916 peak=3683 ppm1=1.141 ppm2=0.494 assign ( resid 167 and name HN ) ( resid 166 and name HN ) 3.6 1.9 1.4 volume=0.481 peak=350 ppm1=8.642 ppm2=8.967 assign ( resid 158 and name HA ) ( resid 158 and name HB1 ) 3.6 1.9 1.5 volume=0.467 peak=2994 ppm1=4.139 ppm2=2.214 assign ( resid 4 and name HN ) ( resid 2 and name HB2 or resid 2 and name HB1 ) 3.2 1.5 1.3 volume=0.986 peak=1172 ppm1=8.187 ppm2=2.837 assign ( resid 166 and name HG1 ) ( resid 166 and name HB1 ) 2.4 0.7 1.0 volume=5.091 peak=2826 ppm1=1.209 ppm2=1.649 assign ( resid 38 and name HN ) ( resid 49 and name HN ) 3.5 1.8 1.4 volume=0.557 peak=415 ppm1=8.467 ppm2=8.955 assign ( resid 153 and name HB1 ) ( resid 154 and name HA ) 4.2 2.5 1.7 volume=0.199 peak=3354 ppm1=2.853 ppm2=4.671 assign ( resid 136 and name HN ) ( resid 137 and name HN ) 3.0 1.3 1.2 volume=1.344 peak=2453 ppm1=6.893 ppm2=8.049 assign ( resid 111 and name HN ) ( resid 111 and name HB2 ) 3.4 1.7 1.4 volume=0.717 peak=1340 ppm1=8.631 ppm2=2.969 assign ( resid 57 and name HN ) ( resid 57 and name HA ) 3.0 1.2 1.2 volume=1.615 peak=1038 ppm1=9.220 ppm2=4.139 assign ( resid 159 and name HA ) ( resid 159 and name HG1 ) 2.9 1.2 1.2 volume=1.674 peak=2808 ppm1=3.773 ppm2=2.239 assign ( resid 64 and name HE1 or resid 64 and name HE2 ) ( resid 199 and name HB# ) 3.4 1.7 1.4 volume=0.669 peak=5 ppm1=6.486 ppm2=0.688 assign ( resid 186 and name HG2 ) ( resid 186 and name HD1 ) 2.3 0.6 0.9 volume=7.192 peak=2461 ppm1=1.479 ppm2=1.678 assign ( resid 92 and name HN ) ( resid 116 and name HA ) 3.6 1.9 1.4 volume=0.476 peak=420 ppm1=9.456 ppm2=6.157 assign ( resid 184 and name HD1# ) ( resid 187 and name HB ) 3.7 2.0 1.5 volume=0.396 peak=3234 ppm1=0.889 ppm2=4.104 assign ( resid 183 and name HN ) ( resid 183 and name HG12 ) 2.8 1.1 1.1 volume=2.180 peak=1122 ppm1=7.421 ppm2=1.531 assign ( resid 72 and name HB ) ( resid 72 and name HA ) 3.6 1.9 1.5 volume=0.457 peak=3830 ppm1=1.856 ppm2=3.633 assign ( resid 151 and name HN ) ( resid 150 and name HB2 ) 3.6 1.9 1.4 volume=0.480 peak=196 ppm1=8.646 ppm2=2.256 assign ( resid 79 and name HG1 ) ( resid 80 and name HG2# ) 3.1 1.4 1.3 volume=1.151 peak=4609 ppm1=1.916 ppm2=0.731 assign ( resid 199 and name HN ) ( resid 197 and name HB2 ) 3.4 1.7 1.4 volume=0.680 peak=673 ppm1=8.633 ppm2=1.791 assign ( resid 96 and name HN ) ( resid 112 and name HD1# ) 3.3 1.6 1.3 volume=0.843 peak=2239 ppm1=8.474 ppm2=0.364 assign ( resid 112 and name HB ) ( resid 112 and name HG2# ) 3.5 1.8 1.4 volume=0.537 peak=3003 ppm1=2.172 ppm2=0.683 assign ( resid 121 and name HA ) ( resid 122 and name HN ) 4.2 2.5 1.7 volume=0.195 peak=2478 ppm1=4.144 ppm2=8.645 assign ( resid 36 and name HA ) ( resid 25 and name HN ) 3.9 2.2 1.6 volume=0.300 peak=3121 ppm1=5.851 ppm2=9.057 assign ( resid 35 and name HA ) ( resid 50 and name HB ) 4.1 2.4 1.6 volume=0.218 peak=5023 ppm1=4.916 ppm2=1.827 assign ( resid 7 and name HN ) ( resid 6 and name HN ) 3.3 1.5 1.3 volume=0.894 peak=816 ppm1=8.426 ppm2=7.759 assign ( resid 178 and name HB1 ) ( resid 178 and name HA ) 3.6 1.9 1.5 volume=0.466 peak=3048 ppm1=1.665 ppm2=4.257 assign ( resid 72 and name HD1# ) ( resid 72 and name HG11 ) 2.6 0.9 1.0 volume=3.343 peak=3028 ppm1=0.588 ppm2=1.169 assign ( resid 47 and name HN ) ( resid 40 and name HN ) 3.2 1.5 1.3 volume=0.969 peak=681 ppm1=8.701 ppm2=8.548 assign ( resid 60 and name HN ) ( resid 63 and name HB2 ) 3.5 1.8 1.4 volume=0.548 peak=1945 ppm1=7.265 ppm2=2.703 assign ( resid 40 and name HN ) ( resid 39 and name HN ) 4.0 2.3 1.6 volume=0.268 peak=166 ppm1=8.526 ppm2=8.238 assign ( resid 67 and name HN ) ( resid 69 and name HN ) 3.2 1.5 1.3 volume=1.042 peak=2353 ppm1=7.602 ppm2=8.221 assign ( resid 76 and name HN ) ( resid 75 and name HB1 ) 3.7 2.0 1.5 volume=0.419 peak=1712 ppm1=6.701 ppm2=2.839 assign ( resid 155 and name HA ) ( resid 156 and name HN ) 4.7 3.0 1.3 volume=0.098 peak=2982 ppm1=5.242 ppm2=8.578 assign ( resid 210 and name HN ) ( resid 210 and name HB2 ) 4.0 2.3 1.6 volume=0.265 peak=217 ppm1=8.308 ppm2=3.746 assign ( resid 60 and name HN ) ( resid 57 and name HN ) 4.1 2.4 1.7 volume=0.211 peak=1651 ppm1=7.266 ppm2=9.213 assign ( resid 163 and name HA ) ( resid 163 and name HN ) 4.1 2.3 1.6 volume=0.238 peak=3481 ppm1=4.137 ppm2=7.346 assign ( resid 184 and name HN ) ( resid 183 and name HB ) 3.1 1.4 1.3 volume=1.146 peak=2446 ppm1=7.499 ppm2=1.937 assign ( resid 51 and name HN ) ( resid 33 and name HA ) 3.6 1.9 1.4 volume=0.502 peak=649 ppm1=8.424 ppm2=4.662 assign ( resid 179 and name HD2# ) ( resid 179 and name HD1# ) 3.0 1.3 1.2 volume=1.431 peak=3551 ppm1=0.743 ppm2=0.526 assign ( resid 194 and name HA ) ( resid 194 and name HB1 ) 3.2 1.5 1.3 volume=1.019 peak=3930 ppm1=4.324 ppm2=2.740 assign ( resid 85 and name HN ) ( resid 134 and name HZ ) 3.9 2.1 1.5 volume=0.323 peak=2210 ppm1=7.150 ppm2=6.638 assign ( resid 144 and name HG2# ) ( resid 110 and name HN ) 3.7 2.0 1.5 volume=0.404 peak=3890 ppm1=0.767 ppm2=8.751 assign ( resid 9 and name HN ) ( resid 7 and name HB# ) 2.8 1.1 1.1 volume=2.178 peak=1298 ppm1=7.988 ppm2=0.753 assign ( resid 203 and name HD1# ) ( resid 60 and name HN ) 4.1 2.4 1.6 volume=0.234 peak=5109 ppm1=-0.012 ppm2=7.289 assign ( resid 204 and name HB2 ) ( resid 204 and name HD2 ) 2.3 0.6 0.9 volume=6.505 peak=3368 ppm1=1.711 ppm2=1.484 assign ( resid 80 and name HN ) ( resid 80 and name HG2# ) 3.0 1.2 1.2 volume=1.599 peak=2417 ppm1=7.525 ppm2=0.727 assign ( resid 112 and name HD1# ) ( resid 93 and name HG2# ) 3.4 1.6 1.3 volume=0.751 peak=3430 ppm1=0.373 ppm2=-0.009 assign ( resid 155 and name HN ) ( resid 156 and name HN ) 4.0 2.2 1.6 volume=0.278 peak=2202 ppm1=8.977 ppm2=8.571 assign ( resid 11 and name HB# ) ( resid 10 and name HN ) 4.0 2.2 1.6 volume=0.282 peak=4993 ppm1=1.631 ppm2=8.325 assign ( resid 109 and name HG1 ) ( resid 109 and name HD2 ) 2.8 1.1 1.1 volume=2.140 peak=3103 ppm1=1.545 ppm2=3.100 assign ( resid 143 and name HN ) ( resid 142 and name HN ) 2.9 1.2 1.2 volume=1.791 peak=1317 ppm1=6.898 ppm2=7.903 assign ( resid 137 and name HB2 ) ( resid 134 and name HZ ) 4.1 2.4 1.6 volume=0.221 peak=4738 ppm1=2.577 ppm2=6.642 assign ( resid 45 and name HN ) ( resid 44 and name HA ) 4.3 2.5 1.7 volume=0.182 peak=438 ppm1=6.655 ppm2=4.650 assign ( resid 19 and name HN ) ( resid 18 and name HB2 ) 3.7 2.0 1.5 volume=0.428 peak=518 ppm1=7.481 ppm2=2.452 assign ( resid 205 and name HA ) ( resid 205 and name HN ) 3.7 2.0 1.5 volume=0.429 peak=3855 ppm1=4.139 ppm2=7.182 assign ( resid 134 and name HE1 or resid 134 and name HE2 ) ( resid 93 and name HD1# ) 3.5 1.8 1.4 volume=0.609 peak=75 ppm1=7.141 ppm2=-0.272 assign ( resid 80 and name HB ) ( resid 97 and name HG2# ) 4.1 2.3 1.6 volume=0.237 peak=4390 ppm1=1.397 ppm2=0.245 assign ( resid 197 and name HA ) ( resid 197 and name HN ) 3.2 1.5 1.3 volume=0.985 peak=3136 ppm1=3.795 ppm2=7.987 assign ( resid 34 and name HG2# ) ( resid 26 and name HG1# ) 2.4 0.7 1.0 volume=5.935 peak=3131 ppm1=1.100 ppm2=0.773 assign ( resid 210 and name HN ) ( resid 209 and name HD2 ) 3.8 2.1 1.5 volume=0.358 peak=422 ppm1=8.307 ppm2=3.630 assign ( resid 29 and name HB ) ( resid 29 and name HG2# ) 2.6 0.8 1.0 volume=3.804 peak=3653 ppm1=3.930 ppm2=1.066 assign ( resid 91 and name HN ) ( resid 87 and name HN ) 3.8 2.1 1.5 volume=0.371 peak=1344 ppm1=7.216 ppm2=8.050 assign ( resid 102 and name HA ) ( resid 103 and name HN ) 3.6 1.9 1.4 volume=0.474 peak=3815 ppm1=4.115 ppm2=8.450 assign ( resid 172 and name HG1 ) ( resid 47 and name HB2 ) 3.8 2.1 1.5 volume=0.341 peak=2950 ppm1=2.290 ppm2=0.759 assign ( resid 196 and name HB ) ( resid 196 and name HG11 ) 3.4 1.7 1.4 volume=0.641 peak=3680 ppm1=2.252 ppm2=1.809 assign ( resid 121 and name HN ) ( resid 121 and name HB1 ) 2.9 1.2 1.2 volume=1.893 peak=2170 ppm1=8.586 ppm2=2.059 assign ( resid 10 and name HN ) ( resid 9 and name HN ) 3.4 1.6 1.3 volume=0.752 peak=1205 ppm1=8.318 ppm2=7.988 assign ( resid 187 and name HG2# ) ( resid 185 and name HN ) 3.7 2.0 1.5 volume=0.433 peak=4245 ppm1=1.051 ppm2=8.191 assign ( resid 117 and name HD1# ) ( resid 117 and name HA ) 4.4 2.7 1.6 volume=0.139 peak=3569 ppm1=0.245 ppm2=5.015 assign ( resid 129 and name HN ) ( resid 130 and name HN ) 4.0 2.2 1.6 volume=0.279 peak=2002 ppm1=8.719 ppm2=7.652 assign ( resid 201 and name HN ) ( resid 204 and name HN ) 3.9 2.1 1.5 volume=0.321 peak=898 ppm1=7.404 ppm2=6.738 assign ( resid 93 and name HD1# ) ( resid 84 and name HG2# ) 3.1 1.4 1.2 volume=1.196 peak=3295 ppm1=-0.273 ppm2=0.117 assign ( resid 180 and name HN ) ( resid 179 and name HD2# ) 3.9 2.1 1.5 volume=0.327 peak=1077 ppm1=8.352 ppm2=0.757 assign ( resid 144 and name HG2# ) ( resid 109 and name HB1 ) 2.5 0.8 1.0 volume=3.962 peak=3171 ppm1=0.767 ppm2=1.734 assign ( resid 201 and name HA ) ( resid 204 and name HD2 ) 3.3 1.6 1.3 volume=0.801 peak=3472 ppm1=4.337 ppm2=1.498 assign ( resid 60 and name HB2 ) ( resid 60 and name HG2 ) 2.6 0.9 1.1 volume=3.164 peak=4183 ppm1=1.717 ppm2=1.317 assign ( resid 158 and name HB1 ) ( resid 160 and name HN ) 4.3 2.6 1.7 volume=0.168 peak=4088 ppm1=2.219 ppm2=8.821 assign ( resid 134 and name HE1 or resid 134 and name HE2 ) ( resid 93 and name HG2# ) 3.5 1.7 1.4 volume=0.620 peak=129 ppm1=7.140 ppm2=-0.014 assign ( resid 205 and name HN ) ( resid 207 and name HN ) 3.4 1.7 1.4 volume=0.714 peak=526 ppm1=7.185 ppm2=7.784 assign ( resid 157 and name HB1 ) ( resid 58 and name HB1 or resid 58 and name HB2 ) 4.1 2.4 1.6 volume=0.226 peak=3692 ppm1=2.307 ppm2=2.143 assign ( resid 114 and name HD1# ) ( resid 92 and name HN ) 3.8 2.1 1.5 volume=0.340 peak=4794 ppm1=0.537 ppm2=9.498 assign ( resid 109 and name HN ) ( resid 109 and name HA ) 2.9 1.1 1.1 volume=1.975 peak=739 ppm1=8.165 ppm2=3.880 assign ( resid 74 and name HN ) ( resid 73 and name HG2# ) 3.1 1.4 1.2 volume=1.168 peak=281 ppm1=6.494 ppm2=1.221 assign ( resid 127 and name HG12 ) ( resid 127 and name HD1# ) 3.5 1.8 1.4 volume=0.561 peak=2540 ppm1=1.044 ppm2=0.280 assign ( resid 6 and name HA ) ( resid 6 and name HD1# ) 2.9 1.2 1.2 volume=1.658 peak=4329 ppm1=3.617 ppm2=0.783 assign ( resid 156 and name HN ) ( resid 156 and name HB1 ) 3.2 1.5 1.3 volume=0.912 peak=733 ppm1=8.551 ppm2=3.357 assign ( resid 3 and name HD1 or resid 3 and name HD2 ) ( resid 114 and name HB1 ) 3.5 1.8 1.4 volume=0.562 peak=50 ppm1=7.380 ppm2=1.052 assign ( resid 54 and name HG12 ) ( resid 54 and name HD1# ) 2.9 1.2 1.2 volume=1.633 peak=3457 ppm1=1.235 ppm2=0.491 assign ( resid 134 and name HE1 or resid 134 and name HE2 ) ( resid 134 and name HN ) 3.5 1.7 1.4 volume=0.622 peak=28 ppm1=7.140 ppm2=8.742 assign ( resid 59 and name HN ) ( resid 58 and name HG2 ) 3.6 1.8 1.4 volume=0.526 peak=1339 ppm1=8.089 ppm2=1.780 assign ( resid 183 and name HD1# ) ( resid 183 and name HB ) 2.8 1.1 1.1 volume=2.145 peak=4634 ppm1=0.871 ppm2=1.976 assign ( resid 144 and name HG2# ) ( resid 145 and name HA ) 4.5 2.8 1.5 volume=0.131 peak=4148 ppm1=0.766 ppm2=4.978 assign ( resid 169 and name HN ) ( resid 170 and name HA ) 4.2 2.5 1.7 volume=0.190 peak=1870 ppm1=9.256 ppm2=5.811 assign ( resid 30 and name HN ) ( resid 31 and name HN ) 3.6 1.9 1.5 volume=0.473 peak=2178 ppm1=8.721 ppm2=9.262 assign ( resid 128 and name HA ) ( resid 129 and name HN ) 4.3 2.6 1.7 volume=0.168 peak=4978 ppm1=5.581 ppm2=8.721 assign ( resid 149 and name HN ) ( resid 148 and name HN ) 3.9 2.2 1.6 volume=0.306 peak=1650 ppm1=7.758 ppm2=9.139 assign ( resid 19 and name HN ) ( resid 18 and name HA ) 3.4 1.7 1.4 volume=0.657 peak=2106 ppm1=7.477 ppm2=4.514 assign ( resid 197 and name HN ) ( resid 195 and name HN ) 4.0 2.2 1.6 volume=0.274 peak=169 ppm1=7.988 ppm2=7.911 assign ( resid 179 and name HD1# ) ( resid 179 and name HN ) 4.1 2.4 1.6 volume=0.236 peak=3348 ppm1=0.530 ppm2=7.350 assign ( resid 80 and name HG2# ) ( resid 80 and name HN ) 4.2 2.5 1.7 volume=0.192 peak=3744 ppm1=0.708 ppm2=7.524 assign ( resid 123 and name HA ) ( resid 122 and name HA1 ) 3.7 2.0 1.5 volume=0.427 peak=3087 ppm1=4.354 ppm2=3.837 assign ( resid 207 and name HD1 ) ( resid 207 and name HG2 ) 2.2 0.5 0.9 volume=9.905 peak=4835 ppm1=3.045 ppm2=1.467 assign ( resid 112 and name HN ) ( resid 95 and name HA ) 4.4 2.7 1.6 volume=0.151 peak=231 ppm1=8.134 ppm2=5.560 assign ( resid 91 and name HN ) ( resid 91 and name HG2# ) 3.3 1.5 1.3 volume=0.899 peak=2423 ppm1=7.218 ppm2=1.008 assign ( resid 111 and name HN ) ( resid 111 and name HA ) 3.9 2.2 1.5 volume=0.317 peak=2209 ppm1=8.630 ppm2=4.801 assign ( resid 179 and name HN ) ( resid 179 and name HB2 ) 4.0 2.3 1.6 volume=0.274 peak=1219 ppm1=7.303 ppm2=2.515 assign ( resid 201 and name HA ) ( resid 201 and name HB1 ) 3.7 1.9 1.5 volume=0.444 peak=4814 ppm1=4.332 ppm2=2.595 assign ( resid 114 and name HD1# ) ( resid 114 and name HN ) 4.0 2.3 1.6 volume=0.245 peak=3051 ppm1=0.533 ppm2=8.804 assign ( resid 64 and name HN ) ( resid 63 and name HA ) 3.5 1.8 1.4 volume=0.597 peak=442 ppm1=7.879 ppm2=4.405 assign ( resid 163 and name HB# ) ( resid 160 and name HB1 ) 4.1 2.3 1.6 volume=0.239 peak=3036 ppm1=1.160 ppm2=2.010 assign ( resid 3 and name HZ ) ( resid 87 and name HD1# ) 2.9 1.2 1.2 volume=1.867 peak=63 ppm1=6.203 ppm2=0.435 assign ( resid 73 and name HB ) ( resid 74 and name HN ) 4.2 2.5 1.7 volume=0.189 peak=2695 ppm1=4.301 ppm2=6.504 assign ( resid 193 and name HG1# ) ( resid 194 and name HN ) 3.4 1.7 1.4 volume=0.689 peak=4320 ppm1=0.787 ppm2=7.802 assign ( resid 93 and name HG12 ) ( resid 85 and name HN ) 4.1 2.4 1.6 volume=0.222 peak=4050 ppm1=0.597 ppm2=7.159 assign ( resid 73 and name HN ) ( resid 74 and name HB2 ) 4.0 2.3 1.6 volume=0.255 peak=1224 ppm1=7.503 ppm2=2.839 assign ( resid 197 and name HD1# ) ( resid 197 and name HA ) 3.5 1.8 1.4 volume=0.559 peak=2574 ppm1=0.756 ppm2=3.766 assign ( resid 40 and name HA ) ( resid 40 and name HB1 ) 4.0 2.3 1.6 volume=0.256 peak=3500 ppm1=3.987 ppm2=3.352 assign ( resid 135 and name HD2 ) ( resid 135 and name HG2 ) 3.2 1.5 1.3 volume=0.968 peak=4847 ppm1=3.227 ppm2=1.749 assign ( resid 131 and name HN ) ( resid 130 and name HA ) 3.3 1.6 1.3 volume=0.828 peak=2007 ppm1=9.295 ppm2=3.883 assign ( resid 124 and name HA ) ( resid 126 and name HG2# ) 4.1 2.4 1.7 volume=0.218 peak=4763 ppm1=5.177 ppm2=0.759 assign ( resid 68 and name HN ) ( resid 67 and name HG2 ) 3.5 1.8 1.4 volume=0.545 peak=1654 ppm1=8.025 ppm2=2.578 assign ( resid 137 and name HB1 ) ( resid 134 and name HE1 or resid 134 and name HE2 ) 3.7 2.0 1.5 volume=0.400 peak=5130 ppm1=2.806 ppm2=7.156 assign ( resid 184 and name HG11 ) ( resid 184 and name HN ) 3.5 1.8 1.4 volume=0.613 peak=3634 ppm1=1.675 ppm2=7.503 assign ( resid 67 and name HA ) ( resid 67 and name HN ) 3.5 1.8 1.4 volume=0.548 peak=4279 ppm1=3.938 ppm2=7.603 assign ( resid 33 and name HN ) ( resid 33 and name HA ) 3.2 1.5 1.3 volume=1.014 peak=644 ppm1=8.167 ppm2=4.662 assign ( resid 22 and name HN ) ( resid 22 and name HB2 or resid 22 and name HB1 ) 2.4 0.6 0.9 volume=6.279 peak=398 ppm1=8.194 ppm2=3.771 assign ( resid 33 and name HG12 ) ( resid 35 and name HG2# or resid 35 and name HG1# ) 4.0 2.3 1.6 volume=0.253 peak=4819 ppm1=1.918 ppm2=0.902 assign ( resid 132 and name HN ) ( resid 112 and name HG2# ) 3.2 1.5 1.3 volume=1.047 peak=1675 ppm1=7.894 ppm2=0.628 assign ( resid 64 and name HB2 or resid 64 and name HB1 ) ( resid 64 and name HZ ) 4.2 2.5 1.7 volume=0.193 peak=4987 ppm1=3.021 ppm2=7.044 assign ( resid 104 and name HN ) ( resid 103 and name HA ) 3.2 1.5 1.3 volume=0.956 peak=323 ppm1=8.051 ppm2=3.617 assign ( resid 15 and name HD1# ) ( resid 15 and name HG ) 2.8 1.1 1.1 volume=2.225 peak=4204 ppm1=0.439 ppm2=1.240 assign ( resid 180 and name HN ) ( resid 183 and name HN ) 3.3 1.6 1.3 volume=0.862 peak=858 ppm1=8.353 ppm2=7.470 assign ( resid 167 and name HD1# ) ( resid 169 and name HN ) 3.6 1.9 1.4 volume=0.488 peak=2612 ppm1=0.765 ppm2=9.295 assign ( resid 87 and name HD1# ) ( resid 93 and name HG12 ) 2.5 0.8 1.0 volume=3.989 peak=3067 ppm1=0.440 ppm2=0.542 assign ( resid 3 and name HD1 or resid 3 and name HD2 ) ( resid 4 and name HN ) 4.0 2.3 1.6 volume=0.251 peak=35 ppm1=7.379 ppm2=8.150 assign ( resid 2 and name HN ) ( resid 1 and name HG1 ) 3.3 1.6 1.3 volume=0.805 peak=1965 ppm1=8.190 ppm2=2.292 assign ( resid 7 and name HB# ) ( resid 7 and name HA ) 3.2 1.5 1.3 volume=0.920 peak=3240 ppm1=0.752 ppm2=3.714 assign ( resid 28 and name HN ) ( resid 35 and name HB ) 2.9 1.1 1.1 volume=1.977 peak=1513 ppm1=7.808 ppm2=2.049 assign ( resid 62 and name HN ) ( resid 155 and name HB1 ) 3.8 2.1 1.5 volume=0.336 peak=2060 ppm1=8.130 ppm2=3.034 assign ( resid 202 and name HN ) ( resid 201 and name HN ) 3.2 1.4 1.3 volume=1.066 peak=610 ppm1=8.578 ppm2=7.400 assign ( resid 194 and name HB1 ) ( resid 76 and name HG1 ) 3.9 2.2 1.6 volume=0.285 peak=4368 ppm1=2.824 ppm2=1.413 assign ( resid 199 and name HN ) ( resid 199 and name HB# ) 2.7 1.0 1.1 volume=2.825 peak=2016 ppm1=8.633 ppm2=0.631 assign ( resid 71 and name HD2 ) ( resid 65 and name HA ) 3.7 2.0 1.5 volume=0.401 peak=3398 ppm1=2.781 ppm2=3.830 assign ( resid 65 and name HG ) ( resid 65 and name HN ) 4.0 2.3 1.6 volume=0.252 peak=3757 ppm1=1.640 ppm2=7.740 assign ( resid 30 and name HN ) ( resid 34 and name HA ) 3.2 1.5 1.3 volume=0.917 peak=2098 ppm1=8.722 ppm2=4.924 assign ( resid 102 and name HN ) ( resid 102 and name HA ) 4.0 2.3 1.6 volume=0.265 peak=2275 ppm1=8.521 ppm2=4.123 assign ( resid 41 and name HA ) ( resid 41 and name HB2 ) 3.7 2.0 1.5 volume=0.408 peak=3601 ppm1=4.336 ppm2=1.981 assign ( resid 206 and name HN ) ( resid 202 and name HA1 ) 3.3 1.5 1.3 volume=0.888 peak=1283 ppm1=7.463 ppm2=3.061 assign ( resid 179 and name HB1 ) ( resid 179 and name HB2 ) 3.6 1.9 1.4 volume=0.494 peak=4749 ppm1=2.752 ppm2=2.490 assign ( resid 197 and name HA ) ( resid 197 and name HD2# ) 2.8 1.1 1.1 volume=2.072 peak=3747 ppm1=3.792 ppm2=0.759 assign ( resid 126 and name HG2# ) ( resid 124 and name HN ) 4.4 2.7 1.6 volume=0.146 peak=4220 ppm1=0.751 ppm2=6.444 assign ( resid 124 and name HN ) ( resid 125 and name HN ) 3.5 1.8 1.4 volume=0.580 peak=1525 ppm1=6.472 ppm2=8.820 assign ( resid 203 and name HN ) ( resid 202 and name HN ) 3.2 1.5 1.3 volume=1.046 peak=1581 ppm1=7.685 ppm2=8.571 assign ( resid 130 and name HN ) ( resid 115 and name HG1# ) 4.1 2.4 1.6 volume=0.223 peak=339 ppm1=7.617 ppm2=0.290 assign ( resid 130 and name HN ) ( resid 113 and name HA ) 3.8 2.1 1.5 volume=0.372 peak=998 ppm1=7.617 ppm2=5.303 assign ( resid 115 and name HG1# ) ( resid 115 and name HN ) 3.8 2.1 1.5 volume=0.354 peak=4340 ppm1=0.302 ppm2=9.055 assign ( resid 110 and name HN ) ( resid 110 and name HB2 or resid 110 and name HB1 ) 3.2 1.5 1.3 volume=1.014 peak=504 ppm1=8.722 ppm2=2.967 assign ( resid 78 and name HN ) ( resid 78 and name HB2 ) 2.8 1.1 1.1 volume=2.186 peak=199 ppm1=7.149 ppm2=1.401 assign ( resid 98 and name HN ) ( resid 109 and name HN ) 4.0 2.3 1.6 volume=0.250 peak=982 ppm1=9.355 ppm2=8.173 assign ( resid 13 and name HN ) ( resid 12 and name HG2 ) 3.2 1.4 1.3 volume=1.059 peak=1714 ppm1=7.728 ppm2=2.441 assign ( resid 134 and name HN ) ( resid 112 and name HD1# ) 4.2 2.5 1.7 volume=0.191 peak=1968 ppm1=8.747 ppm2=0.396 assign ( resid 95 and name HN ) ( resid 94 and name HN ) 4.2 2.5 1.7 volume=0.194 peak=680 ppm1=9.125 ppm2=9.610 assign ( resid 187 and name HN ) ( resid 189 and name HD2 ) 3.8 2.0 1.5 volume=0.381 peak=1951 ppm1=7.601 ppm2=3.484 assign ( resid 134 and name HE1 or resid 134 and name HE2 ) ( resid 136 and name HB1 ) 2.8 1.1 1.1 volume=2.105 peak=2 ppm1=7.141 ppm2=1.771 assign ( resid 61 and name HN ) ( resid 59 and name HA ) 2.9 1.2 1.1 volume=1.918 peak=1328 ppm1=8.715 ppm2=4.530 assign ( resid 135 and name HD1 ) ( resid 134 and name HA ) 4.1 2.4 1.7 volume=0.215 peak=3647 ppm1=3.223 ppm2=5.260 assign ( resid 49 and name HN ) ( resid 37 and name HA ) 3.7 2.0 1.5 volume=0.417 peak=445 ppm1=8.910 ppm2=5.830 assign ( resid 128 and name HN ) ( resid 152 and name HA1 ) 4.1 2.4 1.6 volume=0.226 peak=365 ppm1=9.932 ppm2=3.603 assign ( resid 34 and name HG2# ) ( resid 26 and name HN ) 3.4 1.7 1.4 volume=0.686 peak=3939 ppm1=1.101 ppm2=8.875 assign ( resid 147 and name HD1 or resid 147 and name HD2 ) ( resid 174 and name HG2 ) 3.9 2.1 1.5 volume=0.329 peak=83 ppm1=6.220 ppm2=2.113 assign ( resid 200 and name HA ) ( resid 54 and name HG2# ) 3.7 2.0 1.5 volume=0.436 peak=2603 ppm1=3.361 ppm2=0.590 assign ( resid 67 and name HA ) ( resid 67 and name HG2 ) 4.2 2.5 1.7 volume=0.203 peak=3588 ppm1=3.936 ppm2=2.534 assign ( resid 126 and name HG2# ) ( resid 154 and name HA ) 4.6 2.9 1.4 volume=0.110 peak=4416 ppm1=0.752 ppm2=4.678 assign ( resid 86 and name HG2 ) ( resid 92 and name HB1 ) 2.6 0.9 1.1 volume=3.236 peak=4602 ppm1=1.459 ppm2=3.051 assign ( resid 38 and name HN ) ( resid 37 and name HB1 ) 3.1 1.4 1.3 volume=1.136 peak=459 ppm1=8.467 ppm2=3.232 assign ( resid 173 and name HA ) ( resid 171 and name HG1# ) 3.3 1.6 1.3 volume=0.839 peak=4660 ppm1=3.613 ppm2=0.839 assign ( resid 17 and name HN ) ( resid 14 and name HG2# ) 3.2 1.5 1.3 volume=1.012 peak=1475 ppm1=7.610 ppm2=0.754 assign ( resid 64 and name HD1 or resid 64 and name HD2 ) ( resid 203 and name HG12 ) 4.2 2.5 1.7 volume=0.196 peak=92 ppm1=5.972 ppm2=0.567 assign ( resid 36 and name HB2 ) ( resid 26 and name HG1# ) 3.6 1.9 1.4 volume=0.493 peak=3271 ppm1=3.526 ppm2=0.770 assign ( resid 156 and name HN ) ( resid 166 and name HA ) 3.0 1.3 1.2 volume=1.476 peak=640 ppm1=8.552 ppm2=4.490 assign ( resid 73 and name HA ) ( resid 72 and name HG12 ) 3.5 1.7 1.4 volume=0.631 peak=4864 ppm1=3.920 ppm2=1.026 assign ( resid 29 and name HN ) ( resid 28 and name HB1 ) 3.2 1.5 1.3 volume=0.946 peak=1709 ppm1=8.567 ppm2=1.919 assign ( resid 166 and name HN ) ( resid 157 and name HA ) 3.7 2.0 1.5 volume=0.396 peak=1960 ppm1=9.000 ppm2=4.786 assign ( resid 6 and name HD1# ) ( resid 6 and name HA ) 3.3 1.6 1.3 volume=0.809 peak=4419 ppm1=0.792 ppm2=3.620 assign ( resid 84 and name HG2# ) ( resid 93 and name HB ) 3.7 1.9 1.5 volume=0.444 peak=3870 ppm1=0.112 ppm2=1.229 assign ( resid 24 and name HZ1 ) ( resid 24 and name HB1 ) 4.1 2.4 1.6 volume=0.222 peak=17 ppm1=7.002 ppm2=2.976 assign ( resid 76 and name HN ) ( resid 78 and name HD1# ) 3.8 2.1 1.5 volume=0.372 peak=1201 ppm1=6.699 ppm2=0.499 assign ( resid 166 and name HD1 ) ( resid 51 and name HG1 ) 3.0 1.3 1.2 volume=1.529 peak=2529 ppm1=1.467 ppm2=1.934 assign ( resid 134 and name HE1 or resid 134 and name HE2 ) ( resid 134 and name HZ ) 3.8 2.0 1.5 volume=0.380 peak=138 ppm1=7.139 ppm2=6.645 assign ( resid 21 and name HG2# ) ( resid 21 and name HN ) 4.0 2.3 1.6 volume=0.260 peak=3631 ppm1=1.147 ppm2=8.247 assign ( resid 72 and name HA ) ( resid 71 and name HG2 ) 4.3 2.6 1.7 volume=0.167 peak=4926 ppm1=3.631 ppm2=0.329 assign ( resid 185 and name HA ) ( resid 185 and name HG1 ) 3.4 1.7 1.4 volume=0.650 peak=4192 ppm1=3.895 ppm2=2.346 assign ( resid 5 and name HA ) ( resid 8 and name HB2 ) 4.0 2.3 1.6 volume=0.251 peak=3361 ppm1=4.024 ppm2=2.041 assign ( resid 155 and name HN ) ( resid 154 and name HA ) 3.2 1.5 1.3 volume=1.050 peak=1279 ppm1=8.977 ppm2=4.663 assign ( resid 14 and name HA ) ( resid 14 and name HN ) 3.8 2.1 1.5 volume=0.361 peak=5004 ppm1=2.818 ppm2=7.800 assign ( resid 3 and name HD1 or resid 3 and name HD2 ) ( resid 132 and name HB ) 3.6 1.9 1.4 volume=0.483 peak=38 ppm1=7.379 ppm2=2.254 assign ( resid 64 and name HA ) ( resid 65 and name HN ) 4.0 2.3 1.6 volume=0.267 peak=3122 ppm1=3.862 ppm2=7.738 assign ( resid 68 and name HN ) ( resid 67 and name HB2 ) 3.3 1.6 1.3 volume=0.841 peak=452 ppm1=8.024 ppm2=2.050 assign ( resid 33 and name HG11 ) ( resid 196 and name HG2# ) 3.6 1.9 1.4 volume=0.510 peak=4696 ppm1=1.885 ppm2=0.774 assign ( resid 172 and name HN ) ( resid 47 and name HG ) 3.9 2.2 1.6 volume=0.313 peak=2388 ppm1=8.856 ppm2=0.658 assign ( resid 98 and name HG2# ) ( resid 98 and name HN ) 4.7 3.0 1.3 volume=0.097 peak=3273 ppm1=1.325 ppm2=9.354 assign ( resid 61 and name HD1# ) ( resid 58 and name HD1 ) 3.1 1.3 1.2 volume=1.317 peak=2914 ppm1=0.746 ppm2=3.792 assign ( resid 116 and name HA ) ( resid 115 and name HB ) 3.7 2.0 1.5 volume=0.390 peak=3531 ppm1=6.163 ppm2=0.256 assign ( resid 34 and name HN ) ( resid 51 and name HN ) 3.5 1.7 1.4 volume=0.619 peak=2124 ppm1=8.137 ppm2=8.429 assign ( resid 73 and name HN ) ( resid 72 and name HA ) 3.5 1.8 1.4 volume=0.586 peak=2072 ppm1=7.501 ppm2=3.616 assign ( resid 134 and name HN ) ( resid 134 and name HB2 ) 3.1 1.3 1.2 volume=1.317 peak=262 ppm1=8.745 ppm2=2.977 assign ( resid 186 and name HG2 ) ( resid 186 and name HB1 ) 3.8 2.1 1.5 volume=0.344 peak=3421 ppm1=1.478 ppm2=1.873 assign ( resid 84 and name HN ) ( resid 86 and name HG2 ) 3.3 1.6 1.3 volume=0.773 peak=336 ppm1=8.504 ppm2=1.403 assign ( resid 98 and name HN ) ( resid 111 and name HN ) 4.1 2.3 1.6 volume=0.238 peak=1611 ppm1=9.354 ppm2=8.634 assign ( resid 37 and name HN ) ( resid 27 and name HB ) 3.8 2.1 1.5 volume=0.355 peak=679 ppm1=9.660 ppm2=2.036 assign ( resid 56 and name HN ) ( resid 164 and name HN ) 3.9 2.2 1.6 volume=0.307 peak=1530 ppm1=8.641 ppm2=7.994 assign ( resid 75 and name HA ) ( resid 76 and name HG1 ) 3.7 2.0 1.5 volume=0.393 peak=4473 ppm1=4.152 ppm2=1.365 assign ( resid 11 and name HA ) ( resid 128 and name HB1 or resid 128 and name HB2 ) 3.9 2.2 1.6 volume=0.307 peak=4341 ppm1=3.953 ppm2=3.744 assign ( resid 17 and name HN ) ( resid 17 and name HB1 or resid 17 and name HB2 ) 3.2 1.5 1.3 volume=1.026 peak=740 ppm1=7.608 ppm2=2.834 assign ( resid 114 and name HD1# ) ( resid 114 and name HB2 ) 3.2 1.5 1.3 volume=0.920 peak=4839 ppm1=0.537 ppm2=1.702 assign ( resid 39 and name HN ) ( resid 46 and name HB1 ) 3.2 1.4 1.3 volume=1.070 peak=1195 ppm1=8.247 ppm2=1.538 assign ( resid 14 and name HG2# ) ( resid 128 and name HA ) 3.8 2.0 1.5 volume=0.380 peak=4650 ppm1=0.758 ppm2=5.595 assign ( resid 200 and name HB2 ) ( resid 201 and name HA ) 3.9 2.2 1.6 volume=0.292 peak=4285 ppm1=1.670 ppm2=4.226 assign ( resid 64 and name HD1 or resid 64 and name HD2 ) ( resid 64 and name HE1 or resid 64 and name HE2 ) 3.5 1.8 1.4 volume=0.589 peak=121 ppm1=5.971 ppm2=6.486 assign ( resid 124 and name HA ) ( resid 125 and name HN ) 4.1 2.4 1.6 volume=0.224 peak=4919 ppm1=5.179 ppm2=8.764 assign ( resid 66 and name HN ) ( resid 65 and name HN ) 3.1 1.4 1.2 volume=1.163 peak=1739 ppm1=8.049 ppm2=7.655 assign ( resid 102 and name HN ) ( resid 102 and name HB# ) 4.0 2.2 1.6 volume=0.278 peak=1140 ppm1=8.524 ppm2=1.275 assign ( resid 129 and name HN ) ( resid 153 and name HN ) 4.0 2.2 1.6 volume=0.279 peak=1274 ppm1=8.718 ppm2=9.343 assign ( resid 101 and name HN ) ( resid 99 and name HB1 ) 3.3 1.6 1.3 volume=0.859 peak=903 ppm1=8.477 ppm2=1.795 assign ( resid 169 and name HB1 ) ( resid 169 and name HN ) 4.6 2.9 1.4 volume=0.112 peak=4904 ppm1=1.788 ppm2=9.243 assign ( resid 93 and name HD1# ) ( resid 93 and name HG11 ) 2.7 0.9 1.1 volume=2.969 peak=3652 ppm1=-0.273 ppm2=0.690 assign ( resid 26 and name HB ) ( resid 27 and name HN ) 4.0 2.3 1.6 volume=0.264 peak=2543 ppm1=1.922 ppm2=9.309 assign ( resid 50 and name HN ) ( resid 49 and name HG2 ) 3.6 1.8 1.4 volume=0.530 peak=434 ppm1=9.301 ppm2=1.588 assign ( resid 204 and name HN ) ( resid 204 and name HA ) 2.8 1.1 1.1 volume=2.161 peak=646 ppm1=6.745 ppm2=3.870 assign ( resid 36 and name HB2 ) ( resid 36 and name HB1 ) 5.2 3.5 0.8 volume=0.054 peak=3883 ppm1=3.519 ppm2=3.864 assign ( resid 186 and name HG1 ) ( resid 186 and name HE2 ) 2.9 1.2 1.2 volume=1.810 peak=2839 ppm1=1.479 ppm2=2.920 assign ( resid 54 and name HG2# ) ( resid 56 and name HN ) 3.5 1.8 1.4 volume=0.589 peak=3740 ppm1=0.576 ppm2=8.653 assign ( resid 67 and name HB1 ) ( resid 68 and name HN ) 3.4 1.6 1.3 volume=0.753 peak=3024 ppm1=2.150 ppm2=7.997 assign ( resid 133 and name HN ) ( resid 132 and name HN ) 4.2 2.5 1.7 volume=0.184 peak=2152 ppm1=8.127 ppm2=7.898 assign ( resid 169 and name HA ) ( resid 50 and name HG1# ) 3.7 2.0 1.5 volume=0.405 peak=2577 ppm1=5.233 ppm2=0.678 assign ( resid 91 and name HG2# ) ( resid 116 and name HA ) 3.7 2.0 1.5 volume=0.399 peak=2568 ppm1=1.019 ppm2=6.173 assign ( resid 187 and name HG2# ) ( resid 187 and name HB ) 2.7 1.0 1.1 volume=2.806 peak=2607 ppm1=1.057 ppm2=4.047 assign ( resid 101 and name HN ) ( resid 98 and name HG2# ) 3.6 1.9 1.4 volume=0.511 peak=1923 ppm1=8.477 ppm2=1.405 assign ( resid 99 and name HN ) ( resid 100 and name HN ) 3.7 2.0 1.5 volume=0.393 peak=2370 ppm1=7.801 ppm2=8.437 assign ( resid 172 and name HN ) ( resid 151 and name HN ) 3.7 2.0 1.5 volume=0.407 peak=548 ppm1=8.856 ppm2=8.613 assign ( resid 132 and name HN ) ( resid 131 and name HN ) 3.8 2.0 1.5 volume=0.380 peak=842 ppm1=7.895 ppm2=9.294 assign ( resid 115 and name HN ) ( resid 93 and name HN ) 3.4 1.7 1.4 volume=0.674 peak=2125 ppm1=9.054 ppm2=8.915 assign ( resid 184 and name HG2# ) ( resid 184 and name HB ) 2.8 1.1 1.1 volume=2.255 peak=3967 ppm1=1.095 ppm2=2.057 assign ( resid 74 and name HZ2 ) ( resid 64 and name HD1 or resid 64 and name HD2 ) 3.6 1.9 1.4 volume=0.508 peak=142 ppm1=6.458 ppm2=5.974 assign ( resid 130 and name HB1 ) ( resid 131 and name HN ) 4.3 2.6 1.7 volume=0.169 peak=2754 ppm1=1.885 ppm2=9.302 assign ( resid 15 and name HG ) ( resid 16 and name HN ) 4.2 2.5 1.7 volume=0.197 peak=4435 ppm1=1.242 ppm2=7.490 assign ( resid 159 and name HG1 or resid 159 and name HG2 ) ( resid 159 and name HA ) 3.7 1.9 1.5 volume=0.445 peak=2741 ppm1=2.241 ppm2=3.777 assign ( resid 145 and name HB2 ) ( resid 110 and name HB1 ) 4.2 2.5 1.7 volume=0.199 peak=4867 ppm1=1.930 ppm2=2.985 assign ( resid 7 and name HB# ) ( resid 91 and name HG2# ) 2.9 1.2 1.2 volume=1.747 peak=4462 ppm1=0.751 ppm2=1.031 assign ( resid 6 and name HD1# ) ( resid 2 and name HB1 ) 3.9 2.2 1.6 volume=0.313 peak=3905 ppm1=0.794 ppm2=2.860 assign ( resid 93 and name HN ) ( resid 87 and name HN ) 4.0 2.3 1.6 volume=0.265 peak=1600 ppm1=8.908 ppm2=8.049 assign ( resid 91 and name HG2# ) ( resid 92 and name HN ) 3.3 1.6 1.3 volume=0.818 peak=3727 ppm1=1.020 ppm2=9.493 assign ( resid 168 and name HG1# ) ( resid 51 and name HA ) 3.7 2.0 1.5 volume=0.389 peak=3306 ppm1=0.769 ppm2=5.625 assign ( resid 36 and name HB1 ) ( resid 37 and name HN ) 3.9 2.1 1.5 volume=0.322 peak=4038 ppm1=3.859 ppm2=9.632 assign ( resid 163 and name HB# ) ( resid 164 and name HN ) 3.2 1.5 1.3 volume=0.984 peak=5002 ppm1=1.158 ppm2=7.999 assign ( resid 128 and name HB1 or resid 128 and name HB2 ) ( resid 11 and name HA ) 4.5 2.8 1.5 volume=0.126 peak=3999 ppm1=3.745 ppm2=3.925 assign ( resid 163 and name HB# ) ( resid 161 and name HN ) 3.9 2.1 1.5 volume=0.330 peak=4359 ppm1=1.161 ppm2=6.888 assign ( resid 25 and name HN ) ( resid 36 and name HB2 ) 3.1 1.3 1.2 volume=1.302 peak=155 ppm1=9.009 ppm2=3.481 assign ( resid 119 and name HN ) ( resid 119 and name HA ) 3.8 2.1 1.5 volume=0.371 peak=853 ppm1=8.056 ppm2=4.818 assign ( resid 193 and name HN ) ( resid 192 and name HG ) 3.0 1.3 1.2 volume=1.411 peak=1914 ppm1=7.621 ppm2=1.714 assign ( resid 73 and name HG2# ) ( resid 70 and name HN ) 3.6 1.9 1.5 volume=0.460 peak=4481 ppm1=1.217 ppm2=8.575 assign ( resid 102 and name HB# ) ( resid 106 and name HD1# ) 2.7 1.0 1.1 volume=2.903 peak=4193 ppm1=1.279 ppm2=0.775 assign ( resid 199 and name HB# ) ( resid 200 and name HD1 or resid 200 and name HD2 ) 3.1 1.4 1.2 volume=1.243 peak=3294 ppm1=0.692 ppm2=1.546 assign ( resid 184 and name HA ) ( resid 183 and name HB ) 3.5 1.7 1.4 volume=0.635 peak=3081 ppm1=3.626 ppm2=1.962 assign ( resid 81 and name HN ) ( resid 72 and name HD1# ) 2.5 0.8 1.0 volume=4.453 peak=251 ppm1=8.509 ppm2=0.620 assign ( resid 96 and name HN ) ( resid 94 and name HN ) 4.5 2.7 1.5 volume=0.137 peak=266 ppm1=8.473 ppm2=9.603 assign ( resid 18 and name HB1 ) ( resid 15 and name HD1# ) 4.0 2.3 1.6 volume=0.256 peak=2962 ppm1=2.970 ppm2=0.428 assign ( resid 42 and name HN ) ( resid 172 and name HG2 ) 3.8 2.1 1.5 volume=0.341 peak=1922 ppm1=8.699 ppm2=2.317 assign ( resid 37 and name HN ) ( resid 25 and name HB2 ) 3.3 1.6 1.3 volume=0.828 peak=815 ppm1=9.659 ppm2=1.774 assign ( resid 6 and name HB ) ( resid 10 and name HN ) 4.4 2.7 1.6 volume=0.143 peak=2970 ppm1=1.724 ppm2=8.328 assign ( resid 176 and name HN ) ( resid 175 and name HB1 ) 3.4 1.7 1.4 volume=0.676 peak=1537 ppm1=8.404 ppm2=2.441 assign ( resid 24 and name HH2 ) ( resid 24 and name HZ1 ) 3.7 2.0 1.5 volume=0.398 peak=58 ppm1=6.801 ppm2=7.021 assign ( resid 29 and name HA ) ( resid 30 and name HN ) 4.5 2.8 1.5 volume=0.122 peak=5029 ppm1=5.251 ppm2=8.726 assign ( resid 112 and name HN ) ( resid 111 and name HB1 ) 3.6 1.9 1.4 volume=0.495 peak=1188 ppm1=8.136 ppm2=2.971 assign ( resid 145 and name HN ) ( resid 146 and name HN ) 3.3 1.5 1.3 volume=0.899 peak=2347 ppm1=8.381 ppm2=8.441 assign ( resid 129 and name HB1 ) ( resid 130 and name HN ) 4.3 2.5 1.7 volume=0.179 peak=3866 ppm1=3.365 ppm2=7.629 assign ( resid 72 and name HG2# ) ( resid 72 and name HB ) 2.9 1.1 1.1 volume=1.934 peak=3137 ppm1=0.603 ppm2=1.856 assign ( resid 125 and name HN ) ( resid 126 and name HA ) 3.2 1.4 1.3 volume=1.084 peak=2039 ppm1=8.772 ppm2=5.314 assign ( resid 208 and name HN ) ( resid 207 and name HN ) 3.4 1.6 1.3 volume=0.754 peak=301 ppm1=8.013 ppm2=7.855 assign ( resid 176 and name HN ) ( resid 177 and name HN ) 4.2 2.5 1.7 volume=0.202 peak=1719 ppm1=8.404 ppm2=8.487 assign ( resid 165 and name HA ) ( resid 58 and name HD1 ) 3.8 2.1 1.5 volume=0.344 peak=2852 ppm1=5.226 ppm2=3.889 assign ( resid 120 and name HN ) ( resid 121 and name HN ) 3.9 2.2 1.6 volume=0.311 peak=2443 ppm1=8.914 ppm2=8.570 assign ( resid 102 and name HA ) ( resid 103 and name HA ) 4.1 2.4 1.6 volume=0.228 peak=2890 ppm1=4.117 ppm2=3.646 assign ( resid 49 and name HN ) ( resid 50 and name HN ) 3.9 2.1 1.5 volume=0.321 peak=1645 ppm1=8.910 ppm2=9.309 assign ( resid 54 and name HD1# ) ( resid 167 and name HD1# ) 2.3 0.6 0.9 volume=7.541 peak=4697 ppm1=0.491 ppm2=0.709 assign ( resid 140 and name HN ) ( resid 139 and name HG1 ) 2.9 1.2 1.2 volume=1.775 peak=642 ppm1=9.582 ppm2=1.797 assign ( resid 167 and name HN ) ( resid 54 and name HB ) 3.2 1.5 1.3 volume=0.951 peak=1294 ppm1=8.642 ppm2=1.799 assign ( resid 137 and name HB2 ) ( resid 112 and name HG12 ) 4.4 2.7 1.6 volume=0.153 peak=3186 ppm1=2.574 ppm2=1.281 assign ( resid 208 and name HG2# ) ( resid 209 and name HD2 or resid 209 and name HD1 ) 3.3 1.6 1.3 volume=0.848 peak=4379 ppm1=1.137 ppm2=3.580 assign ( resid 64 and name HN ) ( resid 64 and name HA ) 2.9 1.2 1.2 volume=1.895 peak=787 ppm1=7.881 ppm2=3.868 assign ( resid 50 and name HN ) ( resid 170 and name HA ) 4.0 2.3 1.6 volume=0.251 peak=2311 ppm1=9.298 ppm2=5.832 assign ( resid 65 and name HD1# ) ( resid 127 and name HG11 or resid 127 and name HG12 ) 3.3 1.6 1.3 volume=0.830 peak=4701 ppm1=0.175 ppm2=1.078 assign ( resid 172 and name HG1 ) ( resid 172 and name HA ) 4.2 2.5 1.7 volume=0.186 peak=4456 ppm1=2.294 ppm2=3.100 assign ( resid 84 and name HG2# ) ( resid 82 and name HB1 ) 3.7 2.0 1.5 volume=0.398 peak=2926 ppm1=0.112 ppm2=2.464 assign ( resid 44 and name HN ) ( resid 43 and name HB1 ) 4.8 3.1 1.2 volume=0.090 peak=2018 ppm1=8.377 ppm2=2.967 assign ( resid 134 and name HD1 or resid 134 and name HD2 ) ( resid 134 and name HZ ) 4.0 2.3 1.6 volume=0.244 peak=146 ppm1=6.862 ppm2=6.646 assign ( resid 208 and name HA ) ( resid 208 and name HB ) 4.6 2.9 1.4 volume=0.106 peak=3577 ppm1=4.406 ppm2=4.032 assign ( resid 51 and name HN ) ( resid 35 and name HA ) 3.3 1.5 1.3 volume=0.897 peak=1721 ppm1=8.424 ppm2=4.915 assign ( resid 169 and name HB2 ) ( resid 167 and name HD1# ) 3.6 1.8 1.4 volume=0.531 peak=2872 ppm1=1.787 ppm2=0.782 assign ( resid 204 and name HG1 ) ( resid 204 and name HE2 ) 2.9 1.2 1.2 volume=1.664 peak=2592 ppm1=1.445 ppm2=2.836 assign ( resid 130 and name HD2 ) ( resid 10 and name HG2# ) 2.7 1.0 1.1 volume=2.691 peak=3612 ppm1=1.660 ppm2=1.092 assign ( resid 87 and name HG2# ) ( resid 87 and name HA ) 3.2 1.5 1.3 volume=0.989 peak=5122 ppm1=0.852 ppm2=3.870 assign ( resid 199 and name HB# ) ( resid 203 and name HD1# ) 3.7 1.9 1.5 volume=0.454 peak=3522 ppm1=0.692 ppm2=-0.013 assign ( resid 163 and name HN ) ( resid 164 and name HN ) 2.7 1.0 1.1 volume=2.597 peak=1044 ppm1=7.326 ppm2=7.980 assign ( resid 112 and name HN ) ( resid 113 and name HN ) 2.7 1.0 1.1 volume=2.660 peak=214 ppm1=8.136 ppm2=8.240 assign ( resid 163 and name HA ) ( resid 163 and name HB# ) 2.6 0.9 1.0 volume=3.555 peak=3202 ppm1=4.139 ppm2=1.156 assign ( resid 14 and name HB ) ( resid 14 and name HG1# ) 3.0 1.3 1.2 volume=1.559 peak=2675 ppm1=1.713 ppm2=0.680 assign ( resid 134 and name HN ) ( resid 134 and name HD1 or resid 134 and name HD2 ) 4.0 2.3 1.6 volume=0.261 peak=451 ppm1=8.747 ppm2=6.897 assign ( resid 157 and name HD2 ) ( resid 124 and name HB2 ) 3.6 1.8 1.4 volume=0.525 peak=4616 ppm1=3.626 ppm2=2.069 assign ( resid 203 and name HG11 ) ( resid 54 and name HG2# ) 4.2 2.5 1.7 volume=0.203 peak=4530 ppm1=0.516 ppm2=0.590 assign ( resid 204 and name HN ) ( resid 203 and name HG12 ) 3.6 1.9 1.5 volume=0.461 peak=765 ppm1=6.744 ppm2=0.515 assign ( resid 203 and name HG2# ) ( resid 204 and name HA ) 3.7 1.9 1.5 volume=0.451 peak=3810 ppm1=0.340 ppm2=3.832 assign ( resid 203 and name HB ) ( resid 54 and name HG2# ) 4.2 2.5 1.7 volume=0.196 peak=2818 ppm1=0.122 ppm2=0.573 assign ( resid 171 and name HN ) ( resid 169 and name HG2 ) 3.4 1.7 1.4 volume=0.672 peak=346 ppm1=9.062 ppm2=1.928 assign ( resid 15 and name HB2 ) ( resid 15 and name HN ) 4.2 2.5 1.7 volume=0.203 peak=3906 ppm1=1.368 ppm2=7.810 assign ( resid 97 and name HG2# ) ( resid 98 and name HN ) 3.9 2.1 1.5 volume=0.329 peak=2765 ppm1=0.215 ppm2=9.365 assign ( resid 71 and name HB2 ) ( resid 68 and name HN ) 3.9 2.2 1.6 volume=0.303 peak=3886 ppm1=1.530 ppm2=8.069 assign ( resid 95 and name HN ) ( resid 84 and name HG1# ) 3.3 1.6 1.3 volume=0.843 peak=525 ppm1=9.125 ppm2=0.523 assign ( resid 131 and name HN ) ( resid 130 and name HG2 ) 3.6 1.9 1.4 volume=0.480 peak=334 ppm1=9.292 ppm2=1.281 assign ( resid 114 and name HD1# ) ( resid 114 and name HD2# ) 2.5 0.8 1.0 volume=3.995 peak=3276 ppm1=0.537 ppm2=0.782 assign ( resid 158 and name HG1 ) ( resid 53 and name HD1# ) 3.1 1.4 1.2 volume=1.262 peak=3332 ppm1=2.439 ppm2=0.779 assign ( resid 74 and name HD1 ) ( resid 74 and name HB2 ) 3.6 1.9 1.4 volume=0.477 peak=26 ppm1=6.939 ppm2=2.850 assign ( resid 72 and name HN ) ( resid 72 and name HD1# ) 2.7 1.0 1.1 volume=2.577 peak=270 ppm1=7.536 ppm2=0.623 assign ( resid 80 and name HA ) ( resid 80 and name HB ) 4.2 2.5 1.7 volume=0.203 peak=2877 ppm1=3.986 ppm2=1.396 assign ( resid 114 and name HN ) ( resid 114 and name HA ) 3.9 2.2 1.6 volume=0.295 peak=628 ppm1=8.799 ppm2=4.402 assign ( resid 27 and name HN ) ( resid 26 and name HA ) 3.4 1.7 1.4 volume=0.694 peak=409 ppm1=9.278 ppm2=3.969 assign ( resid 196 and name HG12 ) ( resid 196 and name HG2# ) 2.6 0.9 1.0 volume=3.516 peak=4438 ppm1=1.476 ppm2=0.819 assign ( resid 132 and name HG2# ) ( resid 131 and name HN ) 3.7 2.0 1.5 volume=0.402 peak=4307 ppm1=0.936 ppm2=9.299 assign ( resid 98 and name HN ) ( resid 79 and name HG1 ) 3.8 2.1 1.5 volume=0.374 peak=189 ppm1=9.355 ppm2=1.925 assign ( resid 109 and name HN ) ( resid 97 and name HG2# ) 2.7 1.0 1.1 volume=2.535 peak=2278 ppm1=8.165 ppm2=0.234 assign ( resid 154 and name HN ) ( resid 154 and name HB ) 3.4 1.7 1.4 volume=0.709 peak=1011 ppm1=10.007 ppm2=2.185 assign ( resid 136 and name HB1 ) ( resid 134 and name HZ ) 3.7 2.0 1.5 volume=0.427 peak=3252 ppm1=1.745 ppm2=6.644 assign ( resid 115 and name HN ) ( resid 114 and name HD1# ) 3.3 1.5 1.3 volume=0.902 peak=1364 ppm1=9.052 ppm2=0.552 assign ( resid 130 and name HN ) ( resid 114 and name HB2 ) 3.5 1.8 1.4 volume=0.589 peak=470 ppm1=7.617 ppm2=1.665 assign ( resid 167 and name HB1 ) ( resid 166 and name HE2 ) 4.6 2.8 1.4 volume=0.118 peak=4710 ppm1=1.680 ppm2=2.665 assign ( resid 150 and name HB2 ) ( resid 14 and name HG2# ) 3.7 2.0 1.5 volume=0.428 peak=3242 ppm1=2.308 ppm2=0.765 assign ( resid 195 and name HN ) ( resid 193 and name HN ) 3.1 1.4 1.2 volume=1.163 peak=684 ppm1=7.971 ppm2=7.644 assign ( resid 54 and name HD1# ) ( resid 197 and name HA ) 4.2 2.4 1.7 volume=0.208 peak=4358 ppm1=0.490 ppm2=3.754 assign ( resid 15 and name HD2# ) ( resid 15 and name HB1 ) 3.0 1.2 1.2 volume=1.587 peak=4214 ppm1=0.683 ppm2=1.709 assign ( resid 200 and name HB2 ) ( resid 201 and name HN ) 4.0 2.3 1.6 volume=0.260 peak=2667 ppm1=1.670 ppm2=7.409 assign ( resid 93 and name HG2# ) ( resid 93 and name HD1# ) 3.0 1.3 1.2 volume=1.472 peak=5087 ppm1=-0.013 ppm2=-0.270 assign ( resid 200 and name HN ) ( resid 200 and name HB2 ) 2.6 0.9 1.0 volume=3.549 peak=221 ppm1=8.085 ppm2=1.658 assign ( resid 200 and name HA ) ( resid 201 and name HN ) 4.9 3.2 1.1 volume=0.074 peak=3833 ppm1=3.364 ppm2=7.414 assign ( resid 142 and name HN ) ( resid 143 and name HN ) 3.4 1.6 1.3 volume=0.742 peak=708 ppm1=7.901 ppm2=6.884 assign ( resid 88 and name HN ) ( resid 87 and name HA ) 3.3 1.6 1.3 volume=0.875 peak=384 ppm1=8.595 ppm2=3.879 assign ( resid 65 and name HB1 or resid 65 and name HB2 ) ( resid 65 and name HD1# ) 4.0 2.3 1.6 volume=0.263 peak=4384 ppm1=1.640 ppm2=0.174 assign ( resid 129 and name HN ) ( resid 14 and name HG2# ) 3.0 1.3 1.2 volume=1.407 peak=2116 ppm1=8.719 ppm2=0.749 assign ( resid 71 and name HB1 ) ( resid 72 and name HN ) 4.3 2.6 1.7 volume=0.172 peak=3004 ppm1=1.529 ppm2=7.479 assign ( resid 186 and name HA ) ( resid 186 and name HG2 ) 4.3 2.6 1.7 volume=0.165 peak=3080 ppm1=4.212 ppm2=1.476 assign ( resid 26 and name HB ) ( resid 26 and name HN ) 3.9 2.1 1.5 volume=0.323 peak=4108 ppm1=1.924 ppm2=8.857 assign ( resid 203 and name HG2# ) ( resid 203 and name HG11 or resid 203 and name HG12 ) 2.6 0.9 1.0 volume=3.338 peak=2619 ppm1=0.341 ppm2=0.512 assign ( resid 154 and name HG1# ) ( resid 155 and name HN ) 3.9 2.2 1.6 volume=0.293 peak=4404 ppm1=0.910 ppm2=8.977 assign ( resid 110 and name HN ) ( resid 110 and name HA ) 3.1 1.4 1.2 volume=1.165 peak=2001 ppm1=8.721 ppm2=5.441 assign ( resid 165 and name HN ) ( resid 165 and name HA ) 3.6 1.9 1.4 volume=0.503 peak=1952 ppm1=8.465 ppm2=5.182 assign ( resid 52 and name HN ) ( resid 167 and name HA ) 3.8 2.1 1.5 volume=0.363 peak=2449 ppm1=8.613 ppm2=5.185 assign ( resid 68 and name HN ) ( resid 70 and name HN ) 3.9 2.2 1.6 volume=0.313 peak=1983 ppm1=8.024 ppm2=8.569 assign ( resid 73 and name HA ) ( resid 72 and name HD1# ) 3.9 2.2 1.5 volume=0.318 peak=3110 ppm1=3.919 ppm2=0.575 assign ( resid 156 and name HN ) ( resid 156 and name HB2 ) 3.2 1.5 1.3 volume=0.912 peak=1072 ppm1=8.550 ppm2=3.224 assign ( resid 46 and name HB1 ) ( resid 47 and name HB1 ) 3.7 2.0 1.5 volume=0.388 peak=4113 ppm1=1.542 ppm2=0.777 assign ( resid 205 and name HN ) ( resid 204 and name HA ) 3.9 2.2 1.6 volume=0.305 peak=2399 ppm1=7.180 ppm2=3.872 assign ( resid 10 and name HN ) ( resid 11 and name HN ) 3.4 1.6 1.3 volume=0.752 peak=793 ppm1=8.322 ppm2=8.165 assign ( resid 126 and name HG2# ) ( resid 125 and name HN ) 4.1 2.4 1.6 volume=0.219 peak=4702 ppm1=0.753 ppm2=8.783 assign ( resid 35 and name HB ) ( resid 35 and name HG1# ) 2.6 0.9 1.1 volume=3.147 peak=3845 ppm1=2.051 ppm2=0.967 assign ( resid 61 and name HG ) ( resid 56 and name HG2 ) 2.9 1.2 1.2 volume=1.808 peak=3729 ppm1=1.719 ppm2=2.015 assign ( resid 75 and name HA ) ( resid 76 and name HB2 ) 4.3 2.6 1.7 volume=0.171 peak=3148 ppm1=4.153 ppm2=2.075 assign ( resid 3 and name HN ) ( resid 87 and name HD1# ) 3.4 1.7 1.4 volume=0.699 peak=593 ppm1=7.915 ppm2=0.495 assign ( resid 160 and name HA ) ( resid 160 and name HG2 ) 2.8 1.1 1.1 volume=2.114 peak=2781 ppm1=4.009 ppm2=2.196 assign ( resid 123 and name HN ) ( resid 123 and name HB1 ) 3.2 1.4 1.3 volume=1.099 peak=1860 ppm1=8.404 ppm2=2.714 assign ( resid 147 and name HN ) ( resid 144 and name HG12 ) 3.6 1.9 1.4 volume=0.503 peak=1347 ppm1=8.785 ppm2=1.275 assign ( resid 80 and name HG2# ) ( resid 97 and name HG2# ) 2.7 1.0 1.1 volume=2.757 peak=4983 ppm1=0.708 ppm2=0.249 assign ( resid 67 and name HA ) ( resid 68 and name HG2# ) 4.4 2.6 1.6 volume=0.157 peak=3681 ppm1=3.930 ppm2=0.734 assign ( resid 173 and name HG2# ) ( resid 173 and name HB ) 3.1 1.3 1.2 volume=1.332 peak=4297 ppm1=1.033 ppm2=3.610 assign ( resid 122 and name HN ) ( resid 121 and name HG1 or resid 121 and name HG2 ) 3.9 2.2 1.6 volume=0.298 peak=1796 ppm1=8.645 ppm2=2.315 assign ( resid 204 and name HN ) ( resid 203 and name HB ) 2.8 1.1 1.1 volume=2.051 peak=1702 ppm1=6.743 ppm2=0.124 assign ( resid 173 and name HB ) ( resid 173 and name HN ) 4.1 2.4 1.7 volume=0.210 peak=4977 ppm1=3.614 ppm2=8.531 assign ( resid 183 and name HG11 ) ( resid 183 and name HD1# ) 2.7 0.9 1.1 volume=3.090 peak=5030 ppm1=1.268 ppm2=0.871 assign ( resid 63 and name HA ) ( resid 63 and name HB2 or resid 63 and name HB1 ) 3.9 2.2 1.6 volume=0.296 peak=5132 ppm1=4.393 ppm2=2.688 assign ( resid 47 and name HN ) ( resid 47 and name HD1# ) 4.6 2.8 1.4 volume=0.120 peak=2118 ppm1=8.701 ppm2=0.092 assign ( resid 105 and name HB2 ) ( resid 179 and name HG ) 3.3 1.6 1.3 volume=0.876 peak=3397 ppm1=3.870 ppm2=1.549 assign ( resid 114 and name HN ) ( resid 115 and name HN ) 4.0 2.3 1.6 volume=0.259 peak=528 ppm1=8.799 ppm2=9.013 assign ( resid 76 and name HB1 ) ( resid 76 and name HD1 ) 4.2 2.5 1.7 volume=0.188 peak=2855 ppm1=1.986 ppm2=1.550 assign ( resid 20 and name HN ) ( resid 21 and name HG2# ) 3.5 1.8 1.4 volume=0.615 peak=835 ppm1=7.408 ppm2=1.134 assign ( resid 69 and name HN ) ( resid 69 and name HA2 ) 2.6 0.9 1.0 volume=3.316 peak=742 ppm1=8.218 ppm2=3.748 assign ( resid 40 and name HA ) ( resid 41 and name HN ) 3.5 1.8 1.4 volume=0.565 peak=3463 ppm1=3.988 ppm2=8.868 assign ( resid 74 and name HN ) ( resid 73 and name HA ) 3.1 1.4 1.2 volume=1.203 peak=498 ppm1=6.491 ppm2=3.906 assign ( resid 26 and name HG2# ) ( resid 37 and name HN ) 3.7 2.0 1.5 volume=0.400 peak=4783 ppm1=0.913 ppm2=9.695 assign ( resid 144 and name HN ) ( resid 109 and name HA ) 3.5 1.8 1.4 volume=0.588 peak=980 ppm1=7.537 ppm2=3.866 assign ( resid 39 and name HN ) ( resid 39 and name HA ) 3.0 1.3 1.2 volume=1.551 peak=734 ppm1=8.242 ppm2=4.139 assign ( resid 37 and name HN ) ( resid 28 and name HN ) 4.1 2.3 1.6 volume=0.240 peak=273 ppm1=9.659 ppm2=7.811 assign ( resid 2 and name HN ) ( resid 5 and name HB# ) 4.3 2.6 1.7 volume=0.162 peak=1630 ppm1=8.190 ppm2=1.280 assign ( resid 73 and name HG2# ) ( resid 72 and name HD1# ) 3.3 1.6 1.3 volume=0.786 peak=3618 ppm1=1.215 ppm2=0.576 assign ( resid 206 and name HN ) ( resid 208 and name HN ) 4.2 2.5 1.7 volume=0.203 peak=1967 ppm1=7.462 ppm2=8.049 assign ( resid 193 and name HN ) ( resid 193 and name HB ) 2.9 1.2 1.2 volume=1.824 peak=1084 ppm1=7.621 ppm2=2.057 assign ( resid 14 and name HB ) ( resid 15 and name HN ) 3.7 2.0 1.5 volume=0.391 peak=3233 ppm1=1.714 ppm2=7.863 assign ( resid 54 and name HB ) ( resid 54 and name HG2# ) 3.3 1.5 1.3 volume=0.900 peak=4547 ppm1=1.777 ppm2=0.574 assign ( resid 117 and name HD1# ) ( resid 117 and name HN ) 3.3 1.6 1.3 volume=0.800 peak=3016 ppm1=0.245 ppm2=8.236 assign ( resid 127 and name HD1# ) ( resid 115 and name HG2# ) 2.7 1.0 1.1 volume=2.869 peak=3960 ppm1=0.284 ppm2=0.702 assign ( resid 183 and name HG12 ) ( resid 183 and name HD1# ) 2.4 0.7 1.0 volume=5.550 peak=3714 ppm1=1.541 ppm2=0.865 assign ( resid 54 and name HN ) ( resid 55 and name HD1 ) 3.5 1.8 1.4 volume=0.557 peak=761 ppm1=9.022 ppm2=3.356 assign ( resid 53 and name HD1# ) ( resid 32 and name HE2 ) 3.7 2.0 1.5 volume=0.419 peak=4807 ppm1=0.796 ppm2=2.849 assign ( resid 184 and name HD1# ) ( resid 184 and name HG11 ) 2.6 0.9 1.1 volume=3.157 peak=4321 ppm1=0.895 ppm2=1.677 assign ( resid 30 and name HN ) ( resid 33 and name HG2# ) 3.8 2.1 1.5 volume=0.371 peak=2292 ppm1=8.722 ppm2=0.502 assign ( resid 62 and name HA ) ( resid 62 and name HN ) 3.9 2.2 1.6 volume=0.286 peak=3936 ppm1=3.963 ppm2=8.129 assign ( resid 196 and name HG2# ) ( resid 197 and name HG ) 2.8 1.1 1.1 volume=2.043 peak=4207 ppm1=0.812 ppm2=1.282 assign ( resid 53 and name HN ) ( resid 53 and name HG12 ) 2.9 1.2 1.2 volume=1.698 peak=1305 ppm1=8.309 ppm2=1.407 assign ( resid 36 and name HA ) ( resid 36 and name HB2 ) 4.4 2.7 1.6 volume=0.146 peak=3910 ppm1=5.852 ppm2=3.493 assign ( resid 171 and name HN ) ( resid 171 and name HA ) 4.0 2.3 1.6 volume=0.264 peak=2316 ppm1=9.062 ppm2=4.141 assign ( resid 112 and name HG2# ) ( resid 112 and name HD1# ) 2.7 1.0 1.1 volume=2.780 peak=3771 ppm1=0.679 ppm2=0.378 assign ( resid 51 and name HN ) ( resid 51 and name HA ) 3.7 2.0 1.5 volume=0.435 peak=1066 ppm1=8.427 ppm2=5.626 assign ( resid 75 and name HA ) ( resid 74 and name HA ) 3.9 2.1 1.5 volume=0.326 peak=2561 ppm1=4.153 ppm2=4.812 assign ( resid 64 and name HD1 or resid 64 and name HD2 ) ( resid 65 and name HD2# ) 4.0 2.3 1.6 volume=0.274 peak=86 ppm1=5.973 ppm2=0.344 assign ( resid 171 and name HN ) ( resid 47 and name HA ) 3.6 1.9 1.5 volume=0.471 peak=2363 ppm1=9.063 ppm2=4.783 assign ( resid 5 and name HA ) ( resid 4 and name HN ) 4.9 3.2 1.1 volume=0.079 peak=3017 ppm1=4.023 ppm2=8.192 assign ( resid 106 and name HA ) ( resid 105 and name HB2 ) 4.5 2.8 1.5 volume=0.125 peak=3982 ppm1=4.143 ppm2=3.903 assign ( resid 148 and name HN ) ( resid 147 and name HA ) 3.8 2.0 1.5 volume=0.383 peak=650 ppm1=9.152 ppm2=4.263 assign ( resid 57 and name HA ) ( resid 57 and name HN ) 4.0 2.3 1.6 volume=0.269 peak=3230 ppm1=4.134 ppm2=9.215 assign ( resid 199 and name HN ) ( resid 196 and name HA ) 3.1 1.4 1.3 volume=1.103 peak=360 ppm1=8.633 ppm2=3.477 assign ( resid 158 and name HN ) ( resid 165 and name HB2 ) 3.5 1.8 1.4 volume=0.581 peak=247 ppm1=8.219 ppm2=2.968 assign ( resid 208 and name HG2# ) ( resid 204 and name HB2 ) 3.3 1.6 1.3 volume=0.872 peak=3954 ppm1=1.139 ppm2=1.618 assign ( resid 176 and name HA ) ( resid 174 and name HG2 ) 3.0 1.3 1.2 volume=1.547 peak=3703 ppm1=3.997 ppm2=2.143 assign ( resid 3 and name HZ ) ( resid 134 and name HB1 ) 3.9 2.2 1.6 volume=0.289 peak=13 ppm1=6.204 ppm2=3.042 assign ( resid 94 and name HN ) ( resid 115 and name HG2# ) 3.8 2.1 1.5 volume=0.358 peak=385 ppm1=9.602 ppm2=0.620 assign ( resid 21 and name HN ) ( resid 22 and name HB2 ) 4.0 2.3 1.6 volume=0.262 peak=1469 ppm1=8.289 ppm2=3.740 assign ( resid 8 and name HB2 or resid 8 and name HB1 ) ( resid 4 and name HG1 or resid 4 and name HG2 ) 3.7 2.0 1.5 volume=0.419 peak=4129 ppm1=2.049 ppm2=1.355 assign ( resid 17 and name HD1 or resid 17 and name HD2 ) ( resid 17 and name HB1 or resid 17 and name HB2 ) 4.2 2.5 1.7 volume=0.203 peak=88 ppm1=6.485 ppm2=2.838 assign ( resid 15 and name HD2# ) ( resid 15 and name HN ) 3.4 1.7 1.3 volume=0.731 peak=4924 ppm1=0.684 ppm2=7.808 assign ( resid 167 and name HN ) ( resid 167 and name HB1 ) 3.2 1.5 1.3 volume=0.924 peak=1800 ppm1=8.643 ppm2=1.669 assign ( resid 93 and name HB ) ( resid 85 and name HN ) 4.2 2.5 1.7 volume=0.196 peak=3109 ppm1=1.224 ppm2=7.160 assign ( resid 26 and name HN ) ( resid 26 and name HB ) 2.7 1.0 1.1 volume=2.672 peak=2083 ppm1=8.863 ppm2=1.921 assign ( resid 192 and name HN ) ( resid 194 and name HB2 ) 3.3 1.6 1.3 volume=0.788 peak=1264 ppm1=8.208 ppm2=2.842 assign ( resid 199 and name HB# ) ( resid 198 and name HN ) 3.1 1.4 1.2 volume=1.187 peak=3199 ppm1=0.692 ppm2=8.719 assign ( resid 187 and name HG2# ) ( resid 188 and name HA ) 3.5 1.7 1.4 volume=0.618 peak=5021 ppm1=1.056 ppm2=4.219 assign ( resid 100 and name HN ) ( resid 101 and name HN ) 3.5 1.8 1.4 volume=0.601 peak=1199 ppm1=8.396 ppm2=8.437 assign ( resid 126 and name HD1# ) ( resid 14 and name HB ) 3.8 2.1 1.5 volume=0.366 peak=4742 ppm1=0.348 ppm2=1.711 assign ( resid 166 and name HN ) ( resid 165 and name HN ) 3.8 2.1 1.5 volume=0.347 peak=1252 ppm1=9.001 ppm2=8.474 assign ( resid 144 and name HG2# ) ( resid 144 and name HD1# ) 4.6 2.9 1.4 volume=0.113 peak=4663 ppm1=0.767 ppm2=0.622 assign ( resid 170 and name HA ) ( resid 171 and name HG1# ) 3.9 2.2 1.6 volume=0.311 peak=3891 ppm1=5.822 ppm2=0.900 assign ( resid 51 and name HA ) ( resid 169 and name HN ) 4.5 2.8 1.5 volume=0.128 peak=4675 ppm1=5.621 ppm2=9.300 assign ( resid 166 and name HN ) ( resid 158 and name HG1 ) 3.8 2.1 1.5 volume=0.339 peak=984 ppm1=9.000 ppm2=2.445 assign ( resid 136 and name HA ) ( resid 84 and name HG1# ) 2.9 1.2 1.2 volume=1.837 peak=4413 ppm1=3.792 ppm2=0.527 assign ( resid 168 and name HG1# ) ( resid 168 and name HA ) 3.2 1.4 1.3 volume=1.066 peak=3642 ppm1=0.768 ppm2=4.808 assign ( resid 34 and name HG2# ) ( resid 29 and name HA ) 4.0 2.3 1.6 volume=0.247 peak=5162 ppm1=1.102 ppm2=5.266 assign ( resid 204 and name HD2 ) ( resid 204 and name HE1 ) 2.9 1.1 1.1 volume=1.992 peak=4137 ppm1=1.485 ppm2=2.840 assign ( resid 46 and name HN ) ( resid 46 and name HB1 ) 2.9 1.1 1.1 volume=1.964 peak=942 ppm1=8.557 ppm2=1.529 assign ( resid 205 and name HN ) ( resid 208 and name HN ) 3.2 1.5 1.3 volume=1.050 peak=914 ppm1=7.186 ppm2=8.019 assign ( resid 75 and name HN ) ( resid 75 and name HA ) 3.1 1.4 1.2 volume=1.257 peak=990 ppm1=7.479 ppm2=4.147 assign ( resid 184 and name HG2# ) ( resid 184 and name HA ) 3.8 2.0 1.5 volume=0.380 peak=4105 ppm1=1.093 ppm2=3.643 assign ( resid 184 and name HG2# ) ( resid 184 and name HN ) 3.4 1.7 1.4 volume=0.721 peak=5047 ppm1=1.095 ppm2=7.503 assign ( resid 162 and name HA ) ( resid 158 and name HN ) 4.8 3.0 1.2 volume=0.092 peak=4091 ppm1=3.650 ppm2=8.226 assign ( resid 37 and name HN ) ( resid 36 and name HB1 ) 3.0 1.3 1.2 volume=1.336 peak=605 ppm1=9.657 ppm2=3.876 assign ( resid 96 and name HG2# ) ( resid 97 and name HN ) 3.9 2.1 1.5 volume=0.326 peak=3603 ppm1=1.143 ppm2=8.392 assign ( resid 61 and name HD1# ) ( resid 61 and name HG ) 3.1 1.4 1.2 volume=1.155 peak=2544 ppm1=0.748 ppm2=1.716 assign ( resid 115 and name HB ) ( resid 115 and name HG1# ) 3.6 1.9 1.5 volume=0.472 peak=2758 ppm1=0.231 ppm2=0.301 assign ( resid 1 and name HN# ) ( resid 1 and name HG1 ) 3.4 1.7 1.4 volume=0.655 peak=2394 ppm1=8.201 ppm2=2.313 assign ( resid 130 and name HN ) ( resid 130 and name HG2 or resid 130 and name HG1 ) 3.6 1.8 1.4 volume=0.524 peak=861 ppm1=7.617 ppm2=1.296 assign ( resid 153 and name HA ) ( resid 169 and name HB2 ) 4.2 2.5 1.7 volume=0.185 peak=4946 ppm1=5.317 ppm2=1.777 assign ( resid 114 and name HA ) ( resid 114 and name HB2 ) 4.1 2.4 1.6 volume=0.226 peak=5094 ppm1=4.461 ppm2=1.701 assign ( resid 111 and name HN ) ( resid 110 and name HN ) 3.2 1.4 1.3 volume=1.095 peak=981 ppm1=8.631 ppm2=8.733 assign ( resid 184 and name HD1# ) ( resid 179 and name HD2# ) 3.1 1.4 1.2 volume=1.198 peak=4282 ppm1=0.890 ppm2=0.733 assign ( resid 8 and name HB2 or resid 8 and name HB1 ) ( resid 8 and name HN ) 3.1 1.3 1.2 volume=1.317 peak=3189 ppm1=2.048 ppm2=7.610 assign ( resid 185 and name HN ) ( resid 184 and name HN ) 2.8 1.1 1.1 volume=2.183 peak=370 ppm1=8.186 ppm2=7.518 assign ( resid 15 and name HD1# ) ( resid 15 and name HB1 ) 2.8 1.1 1.1 volume=2.246 peak=2971 ppm1=0.439 ppm2=1.715 assign ( resid 151 and name HN ) ( resid 14 and name HB ) 3.8 2.0 1.5 volume=0.375 peak=294 ppm1=8.646 ppm2=1.663 assign ( resid 205 and name HA ) ( resid 204 and name HN ) 3.6 1.9 1.5 volume=0.463 peak=4782 ppm1=4.140 ppm2=6.761 assign ( resid 28 and name HN ) ( resid 26 and name HG1# ) 2.6 0.9 1.0 volume=3.482 peak=1226 ppm1=7.808 ppm2=0.753 assign ( resid 163 and name HN ) ( resid 162 and name HD2 ) 3.2 1.5 1.3 volume=1.054 peak=480 ppm1=7.324 ppm2=3.485 assign ( resid 131 and name HN ) ( resid 132 and name HN ) 3.8 2.1 1.5 volume=0.359 peak=1745 ppm1=9.293 ppm2=7.912 assign ( resid 115 and name HG2# ) ( resid 115 and name HA ) 4.0 2.3 1.6 volume=0.260 peak=2903 ppm1=0.660 ppm2=4.403 assign ( resid 60 and name HE1 ) ( resid 203 and name HD1# ) 2.8 1.1 1.1 volume=2.049 peak=4327 ppm1=2.834 ppm2=-0.017 assign ( resid 73 and name HB ) ( resid 72 and name HA ) 4.5 2.8 1.5 volume=0.129 peak=4024 ppm1=4.301 ppm2=3.643 assign ( resid 184 and name HG12 ) ( resid 184 and name HA ) 4.1 2.4 1.6 volume=0.222 peak=4908 ppm1=1.094 ppm2=3.629 assign ( resid 15 and name HD1# ) ( resid 126 and name HD1# ) 2.0 0.3 0.8 volume=14.791 peak=3047 ppm1=0.439 ppm2=0.349 assign ( resid 145 and name HB2 ) ( resid 139 and name HD1 ) 3.0 1.3 1.2 volume=1.399 peak=3995 ppm1=1.932 ppm2=3.632 assign ( resid 80 and name HG1# ) ( resid 81 and name HN ) 3.5 1.8 1.4 volume=0.541 peak=3625 ppm1=0.709 ppm2=8.518 assign ( resid 132 and name HB ) ( resid 133 and name HN ) 4.1 2.4 1.7 volume=0.216 peak=2831 ppm1=2.285 ppm2=8.119 assign ( resid 167 and name HN ) ( resid 166 and name HE1 ) 4.4 2.7 1.6 volume=0.148 peak=1421 ppm1=8.643 ppm2=2.717 assign ( resid 199 and name HA ) ( resid 200 and name HN ) 4.2 2.5 1.7 volume=0.183 peak=4779 ppm1=2.797 ppm2=8.108 assign ( resid 158 and name HG1 ) ( resid 165 and name HN ) 4.7 3.0 1.3 volume=0.099 peak=2848 ppm1=2.438 ppm2=8.449 assign ( resid 206 and name HN ) ( resid 205 and name HN ) 3.1 1.4 1.2 volume=1.213 peak=1552 ppm1=7.463 ppm2=7.135 assign ( resid 114 and name HD2# ) ( resid 7 and name HA ) 3.4 1.7 1.4 volume=0.676 peak=3515 ppm1=0.781 ppm2=3.719 assign ( resid 3 and name HD1 or resid 3 and name HD2 ) ( resid 3 and name HE1 or resid 3 and name HE2 ) 2.3 0.6 0.9 volume=6.904 peak=24 ppm1=7.378 ppm2=7.211 assign ( resid 98 and name HN ) ( resid 110 and name HA ) 3.6 1.9 1.5 volume=0.473 peak=1807 ppm1=9.354 ppm2=5.445 assign ( resid 201 and name HA ) ( resid 203 and name HN ) 4.0 2.2 1.6 volume=0.280 peak=2635 ppm1=4.334 ppm2=7.670 assign ( resid 166 and name HB1 ) ( resid 167 and name HN ) 4.0 2.3 1.6 volume=0.244 peak=3758 ppm1=1.653 ppm2=8.591 assign ( resid 4 and name HN ) ( resid 3 and name HB1 or resid 3 and name HB2 ) 3.3 1.6 1.3 volume=0.858 peak=862 ppm1=8.188 ppm2=2.968 assign ( resid 67 and name HN ) ( resid 65 and name HD2# ) 3.6 1.9 1.4 volume=0.518 peak=1843 ppm1=7.602 ppm2=0.359 assign ( resid 192 and name HD2# ) ( resid 48 and name HB2 ) 4.1 2.4 1.6 volume=0.228 peak=3412 ppm1=0.490 ppm2=2.723 assign ( resid 134 and name HD1 or resid 134 and name HD2 ) ( resid 134 and name HB2 ) 3.4 1.7 1.4 volume=0.677 peak=20 ppm1=6.862 ppm2=2.931 assign ( resid 136 and name HA ) ( resid 136 and name HG1 ) 3.9 2.2 1.6 volume=0.290 peak=3575 ppm1=3.788 ppm2=1.987 assign ( resid 103 and name HG2# ) ( resid 102 and name HB# ) 3.5 1.8 1.4 volume=0.583 peak=3884 ppm1=0.879 ppm2=1.294 assign ( resid 82 and name HA ) ( resid 82 and name HB1 ) 3.8 2.0 1.5 volume=0.377 peak=2532 ppm1=5.042 ppm2=2.528 assign ( resid 132 and name HG2# ) ( resid 133 and name HN ) 3.7 2.0 1.5 volume=0.433 peak=4824 ppm1=0.936 ppm2=8.125 assign ( resid 104 and name HN ) ( resid 104 and name HA1 ) 3.1 1.4 1.3 volume=1.115 peak=997 ppm1=8.051 ppm2=4.012 assign ( resid 192 and name HN ) ( resid 50 and name HG1# ) 3.3 1.5 1.3 volume=0.902 peak=2147 ppm1=8.209 ppm2=0.628 assign ( resid 24 and name HH2 ) ( resid 24 and name HZ2 ) 3.8 2.1 1.5 volume=0.332 peak=134 ppm1=6.802 ppm2=7.539 assign ( resid 185 and name HN ) ( resid 187 and name HG2# ) 2.9 1.2 1.2 volume=1.827 peak=1073 ppm1=8.185 ppm2=1.009 assign ( resid 101 and name HN ) ( resid 102 and name HN ) 2.9 1.1 1.1 volume=1.946 peak=433 ppm1=8.476 ppm2=8.547 assign ( resid 176 and name HN ) ( resid 173 and name HG2# ) 3.9 2.2 1.6 volume=0.307 peak=2372 ppm1=8.404 ppm2=1.014 assign ( resid 126 and name HN ) ( resid 119 and name HA ) 3.5 1.8 1.4 volume=0.537 peak=331 ppm1=9.104 ppm2=4.805 assign ( resid 183 and name HG2# ) ( resid 183 and name HG12 ) 2.7 1.0 1.1 volume=2.734 peak=4694 ppm1=0.932 ppm2=1.543 assign ( resid 98 and name HN ) ( resid 96 and name HG2# ) 3.7 2.0 1.5 volume=0.433 peak=1276 ppm1=9.355 ppm2=1.135 assign ( resid 15 and name HN ) ( resid 12 and name HA ) 2.9 1.2 1.2 volume=1.703 peak=1012 ppm1=7.810 ppm2=3.862 assign ( resid 130 and name HN ) ( resid 130 and name HA ) 3.3 1.6 1.3 volume=0.762 peak=2021 ppm1=7.617 ppm2=3.877 assign ( resid 169 and name HN ) ( resid 168 and name HB ) 3.3 1.6 1.3 volume=0.812 peak=1568 ppm1=9.258 ppm2=1.688 assign ( resid 201 and name HB2 ) ( resid 200 and name HN ) 4.0 2.3 1.6 volume=0.273 peak=3333 ppm1=2.581 ppm2=8.124 assign ( resid 71 and name HN ) ( resid 71 and name HG1 ) 3.5 1.8 1.4 volume=0.542 peak=1588 ppm1=7.219 ppm2=0.297 assign ( resid 200 and name HE1 ) ( resid 54 and name HD1# ) 3.4 1.6 1.3 volume=0.738 peak=3821 ppm1=2.805 ppm2=0.510 assign ( resid 113 and name HN ) ( resid 112 and name HN ) 2.6 0.9 1.0 volume=3.335 peak=1942 ppm1=8.232 ppm2=8.136 assign ( resid 154 and name HG2# ) ( resid 168 and name HG2# ) 3.6 1.9 1.4 volume=0.508 peak=4202 ppm1=0.843 ppm2=0.183 assign ( resid 197 and name HA ) ( resid 197 and name HB1 ) 2.8 1.1 1.1 volume=2.376 peak=2924 ppm1=3.793 ppm2=1.782 assign ( resid 137 and name HB1 ) ( resid 112 and name HD1# ) 3.8 2.1 1.5 volume=0.350 peak=2820 ppm1=2.808 ppm2=0.376 assign ( resid 156 and name HN ) ( resid 155 and name HN ) 3.1 1.3 1.2 volume=1.310 peak=1612 ppm1=8.551 ppm2=8.958 assign ( resid 115 and name HN ) ( resid 114 and name HA ) 3.3 1.6 1.3 volume=0.861 peak=1533 ppm1=9.053 ppm2=4.451 assign ( resid 136 and name HG1 ) ( resid 136 and name HA ) 3.6 1.9 1.4 volume=0.487 peak=4959 ppm1=1.953 ppm2=3.774 assign ( resid 17 and name HD1 or resid 17 and name HD2 ) ( resid 18 and name HN ) 3.1 1.4 1.2 volume=1.280 peak=53 ppm1=6.484 ppm2=7.792 assign ( resid 51 and name HN ) ( resid 34 and name HB ) 3.0 1.3 1.2 volume=1.399 peak=638 ppm1=8.424 ppm2=3.846 assign ( resid 94 and name HN ) ( resid 94 and name HA ) 3.6 1.8 1.4 volume=0.522 peak=2079 ppm1=9.601 ppm2=5.047 assign ( resid 180 and name HN ) ( resid 184 and name HB ) 3.6 1.8 1.4 volume=0.535 peak=808 ppm1=8.352 ppm2=2.058 assign ( resid 121 and name HN ) ( resid 119 and name HN ) 4.0 2.3 1.6 volume=0.254 peak=2344 ppm1=8.585 ppm2=8.055 assign ( resid 193 and name HB ) ( resid 33 and name HG2# ) 4.1 2.4 1.6 volume=0.226 peak=2882 ppm1=2.055 ppm2=0.515 assign ( resid 174 and name HN ) ( resid 173 and name HG2# ) 3.1 1.4 1.2 volume=1.158 peak=1404 ppm1=9.152 ppm2=1.028 assign ( resid 186 and name HA ) ( resid 186 and name HN ) 3.6 1.9 1.4 volume=0.518 peak=3778 ppm1=4.216 ppm2=7.370 assign ( resid 124 and name HN ) ( resid 122 and name HN ) 3.2 1.5 1.3 volume=1.017 peak=952 ppm1=6.471 ppm2=8.699 assign ( resid 158 and name HG1 ) ( resid 53 and name HG2# ) 3.7 2.0 1.5 volume=0.413 peak=2579 ppm1=2.440 ppm2=0.918 assign ( resid 174 and name HN ) ( resid 173 and name HN ) 3.5 1.7 1.4 volume=0.623 peak=1234 ppm1=9.152 ppm2=8.561 assign ( resid 28 and name HN ) ( resid 29 and name HA ) 3.9 2.2 1.6 volume=0.291 peak=904 ppm1=7.810 ppm2=5.263 assign ( resid 190 and name HA ) ( resid 194 and name HN ) 4.1 2.3 1.6 volume=0.242 peak=2472 ppm1=3.977 ppm2=7.780 assign ( resid 196 and name HD1# ) ( resid 196 and name HN ) 3.4 1.7 1.4 volume=0.639 peak=2876 ppm1=0.724 ppm2=7.475 assign ( resid 125 and name HN ) ( resid 155 and name HB2 ) 2.8 1.1 1.1 volume=2.345 peak=758 ppm1=8.772 ppm2=2.573 assign ( resid 155 and name HN ) ( resid 124 and name HB1 ) 3.6 1.9 1.4 volume=0.473 peak=639 ppm1=8.977 ppm2=2.056 assign ( resid 80 and name HA ) ( resid 81 and name HN ) 3.7 2.0 1.5 volume=0.413 peak=4680 ppm1=3.985 ppm2=8.476 assign ( resid 26 and name HA ) ( resid 36 and name HA ) 3.9 2.2 1.6 volume=0.287 peak=3804 ppm1=3.980 ppm2=5.914 assign ( resid 106 and name HN ) ( resid 106 and name HA ) 2.8 1.1 1.1 volume=2.187 peak=1908 ppm1=7.942 ppm2=4.138 assign ( resid 179 and name HD2# ) ( resid 179 and name HB1 ) 4.1 2.4 1.6 volume=0.222 peak=4173 ppm1=0.743 ppm2=2.754 assign ( resid 71 and name HN ) ( resid 69 and name HA1 ) 3.3 1.6 1.3 volume=0.796 peak=813 ppm1=7.222 ppm2=3.751 assign ( resid 197 and name HA ) ( resid 199 and name HB# ) 2.9 1.2 1.2 volume=1.876 peak=3070 ppm1=3.793 ppm2=0.701 assign ( resid 175 and name HB2 ) ( resid 175 and name HN ) 4.6 2.8 1.4 volume=0.119 peak=2610 ppm1=2.451 ppm2=8.833 assign ( resid 91 and name HG2# ) ( resid 114 and name HD1# ) 3.4 1.7 1.4 volume=0.672 peak=2775 ppm1=1.017 ppm2=0.513 assign ( resid 207 and name HD2 ) ( resid 207 and name HN ) 4.1 2.4 1.6 volume=0.230 peak=3818 ppm1=3.034 ppm2=7.829 assign ( resid 78 and name HN ) ( resid 99 and name HB2 ) 2.9 1.2 1.2 volume=1.731 peak=1358 ppm1=7.149 ppm2=1.796 assign ( resid 115 and name HG2# ) ( resid 115 and name HB ) 2.4 0.7 1.0 volume=5.374 peak=4356 ppm1=0.660 ppm2=0.233 assign ( resid 19 and name HN ) ( resid 19 and name HG1 or resid 19 and name HG2 ) 2.7 1.0 1.1 volume=2.915 peak=1603 ppm1=7.480 ppm2=1.664 assign ( resid 213 and name HN ) ( resid 212 and name HA ) 4.3 2.6 1.7 volume=0.161 peak=2180 ppm1=8.280 ppm2=4.133 assign ( resid 194 and name HA ) ( resid 196 and name HN ) 2.8 1.1 1.1 volume=2.091 peak=4740 ppm1=4.335 ppm2=7.416 assign ( resid 116 and name HN ) ( resid 128 and name HN ) 4.6 2.9 1.4 volume=0.111 peak=655 ppm1=8.834 ppm2=9.931 assign ( resid 38 and name HN ) ( resid 37 and name HN ) 3.0 1.2 1.2 volume=1.620 peak=1312 ppm1=8.464 ppm2=9.622 assign ( resid 98 and name HG2# ) ( resid 96 and name HG2# ) 2.8 1.1 1.1 volume=2.135 peak=2588 ppm1=1.324 ppm2=1.144 assign ( resid 200 and name HB2 ) ( resid 197 and name HD2# ) 3.4 1.6 1.3 volume=0.739 peak=4286 ppm1=1.670 ppm2=0.773 assign ( resid 180 and name HB2 ) ( resid 183 and name HB ) 3.1 1.4 1.2 volume=1.177 peak=5027 ppm1=3.906 ppm2=1.939 assign ( resid 101 and name HN ) ( resid 106 and name HG2# ) 3.3 1.6 1.3 volume=0.786 peak=1607 ppm1=8.464 ppm2=0.876 assign ( resid 167 and name HN ) ( resid 54 and name HG11 or resid 54 and name HG12 ) 3.2 1.5 1.3 volume=0.979 peak=1578 ppm1=8.642 ppm2=1.149 assign ( resid 57 and name HN ) ( resid 56 and name HA ) 2.8 1.0 1.1 volume=2.388 peak=1056 ppm1=9.217 ppm2=4.535 assign ( resid 126 and name HG2# ) ( resid 126 and name HB ) 2.8 1.1 1.1 volume=2.016 peak=2952 ppm1=0.751 ppm2=1.598 assign ( resid 159 and name HN ) ( resid 158 and name HN ) 3.9 2.2 1.6 volume=0.297 peak=1409 ppm1=9.026 ppm2=8.180 assign ( resid 196 and name HD1# ) ( resid 196 and name HG12 ) 2.9 1.1 1.1 volume=1.929 peak=3880 ppm1=0.727 ppm2=1.480 assign ( resid 203 and name HB ) ( resid 201 and name HN ) 4.5 2.8 1.5 volume=0.123 peak=2804 ppm1=0.127 ppm2=7.404 assign ( resid 162 and name HD1 ) ( resid 162 and name HG1 ) 3.2 1.5 1.3 volume=0.919 peak=3133 ppm1=3.490 ppm2=1.922 assign ( resid 40 and name HN ) ( resid 39 and name HA ) 3.2 1.4 1.3 volume=1.081 peak=1158 ppm1=8.507 ppm2=4.126 assign ( resid 109 and name HN ) ( resid 110 and name HN ) 3.7 2.0 1.5 volume=0.439 peak=2451 ppm1=8.164 ppm2=8.689 assign ( resid 134 and name HZ ) ( resid 84 and name HG1# ) 2.7 1.0 1.1 volume=2.651 peak=110 ppm1=6.643 ppm2=0.536 assign ( resid 50 and name HN ) ( resid 51 and name HN ) 4.1 2.4 1.6 volume=0.221 peak=1119 ppm1=9.299 ppm2=8.430 assign ( resid 81 and name HN ) ( resid 72 and name HG11 ) 3.4 1.7 1.4 volume=0.721 peak=1946 ppm1=8.507 ppm2=1.143 assign ( resid 51 and name HB1 or resid 51 and name HB2 ) ( resid 168 and name HG2# ) 3.1 1.3 1.2 volume=1.298 peak=4194 ppm1=1.781 ppm2=0.190 assign ( resid 87 and name HA ) ( resid 87 and name HD1# ) 3.7 2.0 1.5 volume=0.394 peak=4138 ppm1=3.870 ppm2=0.440 assign ( resid 10 and name HG2# ) ( resid 10 and name HB ) 3.1 1.4 1.2 volume=1.177 peak=4020 ppm1=1.084 ppm2=3.643 assign ( resid 196 and name HG2# ) ( resid 193 and name HB ) 3.3 1.6 1.3 volume=0.806 peak=2896 ppm1=0.813 ppm2=2.034 assign ( resid 74 and name HN ) ( resid 74 and name HB1 ) 3.3 1.6 1.3 volume=0.841 peak=502 ppm1=6.495 ppm2=3.296 assign ( resid 114 and name HD1# ) ( resid 115 and name HG1# ) 3.7 1.9 1.5 volume=0.453 peak=4585 ppm1=0.536 ppm2=0.271 assign ( resid 127 and name HD1# ) ( resid 127 and name HG2# ) 2.9 1.1 1.1 volume=1.961 peak=3039 ppm1=0.286 ppm2=0.793 assign ( resid 35 and name HB ) ( resid 27 and name HG1# ) 2.6 0.9 1.1 volume=3.147 peak=4623 ppm1=2.053 ppm2=0.893 assign ( resid 82 and name HN ) ( resid 81 and name HA ) 3.4 1.7 1.4 volume=0.667 peak=895 ppm1=8.563 ppm2=4.660 assign ( resid 185 and name HN ) ( resid 182 and name HA ) 2.8 1.1 1.1 volume=2.218 peak=2350 ppm1=8.182 ppm2=4.136 assign ( resid 7 and name HA ) ( resid 7 and name HN ) 4.3 2.6 1.7 volume=0.172 peak=4836 ppm1=3.709 ppm2=8.453 assign ( resid 72 and name HN ) ( resid 74 and name HN ) 3.9 2.2 1.6 volume=0.307 peak=213 ppm1=7.535 ppm2=6.484 assign ( resid 169 and name HA ) ( resid 168 and name HG2# ) 3.7 1.9 1.5 volume=0.451 peak=2672 ppm1=5.232 ppm2=0.190 assign ( resid 154 and name HG1# ) ( resid 153 and name HB1 ) 3.7 1.9 1.5 volume=0.446 peak=4707 ppm1=0.916 ppm2=2.856 assign ( resid 184 and name HN ) ( resid 187 and name HG2# ) 2.7 1.0 1.1 volume=2.599 peak=1849 ppm1=7.499 ppm2=1.016 assign ( resid 144 and name HN ) ( resid 110 and name HN ) 4.3 2.6 1.7 volume=0.170 peak=159 ppm1=7.535 ppm2=8.701 assign ( resid 93 and name HG12 ) ( resid 93 and name HB ) 3.8 2.1 1.5 volume=0.341 peak=2938 ppm1=0.597 ppm2=1.231 assign ( resid 84 and name HG1# ) ( resid 134 and name HZ ) 3.4 1.6 1.3 volume=0.739 peak=3018 ppm1=0.533 ppm2=6.647 assign ( resid 61 and name HN ) ( resid 60 and name HN ) 3.4 1.7 1.4 volume=0.698 peak=1762 ppm1=8.715 ppm2=7.270 assign ( resid 167 and name HD2# ) ( resid 54 and name HD1# ) 3.1 1.3 1.2 volume=1.301 peak=4739 ppm1=0.764 ppm2=0.498 assign ( resid 105 and name HN ) ( resid 105 and name HA ) 3.0 1.3 1.2 volume=1.377 peak=2442 ppm1=7.944 ppm2=4.138 assign ( resid 169 and name HG2 ) ( resid 169 and name HB1 ) 3.1 1.4 1.2 volume=1.279 peak=3578 ppm1=1.934 ppm2=1.789 assign ( resid 54 and name HG2# ) ( resid 54 and name HG12 ) 2.9 1.2 1.2 volume=1.728 peak=2908 ppm1=0.577 ppm2=1.233 assign ( resid 37 and name HN ) ( resid 25 and name HB1 ) 3.3 1.6 1.3 volume=0.807 peak=866 ppm1=9.659 ppm2=1.660 assign ( resid 196 and name HN ) ( resid 195 and name HA ) 3.4 1.7 1.4 volume=0.642 peak=1296 ppm1=7.438 ppm2=4.436 assign ( resid 29 and name HA ) ( resid 29 and name HB ) 4.3 2.6 1.7 volume=0.176 peak=4671 ppm1=5.251 ppm2=3.905 assign ( resid 143 and name HN ) ( resid 140 and name HB2 ) 3.2 1.4 1.3 volume=1.065 peak=1498 ppm1=6.899 ppm2=4.048 assign ( resid 98 and name HN ) ( resid 99 and name HN ) 4.0 2.3 1.6 volume=0.245 peak=2374 ppm1=9.353 ppm2=7.787 assign ( resid 7 and name HB# ) ( resid 8 and name HN ) 3.3 1.6 1.3 volume=0.772 peak=2497 ppm1=0.752 ppm2=7.614 assign ( resid 151 and name HN ) ( resid 149 and name HB2 ) 3.4 1.7 1.4 volume=0.723 peak=1690 ppm1=8.645 ppm2=2.835 assign ( resid 7 and name HN ) ( resid 6 and name HB ) 2.9 1.1 1.1 volume=1.938 peak=2411 ppm1=8.434 ppm2=1.680 assign ( resid 127 and name HN ) ( resid 126 and name HA ) 3.6 1.8 1.4 volume=0.535 peak=1816 ppm1=9.383 ppm2=5.428 assign ( resid 145 and name HN ) ( resid 144 and name HD1# ) 3.1 1.4 1.2 volume=1.275 peak=1886 ppm1=8.380 ppm2=0.622 assign ( resid 114 and name HD2# ) ( resid 3 and name HD1 or resid 3 and name HD2 ) 3.6 1.9 1.5 volume=0.466 peak=3445 ppm1=0.781 ppm2=7.375 assign ( resid 190 and name HN ) ( resid 188 and name HB2 ) 3.6 1.9 1.4 volume=0.501 peak=821 ppm1=7.520 ppm2=1.396 assign ( resid 153 and name HA ) ( resid 154 and name HG1# ) 3.8 2.1 1.5 volume=0.372 peak=4189 ppm1=5.318 ppm2=0.867 assign ( resid 196 and name HD1# ) ( resid 167 and name HG ) 2.6 0.9 1.1 volume=3.212 peak=2462 ppm1=0.728 ppm2=0.940 assign ( resid 15 and name HN ) ( resid 154 and name HG1# ) 2.8 1.1 1.1 volume=2.374 peak=2329 ppm1=7.811 ppm2=0.881 assign ( resid 155 and name HB1 ) ( resid 155 and name HB2 ) 4.2 2.4 1.7 volume=0.208 peak=2590 ppm1=3.006 ppm2=2.577 assign ( resid 8 and name HG1 or resid 8 and name HG2 ) ( resid 4 and name HD2 or resid 4 and name HD1 ) 3.9 2.2 1.6 volume=0.290 peak=3633 ppm1=2.320 ppm2=1.486 assign ( resid 3 and name HE1 or resid 3 and name HE2 ) ( resid 3 and name HD1 or resid 3 and name HD2 ) 2.3 0.5 0.9 volume=8.162 peak=69 ppm1=7.213 ppm2=7.380 assign ( resid 76 and name HE2 ) ( resid 76 and name HG1 ) 2.3 0.6 0.9 volume=7.304 peak=4708 ppm1=2.912 ppm2=1.385 assign ( resid 80 and name HN ) ( resid 80 and name HA ) 3.5 1.7 1.4 volume=0.624 peak=1176 ppm1=7.524 ppm2=4.008 assign ( resid 28 and name HB1 or resid 28 and name HB2 ) ( resid 28 and name HE2 ) 3.7 2.0 1.5 volume=0.414 peak=4393 ppm1=1.911 ppm2=2.827 assign ( resid 62 and name HN ) ( resid 61 and name HD2# ) 3.3 1.5 1.3 volume=0.900 peak=449 ppm1=8.131 ppm2=0.744 assign ( resid 67 and name HG2 ) ( resid 67 and name HA ) 4.1 2.4 1.7 volume=0.216 peak=5012 ppm1=2.570 ppm2=3.936 assign ( resid 202 and name HN ) ( resid 199 and name HB# ) 3.3 1.6 1.3 volume=0.772 peak=356 ppm1=8.576 ppm2=0.685 assign ( resid 102 and name HB# ) ( resid 101 and name HA ) 4.1 2.4 1.7 volume=0.216 peak=4986 ppm1=1.279 ppm2=4.678 assign ( resid 7 and name HN ) ( resid 7 and name HB# ) 2.4 0.7 1.0 volume=5.439 peak=1194 ppm1=8.424 ppm2=0.753 assign ( resid 192 and name HG ) ( resid 189 and name HA ) 5.1 3.4 0.9 volume=0.062 peak=3753 ppm1=1.754 ppm2=4.617 assign ( resid 94 and name HN ) ( resid 93 and name HD1# ) 3.7 1.9 1.5 volume=0.443 peak=1506 ppm1=9.604 ppm2=-0.277 assign ( resid 51 and name HN ) ( resid 50 and name HN ) 3.8 2.1 1.5 volume=0.335 peak=1203 ppm1=8.428 ppm2=9.313 assign ( resid 106 and name HA ) ( resid 106 and name HG2# ) 3.1 1.4 1.2 volume=1.198 peak=5060 ppm1=4.143 ppm2=0.893 assign ( resid 100 and name HB1 ) ( resid 101 and name HA ) 3.8 2.1 1.5 volume=0.340 peak=3210 ppm1=3.736 ppm2=4.686 assign ( resid 5 and name HB# ) ( resid 9 and name HN ) 3.9 2.2 1.6 volume=0.295 peak=2832 ppm1=1.341 ppm2=7.997 assign ( resid 8 and name HB2 or resid 8 and name HB1 ) ( resid 9 and name HN ) 3.3 1.6 1.3 volume=0.760 peak=3066 ppm1=2.047 ppm2=7.992 assign ( resid 5 and name HA ) ( resid 5 and name HN ) 4.7 3.0 1.3 volume=0.103 peak=4068 ppm1=4.023 ppm2=7.469 assign ( resid 93 and name HN ) ( resid 94 and name HN ) 4.1 2.4 1.6 volume=0.226 peak=566 ppm1=8.908 ppm2=9.613 assign ( resid 166 and name HG2 ) ( resid 166 and name HD2 ) 2.4 0.6 0.9 volume=6.190 peak=3000 ppm1=1.254 ppm2=1.447 assign ( resid 199 and name HA ) ( resid 199 and name HB# ) 3.3 1.5 1.3 volume=0.910 peak=2616 ppm1=2.796 ppm2=0.692 assign ( resid 194 and name HN ) ( resid 193 and name HN ) 2.7 1.0 1.1 volume=2.675 peak=1376 ppm1=7.774 ppm2=7.631 assign ( resid 87 and name HD1# ) ( resid 87 and name HA ) 3.7 1.9 1.5 volume=0.447 peak=2479 ppm1=0.440 ppm2=3.858 assign ( resid 46 and name HB1 ) ( resid 46 and name HN ) 4.4 2.7 1.6 volume=0.143 peak=4685 ppm1=1.542 ppm2=8.564 assign ( resid 169 and name HN ) ( resid 168 and name HA ) 3.4 1.6 1.3 volume=0.758 peak=1441 ppm1=9.256 ppm2=4.792 assign ( resid 179 and name HG ) ( resid 179 and name HD1# ) 3.3 1.5 1.3 volume=0.907 peak=5020 ppm1=1.516 ppm2=0.522 assign ( resid 154 and name HG1# ) ( resid 124 and name HG2 ) 3.0 1.3 1.2 volume=1.455 peak=4823 ppm1=0.917 ppm2=2.369 assign ( resid 72 and name HD1# ) ( resid 71 and name HD2 or resid 71 and name HD1 ) 4.2 2.5 1.7 volume=0.189 peak=2487 ppm1=0.590 ppm2=2.818 assign ( resid 73 and name HG2# ) ( resid 73 and name HA ) 3.1 1.4 1.3 volume=1.149 peak=4009 ppm1=1.218 ppm2=3.918 assign ( resid 60 and name HB1 ) ( resid 203 and name HG11 ) 3.4 1.6 1.3 volume=0.749 peak=4092 ppm1=1.719 ppm2=0.506 assign ( resid 92 and name HE1 or resid 92 and name HE2 ) ( resid 91 and name HA ) 3.2 1.5 1.3 volume=0.982 peak=114 ppm1=6.750 ppm2=5.919 assign ( resid 86 and name HD1 ) ( resid 86 and name HB2 ) 2.2 0.5 0.9 volume=9.876 peak=2676 ppm1=2.929 ppm2=1.555 assign ( resid 106 and name HG2# ) ( resid 106 and name HA ) 4.0 2.3 1.6 volume=0.262 peak=4810 ppm1=0.896 ppm2=4.140 assign ( resid 121 and name HB1 ) ( resid 121 and name HG2 ) 2.6 0.9 1.0 volume=3.483 peak=3441 ppm1=2.052 ppm2=2.311 assign ( resid 110 and name HN ) ( resid 143 and name HA ) 3.2 1.5 1.3 volume=0.948 peak=543 ppm1=8.719 ppm2=4.661 assign ( resid 3 and name HE1 or resid 3 and name HE2 ) ( resid 114 and name HB2 ) 3.4 1.7 1.3 volume=0.729 peak=57 ppm1=7.212 ppm2=1.709 assign ( resid 14 and name HG1# ) ( resid 14 and name HB ) 2.8 1.1 1.1 volume=2.243 peak=3813 ppm1=0.675 ppm2=1.715 assign ( resid 202 and name HN ) ( resid 201 and name HA ) 3.3 1.6 1.3 volume=0.808 peak=1447 ppm1=8.577 ppm2=4.275 assign ( resid 120 and name HA ) ( resid 120 and name HB1 ) 3.6 1.9 1.4 volume=0.486 peak=3852 ppm1=4.501 ppm2=2.999 assign ( resid 184 and name HA ) ( resid 179 and name HB2 ) 3.9 2.2 1.6 volume=0.285 peak=4133 ppm1=3.628 ppm2=2.398 assign ( resid 36 and name HB1 ) ( resid 24 and name HD1 ) 4.6 2.9 1.4 volume=0.114 peak=3469 ppm1=3.860 ppm2=6.773 assign ( resid 160 and name HG2 ) ( resid 160 and name HA ) 4.9 3.2 1.1 volume=0.079 peak=3424 ppm1=2.201 ppm2=4.008 assign ( resid 60 and name HG1 ) ( resid 63 and name HB2 ) 3.5 1.8 1.4 volume=0.566 peak=4516 ppm1=1.322 ppm2=2.727 assign ( resid 112 and name HN ) ( resid 113 and name HA ) 4.2 2.5 1.7 volume=0.182 peak=2296 ppm1=8.135 ppm2=5.314 assign ( resid 13 and name HN ) ( resid 11 and name HB# ) 2.8 1.1 1.1 volume=2.324 peak=464 ppm1=7.727 ppm2=1.668 assign ( resid 188 and name HA ) ( resid 191 and name HN ) 4.4 2.7 1.6 volume=0.152 peak=4591 ppm1=4.217 ppm2=7.671 assign ( resid 72 and name HG12 ) ( resid 72 and name HA ) 4.4 2.7 1.6 volume=0.140 peak=5142 ppm1=1.044 ppm2=3.632 assign ( resid 197 and name HN ) ( resid 196 and name HB ) 3.3 1.6 1.3 volume=0.799 peak=874 ppm1=7.988 ppm2=2.249 assign ( resid 35 and name HB ) ( resid 192 and name HD1# ) 3.9 2.2 1.6 volume=0.285 peak=4863 ppm1=2.051 ppm2=0.522 assign ( resid 191 and name HA ) ( resid 195 and name HN ) 4.7 3.0 1.3 volume=0.094 peak=3980 ppm1=4.272 ppm2=8.000 assign ( resid 196 and name HN ) ( resid 196 and name HD1# ) 2.5 0.8 1.0 volume=4.332 peak=516 ppm1=7.438 ppm2=0.749 assign ( resid 196 and name HG11 ) ( resid 196 and name HD1# ) 2.8 1.1 1.1 volume=2.103 peak=3191 ppm1=1.806 ppm2=0.720 assign ( resid 110 and name HN ) ( resid 144 and name HG2# ) 3.5 1.8 1.4 volume=0.546 peak=261 ppm1=8.721 ppm2=0.754 assign ( resid 155 and name HN ) ( resid 127 and name HN ) 3.9 2.2 1.5 volume=0.318 peak=1060 ppm1=8.976 ppm2=9.354 assign ( resid 204 and name HN ) ( resid 201 and name HA ) 3.5 1.7 1.4 volume=0.617 peak=2040 ppm1=6.748 ppm2=4.272 assign ( resid 112 and name HD1# ) ( resid 112 and name HG11 ) 3.4 1.7 1.4 volume=0.706 peak=2900 ppm1=0.373 ppm2=1.604 assign ( resid 153 and name HN ) ( resid 127 and name HN ) 2.9 1.2 1.2 volume=1.732 peak=1982 ppm1=9.329 ppm2=9.377 assign ( resid 132 and name HN ) ( resid 130 and name HA ) 4.0 2.3 1.6 volume=0.252 peak=1950 ppm1=7.893 ppm2=3.882 assign ( resid 61 and name HN ) ( resid 61 and name HA ) 3.2 1.5 1.3 volume=0.924 peak=1892 ppm1=8.714 ppm2=4.395 assign ( resid 169 and name HG2 ) ( resid 171 and name HA ) 3.9 2.2 1.6 volume=0.315 peak=3719 ppm1=1.934 ppm2=4.168 assign ( resid 7 and name HN ) ( resid 8 and name HB2 or resid 8 and name HB1 ) 3.2 1.5 1.3 volume=0.918 peak=795 ppm1=8.421 ppm2=2.045 assign ( resid 114 and name HN ) ( resid 113 and name HA ) 3.4 1.7 1.4 volume=0.711 peak=440 ppm1=8.800 ppm2=5.319 assign ( resid 152 and name HN ) ( resid 14 and name HG1# ) 3.8 2.1 1.5 volume=0.344 peak=1034 ppm1=8.344 ppm2=0.649 assign ( resid 76 and name HD2 ) ( resid 76 and name HN ) 3.8 2.1 1.5 volume=0.356 peak=4306 ppm1=1.552 ppm2=6.696 assign ( resid 84 and name HG1# ) ( resid 134 and name HD1 or resid 134 and name HD2 ) 3.5 1.8 1.4 volume=0.553 peak=3328 ppm1=0.532 ppm2=6.881 assign ( resid 112 and name HD1# ) ( resid 112 and name HG2# ) 3.0 1.2 1.2 volume=1.613 peak=3698 ppm1=0.373 ppm2=0.680 assign ( resid 113 and name HA ) ( resid 132 and name HG1# ) 4.8 3.1 1.2 volume=0.091 peak=2829 ppm1=5.309 ppm2=0.516 assign ( resid 65 and name HG ) ( resid 65 and name HD2# ) 3.6 1.9 1.4 volume=0.513 peak=3367 ppm1=1.641 ppm2=0.317 assign ( resid 64 and name HA ) ( resid 64 and name HB2 or resid 64 and name HB1 ) 4.5 2.8 1.5 volume=0.125 peak=4180 ppm1=3.862 ppm2=3.012 assign ( resid 195 and name HN ) ( resid 196 and name HN ) 3.2 1.4 1.3 volume=1.075 peak=725 ppm1=7.971 ppm2=7.395 assign ( resid 83 and name HN ) ( resid 83 and name HA ) 3.1 1.4 1.3 volume=1.119 peak=1240 ppm1=8.502 ppm2=4.661 assign ( resid 147 and name HB2 ) ( resid 148 and name HN ) 4.3 2.6 1.7 volume=0.161 peak=3662 ppm1=2.704 ppm2=9.109 assign ( resid 82 and name HN ) ( resid 96 and name HA ) 3.2 1.5 1.3 volume=0.924 peak=929 ppm1=8.561 ppm2=4.868 assign ( resid 201 and name HA ) ( resid 204 and name HN ) 4.1 2.4 1.7 volume=0.214 peak=5160 ppm1=4.332 ppm2=6.764 assign ( resid 36 and name HA ) ( resid 26 and name HG1# ) 3.6 1.8 1.4 volume=0.519 peak=2744 ppm1=5.851 ppm2=0.741 assign ( resid 111 and name HN ) ( resid 97 and name HG2# ) 3.6 1.9 1.4 volume=0.482 peak=1700 ppm1=8.631 ppm2=0.227 assign ( resid 87 and name HG11 ) ( resid 87 and name HA ) 3.4 1.7 1.4 volume=0.638 peak=4459 ppm1=1.265 ppm2=3.894 assign ( resid 188 and name HB1 ) ( resid 188 and name HE# ) 3.3 1.5 1.3 volume=0.900 peak=2705 ppm1=1.446 ppm2=1.902 assign ( resid 26 and name HG2# ) ( resid 27 and name HN ) 3.0 1.3 1.2 volume=1.431 peak=3955 ppm1=0.911 ppm2=9.306 assign ( resid 202 and name HN ) ( resid 203 and name HD1# ) 3.9 2.2 1.6 volume=0.300 peak=891 ppm1=8.575 ppm2=-0.002 assign ( resid 193 and name HN ) ( resid 194 and name HN ) 3.1 1.4 1.2 volume=1.180 peak=2327 ppm1=7.621 ppm2=7.791 assign ( resid 80 and name HG2# ) ( resid 79 and name HA ) 4.0 2.3 1.6 volume=0.262 peak=2932 ppm1=0.708 ppm2=4.353 assign ( resid 26 and name HN ) ( resid 36 and name HB2 ) 3.6 1.9 1.4 volume=0.495 peak=1833 ppm1=8.861 ppm2=3.478 assign ( resid 114 and name HG ) ( resid 114 and name HD2# ) 3.4 1.7 1.4 volume=0.663 peak=4134 ppm1=0.952 ppm2=0.777 assign ( resid 204 and name HA ) ( resid 207 and name HG2 ) 3.0 1.3 1.2 volume=1.554 peak=3257 ppm1=3.800 ppm2=1.407 assign ( resid 144 and name HN ) ( resid 109 and name HD1 ) 3.7 2.0 1.5 volume=0.389 peak=2146 ppm1=7.536 ppm2=3.082 assign ( resid 192 and name HN ) ( resid 192 and name HA ) 3.3 1.6 1.3 volume=0.837 peak=716 ppm1=8.210 ppm2=4.140 assign ( resid 167 and name HB1 ) ( resid 166 and name HD1 ) 4.3 2.6 1.7 volume=0.159 peak=3897 ppm1=1.679 ppm2=1.489 assign ( resid 200 and name HN ) ( resid 199 and name HA ) 3.2 1.4 1.3 volume=1.097 peak=493 ppm1=8.086 ppm2=2.762 assign ( resid 203 and name HG2# ) ( resid 200 and name HN ) 4.3 2.6 1.7 volume=0.160 peak=2680 ppm1=0.339 ppm2=8.104 assign ( resid 127 and name HG11 ) ( resid 152 and name HA2 ) 3.4 1.6 1.3 volume=0.733 peak=5017 ppm1=1.045 ppm2=3.819 assign ( resid 92 and name HN ) ( resid 91 and name HA ) 2.8 1.1 1.1 volume=2.163 peak=176 ppm1=9.455 ppm2=5.831 assign ( resid 33 and name HG12 ) ( resid 33 and name HG11 ) 1.9 0.2 0.8 volume=23.203 peak=3837 ppm1=1.918 ppm2=1.884 assign ( resid 155 and name HN ) ( resid 154 and name HG2# ) 2.9 1.2 1.2 volume=1.744 peak=651 ppm1=8.976 ppm2=0.882 assign ( resid 14 and name HN ) ( resid 13 and name HA ) 3.2 1.5 1.3 volume=0.966 peak=620 ppm1=7.789 ppm2=3.640 assign ( resid 72 and name HA ) ( resid 72 and name HG11 ) 3.8 2.0 1.5 volume=0.384 peak=4985 ppm1=3.636 ppm2=1.166 assign ( resid 91 and name HG2# ) ( resid 7 and name HN ) 3.6 1.9 1.4 volume=0.507 peak=4684 ppm1=1.017 ppm2=8.394 assign ( resid 152 and name HN ) ( resid 14 and name HB ) 4.1 2.4 1.6 volume=0.223 peak=607 ppm1=8.344 ppm2=1.661 assign ( resid 175 and name HN ) ( resid 175 and name HG1 ) 3.2 1.4 1.3 volume=1.067 peak=1009 ppm1=8.803 ppm2=2.570 assign ( resid 203 and name HG2# ) ( resid 204 and name HB2 ) 2.9 1.2 1.2 volume=1.705 peak=4998 ppm1=0.340 ppm2=1.590 assign ( resid 61 and name HG ) ( resid 61 and name HB2 ) 2.3 0.6 0.9 volume=7.446 peak=2493 ppm1=1.719 ppm2=1.623 assign ( resid 184 and name HG2# ) ( resid 46 and name HN ) 3.8 2.1 1.5 volume=0.349 peak=4289 ppm1=1.095 ppm2=8.522 assign ( resid 151 and name HN ) ( resid 150 and name HB1 ) 3.7 2.0 1.5 volume=0.439 peak=240 ppm1=8.646 ppm2=2.340 assign ( resid 92 and name HE1 or resid 92 and name HE2 ) ( resid 115 and name HG2# ) 3.5 1.8 1.4 volume=0.599 peak=103 ppm1=6.752 ppm2=0.669 assign ( resid 13 and name HN ) ( resid 13 and name HA ) 2.8 1.1 1.1 volume=2.197 peak=1037 ppm1=7.720 ppm2=3.630 assign ( resid 4 and name HN ) ( resid 4 and name HA ) 2.8 1.1 1.1 volume=2.039 peak=1932 ppm1=8.188 ppm2=3.763 assign ( resid 168 and name HN ) ( resid 167 and name HA ) 3.0 1.3 1.2 volume=1.564 peak=671 ppm1=8.694 ppm2=5.182 assign ( resid 114 and name HN ) ( resid 131 and name HB2 ) 3.9 2.1 1.5 volume=0.321 peak=876 ppm1=8.802 ppm2=3.482 assign ( resid 144 and name HD1# ) ( resid 144 and name HG12 or resid 144 and name HG11 ) 4.7 3.0 1.3 volume=0.099 peak=2585 ppm1=0.621 ppm2=1.267 assign ( resid 157 and name HD1 ) ( resid 58 and name HB1 ) 3.5 1.8 1.4 volume=0.584 peak=2608 ppm1=3.626 ppm2=2.145 assign ( resid 114 and name HN ) ( resid 130 and name HN ) 3.8 2.1 1.5 volume=0.362 peak=233 ppm1=8.798 ppm2=7.648 assign ( resid 64 and name HZ ) ( resid 64 and name HE1 or resid 64 and name HE2 ) 3.2 1.5 1.3 volume=0.947 peak=117 ppm1=7.050 ppm2=6.485 assign ( resid 33 and name HD1# ) ( resid 33 and name HB ) 4.1 2.3 1.6 volume=0.239 peak=2563 ppm1=0.362 ppm2=2.844 assign ( resid 201 and name HN ) ( resid 203 and name HN ) 3.9 2.2 1.6 volume=0.296 peak=1989 ppm1=7.404 ppm2=7.644 assign ( resid 206 and name HN ) ( resid 206 and name HA ) 3.1 1.4 1.3 volume=1.104 peak=1128 ppm1=7.462 ppm2=4.398 assign ( resid 198 and name HN ) ( resid 199 and name HB# ) 3.2 1.5 1.3 volume=1.039 peak=197 ppm1=8.717 ppm2=0.684 assign ( resid 54 and name HD1# ) ( resid 54 and name HN ) 3.9 2.2 1.6 volume=0.299 peak=3150 ppm1=0.492 ppm2=9.027 assign ( resid 84 and name HN ) ( resid 84 and name HB ) 3.0 1.3 1.2 volume=1.338 peak=2365 ppm1=8.504 ppm2=2.052 assign ( resid 98 and name HN ) ( resid 98 and name HG2# ) 3.0 1.3 1.2 volume=1.408 peak=1039 ppm1=9.355 ppm2=1.272 assign ( resid 3 and name HE1 or resid 3 and name HE2 ) ( resid 3 and name HZ ) 3.6 1.9 1.4 volume=0.483 peak=82 ppm1=7.212 ppm2=6.203 assign ( resid 155 and name HN ) ( resid 154 and name HB ) 3.5 1.8 1.4 volume=0.586 peak=2429 ppm1=8.977 ppm2=2.183 assign ( resid 117 and name HD1# ) ( resid 90 and name HB1 ) 4.2 2.5 1.7 volume=0.201 peak=2598 ppm1=0.243 ppm2=3.371 assign ( resid 144 and name HA ) ( resid 109 and name HG2 ) 3.8 2.0 1.5 volume=0.381 peak=3056 ppm1=3.984 ppm2=1.492 assign ( resid 70 and name HB1 ) ( resid 73 and name HN ) 3.8 2.0 1.5 volume=0.380 peak=3536 ppm1=2.587 ppm2=7.510 assign ( resid 193 and name HB ) ( resid 193 and name HN ) 4.0 2.2 1.6 volume=0.280 peak=5113 ppm1=2.054 ppm2=7.633 assign ( resid 191 and name HA ) ( resid 192 and name HD2# ) 3.9 2.2 1.6 volume=0.304 peak=2928 ppm1=4.272 ppm2=0.500 assign ( resid 84 and name HB ) ( resid 84 and name HG1# ) 3.2 1.5 1.3 volume=1.042 peak=3526 ppm1=1.997 ppm2=0.520 assign ( resid 8 and name HB2 or resid 8 and name HB1 ) ( resid 4 and name HN ) 3.8 2.1 1.5 volume=0.364 peak=3093 ppm1=2.048 ppm2=8.199 assign ( resid 92 and name HN ) ( resid 86 and name HA ) 4.1 2.4 1.7 volume=0.217 peak=1548 ppm1=9.456 ppm2=4.286 assign ( resid 5 and name HN ) ( resid 8 and name HG1 ) 3.6 1.8 1.4 volume=0.534 peak=635 ppm1=7.458 ppm2=2.318 assign ( resid 86 and name HN ) ( resid 86 and name HD1 ) 4.3 2.6 1.7 volume=0.159 peak=749 ppm1=8.621 ppm2=2.960 assign ( resid 170 and name HA ) ( resid 171 and name HN ) 4.1 2.4 1.6 volume=0.221 peak=4597 ppm1=5.822 ppm2=9.104 assign ( resid 12 and name HN ) ( resid 118 and name HE1 ) 3.6 1.9 1.5 volume=0.471 peak=1452 ppm1=7.550 ppm2=2.969 assign ( resid 146 and name HN ) ( resid 109 and name HD1 ) 3.5 1.7 1.4 volume=0.616 peak=1997 ppm1=8.401 ppm2=3.085 assign ( resid 176 and name HA ) ( resid 176 and name HD1 ) 4.4 2.7 1.6 volume=0.148 peak=3570 ppm1=3.997 ppm2=3.212 assign ( resid 199 and name HB# ) ( resid 203 and name HG2# ) 3.2 1.4 1.3 volume=1.071 peak=3082 ppm1=0.692 ppm2=0.316 assign ( resid 46 and name HN ) ( resid 45 and name HA1 ) 3.2 1.5 1.3 volume=1.023 peak=2412 ppm1=8.559 ppm2=3.390 assign ( resid 199 and name HN ) ( resid 198 and name HA ) 3.6 1.9 1.4 volume=0.509 peak=1144 ppm1=8.635 ppm2=4.533 assign ( resid 93 and name HD1# ) ( resid 134 and name HD1 or resid 134 and name HD2 ) 3.8 2.0 1.5 volume=0.384 peak=4251 ppm1=-0.271 ppm2=6.855 assign ( resid 167 and name HA ) ( resid 168 and name HN ) 4.1 2.4 1.7 volume=0.215 peak=3909 ppm1=5.217 ppm2=8.718 assign ( resid 194 and name HN ) ( resid 193 and name HB ) 2.8 1.1 1.1 volume=2.104 peak=1590 ppm1=7.774 ppm2=2.051 assign ( resid 188 and name HB2 ) ( resid 188 and name HN ) 4.0 2.3 1.6 volume=0.248 peak=4222 ppm1=1.448 ppm2=8.442 assign ( resid 172 and name HN ) ( resid 171 and name HG1# ) 3.9 2.2 1.6 volume=0.313 peak=1255 ppm1=8.858 ppm2=0.876 assign ( resid 37 and name HA ) ( resid 47 and name HD2# ) 4.4 2.7 1.6 volume=0.146 peak=4283 ppm1=5.821 ppm2=0.100 assign ( resid 79 and name HA ) ( resid 78 and name HA ) 3.6 1.8 1.4 volume=0.535 peak=4139 ppm1=4.396 ppm2=4.675 assign ( resid 126 and name HA ) ( resid 153 and name HB1 ) 4.2 2.5 1.7 volume=0.188 peak=4445 ppm1=5.418 ppm2=2.906 assign ( resid 203 and name HA ) ( resid 203 and name HG11 or resid 203 and name HG12 ) 3.9 2.2 1.6 volume=0.292 peak=2712 ppm1=2.834 ppm2=0.512 assign ( resid 200 and name HE2 ) ( resid 55 and name HD1 ) 3.7 1.9 1.5 volume=0.443 peak=3572 ppm1=2.802 ppm2=3.358 assign ( resid 2 and name HN ) ( resid 2 and name HA ) 3.0 1.3 1.2 volume=1.411 peak=722 ppm1=8.184 ppm2=4.138 assign ( resid 14 and name HG1# ) ( resid 128 and name HA ) 4.2 2.4 1.7 volume=0.208 peak=2951 ppm1=0.678 ppm2=5.583 assign ( resid 18 and name HN ) ( resid 18 and name HA ) 3.2 1.5 1.3 volume=1.008 peak=985 ppm1=7.759 ppm2=4.470 assign ( resid 193 and name HA ) ( resid 196 and name HN ) 4.0 2.3 1.6 volume=0.264 peak=2528 ppm1=3.460 ppm2=7.445 assign ( resid 149 and name HN ) ( resid 172 and name HN ) 4.2 2.4 1.7 volume=0.208 peak=1051 ppm1=7.757 ppm2=8.826 assign ( resid 53 and name HG2# ) ( resid 53 and name HB ) 3.1 1.4 1.3 volume=1.144 peak=4967 ppm1=0.900 ppm2=1.601 assign ( resid 169 and name HN ) ( resid 51 and name HA ) 4.1 2.4 1.6 volume=0.236 peak=2065 ppm1=9.256 ppm2=5.578 assign ( resid 194 and name HN ) ( resid 196 and name HN ) 3.0 1.3 1.2 volume=1.355 peak=993 ppm1=7.774 ppm2=7.441 assign ( resid 167 and name HD1# ) ( resid 169 and name HB2 ) 2.8 1.1 1.1 volume=2.059 peak=4895 ppm1=0.764 ppm2=1.754 assign ( resid 9 and name HN ) ( resid 6 and name HA ) 3.2 1.4 1.3 volume=1.081 peak=613 ppm1=7.983 ppm2=3.626 assign ( resid 121 and name HN ) ( resid 120 and name HA ) 2.7 1.0 1.1 volume=2.710 peak=1978 ppm1=8.585 ppm2=4.533 assign ( resid 80 and name HN ) ( resid 97 and name HG2# ) 3.2 1.5 1.3 volume=0.954 peak=2120 ppm1=7.521 ppm2=0.229 assign ( resid 84 and name HG2# ) ( resid 95 and name HN ) 4.0 2.3 1.6 volume=0.261 peak=4949 ppm1=0.110 ppm2=9.111 assign ( resid 65 and name HD1# ) ( resid 117 and name HG11 or resid 117 and name HG12 ) 3.1 1.4 1.2 volume=1.188 peak=4776 ppm1=0.176 ppm2=0.641 assign ( resid 84 and name HB ) ( resid 85 and name HN ) 3.7 1.9 1.5 volume=0.448 peak=3669 ppm1=1.995 ppm2=7.148 assign ( resid 26 and name HN ) ( resid 28 and name HN ) 4.2 2.5 1.7 volume=0.199 peak=2108 ppm1=8.862 ppm2=7.785 assign ( resid 115 and name HG1# ) ( resid 130 and name HN ) 3.2 1.5 1.3 volume=0.920 peak=3162 ppm1=0.303 ppm2=7.628 assign ( resid 167 and name HN ) ( resid 156 and name HN ) 3.2 1.4 1.3 volume=1.092 peak=1683 ppm1=8.644 ppm2=8.558 assign ( resid 110 and name HN ) ( resid 97 and name HG2# ) 3.8 2.1 1.5 volume=0.347 peak=2188 ppm1=8.721 ppm2=0.235 assign ( resid 203 and name HB ) ( resid 203 and name HG11 or resid 203 and name HG12 ) 3.9 2.1 1.5 volume=0.323 peak=2659 ppm1=0.122 ppm2=0.514 assign ( resid 87 and name HD1# ) ( resid 92 and name HN ) 4.1 2.4 1.6 volume=0.220 peak=2975 ppm1=0.441 ppm2=9.464 assign ( resid 163 and name HN ) ( resid 164 and name HA ) 3.6 1.8 1.4 volume=0.521 peak=632 ppm1=7.325 ppm2=4.867 assign ( resid 126 and name HD1# ) ( resid 128 and name HB2 ) 4.0 2.3 1.6 volume=0.251 peak=3879 ppm1=0.349 ppm2=3.765 assign ( resid 134 and name HZ ) ( resid 84 and name HG2# ) 2.8 1.1 1.1 volume=2.350 peak=99 ppm1=6.643 ppm2=0.121 assign ( resid 93 and name HB ) ( resid 93 and name HG2# ) 4.1 2.3 1.6 volume=0.237 peak=3095 ppm1=1.224 ppm2=-0.014 assign ( resid 53 and name HN ) ( resid 53 and name HB ) 2.8 1.1 1.1 volume=2.352 peak=1785 ppm1=8.309 ppm2=1.633 assign ( resid 146 and name HN ) ( resid 145 and name HN ) 3.7 2.0 1.5 volume=0.434 peak=494 ppm1=8.401 ppm2=8.351 assign ( resid 79 and name HN ) ( resid 97 and name HG2# ) 4.2 2.5 1.7 volume=0.204 peak=1402 ppm1=8.846 ppm2=0.231 assign ( resid 73 and name HA ) ( resid 73 and name HG2# ) 2.8 1.1 1.1 volume=2.098 peak=4709 ppm1=3.919 ppm2=1.219 assign ( resid 116 and name HN ) ( resid 115 and name HG2# ) 3.4 1.6 1.3 volume=0.748 peak=541 ppm1=8.835 ppm2=0.631 assign ( resid 112 and name HG12 ) ( resid 112 and name HN ) 4.3 2.6 1.7 volume=0.171 peak=4013 ppm1=1.249 ppm2=8.132 assign ( resid 85 and name HN ) ( resid 86 and name HN ) 3.0 1.3 1.2 volume=1.417 peak=877 ppm1=7.153 ppm2=8.580 assign ( resid 5 and name HN ) ( resid 4 and name HB1 or resid 4 and name HB2 ) 2.7 1.0 1.1 volume=2.693 peak=1433 ppm1=7.458 ppm2=1.792 assign ( resid 15 and name HD1# ) ( resid 16 and name HN ) 3.8 2.1 1.5 volume=0.362 peak=3203 ppm1=0.439 ppm2=7.479 assign ( resid 147 and name HN ) ( resid 147 and name HA ) 3.3 1.6 1.3 volume=0.778 peak=282 ppm1=8.785 ppm2=4.268 assign ( resid 187 and name HN ) ( resid 187 and name HG2# ) 3.0 1.3 1.2 volume=1.342 peak=2376 ppm1=7.601 ppm2=1.016 assign ( resid 26 and name HG1# ) ( resid 26 and name HA ) 3.3 1.6 1.3 volume=0.851 peak=4203 ppm1=0.779 ppm2=3.976 assign ( resid 193 and name HN ) ( resid 191 and name HA ) 3.3 1.6 1.3 volume=0.795 peak=2318 ppm1=7.622 ppm2=4.271 assign ( resid 200 and name HN ) ( resid 197 and name HA ) 3.3 1.6 1.3 volume=0.774 peak=194 ppm1=8.086 ppm2=3.743 assign ( resid 42 and name HD2 ) ( resid 42 and name HG1 ) 3.3 1.6 1.3 volume=0.854 peak=4918 ppm1=1.530 ppm2=1.289 assign ( resid 205 and name HN ) ( resid 202 and name HN ) 3.7 2.0 1.5 volume=0.405 peak=829 ppm1=7.186 ppm2=8.569 assign ( resid 48 and name HN ) ( resid 47 and name HG ) 3.3 1.6 1.3 volume=0.821 peak=1333 ppm1=9.292 ppm2=0.640 assign ( resid 54 and name HG11 ) ( resid 167 and name HN ) 3.9 2.2 1.6 volume=0.311 peak=3400 ppm1=1.186 ppm2=8.627 assign ( resid 168 and name HB ) ( resid 154 and name HG2# ) 3.2 1.5 1.3 volume=0.972 peak=3277 ppm1=1.725 ppm2=0.903 assign ( resid 101 and name HN ) ( resid 100 and name HB1 ) 3.1 1.4 1.2 volume=1.176 peak=1899 ppm1=8.478 ppm2=3.618 assign ( resid 54 and name HG2# ) ( resid 203 and name HB ) 3.6 1.9 1.4 volume=0.492 peak=2646 ppm1=0.576 ppm2=0.160 assign ( resid 7 and name HB# ) ( resid 8 and name HA ) 3.3 1.6 1.3 volume=0.786 peak=3695 ppm1=0.751 ppm2=3.829 assign ( resid 163 and name HB# ) ( resid 163 and name HN ) 2.7 1.0 1.1 volume=2.520 peak=4838 ppm1=1.160 ppm2=7.343 assign ( resid 75 and name HN ) ( resid 78 and name HD1# ) 3.0 1.3 1.2 volume=1.459 peak=1257 ppm1=7.481 ppm2=0.494 assign ( resid 71 and name HN ) ( resid 74 and name HN ) 3.4 1.7 1.4 volume=0.702 peak=1707 ppm1=7.218 ppm2=6.480 assign ( resid 79 and name HN ) ( resid 78 and name HB2 ) 3.3 1.6 1.3 volume=0.761 peak=2266 ppm1=8.842 ppm2=1.398 assign ( resid 163 and name HB# ) ( resid 162 and name HA ) 3.8 2.1 1.5 volume=0.335 peak=3721 ppm1=1.151 ppm2=3.640 assign ( resid 185 and name HA ) ( resid 185 and name HN ) 4.8 3.1 1.2 volume=0.087 peak=3185 ppm1=3.895 ppm2=8.187 assign ( resid 103 and name HN ) ( resid 101 and name HA ) 3.1 1.4 1.2 volume=1.239 peak=1596 ppm1=8.451 ppm2=4.659 assign ( resid 114 and name HD2# ) ( resid 130 and name HN ) 3.9 2.1 1.5 volume=0.320 peak=2614 ppm1=0.782 ppm2=7.638 assign ( resid 166 and name HG1 ) ( resid 167 and name HN ) 3.6 1.9 1.4 volume=0.495 peak=2966 ppm1=1.209 ppm2=8.650 assign ( resid 168 and name HG2# ) ( resid 169 and name HN ) 4.0 2.3 1.6 volume=0.248 peak=4035 ppm1=0.199 ppm2=9.236 assign ( resid 51 and name HA ) ( resid 168 and name HN ) 3.9 2.2 1.6 volume=0.308 peak=4966 ppm1=5.621 ppm2=8.721 assign ( resid 96 and name HN ) ( resid 96 and name HB ) 3.6 1.9 1.5 volume=0.462 peak=1665 ppm1=8.472 ppm2=3.878 assign ( resid 30 and name HN ) ( resid 29 and name HN ) 3.5 1.7 1.4 volume=0.617 peak=922 ppm1=8.721 ppm2=8.551 assign ( resid 134 and name HZ ) ( resid 134 and name HD1 or resid 134 and name HD2 ) 3.7 2.0 1.5 volume=0.423 peak=123 ppm1=6.644 ppm2=6.857 assign ( resid 11 and name HB# ) ( resid 15 and name HB2 ) 3.3 1.6 1.3 volume=0.769 peak=3871 ppm1=1.630 ppm2=1.359 assign ( resid 200 and name HA ) ( resid 54 and name HD1# ) 3.6 1.9 1.4 volume=0.512 peak=4395 ppm1=3.362 ppm2=0.424 assign ( resid 208 and name HG2# ) ( resid 207 and name HN ) 4.3 2.6 1.7 volume=0.169 peak=4392 ppm1=1.137 ppm2=7.852 assign ( resid 71 and name HN ) ( resid 73 and name HG2# ) 3.4 1.7 1.4 volume=0.662 peak=2306 ppm1=7.217 ppm2=1.140 assign ( resid 34 and name HB ) ( resid 51 and name HN ) 4.5 2.8 1.5 volume=0.124 peak=4150 ppm1=3.827 ppm2=8.457 assign ( resid 18 and name HB2 ) ( resid 49 and name HG1 ) 4.1 2.3 1.6 volume=0.239 peak=3966 ppm1=2.447 ppm2=1.567 assign ( resid 73 and name HG2# ) ( resid 71 and name HN ) 3.9 2.1 1.5 volume=0.322 peak=5018 ppm1=1.218 ppm2=7.224 assign ( resid 196 and name HN ) ( resid 197 and name HA ) 3.7 2.0 1.5 volume=0.416 peak=249 ppm1=7.439 ppm2=3.750 assign ( resid 105 and name HN ) ( resid 105 and name HB1 ) 3.0 1.3 1.2 volume=1.368 peak=2080 ppm1=7.944 ppm2=3.874 assign ( resid 168 and name HG1# ) ( resid 166 and name HD2 ) 2.8 1.1 1.1 volume=2.067 peak=4580 ppm1=0.768 ppm2=1.490 assign ( resid 186 and name HE1 ) ( resid 186 and name HD2 ) 2.5 0.8 1.0 volume=4.565 peak=4391 ppm1=2.956 ppm2=1.672 assign ( resid 52 and name HN ) ( resid 51 and name HA ) 3.0 1.3 1.2 volume=1.502 peak=1613 ppm1=8.619 ppm2=5.623 assign ( resid 51 and name HB1 or resid 51 and name HB2 ) ( resid 51 and name HG1 or resid 51 and name HG2 ) 3.3 1.6 1.3 volume=0.769 peak=2719 ppm1=1.780 ppm2=1.965 assign ( resid 74 and name HN ) ( resid 74 and name HD1 ) 3.1 1.4 1.2 volume=1.259 peak=392 ppm1=6.493 ppm2=6.922 assign ( resid 26 and name HB ) ( resid 26 and name HA ) 2.6 0.9 1.0 volume=3.381 peak=4000 ppm1=1.922 ppm2=3.974 assign ( resid 157 and name HG2 ) ( resid 122 and name HA1 ) 3.5 1.7 1.4 volume=0.626 peak=3179 ppm1=1.791 ppm2=3.835 assign ( resid 49 and name HN ) ( resid 36 and name HN ) 4.1 2.4 1.6 volume=0.219 peak=1004 ppm1=8.910 ppm2=9.872 assign ( resid 204 and name HG2 ) ( resid 204 and name HD1 ) 3.3 1.6 1.3 volume=0.864 peak=4850 ppm1=1.298 ppm2=1.486 assign ( resid 188 and name HA ) ( resid 188 and name HN ) 3.9 2.2 1.6 volume=0.295 peak=4288 ppm1=4.214 ppm2=8.448 assign ( resid 115 and name HN ) ( resid 115 and name HB ) 3.0 1.3 1.2 volume=1.355 peak=1407 ppm1=9.052 ppm2=0.233 assign ( resid 169 and name HA ) ( resid 49 and name HG1 ) 4.4 2.7 1.6 volume=0.147 peak=2468 ppm1=5.237 ppm2=1.621 assign ( resid 105 and name HB2 ) ( resid 180 and name HN ) 4.3 2.6 1.7 volume=0.171 peak=3127 ppm1=3.870 ppm2=8.390 assign ( resid 92 and name HN ) ( resid 117 and name HN ) 4.2 2.5 1.7 volume=0.192 peak=1231 ppm1=9.456 ppm2=8.235 assign ( resid 50 and name HA ) ( resid 51 and name HN ) 4.0 2.3 1.6 volume=0.261 peak=2933 ppm1=5.178 ppm2=8.458 assign ( resid 170 and name HA ) ( resid 47 and name HD2# ) 4.2 2.5 1.7 volume=0.194 peak=3811 ppm1=5.821 ppm2=0.126 assign ( resid 98 and name HG2# ) ( resid 99 and name HN ) 4.1 2.4 1.7 volume=0.212 peak=3842 ppm1=1.322 ppm2=7.802 assign ( resid 76 and name HD1 ) ( resid 76 and name HA ) 2.7 1.0 1.1 volume=2.631 peak=3069 ppm1=1.553 ppm2=4.159 assign ( resid 179 and name HB2 ) ( resid 184 and name HG11 ) 4.2 2.5 1.7 volume=0.194 peak=3735 ppm1=2.494 ppm2=1.678 assign ( resid 97 and name HN ) ( resid 81 and name HA ) 3.4 1.7 1.4 volume=0.643 peak=2436 ppm1=8.362 ppm2=4.662 assign ( resid 132 and name HB ) ( resid 3 and name HD1 or resid 3 and name HD2 ) 3.8 2.1 1.5 volume=0.338 peak=3722 ppm1=2.284 ppm2=7.353 assign ( resid 126 and name HD1# ) ( resid 152 and name HN ) 3.8 2.0 1.5 volume=0.379 peak=2697 ppm1=0.349 ppm2=8.259 assign ( resid 196 and name HG2# ) ( resid 197 and name HA ) 3.5 1.7 1.4 volume=0.621 peak=3138 ppm1=0.812 ppm2=3.739 assign ( resid 33 and name HG12 ) ( resid 196 and name HG2# ) 3.8 2.1 1.5 volume=0.357 peak=3792 ppm1=1.919 ppm2=0.784 assign ( resid 30 and name HN ) ( resid 29 and name HA ) 3.1 1.4 1.2 volume=1.197 peak=1290 ppm1=8.722 ppm2=5.228 assign ( resid 97 and name HG2# ) ( resid 108 and name HB1 ) 4.0 2.3 1.6 volume=0.259 peak=4692 ppm1=0.219 ppm2=2.263 assign ( resid 160 and name HN ) ( resid 158 and name HG2 ) 3.2 1.5 1.3 volume=0.937 peak=2455 ppm1=8.833 ppm2=2.385 assign ( resid 91 and name HN ) ( resid 90 and name HA ) 3.2 1.5 1.3 volume=0.957 peak=2369 ppm1=7.218 ppm2=4.878 assign ( resid 179 and name HG ) ( resid 179 and name HD2# ) 2.6 0.9 1.0 volume=3.486 peak=4861 ppm1=1.515 ppm2=0.739 assign ( resid 200 and name HN ) ( resid 54 and name HD1# ) 3.4 1.7 1.4 volume=0.688 peak=1236 ppm1=8.085 ppm2=0.481 assign ( resid 36 and name HB2 ) ( resid 26 and name HG2# ) 3.6 1.9 1.4 volume=0.475 peak=5151 ppm1=3.525 ppm2=0.906 assign ( resid 168 and name HG2# ) ( resid 168 and name HN ) 3.6 1.9 1.5 volume=0.467 peak=2916 ppm1=0.200 ppm2=8.703 assign ( resid 192 and name HN ) ( resid 194 and name HN ) 3.7 1.9 1.5 volume=0.446 peak=2134 ppm1=8.209 ppm2=7.787 assign ( resid 97 and name HG2# ) ( resid 79 and name HB2 ) 3.5 1.7 1.4 volume=0.636 peak=5158 ppm1=0.219 ppm2=1.798 assign ( resid 196 and name HG12 ) ( resid 196 and name HD1# ) 2.6 0.9 1.0 volume=3.541 peak=2898 ppm1=1.475 ppm2=0.720 assign ( resid 112 and name HD1# ) ( resid 134 and name HZ ) 3.4 1.7 1.4 volume=0.680 peak=2899 ppm1=0.373 ppm2=6.634 assign ( resid 158 and name HA ) ( resid 158 and name HG2 ) 3.7 2.0 1.5 volume=0.394 peak=2991 ppm1=4.137 ppm2=2.437 assign ( resid 129 and name HB1 ) ( resid 129 and name HA ) 4.2 2.5 1.7 volume=0.183 peak=4033 ppm1=3.368 ppm2=5.711 assign ( resid 43 and name HN ) ( resid 43 and name HA ) 2.9 1.1 1.1 volume=1.949 peak=1542 ppm1=7.304 ppm2=4.475 assign ( resid 183 and name HG12 ) ( resid 183 and name HA ) 3.1 1.4 1.3 volume=1.135 peak=5134 ppm1=1.542 ppm2=3.908 assign ( resid 123 and name HN ) ( resid 157 and name HG2 ) 3.2 1.5 1.3 volume=0.944 peak=191 ppm1=8.406 ppm2=1.786 assign ( resid 112 and name HD1# ) ( resid 137 and name HN ) 4.1 2.4 1.6 volume=0.234 peak=3044 ppm1=0.371 ppm2=8.065 assign ( resid 79 and name HN ) ( resid 78 and name HN ) 4.2 2.5 1.7 volume=0.192 peak=1481 ppm1=8.846 ppm2=7.128 assign ( resid 203 and name HD1# ) ( resid 60 and name HB1 ) 3.0 1.3 1.2 volume=1.443 peak=2827 ppm1=-0.010 ppm2=1.747 assign ( resid 203 and name HD1# ) ( resid 54 and name HG2# ) 2.6 0.9 1.0 volume=3.296 peak=4931 ppm1=-0.010 ppm2=0.578 assign ( resid 200 and name HD1 ) ( resid 200 and name HG2 ) 2.5 0.8 1.0 volume=4.325 peak=4177 ppm1=1.550 ppm2=1.133 assign ( resid 192 and name HD1# ) ( resid 50 and name HB ) 3.6 1.8 1.4 volume=0.529 peak=3310 ppm1=0.493 ppm2=1.833 assign ( resid 84 and name HN ) ( resid 95 and name HN ) 3.6 1.9 1.5 volume=0.466 peak=1565 ppm1=8.503 ppm2=9.131 assign ( resid 87 and name HB ) ( resid 87 and name HG2# ) 3.6 1.9 1.5 volume=0.463 peak=4635 ppm1=1.369 ppm2=0.851 assign ( resid 24 and name HN ) ( resid 24 and name HA ) 2.6 0.8 1.0 volume=3.900 peak=1742 ppm1=7.833 ppm2=4.273 assign ( resid 71 and name HD2 ) ( resid 68 and name HN ) 4.0 2.3 1.6 volume=0.251 peak=3134 ppm1=2.779 ppm2=8.075 assign ( resid 115 and name HA ) ( resid 115 and name HG1# ) 4.4 2.7 1.6 volume=0.152 peak=4400 ppm1=4.397 ppm2=0.289 assign ( resid 158 and name HG1 ) ( resid 158 and name HB2 ) 3.9 2.2 1.6 volume=0.293 peak=4477 ppm1=2.439 ppm2=2.207 assign ( resid 72 and name HD1# ) ( resid 71 and name HB2 or resid 71 and name HB1 ) 3.3 1.6 1.3 volume=0.773 peak=3280 ppm1=0.588 ppm2=1.550 assign ( resid 5 and name HN ) ( resid 6 and name HN ) 3.2 1.5 1.3 volume=1.051 peak=1245 ppm1=7.460 ppm2=7.738 assign ( resid 51 and name HG1 or resid 51 and name HG2 ) ( resid 52 and name HN ) 4.2 2.5 1.7 volume=0.197 peak=3063 ppm1=1.972 ppm2=8.622 assign ( resid 90 and name HN ) ( resid 4 and name HE1 ) 3.6 1.9 1.5 volume=0.460 peak=1000 ppm1=8.382 ppm2=3.011 assign ( resid 46 and name HB1 ) ( resid 46 and name HB2 ) 4.1 2.4 1.6 volume=0.227 peak=2795 ppm1=1.542 ppm2=2.049 assign ( resid 166 and name HN ) ( resid 166 and name HB2 ) 2.8 1.0 1.1 volume=2.416 peak=342 ppm1=8.999 ppm2=1.655 assign ( resid 112 and name HG2# ) ( resid 93 and name HG2# ) 2.9 1.2 1.2 volume=1.836 peak=4381 ppm1=0.679 ppm2=-0.010 assign ( resid 65 and name HA ) ( resid 64 and name HE1 or resid 64 and name HE2 ) 4.2 2.5 1.7 volume=0.183 peak=4206 ppm1=3.890 ppm2=6.487 assign ( resid 179 and name HD1# ) ( resid 183 and name HG2# ) 2.9 1.2 1.2 volume=1.879 peak=4560 ppm1=0.531 ppm2=1.030 assign ( resid 184 and name HB ) ( resid 187 and name HG2# ) 3.5 1.8 1.4 volume=0.584 peak=4267 ppm1=2.045 ppm2=1.003 assign ( resid 158 and name HG1 ) ( resid 165 and name HA ) 3.4 1.7 1.4 volume=0.651 peak=3206 ppm1=2.439 ppm2=5.204 assign ( resid 7 and name HA ) ( resid 8 and name HN ) 4.6 2.9 1.4 volume=0.108 peak=5119 ppm1=3.709 ppm2=7.613 assign ( resid 154 and name HG1# ) ( resid 154 and name HA ) 3.7 2.0 1.5 volume=0.392 peak=4969 ppm1=0.911 ppm2=4.651 assign ( resid 203 and name HB ) ( resid 61 and name HD2# ) 4.9 3.2 1.1 volume=0.074 peak=4712 ppm1=0.122 ppm2=0.747 assign ( resid 208 and name HN ) ( resid 208 and name HA ) 3.0 1.3 1.2 volume=1.370 peak=809 ppm1=8.012 ppm2=4.443 assign ( resid 185 and name HB2 ) ( resid 182 and name HA ) 3.5 1.8 1.4 volume=0.585 peak=5035 ppm1=2.152 ppm2=4.096 assign ( resid 194 and name HN ) ( resid 192 and name HN ) 3.5 1.8 1.4 volume=0.594 peak=2048 ppm1=7.774 ppm2=8.184 assign ( resid 79 and name HN ) ( resid 97 and name HN ) 4.0 2.3 1.6 volume=0.251 peak=1520 ppm1=8.843 ppm2=8.441 assign ( resid 132 and name HN ) ( resid 113 and name HA ) 3.4 1.7 1.4 volume=0.712 peak=322 ppm1=7.895 ppm2=5.311 assign ( resid 8 and name HB2 or resid 8 and name HB1 ) ( resid 10 and name HN ) 3.7 2.0 1.5 volume=0.423 peak=4300 ppm1=2.047 ppm2=8.321 assign ( resid 112 and name HD1# ) ( resid 84 and name HG1# ) 2.9 1.1 1.1 volume=1.949 peak=3465 ppm1=0.372 ppm2=0.509 assign ( resid 183 and name HG12 ) ( resid 184 and name HN ) 3.4 1.7 1.4 volume=0.718 peak=3724 ppm1=1.541 ppm2=7.482 assign ( resid 169 and name HN ) ( resid 52 and name HN ) 4.0 2.2 1.6 volume=0.276 peak=949 ppm1=9.258 ppm2=8.629 assign ( resid 74 and name HH2 ) ( resid 65 and name HB1 or resid 65 and name HB2 ) 3.7 2.0 1.5 volume=0.424 peak=152 ppm1=6.508 ppm2=1.641 assign ( resid 142 and name HB1 ) ( resid 142 and name HB2 ) 3.9 2.2 1.6 volume=0.285 peak=3964 ppm1=1.884 ppm2=1.837 assign ( resid 79 and name HB2 ) ( resid 79 and name HG1 ) 3.1 1.3 1.2 volume=1.317 peak=3395 ppm1=1.779 ppm2=1.913 assign ( resid 155 and name HN ) ( resid 155 and name HA ) 3.4 1.7 1.4 volume=0.707 peak=868 ppm1=8.977 ppm2=5.269 assign ( resid 72 and name HB ) ( resid 73 and name HA ) 4.3 2.6 1.7 volume=0.164 peak=2534 ppm1=1.852 ppm2=3.882 assign ( resid 183 and name HG12 ) ( resid 183 and name HD1# ) 2.4 0.7 1.0 volume=5.026 peak=2859 ppm1=1.541 ppm2=0.928 assign ( resid 186 and name HN ) ( resid 186 and name HE1 ) 3.5 1.8 1.4 volume=0.601 peak=2415 ppm1=7.370 ppm2=2.958 assign ( resid 74 and name HH2 ) ( resid 199 and name HB# ) 3.0 1.3 1.2 volume=1.347 peak=5164 ppm1=6.509 ppm2=0.683 assign ( resid 195 and name HN ) ( resid 196 and name HB ) 3.4 1.7 1.4 volume=0.682 peak=1819 ppm1=7.971 ppm2=2.236 assign ( resid 54 and name HN ) ( resid 53 and name HN ) 3.9 2.2 1.6 volume=0.315 peak=2201 ppm1=9.020 ppm2=8.308 assign ( resid 95 and name HN ) ( resid 95 and name HB1 ) 3.6 1.9 1.4 volume=0.494 peak=1728 ppm1=9.125 ppm2=2.575 assign ( resid 179 and name HG ) ( resid 179 and name HA ) 3.1 1.4 1.2 volume=1.184 peak=2594 ppm1=1.514 ppm2=3.819 assign ( resid 73 and name HG2# ) ( resid 73 and name HN ) 3.2 1.5 1.3 volume=1.000 peak=3926 ppm1=1.218 ppm2=7.478 assign ( resid 68 and name HN ) ( resid 67 and name HB1 ) 3.4 1.6 1.3 volume=0.749 peak=964 ppm1=8.025 ppm2=2.146 assign ( resid 171 and name HA ) ( resid 171 and name HG2# ) 4.1 2.3 1.6 volume=0.241 peak=5077 ppm1=4.148 ppm2=0.799 assign ( resid 109 and name HN ) ( resid 144 and name HN ) 3.8 2.1 1.5 volume=0.337 peak=592 ppm1=8.164 ppm2=7.562 assign ( resid 126 and name HA ) ( resid 127 and name HN ) 4.0 2.3 1.6 volume=0.246 peak=3697 ppm1=5.438 ppm2=9.352 assign ( resid 91 and name HA ) ( resid 92 and name HN ) 4.0 2.3 1.6 volume=0.271 peak=3690 ppm1=5.876 ppm2=9.465 assign ( resid 163 and name HA ) ( resid 164 and name HN ) 3.7 2.0 1.5 volume=0.431 peak=3355 ppm1=4.137 ppm2=7.979 assign ( resid 73 and name HN ) ( resid 78 and name HD1# ) 3.3 1.6 1.3 volume=0.873 peak=275 ppm1=7.506 ppm2=0.498 assign ( resid 5 and name HB# ) ( resid 2 and name HB2 or resid 2 and name HB1 ) 3.3 1.6 1.3 volume=0.773 peak=3172 ppm1=1.341 ppm2=2.789 assign ( resid 160 and name HA ) ( resid 160 and name HN ) 4.3 2.6 1.7 volume=0.169 peak=4102 ppm1=4.010 ppm2=8.823 assign ( resid 142 and name HA ) ( resid 142 and name HB1 ) 3.0 1.2 1.2 volume=1.588 peak=4614 ppm1=4.138 ppm2=1.886 assign ( resid 29 and name HG2# ) ( resid 30 and name HA ) 4.2 2.4 1.7 volume=0.209 peak=3762 ppm1=1.066 ppm2=4.679 assign ( resid 41 and name HG2 or resid 41 and name HG1 ) ( resid 41 and name HB1 or resid 41 and name HB2 ) 3.8 2.0 1.5 volume=0.377 peak=4004 ppm1=1.539 ppm2=1.975 assign ( resid 115 and name HG2# ) ( resid 92 and name HE1 or resid 92 and name HE2 ) 3.0 1.3 1.2 volume=1.339 peak=4773 ppm1=0.660 ppm2=6.750 assign ( resid 125 and name HN ) ( resid 126 and name HG2# ) 3.6 1.9 1.4 volume=0.485 peak=1994 ppm1=8.772 ppm2=0.749 assign ( resid 63 and name HN ) ( resid 203 and name HD1# ) 4.2 2.4 1.7 volume=0.209 peak=896 ppm1=7.301 ppm2=-0.017 assign ( resid 149 and name HN ) ( resid 173 and name HG2# ) 3.7 2.0 1.5 volume=0.423 peak=1136 ppm1=7.759 ppm2=1.011 assign ( resid 29 and name HG2# ) ( resid 30 and name HN ) 4.3 2.6 1.7 volume=0.175 peak=3858 ppm1=1.067 ppm2=8.716 assign ( resid 172 and name HG2 ) ( resid 172 and name HB1 ) 3.4 1.7 1.4 volume=0.685 peak=3065 ppm1=2.292 ppm2=1.806 assign ( resid 130 and name HB1 ) ( resid 7 and name HA ) 4.0 2.3 1.6 volume=0.257 peak=5137 ppm1=1.887 ppm2=3.698 assign ( resid 63 and name HN ) ( resid 62 and name HB1 ) 3.0 1.3 1.2 volume=1.512 peak=2141 ppm1=7.296 ppm2=3.878 assign ( resid 132 and name HG2# ) ( resid 93 and name HD1# ) 3.9 2.1 1.5 volume=0.327 peak=4085 ppm1=0.936 ppm2=-0.273 assign ( resid 80 and name HN ) ( resid 96 and name HG2# ) 3.1 1.4 1.2 volume=1.215 peak=2194 ppm1=7.524 ppm2=1.126 assign ( resid 75 and name HB1 or resid 75 and name HB2 ) ( resid 75 and name HN ) 4.4 2.7 1.6 volume=0.144 peak=4067 ppm1=2.849 ppm2=7.480 assign ( resid 203 and name HD1# ) ( resid 60 and name HA ) 4.1 2.4 1.7 volume=0.217 peak=2834 ppm1=-0.010 ppm2=3.841 assign ( resid 139 and name HA ) ( resid 140 and name HN ) 6.0 4.3 0.0 volume=0.008 peak=4891 ppm1=4.290 ppm2=9.630 assign ( resid 17 and name HN ) ( resid 14 and name HG1# ) 3.3 1.6 1.3 volume=0.817 peak=1606 ppm1=7.608 ppm2=0.640 assign ( resid 25 and name HN ) ( resid 24 and name HE1 ) 3.4 1.7 1.3 volume=0.728 peak=746 ppm1=9.014 ppm2=7.005 assign ( resid 167 and name HA ) ( resid 196 and name HD1# ) 3.7 2.0 1.5 volume=0.397 peak=2481 ppm1=5.218 ppm2=0.731 assign ( resid 130 and name HG2 ) ( resid 131 and name HN ) 4.1 2.4 1.7 volume=0.214 peak=4948 ppm1=1.309 ppm2=9.375 assign ( resid 14 and name HN ) ( resid 14 and name HG2# ) 2.6 0.9 1.1 volume=3.202 peak=975 ppm1=7.792 ppm2=0.752 assign ( resid 154 and name HG1# ) ( resid 15 and name HB2 ) 3.1 1.4 1.2 volume=1.248 peak=3108 ppm1=0.915 ppm2=1.346 assign ( resid 200 and name HG1 ) ( resid 200 and name HB2 ) 2.8 1.0 1.1 volume=2.389 peak=2524 ppm1=1.129 ppm2=1.660 assign ( resid 176 and name HA ) ( resid 176 and name HN ) 3.8 2.0 1.5 volume=0.381 peak=4653 ppm1=3.998 ppm2=8.406 assign ( resid 85 and name HB1 ) ( resid 93 and name HB ) 4.5 2.8 1.5 volume=0.125 peak=3985 ppm1=3.051 ppm2=1.223 assign ( resid 188 and name HN ) ( resid 188 and name HE# ) 2.8 1.1 1.1 volume=2.079 peak=687 ppm1=8.442 ppm2=1.925 assign ( resid 87 and name HG11 ) ( resid 93 and name HG11 ) 3.7 2.0 1.5 volume=0.409 peak=4543 ppm1=1.265 ppm2=0.706 assign ( resid 14 and name HN ) ( resid 15 and name HB2 ) 3.5 1.8 1.4 volume=0.542 peak=1868 ppm1=7.793 ppm2=1.376 assign ( resid 3 and name HN ) ( resid 3 and name HA ) 3.0 1.3 1.2 volume=1.369 peak=1438 ppm1=7.914 ppm2=4.324 assign ( resid 79 and name HN ) ( resid 79 and name HG2 ) 3.8 2.1 1.5 volume=0.369 peak=1449 ppm1=8.842 ppm2=1.912 assign ( resid 48 and name HN ) ( resid 171 and name HG2# ) 3.6 1.9 1.4 volume=0.495 peak=2089 ppm1=9.292 ppm2=0.828 assign ( resid 11 and name HN ) ( resid 116 and name HB2 ) 3.6 1.9 1.4 volume=0.493 peak=2148 ppm1=8.181 ppm2=2.835 assign ( resid 201 and name HN ) ( resid 200 and name HG2 ) 3.5 1.8 1.4 volume=0.542 peak=2447 ppm1=7.401 ppm2=1.142 assign ( resid 50 and name HN ) ( resid 169 and name HN ) 4.3 2.6 1.7 volume=0.167 peak=954 ppm1=9.302 ppm2=9.219 assign ( resid 10 and name HB ) ( resid 13 and name HN ) 4.2 2.5 1.7 volume=0.186 peak=3373 ppm1=3.687 ppm2=7.740 assign ( resid 131 and name HN ) ( resid 131 and name HB1 or resid 131 and name HB2 ) 3.6 1.8 1.4 volume=0.535 peak=2297 ppm1=9.294 ppm2=3.491 assign ( resid 37 and name HA ) ( resid 48 and name HB1 ) 4.2 2.5 1.7 volume=0.192 peak=4099 ppm1=5.823 ppm2=2.640 assign ( resid 208 and name HN ) ( resid 207 and name HD1 ) 3.3 1.6 1.3 volume=0.770 peak=1302 ppm1=8.013 ppm2=3.077 assign ( resid 73 and name HG2# ) ( resid 70 and name HB2 ) 4.2 2.5 1.7 volume=0.203 peak=4678 ppm1=1.217 ppm2=2.572 assign ( resid 170 and name HN ) ( resid 153 and name HA ) 3.4 1.6 1.3 volume=0.742 peak=1771 ppm1=9.147 ppm2=5.327 assign ( resid 77 and name HN ) ( resid 78 and name HA ) 3.2 1.5 1.3 volume=0.947 peak=1277 ppm1=8.057 ppm2=4.661 assign ( resid 154 and name HN ) ( resid 168 and name HG2# ) 3.7 2.0 1.5 volume=0.416 peak=2207 ppm1=10.006 ppm2=0.232 assign ( resid 154 and name HN ) ( resid 154 and name HA ) 3.8 2.1 1.5 volume=0.349 peak=482 ppm1=10.006 ppm2=4.663 assign ( resid 97 and name HG2# ) ( resid 97 and name HD1# ) 2.5 0.8 1.0 volume=4.073 peak=5068 ppm1=0.219 ppm2=0.095 assign ( resid 185 and name HN ) ( resid 184 and name HG2# ) 2.9 1.1 1.1 volume=1.973 peak=436 ppm1=8.185 ppm2=1.093 assign ( resid 62 and name HN ) ( resid 63 and name HN ) 3.6 1.9 1.4 volume=0.506 peak=595 ppm1=8.131 ppm2=7.276 assign ( resid 91 and name HG2# ) ( resid 92 and name HA ) 3.3 1.6 1.3 volume=0.830 peak=3205 ppm1=1.019 ppm2=4.937 assign ( resid 133 and name HN ) ( resid 132 and name HG1# ) 3.2 1.5 1.3 volume=0.938 peak=476 ppm1=8.123 ppm2=0.542 assign ( resid 80 and name HG2# ) ( resid 79 and name HB1 ) 2.6 0.9 1.1 volume=3.248 peak=5037 ppm1=0.709 ppm2=1.779 assign ( resid 29 and name HG2# ) ( resid 33 and name HN ) 4.3 2.6 1.7 volume=0.175 peak=4529 ppm1=1.066 ppm2=8.193 assign ( resid 37 and name HN ) ( resid 24 and name HB2 or resid 24 and name HB1 ) 3.6 1.9 1.4 volume=0.517 peak=2055 ppm1=9.660 ppm2=2.968 assign ( resid 134 and name HA ) ( resid 134 and name HN ) 4.5 2.8 1.5 volume=0.128 peak=3518 ppm1=5.189 ppm2=8.781 assign ( resid 158 and name HB1 ) ( resid 158 and name HG2 ) 3.6 1.8 1.4 volume=0.529 peak=3438 ppm1=2.219 ppm2=2.440 assign ( resid 11 and name HA ) ( resid 14 and name HB ) 3.3 1.6 1.3 volume=0.760 peak=3764 ppm1=3.956 ppm2=1.684 assign ( resid 54 and name HG12 ) ( resid 200 and name HE1 ) 3.8 2.1 1.5 volume=0.343 peak=3561 ppm1=1.219 ppm2=2.840 assign ( resid 203 and name HG2# ) ( resid 204 and name HB1 ) 2.9 1.2 1.2 volume=1.751 peak=4284 ppm1=0.341 ppm2=1.745 assign ( resid 75 and name HN ) ( resid 74 and name HB1 ) 4.0 2.3 1.6 volume=0.266 peak=2174 ppm1=7.480 ppm2=3.246 assign ( resid 184 and name HN ) ( resid 184 and name HA ) 3.0 1.3 1.2 volume=1.541 peak=1079 ppm1=7.498 ppm2=3.616 assign ( resid 128 and name HB2 ) ( resid 10 and name HG2# ) 5.6 3.9 0.4 volume=0.033 peak=3157 ppm1=3.750 ppm2=1.090 assign ( resid 70 and name HB2 ) ( resid 70 and name HN ) 3.6 1.9 1.4 volume=0.490 peak=2940 ppm1=2.588 ppm2=8.581 assign ( resid 193 and name HG1# ) ( resid 190 and name HA ) 3.5 1.7 1.4 volume=0.633 peak=3565 ppm1=0.796 ppm2=3.970 assign ( resid 69 and name HN ) ( resid 72 and name HN ) 3.8 2.1 1.5 volume=0.373 peak=395 ppm1=8.214 ppm2=7.528 assign ( resid 198 and name HN ) ( resid 76 and name HG1 ) 3.1 1.4 1.2 volume=1.187 peak=1250 ppm1=8.716 ppm2=1.405 assign ( resid 197 and name HN ) ( resid 195 and name HA ) 3.5 1.8 1.4 volume=0.564 peak=837 ppm1=7.989 ppm2=4.418 assign ( resid 8 and name HG1 or resid 8 and name HG2 ) ( resid 8 and name HA ) 3.6 1.9 1.4 volume=0.484 peak=3896 ppm1=2.322 ppm2=3.834 assign ( resid 161 and name HN ) ( resid 159 and name HN ) 3.2 1.4 1.3 volume=1.088 peak=718 ppm1=6.905 ppm2=9.000 assign ( resid 160 and name HN ) ( resid 159 and name HB2 ) 2.5 0.8 1.0 volume=4.020 peak=1410 ppm1=8.833 ppm2=1.928 assign ( resid 18 and name HN ) ( resid 15 and name HG ) 3.2 1.5 1.3 volume=1.055 peak=190 ppm1=7.765 ppm2=1.251 assign ( resid 168 and name HG1# ) ( resid 154 and name HN ) 3.5 1.8 1.4 volume=0.603 peak=3135 ppm1=0.768 ppm2=10.021 assign ( resid 127 and name HN ) ( resid 154 and name HA ) 4.1 2.4 1.7 volume=0.213 peak=1271 ppm1=9.384 ppm2=4.656 assign ( resid 147 and name HD1 or resid 147 and name HD2 ) ( resid 145 and name HG1 ) 4.1 2.4 1.6 volume=0.233 peak=34 ppm1=6.221 ppm2=1.417 assign ( resid 170 and name HN ) ( resid 14 and name HG2# ) 3.1 1.4 1.2 volume=1.199 peak=621 ppm1=9.145 ppm2=0.754 assign ( resid 42 and name HN ) ( resid 42 and name HE2 ) 3.5 1.8 1.4 volume=0.604 peak=1083 ppm1=8.699 ppm2=2.970 assign ( resid 85 and name HN ) ( resid 84 and name HG2# ) 2.9 1.2 1.2 volume=1.850 peak=1764 ppm1=7.152 ppm2=0.101 assign ( resid 170 and name HN ) ( resid 170 and name HA ) 3.8 2.1 1.5 volume=0.357 peak=1391 ppm1=9.147 ppm2=5.830 assign ( resid 87 and name HN ) ( resid 88 and name HA ) 4.4 2.6 1.6 volume=0.156 peak=521 ppm1=8.040 ppm2=4.535 assign ( resid 159 and name HB2 or resid 159 and name HB1 ) ( resid 160 and name HN ) 4.2 2.4 1.7 volume=0.209 peak=3953 ppm1=1.877 ppm2=8.842 assign ( resid 132 and name HN ) ( resid 132 and name HG2# ) 3.3 1.6 1.3 volume=0.766 peak=1556 ppm1=7.894 ppm2=0.889 assign ( resid 203 and name HD1# ) ( resid 64 and name HE1 or resid 64 and name HE2 ) 3.6 1.9 1.4 volume=0.515 peak=3823 ppm1=-0.008 ppm2=6.497 assign ( resid 37 and name HN ) ( resid 49 and name HN ) 3.3 1.6 1.3 volume=0.835 peak=2223 ppm1=9.657 ppm2=8.963 assign ( resid 90 and name HN ) ( resid 90 and name HA ) 3.1 1.4 1.2 volume=1.158 peak=1228 ppm1=8.382 ppm2=4.886 assign ( resid 56 and name HN ) ( resid 165 and name HN ) 2.7 1.0 1.1 volume=2.730 peak=2246 ppm1=8.641 ppm2=8.461 assign ( resid 5 and name HB# ) ( resid 6 and name HA ) 3.8 2.1 1.5 volume=0.352 peak=4071 ppm1=1.342 ppm2=3.638 assign ( resid 152 and name HN ) ( resid 169 and name HA ) 3.9 2.2 1.5 volume=0.319 peak=1830 ppm1=8.345 ppm2=5.191 assign ( resid 126 and name HG2# ) ( resid 126 and name HG12 ) 2.6 0.9 1.0 volume=3.632 peak=4901 ppm1=0.751 ppm2=1.000 assign ( resid 196 and name HA ) ( resid 196 and name HN ) 4.9 3.2 1.1 volume=0.078 peak=3916 ppm1=3.454 ppm2=7.442 assign ( resid 61 and name HN ) ( resid 62 and name HN ) 2.9 1.2 1.2 volume=1.651 peak=1459 ppm1=8.715 ppm2=8.175 assign ( resid 192 and name HG ) ( resid 50 and name HG1# ) 3.2 1.4 1.3 volume=1.082 peak=3591 ppm1=1.753 ppm2=0.660 assign ( resid 134 and name HN ) ( resid 93 and name HG2# ) 4.0 2.3 1.6 volume=0.252 peak=1440 ppm1=8.748 ppm2=-0.023 assign ( resid 177 and name HN ) ( resid 144 and name HG2# ) 3.4 1.7 1.4 volume=0.688 peak=1579 ppm1=8.463 ppm2=0.750 assign ( resid 117 and name HD1# ) ( resid 117 and name HG2# ) 2.5 0.8 1.0 volume=4.087 peak=4408 ppm1=0.244 ppm2=0.365 assign ( resid 22 and name HB2 or resid 22 and name HB1 ) ( resid 22 and name HA ) 4.7 2.9 1.3 volume=0.106 peak=2630 ppm1=3.770 ppm2=4.871 assign ( resid 86 and name HN ) ( resid 85 and name HB1 ) 4.4 2.7 1.6 volume=0.152 peak=235 ppm1=8.619 ppm2=3.084 assign ( resid 159 and name HG1 or resid 159 and name HG2 ) ( resid 159 and name HN ) 4.5 2.8 1.5 volume=0.134 peak=4820 ppm1=2.240 ppm2=9.034 assign ( resid 203 and name HD1# ) ( resid 61 and name HN ) 3.7 2.0 1.5 volume=0.433 peak=2564 ppm1=-0.010 ppm2=8.717 assign ( resid 165 and name HN ) ( resid 57 and name HA ) 3.7 2.0 1.5 volume=0.436 peak=1990 ppm1=8.464 ppm2=4.138 assign ( resid 85 and name HN ) ( resid 85 and name HA ) 3.2 1.5 1.3 volume=1.021 peak=1129 ppm1=7.153 ppm2=4.508 assign ( resid 196 and name HA ) ( resid 199 and name HN ) 4.4 2.6 1.6 volume=0.156 peak=3685 ppm1=3.455 ppm2=8.657 assign ( resid 97 and name HN ) ( resid 80 and name HG1# ) 2.9 1.2 1.2 volume=1.630 peak=1222 ppm1=8.361 ppm2=0.740 assign ( resid 2 and name HA ) ( resid 6 and name HN ) 3.7 2.0 1.5 volume=0.393 peak=5145 ppm1=4.146 ppm2=7.742 assign ( resid 115 and name HN ) ( resid 94 and name HN ) 4.2 2.5 1.7 volume=0.184 peak=1325 ppm1=9.053 ppm2=9.603 assign ( resid 41 and name HB1 ) ( resid 41 and name HD1 ) 4.3 2.5 1.7 volume=0.178 peak=4019 ppm1=1.979 ppm2=3.088 assign ( resid 115 and name HG1# ) ( resid 113 and name HB2 ) 3.4 1.7 1.4 volume=0.695 peak=2864 ppm1=0.303 ppm2=2.139 assign ( resid 80 and name HN ) ( resid 78 and name HA ) 3.4 1.7 1.4 volume=0.659 peak=1041 ppm1=7.524 ppm2=4.664 assign ( resid 8 and name HN ) ( resid 7 and name HB# ) 2.6 0.9 1.1 volume=3.277 peak=2331 ppm1=7.610 ppm2=0.745 assign ( resid 98 and name HN ) ( resid 78 and name HD2# ) 3.6 1.9 1.4 volume=0.518 peak=305 ppm1=9.354 ppm2=0.487 assign ( resid 170 and name HA ) ( resid 50 and name HN ) 4.1 2.4 1.6 volume=0.230 peak=2732 ppm1=5.821 ppm2=9.303 assign ( resid 42 and name HN ) ( resid 40 and name HA ) 3.7 2.0 1.5 volume=0.439 peak=661 ppm1=8.699 ppm2=3.978 assign ( resid 204 and name HG1 ) ( resid 204 and name HA ) 3.5 1.8 1.4 volume=0.600 peak=4902 ppm1=1.442 ppm2=3.802 assign ( resid 129 and name HB2 ) ( resid 127 and name HG11 ) 3.6 1.9 1.4 volume=0.512 peak=3350 ppm1=3.366 ppm2=1.025 assign ( resid 180 and name HN ) ( resid 183 and name HG2# ) 3.3 1.6 1.3 volume=0.807 peak=2315 ppm1=8.353 ppm2=0.959 assign ( resid 54 and name HD1# ) ( resid 203 and name HB ) 3.4 1.7 1.4 volume=0.673 peak=4309 ppm1=0.490 ppm2=0.186 assign ( resid 126 and name HA ) ( resid 126 and name HG2# ) 3.5 1.8 1.4 volume=0.542 peak=3504 ppm1=5.429 ppm2=0.753 assign ( resid 76 and name HA ) ( resid 76 and name HD1 ) 3.8 2.1 1.5 volume=0.335 peak=4155 ppm1=4.123 ppm2=1.551 assign ( resid 10 and name HN ) ( resid 11 and name HB# ) 3.3 1.6 1.3 volume=0.819 peak=1367 ppm1=8.319 ppm2=1.644 assign ( resid 134 and name HN ) ( resid 134 and name HB1 ) 3.1 1.3 1.2 volume=1.317 peak=2012 ppm1=8.745 ppm2=3.071 assign ( resid 163 and name HB# ) ( resid 161 and name HA ) 4.2 2.5 1.7 volume=0.191 peak=3630 ppm1=1.158 ppm2=4.672 assign ( resid 127 and name HN ) ( resid 127 and name HB ) 4.1 2.4 1.7 volume=0.217 peak=1663 ppm1=9.382 ppm2=2.058 assign ( resid 65 and name HD1# ) ( resid 64 and name HZ ) 3.6 1.9 1.4 volume=0.505 peak=2474 ppm1=0.175 ppm2=7.064 assign ( resid 15 and name HN ) ( resid 14 and name HG2# ) 2.6 0.9 1.0 volume=3.550 peak=606 ppm1=7.809 ppm2=0.756 assign ( resid 131 and name HN ) ( resid 148 and name HN ) 3.2 1.5 1.3 volume=0.919 peak=1453 ppm1=9.295 ppm2=9.197 assign ( resid 177 and name HA2 ) ( resid 144 and name HG2# ) 4.0 2.3 1.6 volume=0.261 peak=4273 ppm1=3.741 ppm2=0.729 assign ( resid 88 and name HN ) ( resid 91 and name HN ) 3.4 1.7 1.4 volume=0.724 peak=1200 ppm1=8.596 ppm2=7.255 assign ( resid 203 and name HN ) ( resid 203 and name HG2# ) 2.7 1.0 1.1 volume=2.825 peak=1254 ppm1=7.684 ppm2=0.355 assign ( resid 154 and name HG1# ) ( resid 126 and name HG11 or resid 126 and name HG12 ) 2.5 0.8 1.0 volume=3.914 peak=4805 ppm1=0.916 ppm2=1.080 assign ( resid 73 and name HN ) ( resid 70 and name HA ) 3.3 1.5 1.3 volume=0.881 peak=2261 ppm1=7.500 ppm2=4.812 assign ( resid 141 and name HB2 ) ( resid 141 and name HA ) 3.7 2.0 1.5 volume=0.423 peak=4227 ppm1=3.749 ppm2=3.931 assign ( resid 137 and name HN ) ( resid 112 and name HG2# ) 3.4 1.6 1.3 volume=0.739 peak=1570 ppm1=8.049 ppm2=0.666 assign ( resid 3 and name HD1 or resid 3 and name HD2 ) ( resid 87 and name HG11 ) 3.8 2.1 1.5 volume=0.337 peak=132 ppm1=7.379 ppm2=1.306 assign ( resid 200 and name HB1 ) ( resid 200 and name HD2 ) 2.6 0.9 1.1 volume=3.212 peak=4420 ppm1=1.670 ppm2=1.546 assign ( resid 112 and name HG2# ) ( resid 133 and name HA ) 4.3 2.6 1.7 volume=0.174 peak=3787 ppm1=0.678 ppm2=4.678 assign ( resid 27 and name HN ) ( resid 27 and name HB ) 3.5 1.8 1.4 volume=0.565 peak=465 ppm1=9.279 ppm2=2.050 assign ( resid 98 and name HG2# ) ( resid 109 and name HB2 ) 3.4 1.7 1.4 volume=0.725 peak=4554 ppm1=1.324 ppm2=1.740 assign ( resid 126 and name HD1# ) ( resid 14 and name HG1# ) 3.5 1.8 1.4 volume=0.612 peak=4816 ppm1=0.349 ppm2=0.635 assign ( resid 54 and name HB ) ( resid 54 and name HG11 or resid 54 and name HG12 ) 3.5 1.8 1.4 volume=0.550 peak=2634 ppm1=1.777 ppm2=1.192 assign ( resid 114 and name HD2# ) ( resid 114 and name HD1# ) 2.5 0.8 1.0 volume=4.465 peak=4876 ppm1=0.781 ppm2=0.513 assign ( resid 24 and name HN ) ( resid 23 and name HN ) 3.5 1.8 1.4 volume=0.608 peak=1092 ppm1=7.829 ppm2=8.687 assign ( resid 84 and name HA ) ( resid 84 and name HB ) 3.5 1.8 1.4 volume=0.538 peak=3037 ppm1=4.389 ppm2=2.025 assign ( resid 88 and name HN ) ( resid 87 and name HB ) 3.0 1.2 1.2 volume=1.591 peak=2235 ppm1=8.593 ppm2=1.370 assign ( resid 1 and name HN# ) ( resid 1 and name HA ) 3.0 1.3 1.2 volume=1.464 peak=647 ppm1=8.201 ppm2=4.275 assign ( resid 185 and name HN ) ( resid 184 and name HB ) 2.5 0.8 1.0 volume=4.602 peak=2063 ppm1=8.184 ppm2=2.054 assign ( resid 72 and name HG2# ) ( resid 72 and name HA ) 3.4 1.6 1.3 volume=0.755 peak=4803 ppm1=0.603 ppm2=3.634 assign ( resid 30 and name HN ) ( resid 30 and name HA ) 2.8 1.1 1.1 volume=2.161 peak=1917 ppm1=8.721 ppm2=4.667 assign ( resid 130 and name HB2 ) ( resid 10 and name HG2# ) 4.4 2.7 1.6 volume=0.140 peak=2763 ppm1=1.833 ppm2=1.039 assign ( resid 123 and name HN ) ( resid 120 and name HN ) 3.9 2.2 1.6 volume=0.298 peak=629 ppm1=8.404 ppm2=8.911 assign ( resid 132 and name HG2# ) ( resid 133 and name HB2 or resid 133 and name HB1 ) 3.6 1.8 1.4 volume=0.523 peak=4064 ppm1=0.937 ppm2=2.596 assign ( resid 19 and name HN ) ( resid 15 and name HD2# ) 3.5 1.8 1.4 volume=0.595 peak=1521 ppm1=7.482 ppm2=0.685 assign ( resid 41 and name HN ) ( resid 40 and name HA ) 3.3 1.6 1.3 volume=0.817 peak=1585 ppm1=8.907 ppm2=4.006 assign ( resid 81 and name HN ) ( resid 80 and name HB ) 3.3 1.6 1.3 volume=0.764 peak=754 ppm1=8.511 ppm2=1.406 assign ( resid 4 and name HN ) ( resid 4 and name HB1 or resid 4 and name HB2 ) 2.6 0.9 1.0 volume=3.571 peak=884 ppm1=8.189 ppm2=1.789 assign ( resid 134 and name HE1 or resid 134 and name HE2 ) ( resid 85 and name HB2 ) 3.0 1.2 1.2 volume=1.607 peak=119 ppm1=7.141 ppm2=3.060 assign ( resid 107 and name HN ) ( resid 107 and name HA ) 3.7 2.0 1.5 volume=0.397 peak=1718 ppm1=8.394 ppm2=4.503 assign ( resid 197 and name HN ) ( resid 199 and name HN ) 3.3 1.6 1.3 volume=0.761 peak=2177 ppm1=7.990 ppm2=8.638 assign ( resid 2 and name HA ) ( resid 5 and name HB# ) 3.8 2.1 1.5 volume=0.357 peak=5005 ppm1=4.146 ppm2=1.330 assign ( resid 174 and name HN ) ( resid 176 and name HN ) 3.5 1.8 1.4 volume=0.552 peak=1049 ppm1=9.152 ppm2=8.437 assign ( resid 65 and name HA ) ( resid 65 and name HD1# ) 3.7 2.0 1.5 volume=0.408 peak=4015 ppm1=3.888 ppm2=0.174 assign ( resid 101 and name HN ) ( resid 100 and name HB2 ) 3.7 2.0 1.5 volume=0.434 peak=1757 ppm1=8.477 ppm2=3.728 assign ( resid 112 and name HN ) ( resid 112 and name HD1# ) 3.6 1.9 1.5 volume=0.470 peak=2130 ppm1=8.137 ppm2=0.363 assign ( resid 200 and name HN ) ( resid 199 and name HN ) 3.2 1.4 1.3 volume=1.067 peak=1309 ppm1=8.086 ppm2=8.631 assign ( resid 100 and name HN ) ( resid 99 and name HB1 ) 3.6 1.9 1.4 volume=0.489 peak=756 ppm1=8.396 ppm2=1.790 assign ( resid 18 and name HN ) ( resid 17 and name HN ) 2.8 1.1 1.1 volume=2.218 peak=693 ppm1=7.760 ppm2=7.639 assign ( resid 28 and name HB1 or resid 28 and name HB2 ) ( resid 27 and name HG1# ) 3.3 1.6 1.3 volume=0.765 peak=2628 ppm1=1.913 ppm2=0.895 assign ( resid 28 and name HN ) ( resid 36 and name HA ) 3.3 1.6 1.3 volume=0.765 peak=1992 ppm1=7.808 ppm2=5.835 assign ( resid 3 and name HE1 or resid 3 and name HE2 ) ( resid 87 and name HD1# ) 3.6 1.9 1.4 volume=0.486 peak=127 ppm1=7.214 ppm2=0.440 assign ( resid 128 and name HN ) ( resid 127 and name HB ) 4.1 2.4 1.6 volume=0.229 peak=1394 ppm1=9.933 ppm2=2.045 assign ( resid 42 and name HN ) ( resid 43 and name HN ) 3.4 1.7 1.4 volume=0.669 peak=312 ppm1=8.701 ppm2=7.308 assign ( resid 40 and name HN ) ( resid 46 and name HB2 ) 4.2 2.5 1.7 volume=0.186 peak=2019 ppm1=8.512 ppm2=2.048 assign ( resid 161 and name HN ) ( resid 158 and name HB2 ) 2.8 1.1 1.1 volume=2.332 peak=2014 ppm1=6.905 ppm2=2.189 assign ( resid 109 and name HN ) ( resid 98 and name HG2# ) 2.9 1.2 1.2 volume=1.761 peak=1486 ppm1=8.164 ppm2=1.333 assign ( resid 1 and name HA ) ( resid 1 and name HB1 ) 4.4 2.7 1.6 volume=0.152 peak=4412 ppm1=4.282 ppm2=2.057 assign ( resid 203 and name HN ) ( resid 202 and name HA1 ) 3.3 1.6 1.3 volume=0.841 peak=1780 ppm1=7.684 ppm2=3.033 assign ( resid 193 and name HA ) ( resid 196 and name HG11 ) 3.7 2.0 1.5 volume=0.404 peak=4045 ppm1=3.462 ppm2=1.813 assign ( resid 76 and name HB1 ) ( resid 76 and name HA ) 4.1 2.4 1.6 volume=0.218 peak=3873 ppm1=1.983 ppm2=4.157 assign ( resid 122 and name HN ) ( resid 124 and name HN ) 4.0 2.3 1.6 volume=0.263 peak=2053 ppm1=8.645 ppm2=6.483 assign ( resid 143 and name HB1 ) ( resid 144 and name HG2# ) 3.7 2.0 1.5 volume=0.399 peak=3143 ppm1=2.706 ppm2=0.769 assign ( resid 136 and name HG2 ) ( resid 136 and name HN ) 3.0 1.3 1.2 volume=1.460 peak=4096 ppm1=1.952 ppm2=6.868 assign ( resid 11 and name HB# ) ( resid 8 and name HA ) 3.4 1.7 1.3 volume=0.732 peak=4870 ppm1=1.631 ppm2=3.843 assign ( resid 183 and name HN ) ( resid 185 and name HN ) 3.2 1.5 1.3 volume=0.927 peak=1354 ppm1=7.418 ppm2=8.185 assign ( resid 99 and name HN ) ( resid 78 and name HD2# ) 3.3 1.6 1.3 volume=0.767 peak=2258 ppm1=7.801 ppm2=0.490 assign ( resid 170 and name HA ) ( resid 169 and name HB1 ) 4.1 2.4 1.7 volume=0.212 peak=3399 ppm1=5.822 ppm2=1.850 assign ( resid 42 and name HB1 ) ( resid 43 and name HB2 ) 3.5 1.8 1.4 volume=0.595 peak=4161 ppm1=1.666 ppm2=2.856 assign ( resid 179 and name HA ) ( resid 179 and name HG ) 4.1 2.4 1.6 volume=0.222 peak=3307 ppm1=3.821 ppm2=1.514 assign ( resid 154 and name HG2# ) ( resid 18 and name HB2 ) 3.6 1.9 1.4 volume=0.492 peak=4584 ppm1=0.838 ppm2=2.460 assign ( resid 93 and name HG11 ) ( resid 93 and name HD1# ) 3.8 2.1 1.5 volume=0.364 peak=4639 ppm1=0.688 ppm2=-0.270 assign ( resid 174 and name HN ) ( resid 174 and name HA ) 3.1 1.4 1.2 volume=1.249 peak=925 ppm1=9.153 ppm2=4.530 assign ( resid 148 and name HN ) ( resid 131 and name HN ) 4.1 2.4 1.6 volume=0.224 peak=1094 ppm1=9.152 ppm2=9.282 assign ( resid 192 and name HN ) ( resid 191 and name HA ) 3.1 1.4 1.3 volume=1.125 peak=572 ppm1=8.210 ppm2=4.262 assign ( resid 130 and name HE2 ) ( resid 130 and name HG1 ) 2.7 0.9 1.1 volume=2.971 peak=2704 ppm1=2.838 ppm2=1.316 assign ( resid 203 and name HG2# ) ( resid 207 and name HD2 ) 3.9 2.2 1.6 volume=0.299 peak=4078 ppm1=0.340 ppm2=3.068 assign ( resid 57 and name HN ) ( resid 56 and name HN ) 3.7 1.9 1.5 volume=0.441 peak=1416 ppm1=9.217 ppm2=8.677 assign ( resid 54 and name HG12 ) ( resid 200 and name HD1 or resid 200 and name HD2 ) 2.9 1.2 1.2 volume=1.707 peak=4323 ppm1=1.235 ppm2=1.552 assign ( resid 70 and name HN ) ( resid 68 and name HG2# ) 3.7 2.0 1.5 volume=0.436 peak=1944 ppm1=8.575 ppm2=0.734 assign ( resid 15 and name HD2# ) ( resid 19 and name HD1 or resid 19 and name HD2 ) 4.0 2.2 1.6 volume=0.281 peak=2963 ppm1=0.684 ppm2=2.991 assign ( resid 179 and name HA ) ( resid 184 and name HG12 ) 4.0 2.3 1.6 volume=0.261 peak=3645 ppm1=3.821 ppm2=1.109 assign ( resid 146 and name HN ) ( resid 110 and name HA ) 3.7 1.9 1.5 volume=0.453 peak=1614 ppm1=8.401 ppm2=5.438 assign ( resid 88 and name HN ) ( resid 87 and name HG2# ) 3.4 1.7 1.4 volume=0.652 peak=1535 ppm1=8.596 ppm2=0.886 assign ( resid 134 and name HE1 or resid 134 and name HE2 ) ( resid 84 and name HG2# ) 3.1 1.4 1.3 volume=1.124 peak=60 ppm1=7.141 ppm2=0.145 assign ( resid 42 and name HN ) ( resid 42 and name HB2 ) 3.3 1.5 1.3 volume=0.910 peak=1005 ppm1=8.699 ppm2=1.709 assign ( resid 84 and name HN ) ( resid 84 and name HG2# ) 3.1 1.4 1.3 volume=1.102 peak=209 ppm1=8.504 ppm2=0.097 assign ( resid 124 and name HA ) ( resid 157 and name HG1 ) 4.2 2.5 1.7 volume=0.182 peak=3709 ppm1=5.179 ppm2=1.776 assign ( resid 78 and name HN ) ( resid 75 and name HB1 ) 3.6 1.8 1.4 volume=0.529 peak=2041 ppm1=7.148 ppm2=2.838 assign ( resid 97 and name HG2# ) ( resid 80 and name HG2# ) 3.0 1.3 1.2 volume=1.419 peak=4620 ppm1=0.217 ppm2=0.707 assign ( resid 206 and name HA ) ( resid 206 and name HB2 ) 4.1 2.4 1.7 volume=0.214 peak=4541 ppm1=4.366 ppm2=2.956 assign ( resid 84 and name HB ) ( resid 84 and name HG2# ) 3.3 1.6 1.3 volume=0.771 peak=3843 ppm1=1.997 ppm2=0.113 assign ( resid 93 and name HD1# ) ( resid 93 and name HG2# ) 2.7 1.0 1.1 volume=2.811 peak=2723 ppm1=-0.272 ppm2=-0.011 assign ( resid 6 and name HD1# ) ( resid 5 and name HB# ) 3.1 1.4 1.2 volume=1.197 peak=3979 ppm1=0.792 ppm2=1.342 assign ( resid 209 and name HD2 ) ( resid 209 and name HG2 ) 2.7 1.0 1.1 volume=2.834 peak=4981 ppm1=3.603 ppm2=1.894 assign ( resid 131 and name HN ) ( resid 147 and name HA ) 3.8 2.0 1.5 volume=0.381 peak=1883 ppm1=9.294 ppm2=4.267 assign ( resid 86 and name HA ) ( resid 87 and name HN ) 4.2 2.5 1.7 volume=0.200 peak=3854 ppm1=4.234 ppm2=8.055 assign ( resid 203 and name HD1# ) ( resid 60 and name HD1 ) 3.0 1.3 1.2 volume=1.437 peak=2657 ppm1=-0.010 ppm2=1.549 assign ( resid 193 and name HA ) ( resid 193 and name HG2# ) 4.0 2.2 1.6 volume=0.277 peak=4570 ppm1=3.462 ppm2=0.757 assign ( resid 76 and name HB2 ) ( resid 78 and name HN ) 4.0 2.2 1.6 volume=0.274 peak=3030 ppm1=1.984 ppm2=7.143 assign ( resid 35 and name HN ) ( resid 27 and name HG1# ) 3.1 1.4 1.2 volume=1.257 peak=1891 ppm1=9.428 ppm2=0.877 assign ( resid 168 and name HB ) ( resid 168 and name HG2# ) 3.6 1.9 1.4 volume=0.495 peak=4873 ppm1=1.724 ppm2=0.192 assign ( resid 37 and name HN ) ( resid 25 and name HN ) 3.5 1.8 1.4 volume=0.590 peak=873 ppm1=9.659 ppm2=9.094 assign ( resid 171 and name HN ) ( resid 170 and name HB1 ) 3.4 1.7 1.4 volume=0.667 peak=1840 ppm1=9.062 ppm2=1.796 assign ( resid 192 and name HG ) ( resid 188 and name HB1 ) 2.6 0.8 1.0 volume=3.760 peak=4457 ppm1=1.753 ppm2=1.458 assign ( resid 15 and name HD2# ) ( resid 15 and name HD1# ) 2.6 0.9 1.0 volume=3.536 peak=4493 ppm1=0.683 ppm2=0.439 assign ( resid 72 and name HG12 ) ( resid 72 and name HN ) 3.8 2.0 1.5 volume=0.380 peak=2735 ppm1=1.037 ppm2=7.534 assign ( resid 123 and name HN ) ( resid 157 and name HB2 ) 3.7 2.0 1.5 volume=0.387 peak=552 ppm1=8.404 ppm2=2.308 assign ( resid 136 and name HA ) ( resid 137 and name HN ) 3.4 1.7 1.4 volume=0.637 peak=4706 ppm1=3.790 ppm2=8.063 assign ( resid 166 and name HB2 ) ( resid 166 and name HN ) 4.1 2.4 1.6 volume=0.234 peak=4553 ppm1=1.652 ppm2=9.026 assign ( resid 11 and name HA ) ( resid 15 and name HB2 ) 4.2 2.4 1.7 volume=0.206 peak=3794 ppm1=3.956 ppm2=1.356 assign ( resid 134 and name HD1 or resid 134 and name HD2 ) ( resid 112 and name HG2# ) 3.3 1.5 1.3 volume=0.908 peak=144 ppm1=6.862 ppm2=0.703 assign ( resid 26 and name HA ) ( resid 26 and name HG2# ) 3.4 1.6 1.3 volume=0.755 peak=3900 ppm1=3.980 ppm2=0.913 assign ( resid 149 and name HN ) ( resid 147 and name HD1 or resid 147 and name HD2 ) 3.6 1.8 1.4 volume=0.533 peak=1355 ppm1=7.757 ppm2=6.222 assign ( resid 154 and name HG1# ) ( resid 18 and name HN ) 3.9 2.2 1.6 volume=0.311 peak=2459 ppm1=0.909 ppm2=7.804 assign ( resid 132 and name HG1# ) ( resid 133 and name HN ) 3.7 2.0 1.5 volume=0.438 peak=5015 ppm1=0.543 ppm2=8.125 assign ( resid 11 and name HB# ) ( resid 15 and name HD2# ) 3.3 1.5 1.3 volume=0.880 peak=4526 ppm1=1.630 ppm2=0.767 assign ( resid 125 and name HN ) ( resid 155 and name HB1 ) 3.2 1.5 1.3 volume=0.971 peak=959 ppm1=8.771 ppm2=3.023 assign ( resid 134 and name HD1 or resid 134 and name HD2 ) ( resid 112 and name HB ) 3.6 1.8 1.4 volume=0.523 peak=66 ppm1=6.862 ppm2=2.157 assign ( resid 14 and name HG1# ) ( resid 17 and name HN ) 3.3 1.6 1.3 volume=0.805 peak=3321 ppm1=0.677 ppm2=7.607 assign ( resid 114 and name HD1# ) ( resid 93 and name HB ) 3.1 1.4 1.2 volume=1.182 peak=3944 ppm1=0.538 ppm2=1.227 assign ( resid 26 and name HG1# ) ( resid 26 and name HN ) 4.0 2.3 1.6 volume=0.269 peak=4851 ppm1=0.778 ppm2=8.853 assign ( resid 113 and name HB1 ) ( resid 114 and name HN ) 4.4 2.7 1.6 volume=0.150 peak=4365 ppm1=2.067 ppm2=8.782 assign ( resid 156 and name HN ) ( resid 155 and name HB1 ) 3.3 1.6 1.3 volume=0.847 peak=2101 ppm1=8.551 ppm2=2.968 assign ( resid 110 and name HN ) ( resid 144 and name HD1# ) 3.8 2.1 1.5 volume=0.370 peak=1422 ppm1=8.721 ppm2=0.621 assign ( resid 119 and name HN ) ( resid 118 and name HA ) 3.1 1.4 1.2 volume=1.260 peak=495 ppm1=8.055 ppm2=3.809 assign ( resid 106 and name HN ) ( resid 102 and name HB# ) 3.2 1.5 1.3 volume=1.018 peak=1342 ppm1=7.943 ppm2=1.272 assign ( resid 179 and name HG ) ( resid 179 and name HB2 ) 2.6 0.9 1.0 volume=3.658 peak=3486 ppm1=1.516 ppm2=2.495 assign ( resid 71 and name HD2 ) ( resid 67 and name HN ) 3.9 2.2 1.6 volume=0.301 peak=4535 ppm1=2.779 ppm2=7.665 assign ( resid 115 and name HA ) ( resid 7 and name HB# ) 5.0 3.2 1.0 volume=0.071 peak=3388 ppm1=4.398 ppm2=0.771 assign ( resid 156 and name HN ) ( resid 61 and name HD1# ) 3.1 1.3 1.2 volume=1.301 peak=2161 ppm1=8.551 ppm2=0.699 assign ( resid 121 and name HN ) ( resid 121 and name HB2 ) 2.6 0.8 1.0 volume=3.751 peak=574 ppm1=8.585 ppm2=1.921 assign ( resid 91 and name HA ) ( resid 117 and name HG12 ) 4.2 2.5 1.7 volume=0.186 peak=3672 ppm1=5.877 ppm2=0.649 assign ( resid 130 and name HB1 ) ( resid 130 and name HG2 ) 3.2 1.5 1.3 volume=0.989 peak=3632 ppm1=1.887 ppm2=1.362 assign ( resid 20 and name HN ) ( resid 19 and name HN ) 2.6 0.9 1.1 volume=3.138 peak=1120 ppm1=7.404 ppm2=7.476 assign ( resid 95 and name HN ) ( resid 83 and name HA ) 3.4 1.7 1.4 volume=0.642 peak=1875 ppm1=9.125 ppm2=4.682 assign ( resid 73 and name HG2# ) ( resid 73 and name HB ) 3.3 1.6 1.3 volume=0.785 peak=2796 ppm1=1.218 ppm2=4.300 assign ( resid 129 and name HB1 ) ( resid 115 and name HG1# ) 3.9 2.2 1.6 volume=0.309 peak=4574 ppm1=3.368 ppm2=0.305 assign ( resid 129 and name HN ) ( resid 128 and name HA ) 2.9 1.2 1.2 volume=1.666 peak=411 ppm1=8.718 ppm2=5.569 assign ( resid 48 and name HN ) ( resid 49 and name HN ) 3.8 2.1 1.5 volume=0.361 peak=499 ppm1=9.291 ppm2=8.933 assign ( resid 201 and name HN ) ( resid 203 and name HB ) 3.6 1.9 1.4 volume=0.478 peak=577 ppm1=7.404 ppm2=0.113 assign ( resid 74 and name HZ2 ) ( resid 74 and name HZ1 ) 3.6 1.9 1.4 volume=0.491 peak=64 ppm1=6.458 ppm2=5.953 assign ( resid 35 and name HN ) ( resid 34 and name HB ) 3.5 1.8 1.4 volume=0.605 peak=1984 ppm1=9.430 ppm2=3.825 assign ( resid 195 and name HB2 ) ( resid 195 and name HN ) 4.7 3.0 1.3 volume=0.102 peak=5026 ppm1=3.220 ppm2=7.985 assign ( resid 201 and name HA ) ( resid 201 and name HN ) 3.7 1.9 1.5 volume=0.440 peak=4480 ppm1=4.330 ppm2=7.401 assign ( resid 187 and name HN ) ( resid 186 and name HG1 ) 3.3 1.6 1.3 volume=0.832 peak=1010 ppm1=7.601 ppm2=1.469 assign ( resid 154 and name HG2# ) ( resid 18 and name HN ) 3.7 2.0 1.5 volume=0.433 peak=3797 ppm1=0.839 ppm2=7.805 assign ( resid 154 and name HG1# ) ( resid 126 and name HG2# ) 2.3 0.5 0.9 volume=7.861 peak=3480 ppm1=0.915 ppm2=0.753 assign ( resid 160 and name HN ) ( resid 161 and name HN ) 3.3 1.6 1.3 volume=0.812 peak=1191 ppm1=8.835 ppm2=6.884 assign ( resid 193 and name HN ) ( resid 190 and name HA ) 3.1 1.4 1.2 volume=1.185 peak=2057 ppm1=7.621 ppm2=3.998 assign ( resid 132 and name HG1# ) ( resid 130 and name HN ) 3.7 1.9 1.5 volume=0.446 peak=2961 ppm1=0.542 ppm2=7.609 assign ( resid 201 and name HN ) ( resid 201 and name HA ) 3.0 1.2 1.2 volume=1.600 peak=1599 ppm1=7.402 ppm2=4.270 assign ( resid 192 and name HB1 ) ( resid 50 and name HG2# ) 3.9 2.2 1.6 volume=0.288 peak=2665 ppm1=1.331 ppm2=0.770 assign ( resid 186 and name HN ) ( resid 187 and name HG2# ) 3.2 1.5 1.3 volume=0.995 peak=698 ppm1=7.371 ppm2=1.012 assign ( resid 12 and name HN ) ( resid 126 and name HD1# ) 3.7 2.0 1.5 volume=0.396 peak=219 ppm1=7.552 ppm2=0.362 assign ( resid 176 and name HD2 ) ( resid 176 and name HG1 ) 4.0 2.3 1.6 volume=0.261 peak=4254 ppm1=3.216 ppm2=1.664 assign ( resid 126 and name HN ) ( resid 126 and name HB ) 3.4 1.7 1.4 volume=0.718 peak=1856 ppm1=9.105 ppm2=1.596 assign ( resid 143 and name HN ) ( resid 143 and name HB1 ) 3.2 1.5 1.3 volume=0.951 peak=403 ppm1=6.900 ppm2=2.592 assign ( resid 175 and name HN ) ( resid 109 and name HD1 ) 3.9 2.2 1.6 volume=0.309 peak=706 ppm1=8.803 ppm2=3.097 assign ( resid 68 and name HN ) ( resid 72 and name HD1# ) 3.4 1.7 1.3 volume=0.728 peak=2291 ppm1=8.025 ppm2=0.600 assign ( resid 165 and name HN ) ( resid 61 and name HD1# ) 3.1 1.4 1.3 volume=1.150 peak=886 ppm1=8.465 ppm2=0.748 assign ( resid 173 and name HN ) ( resid 173 and name HA ) 3.8 2.0 1.5 volume=0.374 peak=1824 ppm1=8.519 ppm2=3.567 assign ( resid 64 and name HN ) ( resid 64 and name HD1 or resid 64 and name HD2 ) 4.0 2.3 1.6 volume=0.248 peak=193 ppm1=7.876 ppm2=5.969 assign ( resid 76 and name HD2 ) ( resid 76 and name HB2 ) 2.8 1.1 1.1 volume=2.065 peak=4800 ppm1=1.551 ppm2=2.003 assign ( resid 199 and name HN ) ( resid 196 and name HN ) 3.8 2.1 1.5 volume=0.352 peak=1501 ppm1=8.634 ppm2=7.485 assign ( resid 69 and name HN ) ( resid 70 and name HN ) 3.3 1.6 1.3 volume=0.867 peak=256 ppm1=8.214 ppm2=8.566 assign ( resid 184 and name HB ) ( resid 184 and name HN ) 3.4 1.7 1.4 volume=0.676 peak=4669 ppm1=2.045 ppm2=7.506 assign ( resid 102 and name HA ) ( resid 186 and name HB2 ) 4.2 2.5 1.7 volume=0.185 peak=4026 ppm1=4.114 ppm2=1.880 assign ( resid 29 and name HN ) ( resid 28 and name HA ) 3.3 1.6 1.3 volume=0.865 peak=1837 ppm1=8.567 ppm2=4.412 assign ( resid 205 and name HB# ) ( resid 206 and name HN ) 2.9 1.2 1.2 volume=1.825 peak=4430 ppm1=1.294 ppm2=7.474 assign ( resid 82 and name HN ) ( resid 82 and name HB1 ) 2.8 1.1 1.1 volume=2.076 peak=780 ppm1=8.562 ppm2=2.444 assign ( resid 153 and name HN ) ( resid 152 and name HA1 ) 3.2 1.5 1.3 volume=0.946 peak=1888 ppm1=9.329 ppm2=3.742 assign ( resid 139 and name HB1 ) ( resid 144 and name HA ) 3.5 1.8 1.4 volume=0.563 peak=5070 ppm1=2.196 ppm2=4.027 assign ( resid 25 and name HN ) ( resid 24 and name HA ) 2.8 1.1 1.1 volume=2.185 peak=597 ppm1=9.014 ppm2=4.271 assign ( resid 87 and name HA ) ( resid 87 and name HG11 ) 3.0 1.2 1.2 volume=1.588 peak=3224 ppm1=3.871 ppm2=1.263 assign ( resid 123 and name HA ) ( resid 124 and name HN ) 4.1 2.4 1.7 volume=0.211 peak=3229 ppm1=4.349 ppm2=6.501 assign ( resid 129 and name HN ) ( resid 151 and name HA ) 3.7 2.0 1.5 volume=0.415 peak=1503 ppm1=8.720 ppm2=4.923 assign ( resid 162 and name HD2 ) ( resid 163 and name HN ) 4.6 2.9 1.4 volume=0.113 peak=4756 ppm1=3.489 ppm2=7.352 assign ( resid 129 and name HB1 ) ( resid 113 and name HN ) 4.8 3.1 1.2 volume=0.087 peak=3948 ppm1=3.369 ppm2=8.259 assign ( resid 115 and name HG1# ) ( resid 117 and name HN ) 4.2 2.5 1.7 volume=0.197 peak=3699 ppm1=0.304 ppm2=8.258 assign ( resid 106 and name HG2# ) ( resid 106 and name HB ) 3.0 1.3 1.2 volume=1.560 peak=4403 ppm1=0.897 ppm2=1.792 assign ( resid 203 and name HD1# ) ( resid 61 and name HB1 ) 2.9 1.2 1.2 volume=1.719 peak=3352 ppm1=-0.011 ppm2=1.617 assign ( resid 137 and name HB2 ) ( resid 112 and name HG2# ) 4.4 2.7 1.6 volume=0.140 peak=2949 ppm1=2.577 ppm2=0.641 assign ( resid 172 and name HN ) ( resid 151 and name HA ) 4.2 2.5 1.7 volume=0.195 peak=1346 ppm1=8.856 ppm2=4.920 assign ( resid 126 and name HG12 ) ( resid 11 and name HB# ) 3.7 1.9 1.5 volume=0.442 peak=4101 ppm1=1.080 ppm2=1.664 assign ( resid 69 and name HA1 ) ( resid 68 and name HG2# ) 4.2 2.5 1.7 volume=0.201 peak=4154 ppm1=3.778 ppm2=0.716 assign ( resid 168 and name HG2# ) ( resid 51 and name HG2 ) 3.4 1.7 1.3 volume=0.732 peak=3679 ppm1=0.199 ppm2=1.942 assign ( resid 113 and name HN ) ( resid 94 and name HB2 ) 3.3 1.5 1.3 volume=0.885 peak=1206 ppm1=8.232 ppm2=2.290 assign ( resid 161 and name HN ) ( resid 160 and name HN ) 2.9 1.2 1.2 volume=1.643 peak=1979 ppm1=6.905 ppm2=8.832 assign ( resid 155 and name HB2 ) ( resid 155 and name HA ) 4.6 2.9 1.4 volume=0.110 peak=3279 ppm1=2.577 ppm2=5.222 assign ( resid 107 and name HB2 ) ( resid 144 and name HG2# ) 3.4 1.7 1.4 volume=0.671 peak=4786 ppm1=3.876 ppm2=0.773 assign ( resid 94 and name HN ) ( resid 93 and name HN ) 4.1 2.4 1.6 volume=0.223 peak=1075 ppm1=9.600 ppm2=8.842 assign ( resid 36 and name HA ) ( resid 26 and name HB ) 4.3 2.6 1.7 volume=0.172 peak=5133 ppm1=5.852 ppm2=1.877 assign ( resid 134 and name HB1 ) ( resid 134 and name HE1 or resid 134 and name HE2 ) 3.9 2.2 1.6 volume=0.301 peak=4802 ppm1=3.048 ppm2=7.148 assign ( resid 93 and name HN ) ( resid 93 and name HG2# ) 3.6 1.9 1.4 volume=0.482 peak=351 ppm1=8.906 ppm2=-0.028 assign ( resid 64 and name HB2 or resid 64 and name HB1 ) ( resid 61 and name HD2# ) 3.8 2.1 1.5 volume=0.330 peak=2984 ppm1=3.023 ppm2=0.772 assign ( resid 184 and name HG11 ) ( resid 179 and name HB2 ) 3.8 2.1 1.5 volume=0.373 peak=3691 ppm1=1.678 ppm2=2.469 assign ( resid 93 and name HN ) ( resid 92 and name HB1 ) 3.2 1.5 1.3 volume=1.013 peak=1619 ppm1=8.905 ppm2=3.095 assign ( resid 137 and name HN ) ( resid 136 and name HA ) 2.9 1.2 1.2 volume=1.645 peak=738 ppm1=8.052 ppm2=3.746 assign ( resid 10 and name HN ) ( resid 7 and name HB# ) 3.1 1.4 1.3 volume=1.138 peak=280 ppm1=8.316 ppm2=0.751 assign ( resid 10 and name HG2# ) ( resid 7 and name HB# ) 2.4 0.6 0.9 volume=6.249 peak=3311 ppm1=1.085 ppm2=0.772 assign ( resid 22 and name HN ) ( resid 22 and name HA ) 3.0 1.3 1.2 volume=1.546 peak=1268 ppm1=8.193 ppm2=4.877 assign ( resid 140 and name HN ) ( resid 143 and name HN ) 3.9 2.1 1.5 volume=0.325 peak=657 ppm1=9.581 ppm2=6.867 assign ( resid 64 and name HD1 or resid 64 and name HD2 ) ( resid 199 and name HB# ) 3.4 1.7 1.4 volume=0.646 peak=30 ppm1=5.970 ppm2=0.696 assign ( resid 114 and name HB1 ) ( resid 114 and name HD1# ) 3.7 2.0 1.5 volume=0.411 peak=4656 ppm1=1.063 ppm2=0.535 assign ( resid 60 and name HE2 ) ( resid 60 and name HD1 ) 2.4 0.6 0.9 volume=6.087 peak=3997 ppm1=2.833 ppm2=1.536 assign ( resid 117 and name HN ) ( resid 117 and name HA ) 3.8 2.1 1.5 volume=0.363 peak=1867 ppm1=8.232 ppm2=5.029 assign ( resid 190 and name HN ) ( resid 191 and name HB2 ) 3.9 2.2 1.6 volume=0.292 peak=1750 ppm1=7.519 ppm2=2.827 assign ( resid 191 and name HN ) ( resid 192 and name HG ) 3.2 1.5 1.3 volume=0.993 peak=1187 ppm1=7.651 ppm2=1.742 assign ( resid 54 and name HG2# ) ( resid 54 and name HB ) 2.8 1.1 1.1 volume=2.364 peak=3474 ppm1=0.577 ppm2=1.751 assign ( resid 205 and name HB# ) ( resid 202 and name HN ) 3.7 2.0 1.5 volume=0.414 peak=3156 ppm1=1.296 ppm2=8.523 assign ( resid 184 and name HD1# ) ( resid 184 and name HB ) 2.6 0.8 1.0 volume=3.877 peak=3208 ppm1=0.894 ppm2=2.062 assign ( resid 132 and name HG1# ) ( resid 3 and name HB1 or resid 3 and name HB2 ) 4.0 2.3 1.6 volume=0.249 peak=3144 ppm1=0.543 ppm2=3.039 assign ( resid 163 and name HB# ) ( resid 163 and name HA ) 2.8 1.1 1.1 volume=2.243 peak=4447 ppm1=1.151 ppm2=4.137 assign ( resid 183 and name HG2# ) ( resid 183 and name HB ) 2.8 1.0 1.1 volume=2.427 peak=4595 ppm1=0.932 ppm2=1.967 assign ( resid 204 and name HN ) ( resid 207 and name HN ) 4.4 2.6 1.6 volume=0.155 peak=878 ppm1=6.746 ppm2=7.787 assign ( resid 77 and name HB1 ) ( resid 77 and name HA ) 3.6 1.9 1.4 volume=0.483 peak=3613 ppm1=3.888 ppm2=4.267 assign ( resid 204 and name HB1 ) ( resid 204 and name HA ) 2.5 0.8 1.0 volume=4.513 peak=4112 ppm1=1.712 ppm2=3.798 assign ( resid 36 and name HN ) ( resid 26 and name HG1# ) 3.1 1.4 1.3 volume=1.103 peak=1625 ppm1=9.882 ppm2=0.774 assign ( resid 93 and name HG2# ) ( resid 93 and name HG11 ) 2.9 1.1 1.1 volume=1.924 peak=2964 ppm1=-0.013 ppm2=0.688 assign ( resid 132 and name HG2# ) ( resid 130 and name HG2 or resid 130 and name HG1 ) 3.0 1.3 1.2 volume=1.405 peak=3817 ppm1=0.935 ppm2=1.356 assign ( resid 6 and name HN ) ( resid 4 and name HN ) 3.7 1.9 1.5 volume=0.451 peak=182 ppm1=7.720 ppm2=8.181 assign ( resid 96 and name HB ) ( resid 111 and name HN ) 5.2 3.5 0.8 volume=0.053 peak=2559 ppm1=3.865 ppm2=8.579 assign ( resid 159 and name HB2 or resid 159 and name HB1 ) ( resid 159 and name HG1 or resid 159 and name HG2 ) 2.7 1.0 1.1 volume=2.928 peak=3434 ppm1=1.876 ppm2=2.243 assign ( resid 86 and name HA ) ( resid 86 and name HB1 ) 3.0 1.3 1.2 volume=1.562 peak=3443 ppm1=4.286 ppm2=1.554 assign ( resid 73 and name HN ) ( resid 71 and name HA ) 3.7 1.9 1.5 volume=0.450 peak=1270 ppm1=7.502 ppm2=4.895 assign ( resid 10 and name HG2# ) ( resid 11 and name HN ) 3.9 2.2 1.6 volume=0.301 peak=2868 ppm1=1.084 ppm2=8.197 assign ( resid 200 and name HN ) ( resid 201 and name HN ) 3.1 1.4 1.2 volume=1.157 peak=1323 ppm1=8.086 ppm2=7.397 assign ( resid 134 and name HA ) ( resid 135 and name HB2 ) 4.6 2.8 1.4 volume=0.120 peak=2977 ppm1=5.189 ppm2=2.195 assign ( resid 57 and name HN ) ( resid 58 and name HD1 ) 3.0 1.3 1.2 volume=1.378 peak=961 ppm1=9.220 ppm2=3.877 assign ( resid 25 and name HN ) ( resid 24 and name HN ) 3.7 2.0 1.5 volume=0.417 peak=520 ppm1=9.010 ppm2=7.837 assign ( resid 24 and name HZ2 ) ( resid 21 and name HG2# ) 3.9 2.2 1.6 volume=0.307 peak=78 ppm1=7.537 ppm2=1.125 assign ( resid 160 and name HN ) ( resid 159 and name HB2 ) 2.5 0.8 1.0 volume=4.020 peak=478 ppm1=8.833 ppm2=1.878 assign ( resid 76 and name HG1 ) ( resid 76 and name HB2 ) 3.3 1.6 1.3 volume=0.862 peak=3990 ppm1=1.385 ppm2=2.004 assign ( resid 154 and name HG2# ) ( resid 154 and name HB ) 2.8 1.0 1.1 volume=2.402 peak=2842 ppm1=0.838 ppm2=2.179 assign ( resid 79 and name HN ) ( resid 79 and name HB2 ) 3.3 1.5 1.3 volume=0.902 peak=1471 ppm1=8.844 ppm2=1.796 assign ( resid 111 and name HN ) ( resid 112 and name HD1# ) 4.0 2.2 1.6 volume=0.280 peak=930 ppm1=8.631 ppm2=0.356 assign ( resid 145 and name HG1 ) ( resid 145 and name HD2 ) 4.3 2.6 1.7 volume=0.161 peak=3760 ppm1=1.407 ppm2=3.477 assign ( resid 84 and name HA ) ( resid 84 and name HG2# ) 4.0 2.3 1.6 volume=0.258 peak=3785 ppm1=4.398 ppm2=0.122 assign ( resid 9 and name HN ) ( resid 10 and name HN ) 3.3 1.5 1.3 volume=0.906 peak=1988 ppm1=7.985 ppm2=8.306 assign ( resid 199 and name HB# ) ( resid 199 and name HA ) 3.0 1.3 1.2 volume=1.459 peak=3326 ppm1=0.692 ppm2=2.797 assign ( resid 91 and name HA ) ( resid 115 and name HG2# ) 4.3 2.6 1.7 volume=0.171 peak=5056 ppm1=5.876 ppm2=0.656 assign ( resid 162 and name HG2 ) ( resid 162 and name HA ) 3.2 1.5 1.3 volume=1.019 peak=3585 ppm1=1.919 ppm2=3.656 assign ( resid 77 and name HB1 ) ( resid 77 and name HN ) 4.1 2.4 1.6 volume=0.228 peak=2710 ppm1=3.886 ppm2=8.054 assign ( resid 64 and name HB2 or resid 64 and name HB1 ) ( resid 64 and name HE1 or resid 64 and name HE2 ) 4.1 2.4 1.7 volume=0.217 peak=3555 ppm1=3.021 ppm2=6.481 assign ( resid 195 and name HN ) ( resid 194 and name HB2 ) 3.1 1.4 1.2 volume=1.253 peak=397 ppm1=7.972 ppm2=2.822 assign ( resid 179 and name HD1# ) ( resid 179 and name HB1 ) 3.8 2.1 1.5 volume=0.336 peak=4745 ppm1=0.530 ppm2=2.747 assign ( resid 175 and name HN ) ( resid 174 and name HG1 ) 3.1 1.3 1.2 volume=1.329 peak=531 ppm1=8.803 ppm2=2.182 assign ( resid 154 and name HG1# ) ( resid 168 and name HG2# ) 3.5 1.7 1.4 volume=0.618 peak=2557 ppm1=0.914 ppm2=0.188 assign ( resid 74 and name HN ) ( resid 72 and name HA ) 3.2 1.5 1.3 volume=0.927 peak=744 ppm1=6.490 ppm2=3.619 assign ( resid 143 and name HB1 ) ( resid 143 and name HA ) 4.0 2.2 1.6 volume=0.280 peak=4900 ppm1=2.691 ppm2=4.666 assign ( resid 158 and name HB2 ) ( resid 160 and name HA ) 4.0 2.2 1.6 volume=0.275 peak=3180 ppm1=2.219 ppm2=4.026 assign ( resid 207 and name HA ) ( resid 207 and name HG1 ) 3.5 1.7 1.4 volume=0.620 peak=3420 ppm1=4.168 ppm2=1.538 assign ( resid 122 and name HN ) ( resid 121 and name HB1 ) 3.3 1.5 1.3 volume=0.887 peak=461 ppm1=8.645 ppm2=2.054 assign ( resid 74 and name HD1 ) ( resid 74 and name HE1 ) 3.3 1.6 1.3 volume=0.798 peak=40 ppm1=6.939 ppm2=9.624 assign ( resid 114 and name HB1 ) ( resid 114 and name HN ) 4.3 2.6 1.7 volume=0.161 peak=3599 ppm1=1.063 ppm2=8.782 assign ( resid 97 and name HN ) ( resid 80 and name HN ) 3.9 2.2 1.6 volume=0.299 peak=913 ppm1=8.364 ppm2=7.525 assign ( resid 174 and name HN ) ( resid 147 and name HA ) 3.2 1.5 1.3 volume=0.968 peak=1515 ppm1=9.152 ppm2=4.260 assign ( resid 22 and name HN ) ( resid 21 and name HG2# ) 2.8 1.1 1.1 volume=2.208 peak=1390 ppm1=8.191 ppm2=1.147 assign ( resid 202 and name HN ) ( resid 203 and name HB ) 3.4 1.7 1.4 volume=0.644 peak=2253 ppm1=8.576 ppm2=0.123 assign ( resid 114 and name HD2# ) ( resid 130 and name HD2 ) 2.8 1.1 1.1 volume=2.358 peak=4569 ppm1=0.781 ppm2=1.639 assign ( resid 136 and name HA ) ( resid 134 and name HZ ) 4.0 2.3 1.6 volume=0.270 peak=4293 ppm1=3.788 ppm2=6.635 assign ( resid 184 and name HG2# ) ( resid 188 and name HE# ) 2.8 1.0 1.1 volume=2.395 peak=3075 ppm1=1.096 ppm2=1.883 assign ( resid 158 and name HN ) ( resid 157 and name HA ) 2.8 1.1 1.1 volume=2.257 peak=2270 ppm1=8.216 ppm2=4.789 assign ( resid 184 and name HG11 ) ( resid 184 and name HD1# ) 2.6 0.9 1.1 volume=3.271 peak=3609 ppm1=1.676 ppm2=0.897 assign ( resid 106 and name HN ) ( resid 106 and name HB ) 3.1 1.3 1.2 volume=1.329 peak=1293 ppm1=7.944 ppm2=1.793 assign ( resid 190 and name HB1 ) ( resid 102 and name HB# ) 3.5 1.8 1.4 volume=0.573 peak=2622 ppm1=3.882 ppm2=1.285 assign ( resid 154 and name HB ) ( resid 155 and name HA ) 4.4 2.7 1.6 volume=0.142 peak=3300 ppm1=2.180 ppm2=5.244 assign ( resid 12 and name HN ) ( resid 12 and name HA ) 2.7 1.0 1.1 volume=2.899 peak=522 ppm1=7.547 ppm2=3.883 assign ( resid 186 and name HN ) ( resid 189 and name HD2 ) 4.1 2.4 1.6 volume=0.227 peak=2185 ppm1=7.370 ppm2=3.456 assign ( resid 86 and name HB1 ) ( resid 86 and name HD1 ) 4.2 2.5 1.7 volume=0.182 peak=4896 ppm1=1.556 ppm2=2.930 assign ( resid 183 and name HN ) ( resid 182 and name HA ) 3.0 1.3 1.2 volume=1.564 peak=581 ppm1=7.419 ppm2=4.129 assign ( resid 8 and name HA ) ( resid 116 and name HB2 ) 4.2 2.5 1.7 volume=0.204 peak=4198 ppm1=3.839 ppm2=2.853 assign ( resid 93 and name HD1# ) ( resid 3 and name HB1 ) 3.5 1.8 1.4 volume=0.563 peak=4953 ppm1=-0.273 ppm2=2.984 assign ( resid 201 and name HB2 ) ( resid 200 and name HB2 ) 4.2 2.5 1.7 volume=0.191 peak=4862 ppm1=2.581 ppm2=1.674 assign ( resid 184 and name HD1# ) ( resid 179 and name HA ) 3.1 1.4 1.2 volume=1.264 peak=2517 ppm1=0.890 ppm2=3.827 assign ( resid 173 and name HN ) ( resid 172 and name HG1 ) 3.4 1.6 1.3 volume=0.752 peak=1229 ppm1=8.519 ppm2=2.324 assign ( resid 149 and name HN ) ( resid 149 and name HA ) 3.2 1.4 1.3 volume=1.066 peak=201 ppm1=7.757 ppm2=4.481 assign ( resid 167 and name HD2# ) ( resid 167 and name HN ) 4.0 2.3 1.6 volume=0.272 peak=3062 ppm1=0.764 ppm2=8.643 assign ( resid 97 and name HN ) ( resid 96 and name HB ) 3.5 1.8 1.4 volume=0.544 peak=1399 ppm1=8.362 ppm2=3.876 assign ( resid 74 and name HN ) ( resid 74 and name HE1 ) 4.1 2.4 1.6 volume=0.229 peak=1741 ppm1=6.492 ppm2=9.618 assign ( resid 40 and name HN ) ( resid 46 and name HB1 ) 3.6 1.9 1.4 volume=0.483 peak=1755 ppm1=8.511 ppm2=1.527 assign ( resid 114 and name HD2# ) ( resid 114 and name HB2 ) 2.9 1.1 1.1 volume=1.982 peak=2866 ppm1=0.781 ppm2=1.712 assign ( resid 184 and name HG11 ) ( resid 179 and name HD2# ) 2.6 0.9 1.0 volume=3.376 peak=2582 ppm1=1.674 ppm2=0.772 assign ( resid 131 and name HN ) ( resid 130 and name HN ) 4.0 2.3 1.6 volume=0.252 peak=2232 ppm1=9.294 ppm2=7.654 assign ( resid 72 and name HG11 ) ( resid 72 and name HA ) 4.2 2.5 1.7 volume=0.197 peak=3994 ppm1=1.172 ppm2=3.629 assign ( resid 15 and name HD2# ) ( resid 12 and name HA ) 3.7 2.0 1.5 volume=0.428 peak=4187 ppm1=0.684 ppm2=3.894 assign ( resid 154 and name HN ) ( resid 153 and name HN ) 3.6 1.8 1.4 volume=0.529 peak=306 ppm1=10.005 ppm2=9.348 assign ( resid 184 and name HG11 ) ( resid 184 and name HB ) 2.7 0.9 1.1 volume=3.037 peak=3217 ppm1=1.676 ppm2=2.062 assign ( resid 54 and name HD1# ) ( resid 53 and name HN ) 4.3 2.6 1.7 volume=0.161 peak=2845 ppm1=0.493 ppm2=8.328 assign ( resid 76 and name HN ) ( resid 75 and name HA ) 2.8 1.1 1.1 volume=2.298 peak=355 ppm1=6.699 ppm2=4.142 assign ( resid 94 and name HN ) ( resid 93 and name HA ) 3.2 1.4 1.3 volume=1.071 peak=2010 ppm1=9.601 ppm2=4.788 assign ( resid 82 and name HN ) ( resid 95 and name HN ) 3.7 2.0 1.5 volume=0.431 peak=1662 ppm1=8.563 ppm2=9.088 assign ( resid 97 and name HG2# ) ( resid 80 and name HB ) 3.3 1.6 1.3 volume=0.804 peak=5042 ppm1=0.218 ppm2=1.350 assign ( resid 126 and name HG2# ) ( resid 11 and name HA ) 3.4 1.7 1.4 volume=0.695 peak=4106 ppm1=0.751 ppm2=3.955 assign ( resid 154 and name HG1# ) ( resid 18 and name HB2 ) 3.3 1.6 1.3 volume=0.809 peak=3011 ppm1=0.917 ppm2=2.428 assign ( resid 79 and name HA ) ( resid 80 and name HG2# ) 3.9 2.2 1.6 volume=0.296 peak=2548 ppm1=4.398 ppm2=0.701 assign ( resid 22 and name HN ) ( resid 24 and name HE1 ) 3.4 1.7 1.4 volume=0.660 peak=897 ppm1=8.191 ppm2=10.142 assign ( resid 160 and name HA ) ( resid 161 and name HN ) 3.8 2.1 1.5 volume=0.372 peak=2750 ppm1=4.011 ppm2=6.914 assign ( resid 103 and name HN ) ( resid 103 and name HA ) 3.1 1.4 1.2 volume=1.167 peak=643 ppm1=8.453 ppm2=3.615 assign ( resid 188 and name HA ) ( resid 48 and name HB2 ) 4.1 2.4 1.6 volume=0.224 peak=3007 ppm1=4.216 ppm2=2.658 assign ( resid 112 and name HG12 ) ( resid 112 and name HG2# ) 3.5 1.7 1.4 volume=0.621 peak=4075 ppm1=1.249 ppm2=0.680 assign ( resid 33 and name HG11 ) ( resid 33 and name HG12 ) 2.0 0.3 0.8 volume=17.352 peak=4349 ppm1=1.886 ppm2=1.921 assign ( resid 72 and name HG12 ) ( resid 72 and name HG11 ) 3.2 1.4 1.3 volume=1.097 peak=3183 ppm1=1.038 ppm2=1.169 assign ( resid 54 and name HD1# ) ( resid 167 and name HD2# ) 2.3 0.6 0.9 volume=6.846 peak=3338 ppm1=0.491 ppm2=0.768 assign ( resid 154 and name HN ) ( resid 168 and name HA ) 4.1 2.4 1.6 volume=0.221 peak=1584 ppm1=10.005 ppm2=4.814 assign ( resid 167 and name HA ) ( resid 167 and name HN ) 4.3 2.6 1.7 volume=0.176 peak=3768 ppm1=5.217 ppm2=8.644 assign ( resid 49 and name HN ) ( resid 36 and name HB2 ) 3.8 2.0 1.5 volume=0.378 peak=467 ppm1=8.911 ppm2=3.483 assign ( resid 86 and name HD1 ) ( resid 92 and name HE1 or resid 92 and name HE2 ) 3.6 1.9 1.4 volume=0.475 peak=2636 ppm1=2.934 ppm2=6.750 assign ( resid 157 and name HD1 ) ( resid 156 and name HN ) 4.7 3.0 1.3 volume=0.097 peak=4682 ppm1=3.626 ppm2=8.455 assign ( resid 153 and name HN ) ( resid 152 and name HN ) 4.2 2.5 1.7 volume=0.184 peak=848 ppm1=9.328 ppm2=8.326 assign ( resid 154 and name HB ) ( resid 154 and name HA ) 3.2 1.5 1.3 volume=0.960 peak=2555 ppm1=2.180 ppm2=4.669 assign ( resid 88 and name HN ) ( resid 92 and name HA ) 3.7 2.0 1.5 volume=0.418 peak=2122 ppm1=8.594 ppm2=4.916 assign ( resid 208 and name HB ) ( resid 210 and name HB2 or resid 210 and name HB1 ) 3.3 1.6 1.3 volume=0.853 peak=2700 ppm1=4.032 ppm2=3.765 assign ( resid 88 and name HN ) ( resid 88 and name HA ) 3.2 1.5 1.3 volume=0.958 peak=1940 ppm1=8.595 ppm2=4.522 assign ( resid 27 and name HN ) ( resid 36 and name HA ) 3.6 1.9 1.4 volume=0.506 peak=1679 ppm1=9.277 ppm2=5.833 assign ( resid 37 and name HN ) ( resid 27 and name HG1# ) 2.8 1.1 1.1 volume=2.237 peak=559 ppm1=9.656 ppm2=0.882 assign ( resid 76 and name HB2 ) ( resid 76 and name HN ) 4.1 2.3 1.6 volume=0.241 peak=2923 ppm1=1.984 ppm2=6.698 assign ( resid 107 and name HN ) ( resid 106 and name HB ) 3.7 2.0 1.5 volume=0.434 peak=2431 ppm1=8.396 ppm2=1.795 assign ( resid 197 and name HG ) ( resid 197 and name HA ) 3.5 1.8 1.4 volume=0.560 peak=3272 ppm1=1.276 ppm2=3.758 assign ( resid 18 and name HN ) ( resid 17 and name HD1 or resid 17 and name HD2 ) 3.4 1.7 1.4 volume=0.681 peak=2407 ppm1=7.764 ppm2=6.480 assign ( resid 26 and name HN ) ( resid 26 and name HG1# ) 2.7 1.0 1.1 volume=2.868 peak=1529 ppm1=8.863 ppm2=0.759 assign ( resid 154 and name HN ) ( resid 169 and name HB1 ) 3.4 1.7 1.4 volume=0.663 peak=1001 ppm1=10.005 ppm2=1.800 assign ( resid 37 and name HN ) ( resid 36 and name HB2 ) 3.1 1.4 1.3 volume=1.106 peak=1767 ppm1=9.657 ppm2=3.484 assign ( resid 187 and name HN ) ( resid 187 and name HA ) 2.8 1.1 1.1 volume=2.253 peak=1689 ppm1=7.600 ppm2=4.263 assign ( resid 131 and name HN ) ( resid 114 and name HN ) 3.7 2.0 1.5 volume=0.407 peak=206 ppm1=9.293 ppm2=8.798 assign ( resid 4 and name HN ) ( resid 7 and name HB# ) 2.9 1.2 1.2 volume=1.816 peak=1013 ppm1=8.189 ppm2=0.758 assign ( resid 79 and name HA ) ( resid 72 and name HG2# ) 4.0 2.3 1.6 volume=0.273 peak=4797 ppm1=4.398 ppm2=0.584 assign ( resid 115 and name HN ) ( resid 114 and name HG ) 3.6 1.9 1.4 volume=0.503 peak=298 ppm1=9.052 ppm2=0.947 assign ( resid 8 and name HG1 or resid 8 and name HG2 ) ( resid 8 and name HB2 or resid 8 and name HB1 ) 2.6 0.9 1.0 volume=3.502 peak=3298 ppm1=2.321 ppm2=2.048 assign ( resid 5 and name HA ) ( resid 8 and name HG1 or resid 8 and name HG2 ) 3.5 1.8 1.4 volume=0.537 peak=4714 ppm1=4.023 ppm2=2.329 assign ( resid 73 and name HN ) ( resid 74 and name HN ) 3.1 1.4 1.2 volume=1.176 peak=314 ppm1=7.501 ppm2=6.488 assign ( resid 7 and name HN ) ( resid 9 and name HN ) 3.8 2.1 1.5 volume=0.356 peak=1747 ppm1=8.434 ppm2=8.030 assign ( resid 188 and name HN ) ( resid 185 and name HA ) 3.4 1.7 1.4 volume=0.721 peak=1760 ppm1=8.442 ppm2=3.872 assign ( resid 130 and name HN ) ( resid 129 and name HB1 ) 3.2 1.5 1.3 volume=0.966 peak=2221 ppm1=7.616 ppm2=3.362 assign ( resid 183 and name HN ) ( resid 184 and name HA ) 3.6 1.9 1.4 volume=0.485 peak=1345 ppm1=7.420 ppm2=3.618 assign ( resid 5 and name HA ) ( resid 8 and name HN ) 3.6 1.9 1.4 volume=0.486 peak=4354 ppm1=4.023 ppm2=7.605 assign ( resid 145 and name HN ) ( resid 144 and name HA ) 2.9 1.2 1.2 volume=1.790 peak=202 ppm1=8.380 ppm2=4.005 assign ( resid 114 and name HD1# ) ( resid 115 and name HN ) 3.8 2.1 1.5 volume=0.340 peak=3232 ppm1=0.539 ppm2=9.114 assign ( resid 91 and name HB ) ( resid 91 and name HG2# ) 3.6 1.9 1.4 volume=0.493 peak=3023 ppm1=3.641 ppm2=1.029 assign ( resid 51 and name HG1 or resid 51 and name HG2 ) ( resid 34 and name HB ) 3.4 1.6 1.3 volume=0.759 peak=3547 ppm1=1.972 ppm2=3.840 assign ( resid 130 and name HE1 ) ( resid 6 and name HG2# ) 2.7 1.0 1.1 volume=2.810 peak=3654 ppm1=2.836 ppm2=0.838 assign ( resid 165 and name HN ) ( resid 158 and name HB2 ) 4.2 2.5 1.7 volume=0.194 peak=967 ppm1=8.465 ppm2=2.212 assign ( resid 10 and name HN ) ( resid 8 and name HN ) 3.6 1.9 1.4 volume=0.509 peak=429 ppm1=8.317 ppm2=7.659 assign ( resid 76 and name HN ) ( resid 75 and name HN ) 3.8 2.0 1.5 volume=0.379 peak=547 ppm1=6.700 ppm2=7.530 assign ( resid 26 and name HG2# ) ( resid 26 and name HA ) 3.1 1.4 1.2 volume=1.216 peak=3899 ppm1=0.914 ppm2=3.972 assign ( resid 166 and name HB1 ) ( resid 166 and name HD1 ) 3.0 1.2 1.2 volume=1.584 peak=2999 ppm1=1.654 ppm2=1.450 assign ( resid 59 and name HN ) ( resid 59 and name HB# ) 3.4 1.7 1.4 volume=0.672 peak=882 ppm1=8.091 ppm2=1.268 assign ( resid 74 and name HZ2 ) ( resid 202 and name HA2 ) 3.8 2.1 1.5 volume=0.368 peak=19 ppm1=6.459 ppm2=3.369 assign ( resid 160 and name HN ) ( resid 160 and name HB2 ) 2.7 1.0 1.1 volume=2.643 peak=1454 ppm1=8.833 ppm2=2.022 assign ( resid 154 and name HG2# ) ( resid 15 and name HA ) 3.9 2.2 1.6 volume=0.317 peak=4287 ppm1=0.836 ppm2=3.644 assign ( resid 54 and name HD1# ) ( resid 196 and name HN ) 4.1 2.4 1.7 volume=0.216 peak=4144 ppm1=0.491 ppm2=7.466 assign ( resid 98 and name HN ) ( resid 98 and name HB ) 3.0 1.3 1.2 volume=1.372 peak=2099 ppm1=9.354 ppm2=4.568 assign ( resid 144 and name HN ) ( resid 143 and name HA ) 3.3 1.6 1.3 volume=0.866 peak=729 ppm1=7.536 ppm2=4.656 assign ( resid 153 and name HN ) ( resid 152 and name HA2 ) 3.2 1.4 1.3 volume=1.063 peak=1598 ppm1=9.329 ppm2=3.846 assign ( resid 79 and name HG2 ) ( resid 99 and name HB2 ) 2.7 1.0 1.1 volume=2.588 peak=4689 ppm1=1.914 ppm2=1.775 assign ( resid 26 and name HG2# ) ( resid 26 and name HB ) 3.0 1.3 1.2 volume=1.353 peak=3769 ppm1=0.912 ppm2=1.921 assign ( resid 67 and name HB2 ) ( resid 68 and name HG2# ) 3.2 1.5 1.3 volume=0.944 peak=3286 ppm1=2.064 ppm2=0.770 assign ( resid 184 and name HG2# ) ( resid 188 and name HN ) 4.0 2.3 1.6 volume=0.253 peak=3587 ppm1=1.095 ppm2=8.457 assign ( resid 98 and name HN ) ( resid 98 and name HA ) 3.0 1.3 1.2 volume=1.372 peak=330 ppm1=9.353 ppm2=4.662 assign ( resid 159 and name HB2 or resid 159 and name HB1 ) ( resid 159 and name HA ) 3.2 1.5 1.3 volume=0.979 peak=4153 ppm1=1.879 ppm2=3.772 assign ( resid 47 and name HN ) ( resid 46 and name HB1 ) 3.1 1.3 1.2 volume=1.309 peak=1156 ppm1=8.698 ppm2=1.535 assign ( resid 67 and name HN ) ( resid 67 and name HB2 ) 3.1 1.4 1.2 volume=1.209 peak=844 ppm1=7.603 ppm2=2.062 assign ( resid 126 and name HD1# ) ( resid 11 and name HB# ) 3.6 1.8 1.4 volume=0.526 peak=5161 ppm1=0.347 ppm2=1.635 assign ( resid 78 and name HN ) ( resid 78 and name HA ) 2.9 1.1 1.1 volume=1.970 peak=2448 ppm1=7.148 ppm2=4.662 assign ( resid 179 and name HB2 ) ( resid 179 and name HD2# ) 3.4 1.7 1.4 volume=0.661 peak=4611 ppm1=2.494 ppm2=0.742 assign ( resid 203 and name HN ) ( resid 203 and name HD1# ) 3.2 1.5 1.3 volume=1.039 peak=253 ppm1=7.683 ppm2=-0.008 assign ( resid 119 and name HN ) ( resid 119 and name HD2 ) 3.1 1.3 1.2 volume=1.287 peak=2084 ppm1=8.054 ppm2=2.848 assign ( resid 160 and name HN ) ( resid 159 and name HN ) 3.5 1.7 1.4 volume=0.629 peak=320 ppm1=8.833 ppm2=9.022 assign ( resid 65 and name HD1# ) ( resid 64 and name HE1 or resid 64 and name HE2 ) 4.0 2.2 1.6 volume=0.280 peak=4010 ppm1=0.173 ppm2=6.492 assign ( resid 6 and name HN ) ( resid 8 and name HN ) 3.2 1.5 1.3 volume=0.993 peak=173 ppm1=7.722 ppm2=7.600 assign ( resid 122 and name HN ) ( resid 121 and name HA ) 3.2 1.5 1.3 volume=0.956 peak=1396 ppm1=8.645 ppm2=4.144 assign ( resid 200 and name HN ) ( resid 199 and name HB# ) 2.8 1.0 1.1 volume=2.433 peak=496 ppm1=8.086 ppm2=0.627 assign ( resid 203 and name HD1# ) ( resid 203 and name HG11 or resid 203 and name HG12 ) 2.7 1.0 1.1 volume=2.528 peak=4586 ppm1=-0.008 ppm2=0.514 assign ( resid 199 and name HA ) ( resid 64 and name HZ ) 4.6 2.9 1.4 volume=0.117 peak=4458 ppm1=2.796 ppm2=7.022 assign ( resid 173 and name HA ) ( resid 171 and name HG2# ) 3.9 2.2 1.6 volume=0.292 peak=3118 ppm1=3.611 ppm2=0.781 assign ( resid 196 and name HG2# ) ( resid 199 and name HN ) 4.4 2.7 1.6 volume=0.152 peak=3623 ppm1=0.813 ppm2=8.652 assign ( resid 195 and name HN ) ( resid 198 and name HN ) 3.7 2.0 1.5 volume=0.395 peak=1674 ppm1=7.972 ppm2=8.694 assign ( resid 140 and name HN ) ( resid 141 and name HN ) 3.9 2.1 1.5 volume=0.326 peak=812 ppm1=9.580 ppm2=8.438 assign ( resid 117 and name HN ) ( resid 118 and name HA ) 3.8 2.1 1.5 volume=0.342 peak=1393 ppm1=8.231 ppm2=3.753 assign ( resid 137 and name HB1 ) ( resid 136 and name HG1 ) 3.9 2.2 1.6 volume=0.287 peak=2547 ppm1=2.809 ppm2=2.002 assign ( resid 27 and name HN ) ( resid 37 and name HN ) 3.9 2.2 1.6 volume=0.294 peak=377 ppm1=9.278 ppm2=9.685 assign ( resid 15 and name HD1# ) ( resid 18 and name HB1 ) 3.4 1.7 1.4 volume=0.677 peak=4385 ppm1=0.439 ppm2=2.990 assign ( resid 103 and name HG1# ) ( resid 103 and name HB ) 2.9 1.2 1.2 volume=1.667 peak=4100 ppm1=0.878 ppm2=2.588 assign ( resid 167 and name HA ) ( resid 61 and name HD1# ) 3.6 1.8 1.4 volume=0.536 peak=4811 ppm1=5.218 ppm2=0.752 assign ( resid 196 and name HG2# ) ( resid 199 and name HB# ) 2.1 0.3 0.8 volume=13.879 peak=4604 ppm1=0.812 ppm2=0.684 assign ( resid 130 and name HB1 ) ( resid 130 and name HE2 ) 2.9 1.1 1.1 volume=1.973 peak=3315 ppm1=1.887 ppm2=2.843 assign ( resid 196 and name HG2# ) ( resid 200 and name HE1 ) 3.4 1.7 1.3 volume=0.733 peak=4513 ppm1=0.812 ppm2=2.853 assign ( resid 78 and name HN ) ( resid 77 and name HN ) 3.1 1.4 1.2 volume=1.160 peak=770 ppm1=7.150 ppm2=8.052 assign ( resid 166 and name HB2 ) ( resid 166 and name HG2 or resid 166 and name HG1 ) 3.0 1.3 1.2 volume=1.442 peak=3213 ppm1=1.654 ppm2=1.227 assign ( resid 136 and name HN ) ( resid 136 and name HA ) 2.8 1.1 1.1 volume=2.337 peak=1646 ppm1=6.891 ppm2=3.746 assign ( resid 150 and name HB1 ) ( resid 10 and name HG2# ) 4.4 2.7 1.6 volume=0.143 peak=4122 ppm1=2.331 ppm2=1.082 assign ( resid 187 and name HN ) ( resid 185 and name HN ) 4.0 2.3 1.6 volume=0.248 peak=702 ppm1=7.599 ppm2=8.190 assign ( resid 191 and name HN ) ( resid 189 and name HA ) 3.2 1.5 1.3 volume=1.015 peak=1217 ppm1=7.650 ppm2=4.658 assign ( resid 167 and name HN ) ( resid 53 and name HG2# ) 3.1 1.4 1.2 volume=1.239 peak=2109 ppm1=8.642 ppm2=0.906 assign ( resid 62 and name HN ) ( resid 59 and name HN ) 3.2 1.5 1.3 volume=0.999 peak=1838 ppm1=8.132 ppm2=8.042 assign ( resid 200 and name HD1 ) ( resid 200 and name HE2 ) 2.4 0.6 0.9 volume=6.237 peak=3546 ppm1=1.547 ppm2=2.803 assign ( resid 199 and name HB# ) ( resid 198 and name HB2 or resid 198 and name HB1 ) 3.8 2.1 1.5 volume=0.349 peak=3660 ppm1=0.692 ppm2=3.052 assign ( resid 199 and name HN ) ( resid 202 and name HN ) 3.4 1.7 1.3 volume=0.727 peak=966 ppm1=8.633 ppm2=8.566 assign ( resid 51 and name HB1 or resid 51 and name HB2 ) ( resid 51 and name HN ) 4.2 2.5 1.7 volume=0.197 peak=4484 ppm1=1.780 ppm2=8.429 assign ( resid 209 and name HD1 ) ( resid 208 and name HG2# ) 3.5 1.7 1.4 volume=0.632 peak=2488 ppm1=3.605 ppm2=1.136 assign ( resid 5 and name HB# ) ( resid 6 and name HD1# ) 2.9 1.2 1.2 volume=1.701 peak=3882 ppm1=1.343 ppm2=0.773 assign ( resid 54 and name HN ) ( resid 54 and name HG11 or resid 54 and name HG12 ) 3.2 1.5 1.3 volume=1.040 peak=1929 ppm1=9.022 ppm2=1.152 assign ( resid 72 and name HB ) ( resid 72 and name HG12 ) 2.9 1.2 1.2 volume=1.677 peak=3090 ppm1=1.855 ppm2=1.038 assign ( resid 117 and name HN ) ( resid 91 and name HA ) 3.9 2.2 1.6 volume=0.298 peak=1315 ppm1=8.232 ppm2=5.836 assign ( resid 203 and name HG2# ) ( resid 204 and name HG2 ) 3.3 1.5 1.3 volume=0.898 peak=3357 ppm1=0.341 ppm2=1.291 assign ( resid 134 and name HN ) ( resid 112 and name HB ) 3.4 1.7 1.4 volume=0.682 peak=755 ppm1=8.745 ppm2=2.178 assign ( resid 126 and name HN ) ( resid 125 and name HN ) 3.8 2.0 1.5 volume=0.379 peak=2218 ppm1=9.104 ppm2=8.812 assign ( resid 179 and name HB1 ) ( resid 179 and name HD2# ) 2.9 1.2 1.2 volume=1.714 peak=4244 ppm1=2.752 ppm2=0.744 assign ( resid 203 and name HN ) ( resid 201 and name HA ) 3.3 1.6 1.3 volume=0.815 peak=568 ppm1=7.684 ppm2=4.274 assign ( resid 170 and name HA ) ( resid 170 and name HB1 ) 3.8 2.1 1.5 volume=0.345 peak=3484 ppm1=5.822 ppm2=1.795 assign ( resid 153 and name HN ) ( resid 126 and name HB ) 3.8 2.1 1.5 volume=0.333 peak=2320 ppm1=9.331 ppm2=1.553 assign ( resid 110 and name HN ) ( resid 143 and name HB1 ) 3.7 2.0 1.5 volume=0.419 peak=1480 ppm1=8.721 ppm2=2.705 assign ( resid 86 and name HG1 ) ( resid 92 and name HE1 or resid 92 and name HE2 ) 4.0 2.3 1.6 volume=0.253 peak=4159 ppm1=1.473 ppm2=6.747 assign ( resid 56 and name HN ) ( resid 54 and name HN ) 3.6 1.9 1.4 volume=0.488 peak=1180 ppm1=8.641 ppm2=9.076 assign ( resid 119 and name HN ) ( resid 118 and name HD2 or resid 118 and name HD1 ) 3.0 1.2 1.2 volume=1.599 peak=1177 ppm1=8.055 ppm2=1.348 assign ( resid 142 and name HA ) ( resid 143 and name HN ) 4.1 2.4 1.6 volume=0.222 peak=5013 ppm1=4.138 ppm2=6.887 assign ( resid 33 and name HN ) ( resid 33 and name HB ) 3.4 1.7 1.4 volume=0.668 peak=766 ppm1=8.163 ppm2=2.836 assign ( resid 186 and name HB2 ) ( resid 184 and name HA ) 4.2 2.4 1.7 volume=0.205 peak=2809 ppm1=1.903 ppm2=3.632 assign ( resid 115 and name HB ) ( resid 115 and name HG2# ) 3.8 2.1 1.5 volume=0.334 peak=3363 ppm1=0.232 ppm2=0.651 assign ( resid 212 and name HN ) ( resid 212 and name HA ) 3.5 1.8 1.4 volume=0.590 peak=2015 ppm1=8.243 ppm2=4.134 assign ( resid 201 and name HN ) ( resid 198 and name HA ) 3.0 1.3 1.2 volume=1.441 peak=363 ppm1=7.402 ppm2=4.532 assign ( resid 186 and name HN ) ( resid 184 and name HN ) 2.8 1.0 1.1 volume=2.378 peak=689 ppm1=7.369 ppm2=7.525 assign ( resid 204 and name HA ) ( resid 208 and name HN ) 4.3 2.6 1.7 volume=0.172 peak=3278 ppm1=3.800 ppm2=8.059 assign ( resid 135 and name HA ) ( resid 135 and name HG1 ) 3.8 2.1 1.5 volume=0.347 peak=4956 ppm1=4.155 ppm2=1.787 assign ( resid 137 and name HN ) ( resid 137 and name HB2 ) 3.0 1.3 1.2 volume=1.353 peak=268 ppm1=8.050 ppm2=2.577 assign ( resid 8 and name HA ) ( resid 8 and name HN ) 3.5 1.8 1.4 volume=0.581 peak=4074 ppm1=3.838 ppm2=7.618 assign ( resid 208 and name HB ) ( resid 208 and name HA ) 3.9 2.2 1.6 volume=0.302 peak=4575 ppm1=4.031 ppm2=4.407 assign ( resid 130 and name HG2 ) ( resid 130 and name HB1 ) 3.6 1.9 1.5 volume=0.471 peak=3754 ppm1=1.308 ppm2=1.883 assign ( resid 156 and name HN ) ( resid 155 and name HB2 ) 3.1 1.4 1.3 volume=1.142 peak=413 ppm1=8.551 ppm2=2.577 assign ( resid 115 and name HG1# ) ( resid 93 and name HD1# ) 3.6 1.8 1.4 volume=0.526 peak=3153 ppm1=0.302 ppm2=-0.267 assign ( resid 116 and name HN ) ( resid 129 and name HA ) 3.9 2.2 1.6 volume=0.298 peak=1526 ppm1=8.834 ppm2=5.706 assign ( resid 132 and name HG2# ) ( resid 132 and name HN ) 3.7 2.0 1.5 volume=0.414 peak=5110 ppm1=0.936 ppm2=7.868 assign ( resid 147 and name HB2 ) ( resid 147 and name HN ) 4.0 2.3 1.6 volume=0.264 peak=4325 ppm1=2.704 ppm2=8.789 assign ( resid 99 and name HN ) ( resid 98 and name HN ) 4.2 2.5 1.7 volume=0.193 peak=995 ppm1=7.801 ppm2=9.348 assign ( resid 51 and name HG1 or resid 51 and name HG2 ) ( resid 169 and name HN ) 4.5 2.8 1.5 volume=0.133 peak=4163 ppm1=1.973 ppm2=9.239 assign ( resid 72 and name HN ) ( resid 69 and name HN ) 4.3 2.6 1.7 volume=0.163 peak=1161 ppm1=7.534 ppm2=8.180 assign ( resid 8 and name HB2 or resid 8 and name HB1 ) ( resid 4 and name HB1 or resid 4 and name HB2 ) 2.9 1.2 1.2 volume=1.805 peak=4667 ppm1=2.049 ppm2=1.758 assign ( resid 171 and name HN ) ( resid 49 and name HA ) 3.9 2.1 1.5 volume=0.324 peak=386 ppm1=9.065 ppm2=4.917 assign ( resid 101 and name HB1 ) ( resid 101 and name HA ) 3.3 1.6 1.3 volume=0.810 peak=3596 ppm1=2.989 ppm2=4.731 assign ( resid 199 and name HA ) ( resid 202 and name HA1 ) 4.6 2.9 1.4 volume=0.118 peak=3996 ppm1=2.797 ppm2=3.113 assign ( resid 205 and name HA ) ( resid 204 and name HB1 ) 3.8 2.1 1.5 volume=0.357 peak=2463 ppm1=4.140 ppm2=1.726 assign ( resid 192 and name HG ) ( resid 192 and name HN ) 4.3 2.6 1.7 volume=0.174 peak=4997 ppm1=1.755 ppm2=8.207 assign ( resid 149 and name HN ) ( resid 173 and name HN ) 4.1 2.4 1.7 volume=0.212 peak=165 ppm1=7.759 ppm2=8.566 assign ( resid 120 and name HB2 ) ( resid 123 and name HB2 ) 3.1 1.4 1.2 volume=1.245 peak=3265 ppm1=2.999 ppm2=2.806 assign ( resid 99 and name HN ) ( resid 77 and name HB2 ) 3.5 1.8 1.4 volume=0.585 peak=1166 ppm1=7.801 ppm2=3.876 assign ( resid 208 and name HB ) ( resid 207 and name HD1 or resid 207 and name HD2 ) 4.4 2.6 1.6 volume=0.158 peak=4695 ppm1=4.032 ppm2=3.047 assign ( resid 163 and name HN ) ( resid 162 and name HA ) 3.2 1.5 1.3 volume=1.056 peak=2107 ppm1=7.324 ppm2=3.688 assign ( resid 78 and name HN ) ( resid 77 and name HB1 or resid 77 and name HB2 ) 3.3 1.6 1.3 volume=0.843 peak=773 ppm1=7.147 ppm2=3.887 assign ( resid 35 and name HN ) ( resid 34 and name HG2# ) 3.1 1.4 1.3 volume=1.139 peak=404 ppm1=9.428 ppm2=1.096 assign ( resid 52 and name HN ) ( resid 167 and name HB1 ) 3.1 1.4 1.2 volume=1.230 peak=767 ppm1=8.616 ppm2=1.667 assign ( resid 93 and name HB ) ( resid 93 and name HG12 ) 3.9 2.2 1.6 volume=0.303 peak=4515 ppm1=1.224 ppm2=0.598 assign ( resid 194 and name HN ) ( resid 193 and name HG1# ) 2.5 0.8 1.0 volume=4.266 peak=1993 ppm1=7.774 ppm2=0.748 assign ( resid 4 and name HN ) ( resid 1 and name HG1 or resid 1 and name HG2 ) 3.0 1.3 1.2 volume=1.359 peak=909 ppm1=8.189 ppm2=2.299 assign ( resid 92 and name HN ) ( resid 115 and name HG1# ) 3.2 1.5 1.3 volume=1.033 peak=2115 ppm1=9.456 ppm2=0.237 assign ( resid 86 and name HB2 ) ( resid 86 and name HN ) 3.8 2.1 1.5 volume=0.337 peak=4950 ppm1=1.555 ppm2=8.618 assign ( resid 93 and name HN ) ( resid 84 and name HN ) 4.2 2.5 1.7 volume=0.192 peak=1517 ppm1=8.910 ppm2=8.553 assign ( resid 112 and name HD1# ) ( resid 134 and name HD1 or resid 134 and name HD2 ) 3.7 2.0 1.5 volume=0.428 peak=2536 ppm1=0.372 ppm2=6.873 assign ( resid 82 and name HA ) ( resid 82 and name HB2 ) 3.8 2.1 1.5 volume=0.366 peak=4160 ppm1=5.042 ppm2=2.450 assign ( resid 19 and name HN ) ( resid 19 and name HA ) 3.0 1.3 1.2 volume=1.435 peak=1113 ppm1=7.479 ppm2=4.140 assign ( resid 96 and name HG2# ) ( resid 95 and name HN ) 5.0 3.3 1.0 volume=0.066 peak=5149 ppm1=1.144 ppm2=9.108 assign ( resid 100 and name HN ) ( resid 101 and name HA ) 3.6 1.9 1.4 volume=0.515 peak=2034 ppm1=8.395 ppm2=4.679 assign ( resid 203 and name HG2# ) ( resid 203 and name HN ) 3.2 1.5 1.3 volume=1.022 peak=4454 ppm1=0.339 ppm2=7.682 assign ( resid 42 and name HB2 or resid 42 and name HB1 ) ( resid 42 and name HD2 or resid 42 and name HD1 ) 2.4 0.7 1.0 volume=5.158 peak=3029 ppm1=1.666 ppm2=1.531 assign ( resid 59 and name HN ) ( resid 57 and name HA ) 4.1 2.3 1.6 volume=0.241 peak=2200 ppm1=8.092 ppm2=4.134 assign ( resid 132 and name HG2# ) ( resid 3 and name HE1 or resid 3 and name HE2 ) 3.6 1.9 1.4 volume=0.493 peak=4887 ppm1=0.936 ppm2=7.221 assign ( resid 56 and name HN ) ( resid 56 and name HA ) 3.2 1.5 1.3 volume=0.986 peak=823 ppm1=8.637 ppm2=4.535 assign ( resid 87 and name HD1# ) ( resid 93 and name HD1# ) 3.1 1.4 1.2 volume=1.230 peak=5107 ppm1=0.440 ppm2=-0.268 assign ( resid 128 and name HN ) ( resid 152 and name HA2 ) 3.6 1.9 1.4 volume=0.476 peak=1318 ppm1=9.933 ppm2=3.879 assign ( resid 187 and name HG2# ) ( resid 189 and name HD2 ) 4.1 2.4 1.7 volume=0.215 peak=3227 ppm1=1.057 ppm2=3.490 assign ( resid 137 and name HB1 ) ( resid 137 and name HA ) 4.1 2.4 1.6 volume=0.234 peak=3527 ppm1=2.809 ppm2=4.507 assign ( resid 63 and name HN ) ( resid 61 and name HB2 ) 3.1 1.4 1.2 volume=1.259 peak=2323 ppm1=7.298 ppm2=1.664 assign ( resid 157 and name HG1 ) ( resid 123 and name HB2 ) 3.9 2.2 1.6 volume=0.284 peak=2780 ppm1=1.790 ppm2=2.772 assign ( resid 176 and name HA ) ( resid 176 and name HB1 ) 3.0 1.3 1.2 volume=1.403 peak=2819 ppm1=3.998 ppm2=1.872 assign ( resid 87 and name HG11 ) ( resid 87 and name HG12 ) 3.1 1.4 1.2 volume=1.218 peak=3693 ppm1=1.264 ppm2=1.050 assign ( resid 67 and name HN ) ( resid 66 and name HA ) 3.1 1.4 1.2 volume=1.222 peak=1862 ppm1=7.603 ppm2=4.266 assign ( resid 210 and name HB1 ) ( resid 210 and name HA ) 3.0 1.3 1.2 volume=1.557 peak=5001 ppm1=3.759 ppm2=4.268 assign ( resid 130 and name HN ) ( resid 131 and name HA ) 3.2 1.5 1.3 volume=0.941 peak=1467 ppm1=7.615 ppm2=4.472 assign ( resid 157 and name HB1 ) ( resid 157 and name HD1 ) 3.9 2.2 1.6 volume=0.287 peak=3123 ppm1=2.309 ppm2=3.631 assign ( resid 158 and name HB2 ) ( resid 158 and name HN ) 4.6 2.8 1.4 volume=0.118 peak=3814 ppm1=2.217 ppm2=8.209 assign ( resid 203 and name HG2# ) ( resid 204 and name HN ) 3.3 1.6 1.3 volume=0.781 peak=4482 ppm1=0.340 ppm2=6.763 assign ( resid 5 and name HB# ) ( resid 6 and name HG11 or resid 6 and name HG12 ) 3.1 1.3 1.2 volume=1.320 peak=3761 ppm1=1.342 ppm2=1.045 assign ( resid 204 and name HG1 ) ( resid 204 and name HN ) 3.5 1.8 1.4 volume=0.544 peak=4801 ppm1=1.432 ppm2=6.737 assign ( resid 47 and name HN ) ( resid 38 and name HG2 ) 4.3 2.5 1.7 volume=0.178 peak=1207 ppm1=8.701 ppm2=0.481 assign ( resid 198 and name HB2 ) ( resid 199 and name HA ) 4.2 2.5 1.7 volume=0.184 peak=2731 ppm1=3.086 ppm2=2.727 assign ( resid 8 and name HN ) ( resid 9 and name HN ) 2.7 0.9 1.1 volume=2.996 peak=529 ppm1=7.615 ppm2=7.989 assign ( resid 36 and name HB1 ) ( resid 24 and name HE1 ) 4.2 2.5 1.7 volume=0.199 peak=4337 ppm1=3.859 ppm2=7.001 assign ( resid 84 and name HN ) ( resid 95 and name HB2 ) 3.6 1.9 1.4 volume=0.492 peak=2071 ppm1=8.504 ppm2=2.578 assign ( resid 139 and name HG1 ) ( resid 145 and name HB2 ) 2.6 0.9 1.0 volume=3.510 peak=3401 ppm1=1.803 ppm2=1.931 assign ( resid 186 and name HA ) ( resid 188 and name HN ) 4.3 2.6 1.7 volume=0.165 peak=3956 ppm1=4.211 ppm2=8.440 assign ( resid 7 and name HB# ) ( resid 8 and name HG1 ) 3.5 1.8 1.4 volume=0.544 peak=2983 ppm1=0.752 ppm2=2.333 assign ( resid 144 and name HG2# ) ( resid 177 and name HA2 ) 3.9 2.1 1.5 volume=0.323 peak=3674 ppm1=0.766 ppm2=3.720 assign ( resid 167 and name HN ) ( resid 53 and name HN ) 4.3 2.6 1.7 volume=0.167 peak=1248 ppm1=8.642 ppm2=8.310 assign ( resid 123 and name HN ) ( resid 124 and name HN ) 2.9 1.2 1.2 volume=1.805 peak=623 ppm1=8.404 ppm2=6.484 assign ( resid 184 and name HB ) ( resid 183 and name HB ) 2.9 1.2 1.2 volume=1.768 peak=2837 ppm1=2.046 ppm2=1.953 assign ( resid 128 and name HN ) ( resid 116 and name HB2 or resid 116 and name HB1 ) 3.8 2.1 1.5 volume=0.363 peak=1193 ppm1=9.933 ppm2=2.841 assign ( resid 204 and name HN ) ( resid 203 and name HN ) 3.2 1.5 1.3 volume=0.985 peak=714 ppm1=6.746 ppm2=7.665 assign ( resid 120 and name HB1 ) ( resid 15 and name HD1# ) 4.0 2.3 1.6 volume=0.262 peak=4630 ppm1=2.999 ppm2=0.434 assign ( resid 9 and name HN ) ( resid 8 and name HA ) 3.0 1.3 1.2 volume=1.403 peak=977 ppm1=7.983 ppm2=3.838 assign ( resid 88 and name HN ) ( resid 87 and name HG12 ) 3.0 1.3 1.2 volume=1.468 peak=2319 ppm1=8.595 ppm2=1.050 assign ( resid 136 and name HB1 ) ( resid 136 and name HB2 ) 2.7 1.0 1.1 volume=2.945 peak=2670 ppm1=1.746 ppm2=1.905 assign ( resid 198 and name HN ) ( resid 194 and name HA ) 3.5 1.8 1.4 volume=0.548 peak=175 ppm1=8.716 ppm2=4.318 assign ( resid 74 and name HD1 ) ( resid 73 and name HG2# ) 3.7 2.0 1.5 volume=0.397 peak=27 ppm1=6.939 ppm2=1.208 assign ( resid 97 and name HN ) ( resid 97 and name HD1# ) 3.5 1.8 1.4 volume=0.576 peak=1640 ppm1=8.363 ppm2=0.101 assign ( resid 127 and name HD1# ) ( resid 153 and name HB2 ) 3.9 2.2 1.6 volume=0.286 peak=3878 ppm1=0.285 ppm2=2.891 assign ( resid 115 and name HN ) ( resid 92 and name HN ) 3.7 2.0 1.5 volume=0.393 peak=1388 ppm1=9.054 ppm2=9.480 assign ( resid 165 and name HN ) ( resid 55 and name HD1 ) 3.5 1.8 1.4 volume=0.602 peak=622 ppm1=8.464 ppm2=3.360 assign ( resid 99 and name HN ) ( resid 98 and name HA ) 2.8 1.1 1.1 volume=2.154 peak=1638 ppm1=7.801 ppm2=4.655 assign ( resid 153 and name HN ) ( resid 128 and name HN ) 3.8 2.1 1.5 volume=0.331 peak=1637 ppm1=9.328 ppm2=9.938 assign ( resid 164 and name HN ) ( resid 163 and name HA ) 2.9 1.2 1.2 volume=1.692 peak=289 ppm1=7.978 ppm2=4.139 assign ( resid 8 and name HA ) ( resid 9 and name HN ) 3.7 2.0 1.5 volume=0.405 peak=2591 ppm1=3.838 ppm2=8.000 assign ( resid 41 and name HB1 or resid 41 and name HB2 ) ( resid 41 and name HG2 or resid 41 and name HG1 ) 2.7 1.0 1.1 volume=2.615 peak=3965 ppm1=1.980 ppm2=1.548 assign ( resid 2 and name HB2 ) ( resid 5 and name HB# ) 3.4 1.7 1.4 volume=0.669 peak=3935 ppm1=2.827 ppm2=1.355 assign ( resid 197 and name HD1# ) ( resid 197 and name HN ) 3.4 1.7 1.4 volume=0.658 peak=4310 ppm1=0.756 ppm2=7.986 assign ( resid 115 and name HG2# ) ( resid 116 and name HA ) 4.3 2.6 1.7 volume=0.162 peak=5114 ppm1=0.658 ppm2=6.176 assign ( resid 192 and name HN ) ( resid 193 and name HA ) 3.9 2.2 1.6 volume=0.301 peak=1889 ppm1=8.209 ppm2=3.482 assign ( resid 154 and name HN ) ( resid 170 and name HN ) 3.9 2.2 1.6 volume=0.307 peak=1624 ppm1=10.006 ppm2=9.148 assign ( resid 147 and name HD1 or resid 147 and name HD2 ) ( resid 147 and name HN ) 3.9 2.2 1.5 volume=0.319 peak=118 ppm1=6.221 ppm2=8.794 assign ( resid 145 and name HN ) ( resid 139 and name HA ) 3.8 2.0 1.5 volume=0.382 peak=2416 ppm1=8.381 ppm2=4.270 assign ( resid 144 and name HA ) ( resid 144 and name HG11 ) 4.2 2.5 1.7 volume=0.203 peak=4649 ppm1=3.987 ppm2=1.211 assign ( resid 204 and name HN ) ( resid 204 and name HG1 ) 2.7 1.0 1.1 volume=2.606 peak=1986 ppm1=6.743 ppm2=1.359 assign ( resid 24 and name HN ) ( resid 22 and name HN ) 3.5 1.8 1.4 volume=0.549 peak=1126 ppm1=7.826 ppm2=8.167 assign ( resid 184 and name HA ) ( resid 179 and name HD2# ) 2.9 1.2 1.1 volume=1.906 peak=3725 ppm1=3.629 ppm2=0.772 assign ( resid 93 and name HN ) ( resid 92 and name HN ) 4.1 2.4 1.7 volume=0.211 peak=484 ppm1=8.908 ppm2=9.470 assign ( resid 124 and name HG2 ) ( resid 124 and name HB1 ) 2.9 1.1 1.1 volume=1.978 peak=3226 ppm1=2.386 ppm2=2.043 assign ( resid 199 and name HA ) ( resid 201 and name HN ) 4.4 2.6 1.6 volume=0.154 peak=2558 ppm1=2.796 ppm2=7.478 assign ( resid 56 and name HN ) ( resid 53 and name HG2# ) 3.1 1.4 1.2 volume=1.279 peak=361 ppm1=8.639 ppm2=0.881 assign ( resid 207 and name HA ) ( resid 207 and name HG2 ) 2.6 0.9 1.0 volume=3.358 peak=3340 ppm1=4.168 ppm2=1.466 assign ( resid 134 and name HE1 or resid 134 and name HE2 ) ( resid 137 and name HN ) 3.2 1.5 1.3 volume=0.979 peak=79 ppm1=7.141 ppm2=8.054 assign ( resid 18 and name HN ) ( resid 17 and name HA ) 2.9 1.2 1.2 volume=1.713 peak=2330 ppm1=7.761 ppm2=4.655 assign ( resid 26 and name HN ) ( resid 25 and name HB1 ) 3.0 1.3 1.2 volume=1.334 peak=641 ppm1=8.862 ppm2=1.740 assign ( resid 184 and name HD1# ) ( resid 183 and name HG11 ) 2.7 1.0 1.1 volume=2.665 peak=4411 ppm1=0.892 ppm2=1.254 assign ( resid 185 and name HA ) ( resid 187 and name HN ) 3.6 1.9 1.5 volume=0.461 peak=4941 ppm1=3.893 ppm2=7.602 assign ( resid 50 and name HN ) ( resid 50 and name HB ) 3.3 1.5 1.3 volume=0.896 peak=1472 ppm1=9.300 ppm2=1.791 assign ( resid 124 and name HA ) ( resid 124 and name HB2 ) 4.2 2.5 1.7 volume=0.194 peak=4103 ppm1=5.180 ppm2=1.983 assign ( resid 114 and name HN ) ( resid 132 and name HA ) 3.4 1.7 1.4 volume=0.640 peak=1801 ppm1=8.799 ppm2=4.664 assign ( resid 29 and name HN ) ( resid 30 and name HN ) 3.9 2.2 1.6 volume=0.314 peak=1658 ppm1=8.568 ppm2=8.723 assign ( resid 115 and name HG1# ) ( resid 92 and name HE1 or resid 92 and name HE2 ) 3.7 1.9 1.5 volume=0.447 peak=3416 ppm1=0.301 ppm2=6.751 assign ( resid 196 and name HG2# ) ( resid 196 and name HG11 ) 2.9 1.2 1.2 volume=1.755 peak=4271 ppm1=0.812 ppm2=1.809 assign ( resid 134 and name HZ ) ( resid 93 and name HG2# ) 3.4 1.6 1.3 volume=0.748 peak=12 ppm1=6.643 ppm2=-0.013 assign ( resid 205 and name HN ) ( resid 204 and name HN ) 2.8 1.1 1.1 volume=2.128 peak=2409 ppm1=7.186 ppm2=6.741 assign ( resid 167 and name HB2 ) ( resid 54 and name HG11 ) 3.6 1.9 1.4 volume=0.507 peak=3435 ppm1=1.680 ppm2=1.161 assign ( resid 81 and name HN ) ( resid 72 and name HG12 ) 3.4 1.6 1.3 volume=0.745 peak=1686 ppm1=8.510 ppm2=1.006 assign ( resid 6 and name HA ) ( resid 6 and name HG12 ) 3.1 1.3 1.2 volume=1.330 peak=4772 ppm1=3.617 ppm2=1.091 assign ( resid 5 and name HA ) ( resid 4 and name HB2 ) 4.2 2.4 1.7 volume=0.205 peak=3178 ppm1=4.025 ppm2=1.748 assign ( resid 84 and name HN ) ( resid 94 and name HA ) 3.2 1.5 1.3 volume=0.965 peak=1936 ppm1=8.504 ppm2=5.047 assign ( resid 136 and name HB1 ) ( resid 137 and name HN ) 3.6 1.9 1.4 volume=0.481 peak=3877 ppm1=1.750 ppm2=8.050 assign ( resid 74 and name HD1 ) ( resid 202 and name HA2 ) 3.5 1.8 1.4 volume=0.598 peak=49 ppm1=6.939 ppm2=3.337 assign ( resid 136 and name HN ) ( resid 134 and name HZ ) 3.2 1.4 1.3 volume=1.072 peak=1152 ppm1=6.891 ppm2=6.641 assign ( resid 26 and name HG2# ) ( resid 26 and name HN ) 3.1 1.3 1.2 volume=1.328 peak=5088 ppm1=0.913 ppm2=8.858 assign ( resid 96 and name HG2# ) ( resid 79 and name HB2 ) 3.6 1.9 1.4 volume=0.478 peak=3507 ppm1=1.143 ppm2=1.776 assign ( resid 47 and name HN ) ( resid 40 and name HB2 ) 3.6 1.8 1.4 volume=0.521 peak=1147 ppm1=8.698 ppm2=3.305 assign ( resid 47 and name HN ) ( resid 46 and name HA ) 3.3 1.6 1.3 volume=0.844 peak=1395 ppm1=8.699 ppm2=4.932 assign ( resid 186 and name HG1 ) ( resid 183 and name HD1# ) 3.4 1.7 1.4 volume=0.671 peak=2853 ppm1=1.478 ppm2=0.877 assign ( resid 134 and name HN ) ( resid 137 and name HN ) 3.5 1.8 1.4 volume=0.605 peak=1974 ppm1=8.747 ppm2=8.061 assign ( resid 66 and name HN ) ( resid 66 and name HD1 or resid 66 and name HD2 ) 3.2 1.5 1.3 volume=0.986 peak=1562 ppm1=8.053 ppm2=6.998 assign ( resid 186 and name HB2 ) ( resid 106 and name HD1# ) 3.5 1.8 1.4 volume=0.597 peak=4295 ppm1=1.902 ppm2=0.776 assign ( resid 29 and name HN ) ( resid 28 and name HD2 ) 3.2 1.5 1.3 volume=0.977 peak=241 ppm1=8.565 ppm2=1.408 assign ( resid 68 and name HN ) ( resid 71 and name HD2 ) 3.5 1.8 1.4 volume=0.584 peak=598 ppm1=8.026 ppm2=2.727 assign ( resid 173 and name HG2# ) ( resid 173 and name HN ) 3.6 1.9 1.4 volume=0.476 peak=2889 ppm1=1.033 ppm2=8.529 assign ( resid 112 and name HD1# ) ( resid 112 and name HG12 ) 4.1 2.3 1.6 volume=0.240 peak=2921 ppm1=0.373 ppm2=1.248 assign ( resid 91 and name HG2# ) ( resid 93 and name HD1# ) 4.0 2.3 1.6 volume=0.269 peak=3816 ppm1=1.019 ppm2=-0.273 assign ( resid 79 and name HB2 ) ( resid 80 and name HN ) 3.4 1.6 1.3 volume=0.736 peak=2759 ppm1=1.779 ppm2=7.516 assign ( resid 129 and name HB1 ) ( resid 114 and name HN ) 4.2 2.5 1.7 volume=0.202 peak=3374 ppm1=3.365 ppm2=8.814 assign ( resid 136 and name HN ) ( resid 135 and name HA ) 3.1 1.3 1.2 volume=1.325 peak=1461 ppm1=6.891 ppm2=4.133 assign ( resid 116 and name HN ) ( resid 115 and name HA ) 3.1 1.4 1.3 volume=1.142 peak=418 ppm1=8.834 ppm2=4.402 assign ( resid 177 and name HN ) ( resid 177 and name HA2 ) 3.1 1.4 1.2 volume=1.193 peak=1582 ppm1=8.463 ppm2=3.747 assign ( resid 77 and name HN ) ( resid 76 and name HA ) 3.3 1.6 1.3 volume=0.876 peak=441 ppm1=8.057 ppm2=4.106 assign ( resid 24 and name HD1 ) ( resid 24 and name HB2 or resid 24 and name HB1 ) 3.4 1.7 1.4 volume=0.697 peak=96 ppm1=6.801 ppm2=3.008 assign ( resid 36 and name HA ) ( resid 27 and name HG1# ) 3.9 2.2 1.6 volume=0.306 peak=4490 ppm1=5.852 ppm2=0.905 assign ( resid 178 and name HA ) ( resid 178 and name HG2 ) 3.2 1.5 1.3 volume=0.977 peak=3775 ppm1=4.274 ppm2=1.292 assign ( resid 92 and name HE1 or resid 92 and name HE2 ) ( resid 92 and name HB1 or resid 92 and name HB2 ) 3.4 1.7 1.4 volume=0.652 peak=115 ppm1=6.749 ppm2=3.100 assign ( resid 98 and name HG2# ) ( resid 97 and name HG2# ) 4.9 3.1 1.1 volume=0.082 peak=4774 ppm1=1.326 ppm2=0.231 assign ( resid 24 and name HN ) ( resid 24 and name HE1 ) 3.5 1.8 1.4 volume=0.575 peak=1716 ppm1=7.839 ppm2=10.129 assign ( resid 132 and name HG1# ) ( resid 112 and name HG2# ) 2.6 0.8 1.0 volume=3.869 peak=4507 ppm1=0.544 ppm2=0.709 assign ( resid 115 and name HN ) ( resid 129 and name HA ) 4.2 2.5 1.7 volume=0.199 peak=293 ppm1=9.052 ppm2=5.708 assign ( resid 75 and name HN ) ( resid 74 and name HE1 ) 4.2 2.5 1.7 volume=0.186 peak=2383 ppm1=7.485 ppm2=9.625 assign ( resid 44 and name HN ) ( resid 44 and name HA ) 4.3 2.6 1.7 volume=0.171 peak=917 ppm1=8.374 ppm2=4.655 assign ( resid 65 and name HN ) ( resid 64 and name HZ ) 3.2 1.5 1.3 volume=1.019 peak=1744 ppm1=7.742 ppm2=7.052 assign ( resid 10 and name HG2# ) ( resid 129 and name HN ) 3.3 1.6 1.3 volume=0.864 peak=5067 ppm1=1.084 ppm2=8.712 assign ( resid 195 and name HN ) ( resid 192 and name HN ) 3.2 1.5 1.3 volume=1.033 peak=2396 ppm1=7.971 ppm2=8.178 assign ( resid 15 and name HN ) ( resid 14 and name HN ) 2.4 0.7 1.0 volume=5.815 peak=1432 ppm1=7.809 ppm2=7.786 assign ( resid 6 and name HA ) ( resid 6 and name HN ) 3.9 2.2 1.6 volume=0.288 peak=4268 ppm1=3.616 ppm2=7.726 assign ( resid 153 and name HB2 ) ( resid 65 and name HD1# ) 3.8 2.1 1.5 volume=0.373 peak=3098 ppm1=2.853 ppm2=0.178 assign ( resid 21 and name HN ) ( resid 22 and name HA ) 4.1 2.4 1.6 volume=0.221 peak=1865 ppm1=8.287 ppm2=4.837 assign ( resid 183 and name HB ) ( resid 183 and name HN ) 3.4 1.6 1.3 volume=0.749 peak=4053 ppm1=1.976 ppm2=7.484 assign ( resid 102 and name HB# ) ( resid 179 and name HB1 ) 4.3 2.5 1.7 volume=0.180 peak=4030 ppm1=1.280 ppm2=2.795 assign ( resid 190 and name HN ) ( resid 190 and name HA ) 3.2 1.5 1.3 volume=0.935 peak=1476 ppm1=7.518 ppm2=3.966 assign ( resid 62 and name HN ) ( resid 61 and name HB2 ) 3.1 1.4 1.2 volume=1.159 peak=1669 ppm1=8.133 ppm2=1.634 assign ( resid 75 and name HN ) ( resid 72 and name HA ) 3.2 1.5 1.3 volume=0.915 peak=936 ppm1=7.479 ppm2=3.614 assign ( resid 51 and name HA ) ( resid 168 and name HG1# ) 3.9 2.2 1.6 volume=0.283 peak=2689 ppm1=5.619 ppm2=0.770 assign ( resid 126 and name HN ) ( resid 118 and name HA ) 3.8 2.1 1.5 volume=0.371 peak=2179 ppm1=9.104 ppm2=3.762 assign ( resid 84 and name HN ) ( resid 134 and name HZ ) 3.7 1.9 1.5 volume=0.446 peak=1803 ppm1=8.502 ppm2=6.643 assign ( resid 115 and name HA ) ( resid 115 and name HB ) 4.5 2.8 1.5 volume=0.126 peak=3888 ppm1=4.398 ppm2=0.236 assign ( resid 77 and name HN ) ( resid 78 and name HD2# ) 3.7 1.9 1.5 volume=0.445 peak=1485 ppm1=8.057 ppm2=0.501 assign ( resid 76 and name HE2 ) ( resid 76 and name HB2 ) 2.9 1.2 1.2 volume=1.803 peak=4125 ppm1=2.912 ppm2=1.987 assign ( resid 114 and name HD1# ) ( resid 93 and name HG11 ) 2.5 0.8 1.0 volume=4.035 peak=2816 ppm1=0.534 ppm2=0.699 assign ( resid 6 and name HN ) ( resid 6 and name HA ) 3.1 1.4 1.2 volume=1.238 peak=1592 ppm1=7.722 ppm2=3.611 assign ( resid 91 and name HB ) ( resid 87 and name HG2# ) 4.2 2.5 1.7 volume=0.200 peak=2976 ppm1=3.642 ppm2=0.838 assign ( resid 87 and name HN ) ( resid 87 and name HD1# ) 3.8 2.1 1.5 volume=0.358 peak=1258 ppm1=8.039 ppm2=0.448 assign ( resid 66 and name HN ) ( resid 62 and name HA ) 3.4 1.7 1.4 volume=0.646 peak=324 ppm1=8.050 ppm2=3.975 assign ( resid 114 and name HA ) ( resid 114 and name HD2# ) 4.4 2.7 1.6 volume=0.145 peak=3720 ppm1=4.461 ppm2=0.782 assign ( resid 65 and name HN ) ( resid 64 and name HE1 or resid 64 and name HE2 ) 3.3 1.6 1.3 volume=0.840 peak=726 ppm1=7.738 ppm2=6.487 assign ( resid 72 and name HN ) ( resid 68 and name HA ) 4.5 2.8 1.5 volume=0.133 peak=1359 ppm1=7.538 ppm2=4.269 assign ( resid 155 and name HB2 ) ( resid 156 and name HN ) 4.3 2.6 1.7 volume=0.173 peak=4344 ppm1=2.574 ppm2=8.568 assign ( resid 158 and name HB1 ) ( resid 158 and name HA ) 4.1 2.3 1.6 volume=0.240 peak=4963 ppm1=2.216 ppm2=4.148 assign ( resid 96 and name HN ) ( resid 95 and name HB1 ) 3.9 2.2 1.6 volume=0.298 peak=921 ppm1=8.473 ppm2=2.563 assign ( resid 14 and name HG2# ) ( resid 14 and name HA ) 2.4 0.7 1.0 volume=5.360 peak=4718 ppm1=0.757 ppm2=2.817 assign ( resid 24 and name HN ) ( resid 38 and name HB2 ) 3.5 1.8 1.4 volume=0.572 peak=2061 ppm1=7.835 ppm2=1.409 assign ( resid 132 and name HN ) ( resid 114 and name HB1 ) 3.9 2.1 1.5 volume=0.325 peak=1547 ppm1=7.893 ppm2=1.050 assign ( resid 167 and name HN ) ( resid 53 and name HG12 ) 3.2 1.5 1.3 volume=1.019 peak=2123 ppm1=8.642 ppm2=1.392 assign ( resid 144 and name HA ) ( resid 144 and name HD1# ) 3.2 1.5 1.3 volume=1.014 peak=3640 ppm1=3.988 ppm2=0.620 assign ( resid 93 and name HN ) ( resid 92 and name HA ) 3.4 1.7 1.4 volume=0.726 peak=1766 ppm1=8.906 ppm2=4.922 assign ( resid 5 and name HB# ) ( resid 7 and name HN ) 3.8 2.1 1.5 volume=0.344 peak=4996 ppm1=1.341 ppm2=8.454 assign ( resid 199 and name HN ) ( resid 200 and name HN ) 3.1 1.4 1.3 volume=1.125 peak=1939 ppm1=8.633 ppm2=8.045 assign ( resid 168 and name HN ) ( resid 154 and name HG2# ) 2.9 1.1 1.1 volume=1.995 peak=560 ppm1=8.695 ppm2=0.876 assign ( resid 112 and name HD1# ) ( resid 112 and name HN ) 4.0 2.2 1.6 volume=0.277 peak=3850 ppm1=0.371 ppm2=8.134 assign ( resid 164 and name HB1 ) ( resid 53 and name HG2# ) 3.8 2.1 1.5 volume=0.364 peak=2654 ppm1=2.999 ppm2=0.898 assign ( resid 15 and name HN ) ( resid 15 and name HG ) 2.9 1.2 1.2 volume=1.804 peak=2398 ppm1=7.812 ppm2=1.271 assign ( resid 67 and name HA ) ( resid 69 and name HN ) 3.9 2.1 1.5 volume=0.325 peak=3598 ppm1=3.941 ppm2=8.195 assign ( resid 132 and name HG2# ) ( resid 130 and name HE2 or resid 130 and name HE1 ) 3.6 1.8 1.4 volume=0.526 peak=2979 ppm1=0.938 ppm2=2.853 assign ( resid 144 and name HA ) ( resid 144 and name HG2# ) 3.4 1.7 1.4 volume=0.670 peak=4070 ppm1=3.984 ppm2=0.756 assign ( resid 154 and name HG2# ) ( resid 154 and name HA ) 3.1 1.4 1.2 volume=1.189 peak=3176 ppm1=0.835 ppm2=4.672 assign ( resid 93 and name HN ) ( resid 114 and name HD1# ) 3.3 1.6 1.3 volume=0.768 peak=810 ppm1=8.904 ppm2=0.535 assign ( resid 135 and name HB2 ) ( resid 135 and name HD2 ) 4.0 2.3 1.6 volume=0.259 peak=2624 ppm1=2.193 ppm2=3.220 assign ( resid 126 and name HN ) ( resid 125 and name HA ) 3.1 1.3 1.2 volume=1.299 peak=2343 ppm1=9.105 ppm2=5.571 assign ( resid 149 and name HN ) ( resid 172 and name HB1 ) 4.0 2.3 1.6 volume=0.261 peak=375 ppm1=7.757 ppm2=1.786 assign ( resid 192 and name HD1# ) ( resid 50 and name HG1# ) 2.9 1.2 1.2 volume=1.868 peak=3508 ppm1=0.491 ppm2=0.662 assign ( resid 139 and name HA ) ( resid 139 and name HG1 ) 3.0 1.3 1.2 volume=1.523 peak=4724 ppm1=4.305 ppm2=1.806 assign ( resid 98 and name HN ) ( resid 97 and name HA ) 3.2 1.5 1.3 volume=0.939 peak=1142 ppm1=9.353 ppm2=4.531 assign ( resid 87 and name HG12 ) ( resid 87 and name HD1# ) 3.2 1.5 1.3 volume=0.972 peak=4758 ppm1=1.049 ppm2=0.442 assign ( resid 91 and name HN ) ( resid 92 and name HA ) 3.2 1.5 1.3 volume=0.957 peak=309 ppm1=7.218 ppm2=4.923 assign ( resid 97 and name HG2# ) ( resid 110 and name HN ) 4.4 2.6 1.6 volume=0.156 peak=4081 ppm1=0.216 ppm2=8.710 assign ( resid 199 and name HB# ) ( resid 196 and name HB ) 3.6 1.9 1.5 volume=0.471 peak=2874 ppm1=0.692 ppm2=2.220 assign ( resid 71 and name HB1 ) ( resid 78 and name HG ) 4.3 2.6 1.7 volume=0.173 peak=4882 ppm1=1.527 ppm2=1.229 assign ( resid 6 and name HD1# ) ( resid 5 and name HA ) 3.6 1.9 1.4 volume=0.477 peak=3151 ppm1=0.791 ppm2=4.033 assign ( resid 112 and name HG2# ) ( resid 112 and name HA ) 4.3 2.6 1.7 volume=0.174 peak=3422 ppm1=0.681 ppm2=4.976 assign ( resid 169 and name HA ) ( resid 153 and name HB2 ) 4.7 3.0 1.3 volume=0.094 peak=4518 ppm1=5.239 ppm2=2.847 assign ( resid 173 and name HA ) ( resid 173 and name HG2# ) 3.8 2.1 1.5 volume=0.366 peak=2694 ppm1=3.612 ppm2=1.027 assign ( resid 8 and name HN ) ( resid 4 and name HG1 or resid 4 and name HG2 ) 3.2 1.5 1.3 volume=0.919 peak=1266 ppm1=7.611 ppm2=1.397 assign ( resid 8 and name HN ) ( resid 8 and name HG1 ) 2.6 0.9 1.1 volume=3.161 peak=473 ppm1=7.610 ppm2=2.310 assign ( resid 156 and name HN ) ( resid 155 and name HA ) 2.7 1.0 1.1 volume=2.933 peak=1289 ppm1=8.551 ppm2=5.247 assign ( resid 199 and name HA ) ( resid 202 and name HA2 ) 4.3 2.6 1.7 volume=0.160 peak=4210 ppm1=2.797 ppm2=3.381 assign ( resid 199 and name HN ) ( resid 198 and name HB2 ) 3.3 1.5 1.3 volume=0.878 peak=1491 ppm1=8.633 ppm2=3.098 assign ( resid 132 and name HG1# ) ( resid 112 and name HG2# ) 2.2 0.5 0.9 volume=9.762 peak=3275 ppm1=0.543 ppm2=0.576 assign ( resid 80 and name HN ) ( resid 78 and name HD2# ) 3.0 1.3 1.2 volume=1.334 peak=2371 ppm1=7.524 ppm2=0.490 assign ( resid 203 and name HD1# ) ( resid 206 and name HB1 ) 3.3 1.6 1.3 volume=0.806 peak=4540 ppm1=-0.010 ppm2=2.944 assign ( resid 97 and name HN ) ( resid 80 and name HA ) 3.8 2.0 1.5 volume=0.378 peak=2102 ppm1=8.363 ppm2=4.014 assign ( resid 199 and name HB# ) ( resid 54 and name HD1# ) 2.8 1.1 1.1 volume=2.293 peak=2578 ppm1=0.692 ppm2=0.502 assign ( resid 136 and name HN ) ( resid 134 and name HE1 or resid 134 and name HE2 ) 3.1 1.4 1.2 volume=1.179 peak=670 ppm1=6.898 ppm2=7.137 assign ( resid 136 and name HN ) ( resid 136 and name HB2 or resid 136 and name HB1 ) 2.6 0.9 1.1 volume=3.242 peak=2132 ppm1=6.891 ppm2=1.790 assign ( resid 176 and name HN ) ( resid 174 and name HA ) 3.5 1.7 1.4 volume=0.622 peak=486 ppm1=8.404 ppm2=4.516 assign ( resid 11 and name HB# ) ( resid 11 and name HN ) 3.2 1.5 1.3 volume=0.944 peak=3636 ppm1=1.631 ppm2=8.185 assign ( resid 200 and name HG2 ) ( resid 200 and name HN ) 4.5 2.8 1.5 volume=0.127 peak=4914 ppm1=1.132 ppm2=8.090 assign ( resid 15 and name HN ) ( resid 14 and name HA ) 3.2 1.5 1.3 volume=1.054 peak=1966 ppm1=7.810 ppm2=2.817 assign ( resid 126 and name HD1# ) ( resid 126 and name HN ) 4.6 2.8 1.4 volume=0.120 peak=2992 ppm1=0.348 ppm2=9.103 assign ( resid 87 and name HB ) ( resid 87 and name HG12 ) 4.0 2.3 1.6 volume=0.253 peak=3684 ppm1=1.369 ppm2=1.046 assign ( resid 188 and name HN ) ( resid 189 and name HG2 ) 3.3 1.5 1.3 volume=0.882 peak=2268 ppm1=8.442 ppm2=1.766 assign ( resid 159 and name HA ) ( resid 161 and name HN ) 2.8 1.0 1.1 volume=2.397 peak=4270 ppm1=3.773 ppm2=6.934 assign ( resid 185 and name HN ) ( resid 185 and name HB2 ) 2.9 1.2 1.2 volume=1.797 peak=1576 ppm1=8.184 ppm2=2.150 assign ( resid 185 and name HN ) ( resid 184 and name HA ) 3.0 1.3 1.2 volume=1.550 peak=731 ppm1=8.186 ppm2=3.623 assign ( resid 193 and name HN ) ( resid 193 and name HA ) 3.3 1.5 1.3 volume=0.888 peak=1413 ppm1=7.621 ppm2=3.484 assign ( resid 93 and name HD1# ) ( resid 93 and name HN ) 3.5 1.8 1.4 volume=0.588 peak=4483 ppm1=-0.273 ppm2=8.916 assign ( resid 113 and name HN ) ( resid 93 and name HG2# ) 3.5 1.8 1.4 volume=0.587 peak=1879 ppm1=8.233 ppm2=-0.029 assign ( resid 200 and name HE2 ) ( resid 54 and name HG2# ) 3.4 1.7 1.4 volume=0.645 peak=5038 ppm1=2.734 ppm2=0.551 assign ( resid 146 and name HN ) ( resid 144 and name HD1# ) 4.1 2.4 1.6 volume=0.228 peak=972 ppm1=8.401 ppm2=0.608 assign ( resid 111 and name HN ) ( resid 96 and name HN ) 3.9 2.2 1.6 volume=0.313 peak=2286 ppm1=8.631 ppm2=8.485 assign ( resid 164 and name HA ) ( resid 164 and name HN ) 4.6 2.9 1.4 volume=0.115 peak=5063 ppm1=4.904 ppm2=7.987 assign ( resid 196 and name HB ) ( resid 196 and name HD1# ) 3.2 1.4 1.3 volume=1.080 peak=4676 ppm1=2.252 ppm2=0.723 assign ( resid 72 and name HB ) ( resid 72 and name HG11 ) 3.2 1.5 1.3 volume=1.034 peak=4875 ppm1=1.855 ppm2=1.171 assign ( resid 61 and name HN ) ( resid 61 and name HG ) 2.8 1.1 1.1 volume=2.204 peak=1904 ppm1=8.715 ppm2=1.722 assign ( resid 8 and name HN ) ( resid 8 and name HA ) 2.5 0.8 1.0 volume=4.016 peak=1947 ppm1=7.613 ppm2=3.840 assign ( resid 201 and name HN ) ( resid 199 and name HB# ) 3.1 1.4 1.2 volume=1.158 peak=1924 ppm1=7.405 ppm2=0.620 assign ( resid 100 and name HN ) ( resid 98 and name HG2# ) 3.7 2.0 1.5 volume=0.404 peak=1029 ppm1=8.396 ppm2=1.319 assign ( resid 105 and name HB1 ) ( resid 105 and name HA ) 4.5 2.8 1.5 volume=0.128 peak=4927 ppm1=3.870 ppm2=4.143 assign ( resid 73 and name HG2# ) ( resid 72 and name HG12 ) 4.4 2.7 1.6 volume=0.152 peak=3283 ppm1=1.218 ppm2=1.042 assign ( resid 87 and name HN ) ( resid 92 and name HA ) 4.0 2.3 1.6 volume=0.267 peak=1751 ppm1=8.040 ppm2=4.925 assign ( resid 15 and name HG ) ( resid 15 and name HA ) 3.9 2.2 1.6 volume=0.315 peak=4629 ppm1=1.242 ppm2=3.652 assign ( resid 29 and name HN ) ( resid 29 and name HA ) 3.5 1.7 1.4 volume=0.634 peak=690 ppm1=8.568 ppm2=5.188 assign ( resid 144 and name HG2# ) ( resid 143 and name HN ) 4.9 3.2 1.1 volume=0.076 peak=3288 ppm1=0.766 ppm2=6.898 assign ( resid 30 and name HN ) ( resid 35 and name HN ) 3.7 2.0 1.5 volume=0.438 peak=2348 ppm1=8.721 ppm2=9.436 assign ( resid 134 and name HD1 or resid 134 and name HD2 ) ( resid 93 and name HD1# ) 3.9 2.2 1.6 volume=0.300 peak=125 ppm1=6.862 ppm2=-0.245 assign ( resid 196 and name HG11 ) ( resid 196 and name HG2# ) 2.8 1.1 1.1 volume=2.078 peak=4474 ppm1=1.806 ppm2=0.831 assign ( resid 191 and name HN ) ( resid 189 and name HB2 ) 3.8 2.1 1.5 volume=0.366 peak=1019 ppm1=7.651 ppm2=2.035 assign ( resid 87 and name HD1# ) ( resid 87 and name HB ) 2.9 1.2 1.2 volume=1.759 peak=4643 ppm1=0.439 ppm2=1.365 assign ( resid 37 and name HA ) ( resid 37 and name HB1 or resid 37 and name HB2 ) 4.2 2.5 1.7 volume=0.200 peak=2653 ppm1=5.822 ppm2=3.287 assign ( resid 49 and name HN ) ( resid 48 and name HB2 ) 3.9 2.2 1.6 volume=0.312 peak=692 ppm1=8.917 ppm2=2.706 assign ( resid 196 and name HD1# ) ( resid 196 and name HB ) 3.4 1.7 1.4 volume=0.693 peak=4698 ppm1=0.727 ppm2=2.252 assign ( resid 114 and name HG ) ( resid 93 and name HG12 ) 4.5 2.8 1.5 volume=0.133 peak=2494 ppm1=0.954 ppm2=0.594 assign ( resid 64 and name HN ) ( resid 64 and name HE1 or resid 64 and name HE2 ) 3.1 1.4 1.3 volume=1.110 peak=1713 ppm1=7.878 ppm2=6.478 assign ( resid 157 and name HD1 ) ( resid 157 and name HB1 ) 4.1 2.4 1.6 volume=0.234 peak=3846 ppm1=3.627 ppm2=2.308 assign ( resid 188 and name HB2 ) ( resid 190 and name HN ) 4.1 2.3 1.6 volume=0.239 peak=2988 ppm1=1.450 ppm2=7.533 assign ( resid 51 and name HB1 or resid 51 and name HB2 ) ( resid 168 and name HG1# ) 3.7 2.0 1.5 volume=0.413 peak=2878 ppm1=1.780 ppm2=0.778 assign ( resid 14 and name HG1# ) ( resid 14 and name HN ) 3.1 1.4 1.2 volume=1.271 peak=4241 ppm1=0.676 ppm2=7.800 assign ( resid 43 and name HN ) ( resid 40 and name HB2 or resid 40 and name HB1 ) 3.0 1.3 1.2 volume=1.483 peak=1647 ppm1=7.302 ppm2=3.353 assign ( resid 129 and name HN ) ( resid 14 and name HB ) 3.6 1.9 1.4 volume=0.475 peak=399 ppm1=8.718 ppm2=1.707 assign ( resid 203 and name HG2# ) ( resid 202 and name HN ) 3.9 2.2 1.6 volume=0.289 peak=4731 ppm1=0.338 ppm2=8.582 assign ( resid 184 and name HN ) ( resid 179 and name HB1 ) 3.7 2.0 1.5 volume=0.404 peak=701 ppm1=7.499 ppm2=2.764 assign ( resid 128 and name HA ) ( resid 127 and name HG11 ) 4.1 2.4 1.6 volume=0.222 peak=3033 ppm1=5.581 ppm2=1.032 assign ( resid 186 and name HG1 ) ( resid 185 and name HN ) 3.6 1.9 1.4 volume=0.475 peak=4364 ppm1=1.479 ppm2=8.203 assign ( resid 93 and name HG2# ) ( resid 84 and name HG2# ) 2.9 1.2 1.2 volume=1.854 peak=3924 ppm1=-0.013 ppm2=0.100 assign ( resid 1 and name HN# ) ( resid 1 and name HA ) 3.1 1.3 1.2 volume=1.289 peak=867 ppm1=8.196 ppm2=4.277 assign ( resid 27 and name HN ) ( resid 35 and name HN ) 4.1 2.4 1.7 volume=0.211 peak=1295 ppm1=9.278 ppm2=9.406 assign ( resid 203 and name HB ) ( resid 203 and name HG2# ) 3.4 1.7 1.4 volume=0.693 peak=3661 ppm1=0.123 ppm2=0.341 assign ( resid 82 and name HA ) ( resid 80 and name HG1# ) 3.9 2.1 1.5 volume=0.320 peak=3106 ppm1=5.039 ppm2=0.706 assign ( resid 167 and name HN ) ( resid 167 and name HA ) 3.4 1.7 1.4 volume=0.648 peak=2454 ppm1=8.643 ppm2=5.179 assign ( resid 113 and name HA ) ( resid 113 and name HB1 ) 4.6 2.9 1.4 volume=0.112 peak=5111 ppm1=5.310 ppm2=2.019 assign ( resid 187 and name HN ) ( resid 184 and name HA ) 3.4 1.7 1.4 volume=0.692 peak=556 ppm1=7.600 ppm2=3.616 assign ( resid 83 and name HG1 ) ( resid 68 and name HG2# ) 3.0 1.2 1.2 volume=1.606 peak=3262 ppm1=1.722 ppm2=0.739 assign ( resid 114 and name HD1# ) ( resid 115 and name HG2# ) 3.7 1.9 1.5 volume=0.453 peak=2913 ppm1=0.537 ppm2=0.654 assign ( resid 115 and name HG2# ) ( resid 116 and name HN ) 3.3 1.6 1.3 volume=0.844 peak=4854 ppm1=0.659 ppm2=8.833 assign ( resid 176 and name HN ) ( resid 176 and name HB2 ) 3.0 1.3 1.2 volume=1.528 peak=1887 ppm1=8.405 ppm2=1.799 assign ( resid 93 and name HG2# ) ( resid 114 and name HN ) 4.4 2.7 1.6 volume=0.154 peak=3100 ppm1=-0.013 ppm2=8.771 assign ( resid 80 and name HN ) ( resid 79 and name HA ) 3.3 1.6 1.3 volume=0.763 peak=1313 ppm1=7.523 ppm2=4.398 assign ( resid 176 and name HN ) ( resid 109 and name HD1 ) 3.7 2.0 1.5 volume=0.413 peak=2273 ppm1=8.404 ppm2=3.093 assign ( resid 106 and name HG12 or resid 106 and name HG11 ) ( resid 106 and name HG2# ) 3.5 1.8 1.4 volume=0.579 peak=3945 ppm1=1.408 ppm2=0.894 assign ( resid 183 and name HG11 ) ( resid 183 and name HG2# ) 2.6 0.9 1.0 volume=3.401 peak=3342 ppm1=1.267 ppm2=0.930 assign ( resid 77 and name HN ) ( resid 76 and name HN ) 3.6 1.9 1.4 volume=0.496 peak=1482 ppm1=8.056 ppm2=6.740 assign ( resid 33 and name HG12 ) ( resid 193 and name HA ) 3.6 1.9 1.4 volume=0.494 peak=3130 ppm1=1.918 ppm2=3.452 assign ( resid 126 and name HN ) ( resid 125 and name HB1 ) 3.7 2.0 1.5 volume=0.433 peak=1424 ppm1=9.105 ppm2=2.440 assign ( resid 115 and name HG1# ) ( resid 129 and name HA ) 4.3 2.5 1.7 volume=0.179 peak=2787 ppm1=0.302 ppm2=5.723 assign ( resid 34 and name HN ) ( resid 35 and name HN ) 4.4 2.6 1.6 volume=0.157 peak=619 ppm1=8.137 ppm2=9.350 assign ( resid 84 and name HN ) ( resid 83 and name HB1 ) 3.0 1.3 1.2 volume=1.408 peak=1343 ppm1=8.504 ppm2=1.007 assign ( resid 64 and name HZ ) ( resid 65 and name HD1# ) 3.6 1.9 1.4 volume=0.500 peak=9 ppm1=7.051 ppm2=0.177 assign ( resid 184 and name HA ) ( resid 187 and name HG2# ) 2.9 1.2 1.2 volume=1.735 peak=4260 ppm1=3.628 ppm2=1.025 assign ( resid 114 and name HD1# ) ( resid 3 and name HD1 or resid 3 and name HD2 ) 4.0 2.2 1.6 volume=0.282 peak=2769 ppm1=0.537 ppm2=7.355 assign ( resid 160 and name HN ) ( resid 158 and name HA ) 3.2 1.5 1.3 volume=0.920 peak=1995 ppm1=8.833 ppm2=4.131 assign ( resid 72 and name HA ) ( resid 78 and name HD1# ) 3.4 1.7 1.4 volume=0.674 peak=4301 ppm1=3.632 ppm2=0.473 assign ( resid 109 and name HG2 ) ( resid 144 and name HN ) 4.1 2.4 1.7 volume=0.215 peak=4439 ppm1=1.547 ppm2=7.533 assign ( resid 119 and name HG2 or resid 119 and name HG1 ) ( resid 119 and name HD1 ) 3.2 1.5 1.3 volume=0.939 peak=3293 ppm1=1.257 ppm2=2.899 assign ( resid 20 and name HN ) ( resid 18 and name HN ) 3.8 2.1 1.5 volume=0.357 peak=712 ppm1=7.405 ppm2=7.767 assign ( resid 123 and name HN ) ( resid 122 and name HA1 ) 3.1 1.4 1.2 volume=1.212 peak=2140 ppm1=8.405 ppm2=3.872 assign ( resid 182 and name HB2 ) ( resid 183 and name HD1# ) 3.0 1.3 1.2 volume=1.357 peak=4182 ppm1=3.880 ppm2=0.886 assign ( resid 85 and name HN ) ( resid 84 and name HN ) 3.2 1.5 1.3 volume=0.922 peak=1523 ppm1=7.153 ppm2=8.476 assign ( resid 203 and name HD1# ) ( resid 64 and name HN ) 4.0 2.3 1.6 volume=0.269 peak=4505 ppm1=-0.010 ppm2=7.930 assign ( resid 3 and name HN ) ( resid 2 and name HA ) 3.0 1.3 1.2 volume=1.369 peak=503 ppm1=7.914 ppm2=4.142 assign ( resid 54 and name HG12 ) ( resid 54 and name HG11 ) 2.8 1.1 1.1 volume=2.010 peak=2490 ppm1=1.235 ppm2=1.179 assign ( resid 18 and name HB2 ) ( resid 15 and name HB2 ) 3.6 1.9 1.5 volume=0.455 peak=3459 ppm1=2.446 ppm2=1.360 assign ( resid 72 and name HN ) ( resid 71 and name HN ) 3.6 1.9 1.5 volume=0.471 peak=753 ppm1=7.536 ppm2=7.265 assign ( resid 65 and name HG ) ( resid 66 and name HN ) 4.1 2.4 1.7 volume=0.218 peak=5139 ppm1=1.642 ppm2=8.067 assign ( resid 214 and name HN ) ( resid 214 and name HB1 or resid 214 and name HB2 ) 3.7 1.9 1.5 volume=0.451 peak=254 ppm1=7.955 ppm2=2.834 assign ( resid 115 and name HN ) ( resid 116 and name HB2 ) 4.1 2.4 1.7 volume=0.213 peak=510 ppm1=9.052 ppm2=2.830 assign ( resid 48 and name HN ) ( resid 49 and name HA ) 3.4 1.7 1.4 volume=0.704 peak=471 ppm1=9.294 ppm2=4.916 assign ( resid 126 and name HG2# ) ( resid 126 and name HG11 ) 2.8 1.1 1.1 volume=2.368 peak=4940 ppm1=0.754 ppm2=1.096 assign ( resid 129 and name HN ) ( resid 116 and name HN ) 3.1 1.4 1.2 volume=1.171 peak=1022 ppm1=8.718 ppm2=8.832 assign ( resid 132 and name HG2# ) ( resid 3 and name HD1 or resid 3 and name HD2 ) 3.5 1.8 1.4 volume=0.542 peak=5033 ppm1=0.936 ppm2=7.353 assign ( resid 8 and name HA ) ( resid 8 and name HB2 or resid 8 and name HB1 ) 3.1 1.4 1.2 volume=1.229 peak=5117 ppm1=3.838 ppm2=2.047 assign ( resid 143 and name HN ) ( resid 144 and name HN ) 3.4 1.6 1.3 volume=0.740 peak=1437 ppm1=6.900 ppm2=7.541 assign ( resid 87 and name HG11 ) ( resid 87 and name HG2# ) 2.7 1.0 1.1 volume=2.890 peak=3163 ppm1=1.265 ppm2=0.849 assign ( resid 163 and name HN ) ( resid 163 and name HB# ) 2.3 0.6 0.9 volume=7.178 peak=2090 ppm1=7.324 ppm2=1.141 assign ( resid 50 and name HN ) ( resid 168 and name HG2# ) 3.4 1.7 1.4 volume=0.650 peak=1652 ppm1=9.300 ppm2=0.224 assign ( resid 137 and name HB1 ) ( resid 137 and name HB2 ) 2.9 1.2 1.2 volume=1.840 peak=4646 ppm1=2.808 ppm2=2.579 assign ( resid 71 and name HN ) ( resid 70 and name HN ) 3.2 1.5 1.3 volume=1.018 peak=405 ppm1=7.220 ppm2=8.566 assign ( resid 98 and name HG2# ) ( resid 111 and name HN ) 4.1 2.4 1.7 volume=0.217 peak=4006 ppm1=1.322 ppm2=8.660 assign ( resid 7 and name HB# ) ( resid 7 and name HN ) 3.1 1.4 1.2 volume=1.197 peak=4357 ppm1=0.752 ppm2=8.452 assign ( resid 53 and name HD1# ) ( resid 158 and name HG1 or resid 158 and name HG2 ) 3.2 1.5 1.3 volume=0.920 peak=3346 ppm1=0.796 ppm2=2.443 assign ( resid 85 and name HN ) ( resid 93 and name HD1# ) 3.7 2.0 1.5 volume=0.437 peak=786 ppm1=7.151 ppm2=-0.288 assign ( resid 203 and name HN ) ( resid 64 and name HD1 or resid 64 and name HD2 ) 3.4 1.7 1.4 volume=0.666 peak=1734 ppm1=7.685 ppm2=5.964 assign ( resid 28 and name HN ) ( resid 34 and name HA ) 3.4 1.6 1.3 volume=0.758 peak=1311 ppm1=7.810 ppm2=4.911 assign ( resid 186 and name HB2 ) ( resid 186 and name HA ) 3.5 1.8 1.4 volume=0.599 peak=2618 ppm1=1.904 ppm2=4.220 assign ( resid 33 and name HN ) ( resid 33 and name HG11 ) 2.5 0.7 1.0 volume=4.784 peak=227 ppm1=8.165 ppm2=1.888 assign ( resid 87 and name HN ) ( resid 86 and name HA ) 3.8 2.0 1.5 volume=0.380 peak=1871 ppm1=8.038 ppm2=4.269 assign ( resid 73 and name HA ) ( resid 217 and name HN ) 4.3 2.6 1.7 volume=0.174 peak=2792 ppm1=3.921 ppm2=8.137 assign ( resid 91 and name HG2# ) ( resid 91 and name HA ) 3.4 1.7 1.4 volume=0.697 peak=2645 ppm1=1.017 ppm2=5.860 assign ( resid 116 and name HN ) ( resid 117 and name HN ) 4.1 2.4 1.7 volume=0.218 peak=2159 ppm1=8.834 ppm2=8.241 assign ( resid 107 and name HN ) ( resid 106 and name HG12 ) 3.6 1.9 1.5 volume=0.457 peak=1821 ppm1=8.394 ppm2=1.409 assign ( resid 186 and name HD2 ) ( resid 186 and name HA ) 3.5 1.8 1.4 volume=0.606 peak=3225 ppm1=1.674 ppm2=4.142 assign ( resid 59 and name HN ) ( resid 60 and name HN ) 3.9 2.2 1.6 volume=0.299 peak=1733 ppm1=8.091 ppm2=7.264 assign ( resid 38 and name HN ) ( resid 38 and name HA ) 3.3 1.6 1.3 volume=0.830 peak=2119 ppm1=8.464 ppm2=4.272 assign ( resid 115 and name HG2# ) ( resid 129 and name HB2 or resid 129 and name HB1 ) 3.0 1.3 1.2 volume=1.344 peak=5055 ppm1=0.659 ppm2=3.361 assign ( resid 123 and name HN ) ( resid 122 and name HN ) 3.2 1.5 1.3 volume=0.928 peak=515 ppm1=8.405 ppm2=8.650 assign ( resid 158 and name HG1 ) ( resid 164 and name HN ) 4.3 2.6 1.7 volume=0.175 peak=3824 ppm1=2.438 ppm2=7.995 assign ( resid 92 and name HE1 or resid 92 and name HE2 ) ( resid 86 and name HA ) 4.0 2.3 1.6 volume=0.273 peak=4 ppm1=6.749 ppm2=4.352 assign ( resid 75 and name HN ) ( resid 75 and name HB1 or resid 75 and name HB2 ) 3.5 1.7 1.4 volume=0.631 peak=2325 ppm1=7.480 ppm2=2.838 assign ( resid 65 and name HD1# ) ( resid 67 and name HN ) 4.1 2.4 1.6 volume=0.228 peak=2782 ppm1=0.175 ppm2=7.542 assign ( resid 29 and name HN ) ( resid 34 and name HA ) 3.6 1.9 1.4 volume=0.504 peak=2104 ppm1=8.568 ppm2=4.916 assign ( resid 117 and name HD1# ) ( resid 67 and name HG1 ) 3.6 1.9 1.5 volume=0.470 peak=2509 ppm1=0.244 ppm2=2.584 assign ( resid 126 and name HN ) ( resid 117 and name HG2# ) 3.6 1.9 1.4 volume=0.494 peak=1861 ppm1=9.103 ppm2=0.363 assign ( resid 8 and name HN ) ( resid 8 and name HB2 ) 2.4 0.6 0.9 volume=6.247 peak=1242 ppm1=7.609 ppm2=2.057 assign ( resid 21 and name HG2# ) ( resid 20 and name HN ) 4.1 2.4 1.6 volume=0.226 peak=2571 ppm1=1.149 ppm2=7.415 assign ( resid 154 and name HG1# ) ( resid 15 and name HG ) 3.0 1.2 1.2 volume=1.584 peak=2687 ppm1=0.916 ppm2=1.252 assign ( resid 188 and name HN ) ( resid 184 and name HA ) 3.0 1.3 1.2 volume=1.379 peak=1698 ppm1=8.442 ppm2=3.615 assign ( resid 7 and name HB# ) ( resid 116 and name HN ) 4.0 2.3 1.6 volume=0.262 peak=3327 ppm1=0.752 ppm2=8.802 assign ( resid 109 and name HB1 ) ( resid 144 and name HG11 ) 3.8 2.1 1.5 volume=0.344 peak=2597 ppm1=1.719 ppm2=1.243 assign ( resid 3 and name HD1 or resid 3 and name HD2 ) ( resid 3 and name HN ) 3.5 1.8 1.4 volume=0.582 peak=109 ppm1=7.379 ppm2=7.944 assign ( resid 121 and name HA ) ( resid 122 and name HA2 ) 4.2 2.5 1.7 volume=0.184 peak=3704 ppm1=4.145 ppm2=3.633 assign ( resid 34 and name HG2# ) ( resid 36 and name HA ) 4.0 2.3 1.6 volume=0.247 peak=3006 ppm1=1.101 ppm2=5.850 assign ( resid 176 and name HN ) ( resid 174 and name HG2 ) 3.2 1.5 1.3 volume=0.999 peak=1672 ppm1=8.405 ppm2=2.190 assign ( resid 71 and name HD1 ) ( resid 78 and name HD1# ) 3.3 1.6 1.3 volume=0.852 peak=2595 ppm1=2.780 ppm2=0.510 assign ( resid 15 and name HD1# ) ( resid 15 and name HD2# ) 3.7 1.9 1.5 volume=0.452 peak=4136 ppm1=0.439 ppm2=0.686 assign ( resid 1 and name HA ) ( resid 2 and name HA ) 5.1 3.4 0.9 volume=0.062 peak=3742 ppm1=4.281 ppm2=4.167 assign ( resid 160 and name HA ) ( resid 161 and name HA ) 3.7 2.0 1.5 volume=0.439 peak=2500 ppm1=4.012 ppm2=4.679 assign ( resid 167 and name HD1# ) ( resid 154 and name HA ) 4.2 2.5 1.7 volume=0.190 peak=3329 ppm1=0.763 ppm2=4.645 assign ( resid 102 and name HB# ) ( resid 103 and name HN ) 4.2 2.5 1.7 volume=0.202 peak=4118 ppm1=1.279 ppm2=8.458 assign ( resid 143 and name HN ) ( resid 142 and name HB1 ) 2.8 1.1 1.1 volume=2.263 peak=674 ppm1=6.899 ppm2=1.929 assign ( resid 134 and name HE1 or resid 134 and name HE2 ) ( resid 134 and name HD1 or resid 134 and name HD2 ) 2.6 0.8 1.0 volume=3.793 peak=33 ppm1=7.140 ppm2=6.864 assign ( resid 61 and name HN ) ( resid 60 and name HA ) 2.9 1.1 1.1 volume=1.975 peak=2198 ppm1=8.716 ppm2=3.868 assign ( resid 146 and name HN ) ( resid 145 and name HG1 ) 3.5 1.8 1.4 volume=0.613 peak=1639 ppm1=8.400 ppm2=1.405 assign ( resid 102 and name HB# ) ( resid 105 and name HB1 ) 3.2 1.4 1.3 volume=1.076 peak=3868 ppm1=1.279 ppm2=3.828 assign ( resid 83 and name HN ) ( resid 82 and name HA ) 2.9 1.2 1.2 volume=1.682 peak=1082 ppm1=8.503 ppm2=5.048 assign ( resid 109 and name HB1 or resid 109 and name HB2 ) ( resid 98 and name HG2# ) 3.8 2.1 1.5 volume=0.344 peak=4990 ppm1=1.718 ppm2=1.352 assign ( resid 79 and name HN ) ( resid 78 and name HA ) 3.2 1.5 1.3 volume=0.951 peak=2058 ppm1=8.841 ppm2=4.657 assign ( resid 56 and name HN ) ( resid 57 and name HA ) 3.7 2.0 1.5 volume=0.430 peak=662 ppm1=8.639 ppm2=4.139 assign ( resid 152 and name HN ) ( resid 153 and name HN ) 3.6 1.9 1.4 volume=0.513 peak=1555 ppm1=8.345 ppm2=9.330 assign ( resid 42 and name HN ) ( resid 40 and name HN ) 3.7 2.0 1.5 volume=0.395 peak=239 ppm1=8.696 ppm2=8.486 assign ( resid 24 and name HH2 ) ( resid 36 and name HB2 ) 4.0 2.2 1.6 volume=0.280 peak=55 ppm1=6.801 ppm2=3.459 assign ( resid 34 and name HN ) ( resid 33 and name HG2# ) 3.2 1.5 1.3 volume=0.986 peak=1430 ppm1=8.137 ppm2=0.499 assign ( resid 155 and name HN ) ( resid 155 and name HB2 ) 3.5 1.8 1.4 volume=0.595 peak=1720 ppm1=8.976 ppm2=2.575 assign ( resid 76 and name HE1 ) ( resid 76 and name HD2 ) 1.9 0.2 0.8 volume=19.624 peak=2918 ppm1=2.862 ppm2=1.552 assign ( resid 154 and name HG2# ) ( resid 168 and name HB ) 2.8 1.1 1.1 volume=2.247 peak=4442 ppm1=0.838 ppm2=1.736 assign ( resid 54 and name HG11 ) ( resid 54 and name HG12 ) 2.7 1.0 1.1 volume=2.595 peak=4176 ppm1=1.188 ppm2=1.233 assign ( resid 184 and name HG12 ) ( resid 179 and name HB2 ) 4.2 2.5 1.7 volume=0.203 peak=3706 ppm1=1.093 ppm2=2.463 assign ( resid 184 and name HG12 ) ( resid 184 and name HG11 ) 3.2 1.5 1.3 volume=0.912 peak=3175 ppm1=1.092 ppm2=1.673 assign ( resid 144 and name HD1# ) ( resid 144 and name HG2# ) 3.2 1.5 1.3 volume=0.931 peak=3392 ppm1=0.623 ppm2=0.762 assign ( resid 115 and name HG1# ) ( resid 94 and name HN ) 4.3 2.6 1.7 volume=0.175 peak=2546 ppm1=0.303 ppm2=9.584 assign ( resid 205 and name HA ) ( resid 205 and name HB# ) 2.7 1.0 1.1 volume=2.495 peak=2484 ppm1=4.139 ppm2=1.288 assign ( resid 99 and name HG1 ) ( resid 99 and name HN ) 4.2 2.5 1.7 volume=0.204 peak=4855 ppm1=2.440 ppm2=7.797 assign ( resid 87 and name HA ) ( resid 87 and name HG12 ) 3.1 1.4 1.3 volume=1.141 peak=3687 ppm1=3.871 ppm2=1.051 assign ( resid 116 and name HB1 ) ( resid 11 and name HB# ) 3.0 1.3 1.2 volume=1.343 peak=2492 ppm1=2.843 ppm2=1.624 assign ( resid 43 and name HN ) ( resid 42 and name HB2 or resid 42 and name HB1 ) 2.9 1.2 1.2 volume=1.650 peak=1826 ppm1=7.305 ppm2=1.659 assign ( resid 145 and name HN ) ( resid 145 and name HG1 or resid 145 and name HG2 ) 3.2 1.5 1.3 volume=0.956 peak=1130 ppm1=8.379 ppm2=1.404 assign ( resid 199 and name HB# ) ( resid 64 and name HE1 or resid 64 and name HE2 ) 3.4 1.7 1.4 volume=0.666 peak=3214 ppm1=0.694 ppm2=6.495 assign ( resid 153 and name HA ) ( resid 167 and name HD1# ) 3.7 2.0 1.5 volume=0.390 peak=4110 ppm1=5.319 ppm2=0.763 assign ( resid 128 and name HA ) ( resid 152 and name HA2 ) 3.6 1.9 1.4 volume=0.496 peak=3437 ppm1=5.580 ppm2=3.870 assign ( resid 34 and name HN ) ( resid 52 and name HA2 ) 3.6 1.9 1.4 volume=0.508 peak=485 ppm1=8.137 ppm2=4.430 assign ( resid 66 and name HN ) ( resid 66 and name HA ) 3.3 1.6 1.3 volume=0.848 peak=704 ppm1=8.050 ppm2=4.283 assign ( resid 42 and name HN ) ( resid 42 and name HG1 ) 3.1 1.4 1.2 volume=1.159 peak=2225 ppm1=8.698 ppm2=1.319 assign ( resid 114 and name HB2 ) ( resid 114 and name HG ) 3.6 1.9 1.4 volume=0.481 peak=3731 ppm1=1.701 ppm2=0.953 assign ( resid 3 and name HE1 or resid 3 and name HE2 ) ( resid 133 and name HN ) 3.7 1.9 1.5 volume=0.444 peak=81 ppm1=7.213 ppm2=8.216 assign ( resid 185 and name HA ) ( resid 185 and name HB1 ) 3.3 1.6 1.3 volume=0.793 peak=2957 ppm1=3.894 ppm2=2.143 assign ( resid 14 and name HG1# ) ( resid 152 and name HA1 ) 3.8 2.1 1.5 volume=0.347 peak=3336 ppm1=0.677 ppm2=3.637 assign ( resid 6 and name HB ) ( resid 6 and name HA ) 4.1 2.4 1.6 volume=0.230 peak=4410 ppm1=1.725 ppm2=3.628 assign ( resid 205 and name HA ) ( resid 208 and name HN ) 3.4 1.6 1.3 volume=0.751 peak=3091 ppm1=4.139 ppm2=7.996 assign ( resid 202 and name HN ) ( resid 199 and name HA ) 3.5 1.8 1.4 volume=0.540 peak=1546 ppm1=8.577 ppm2=2.776 assign ( resid 144 and name HN ) ( resid 144 and name HA ) 3.5 1.8 1.4 volume=0.543 peak=691 ppm1=7.537 ppm2=3.979 assign ( resid 147 and name HN ) ( resid 147 and name HB2 ) 3.4 1.7 1.4 volume=0.665 peak=2145 ppm1=8.785 ppm2=2.706 assign ( resid 15 and name HB2 ) ( resid 15 and name HD2# ) 3.2 1.5 1.3 volume=0.978 peak=3972 ppm1=1.367 ppm2=0.683 assign ( resid 188 and name HA ) ( resid 188 and name HE# ) 3.2 1.4 1.3 volume=1.069 peak=4536 ppm1=4.211 ppm2=1.888 assign ( resid 77 and name HN ) ( resid 77 and name HB1 ) 3.4 1.7 1.4 volume=0.709 peak=1451 ppm1=8.056 ppm2=3.890 assign ( resid 114 and name HN ) ( resid 132 and name HN ) 3.8 2.1 1.5 volume=0.335 peak=1703 ppm1=8.799 ppm2=7.922 assign ( resid 98 and name HG2# ) ( resid 109 and name HN ) 3.9 2.1 1.5 volume=0.320 peak=4606 ppm1=1.324 ppm2=8.198 assign ( resid 119 and name HD2 ) ( resid 119 and name HN ) 4.5 2.8 1.5 volume=0.126 peak=3583 ppm1=2.900 ppm2=8.052 assign ( resid 114 and name HD2# ) ( resid 6 and name HB ) 2.7 1.0 1.1 volume=2.857 peak=3009 ppm1=0.782 ppm2=1.753 assign ( resid 187 and name HG2# ) ( resid 184 and name HB ) 3.0 1.3 1.2 volume=1.405 peak=4889 ppm1=1.060 ppm2=2.069 assign ( resid 85 and name HN ) ( resid 85 and name HB2 ) 3.2 1.4 1.3 volume=1.081 peak=1253 ppm1=7.153 ppm2=3.096 assign ( resid 134 and name HN ) ( resid 134 and name HZ ) 4.1 2.4 1.6 volume=0.223 peak=841 ppm1=8.745 ppm2=6.648 assign ( resid 93 and name HG12 ) ( resid 93 and name HG11 ) 3.1 1.3 1.2 volume=1.298 peak=4223 ppm1=0.596 ppm2=0.683 assign ( resid 65 and name HN ) ( resid 66 and name HN ) 3.2 1.5 1.3 volume=0.918 peak=747 ppm1=7.741 ppm2=8.042 assign ( resid 12 and name HN ) ( resid 11 and name HB# ) 2.8 1.1 1.1 volume=2.243 peak=721 ppm1=7.552 ppm2=1.663 assign ( resid 161 and name HN ) ( resid 160 and name HA ) 2.9 1.1 1.1 volume=1.943 peak=1676 ppm1=6.906 ppm2=4.011 assign ( resid 156 and name HN ) ( resid 124 and name HG1 ) 3.3 1.6 1.3 volume=0.828 peak=2171 ppm1=8.552 ppm2=2.431 assign ( resid 8 and name HG1 or resid 8 and name HG2 ) ( resid 4 and name HB1 or resid 4 and name HB2 ) 3.7 1.9 1.5 volume=0.439 peak=4729 ppm1=2.320 ppm2=1.751 assign ( resid 116 and name HN ) ( resid 116 and name HB2 ) 3.4 1.7 1.4 volume=0.718 peak=2137 ppm1=8.835 ppm2=2.839 assign ( resid 185 and name HN ) ( resid 183 and name HN ) 2.8 1.1 1.1 volume=2.262 peak=1052 ppm1=8.184 ppm2=7.456 assign ( resid 8 and name HG1 or resid 8 and name HG2 ) ( resid 11 and name HB# ) 3.8 2.1 1.5 volume=0.333 peak=4376 ppm1=2.320 ppm2=1.618 assign ( resid 93 and name HD1# ) ( resid 93 and name HB ) 3.0 1.3 1.2 volume=1.396 peak=5086 ppm1=-0.272 ppm2=1.224 assign ( resid 54 and name HD1# ) ( resid 200 and name HE1 ) 3.3 1.6 1.3 volume=0.826 peak=4047 ppm1=0.490 ppm2=2.793 assign ( resid 78 and name HN ) ( resid 76 and name HA ) 3.7 2.0 1.5 volume=0.396 peak=1975 ppm1=7.148 ppm2=4.145 assign ( resid 203 and name HA ) ( resid 203 and name HD1# ) 3.7 2.0 1.5 volume=0.423 peak=4984 ppm1=2.833 ppm2=-0.001 assign ( resid 46 and name HN ) ( resid 184 and name HG2# ) 3.4 1.7 1.4 volume=0.692 peak=2389 ppm1=8.560 ppm2=1.102 assign ( resid 185 and name HB1 ) ( resid 185 and name HG2 ) 3.7 2.0 1.5 volume=0.397 peak=4021 ppm1=2.151 ppm2=2.344 assign ( resid 127 and name HN ) ( resid 126 and name HD1# ) 4.2 2.4 1.7 volume=0.207 peak=664 ppm1=9.383 ppm2=0.351 assign ( resid 6 and name HA ) ( resid 7 and name HN ) 3.3 1.6 1.3 volume=0.876 peak=3407 ppm1=3.617 ppm2=8.452 assign ( resid 158 and name HN ) ( resid 165 and name HA ) 3.2 1.5 1.3 volume=1.022 peak=652 ppm1=8.217 ppm2=5.183 assign ( resid 161 and name HN ) ( resid 161 and name HA ) 3.3 1.6 1.3 volume=0.820 peak=2008 ppm1=6.905 ppm2=4.661 assign ( resid 185 and name HN ) ( resid 186 and name HN ) 2.8 1.1 1.1 volume=2.246 peak=1278 ppm1=8.184 ppm2=7.391 assign ( resid 194 and name HN ) ( resid 197 and name HG ) 3.3 1.6 1.3 volume=0.806 peak=2274 ppm1=7.773 ppm2=1.300 assign ( resid 23 and name HN ) ( resid 24 and name HB2 or resid 24 and name HB1 ) 3.9 2.2 1.6 volume=0.313 peak=1937 ppm1=8.638 ppm2=2.964 assign ( resid 196 and name HG11 ) ( resid 196 and name HB ) 3.0 1.3 1.2 volume=1.382 peak=4097 ppm1=1.806 ppm2=2.258 assign ( resid 66 and name HN ) ( resid 71 and name HN ) 3.7 1.9 1.5 volume=0.440 peak=1832 ppm1=8.051 ppm2=7.262 assign ( resid 158 and name HA ) ( resid 159 and name HN ) 4.4 2.7 1.6 volume=0.152 peak=2760 ppm1=4.138 ppm2=9.044 assign ( resid 166 and name HN ) ( resid 53 and name HG2# ) 3.1 1.4 1.2 volume=1.243 peak=1460 ppm1=9.001 ppm2=0.884 assign ( resid 113 and name HA ) ( resid 132 and name HG2# ) 4.5 2.8 1.5 volume=0.129 peak=4991 ppm1=5.308 ppm2=0.955 assign ( resid 203 and name HA ) ( resid 203 and name HG2# ) 3.4 1.7 1.4 volume=0.683 peak=4197 ppm1=2.833 ppm2=0.341 assign ( resid 52 and name HN ) ( resid 52 and name HA2 ) 3.5 1.8 1.4 volume=0.565 peak=1114 ppm1=8.617 ppm2=4.525 assign ( resid 112 and name HG2# ) ( resid 112 and name HG11 ) 2.7 1.0 1.1 volume=2.670 peak=3914 ppm1=0.680 ppm2=1.602 assign ( resid 190 and name HN ) ( resid 190 and name HB1 or resid 190 and name HB2 ) 2.7 1.0 1.1 volume=2.596 peak=801 ppm1=7.517 ppm2=3.887 assign ( resid 180 and name HN ) ( resid 183 and name HB ) 3.4 1.7 1.4 volume=0.687 peak=1332 ppm1=8.353 ppm2=1.927 assign ( resid 35 and name HB ) ( resid 27 and name HN ) 4.1 2.4 1.6 volume=0.231 peak=2658 ppm1=2.052 ppm2=9.285 assign ( resid 198 and name HN ) ( resid 196 and name HA ) 3.1 1.4 1.3 volume=1.138 peak=371 ppm1=8.717 ppm2=3.481 assign ( resid 76 and name HN ) ( resid 77 and name HN ) 3.3 1.6 1.3 volume=0.788 peak=1401 ppm1=6.699 ppm2=8.045 assign ( resid 205 and name HN ) ( resid 203 and name HG2# ) 3.1 1.4 1.3 volume=1.132 peak=291 ppm1=7.175 ppm2=0.354 assign ( resid 206 and name HN ) ( resid 204 and name HN ) 4.0 2.3 1.6 volume=0.251 peak=539 ppm1=7.463 ppm2=6.744 assign ( resid 134 and name HZ ) ( resid 134 and name HE1 or resid 134 and name HE2 ) 2.6 0.9 1.1 volume=3.157 peak=51 ppm1=6.643 ppm2=7.138 assign ( resid 162 and name HD1 ) ( resid 162 and name HB1 ) 3.8 2.1 1.5 volume=0.342 peak=2556 ppm1=3.487 ppm2=2.201 assign ( resid 83 and name HN ) ( resid 68 and name HB ) 3.7 2.0 1.5 volume=0.429 peak=1759 ppm1=8.503 ppm2=4.237 assign ( resid 200 and name HG1 ) ( resid 54 and name HG2# ) 4.0 2.3 1.6 volume=0.266 peak=3971 ppm1=1.130 ppm2=0.583 assign ( resid 170 and name HN ) ( resid 169 and name HN ) 3.0 1.3 1.2 volume=1.349 peak=269 ppm1=9.146 ppm2=9.259 assign ( resid 37 and name HA ) ( resid 35 and name HG2# or resid 35 and name HG1# ) 3.7 2.0 1.5 volume=0.435 peak=4753 ppm1=5.823 ppm2=0.929 assign ( resid 52 and name HN ) ( resid 51 and name HB1 or resid 51 and name HB2 ) 3.0 1.3 1.2 volume=1.431 peak=1429 ppm1=8.615 ppm2=1.787 assign ( resid 173 and name HA ) ( resid 174 and name HB2 ) 3.5 1.8 1.4 volume=0.571 peak=3096 ppm1=3.613 ppm2=1.868 assign ( resid 196 and name HB ) ( resid 196 and name HA ) 4.2 2.5 1.7 volume=0.189 peak=3983 ppm1=2.252 ppm2=3.450 assign ( resid 2 and name HN ) ( resid 6 and name HD1# ) 3.3 1.6 1.3 volume=0.764 peak=1225 ppm1=8.191 ppm2=0.757 assign ( resid 3 and name HE1 or resid 3 and name HE2 ) ( resid 132 and name HB ) 3.3 1.6 1.3 volume=0.826 peak=93 ppm1=7.212 ppm2=2.249 assign ( resid 7 and name HB# ) ( resid 11 and name HB# ) 3.4 1.6 1.3 volume=0.742 peak=3523 ppm1=0.751 ppm2=1.633 assign ( resid 183 and name HA ) ( resid 183 and name HB ) 3.0 1.2 1.2 volume=1.569 peak=3105 ppm1=3.917 ppm2=1.959 assign ( resid 191 and name HN ) ( resid 194 and name HN ) 4.0 2.3 1.6 volume=0.271 peak=1338 ppm1=7.650 ppm2=7.782 assign ( resid 60 and name HE2 ) ( resid 60 and name HA ) 3.7 2.0 1.5 volume=0.439 peak=3941 ppm1=2.832 ppm2=3.877 assign ( resid 19 and name HN ) ( resid 18 and name HB1 ) 3.2 1.5 1.3 volume=0.974 peak=1963 ppm1=7.481 ppm2=2.971 assign ( resid 151 and name HN ) ( resid 151 and name HB1 ) 3.2 1.5 1.3 volume=1.040 peak=1549 ppm1=8.646 ppm2=2.969 assign ( resid 85 and name HN ) ( resid 93 and name HG11 ) 3.0 1.3 1.2 volume=1.438 peak=2231 ppm1=7.152 ppm2=0.627 assign ( resid 106 and name HN ) ( resid 104 and name HN ) 2.8 1.1 1.1 volume=2.057 peak=1146 ppm1=7.941 ppm2=8.045 assign ( resid 81 and name HN ) ( resid 81 and name HB1 ) 3.5 1.8 1.4 volume=0.605 peak=2052 ppm1=8.509 ppm2=2.315 assign ( resid 175 and name HN ) ( resid 176 and name HN ) 3.6 1.9 1.4 volume=0.489 peak=901 ppm1=8.804 ppm2=8.437 assign ( resid 142 and name HB2 ) ( resid 142 and name HA ) 4.1 2.4 1.6 volume=0.231 peak=2573 ppm1=1.840 ppm2=4.137 assign ( resid 115 and name HN ) ( resid 93 and name HA ) 3.8 2.1 1.5 volume=0.374 peak=2186 ppm1=9.054 ppm2=4.790 assign ( resid 26 and name HA ) ( resid 26 and name HB ) 4.5 2.8 1.5 volume=0.131 peak=4276 ppm1=3.980 ppm2=1.924 assign ( resid 73 and name HN ) ( resid 72 and name HG11 ) 2.9 1.2 1.2 volume=1.713 peak=1261 ppm1=7.505 ppm2=1.142 assign ( resid 147 and name HB2 ) ( resid 147 and name HD1 or resid 147 and name HD2 ) 4.1 2.4 1.6 volume=0.219 peak=2739 ppm1=2.703 ppm2=6.226 assign ( resid 115 and name HG1# ) ( resid 91 and name HA ) 4.0 2.3 1.6 volume=0.261 peak=4871 ppm1=0.303 ppm2=5.916 assign ( resid 76 and name HN ) ( resid 198 and name HA ) 3.7 2.0 1.5 volume=0.424 peak=1958 ppm1=6.699 ppm2=4.529 assign ( resid 203 and name HD1# ) ( resid 60 and name HG1 ) 3.4 1.7 1.4 volume=0.657 peak=2511 ppm1=-0.009 ppm2=1.355 assign ( resid 158 and name HB2 ) ( resid 165 and name HA ) 3.9 2.2 1.6 volume=0.301 peak=3712 ppm1=2.219 ppm2=5.144 assign ( resid 213 and name HN ) ( resid 213 and name HA1 ) 3.5 1.8 1.4 volume=0.538 peak=435 ppm1=8.280 ppm2=3.749 assign ( resid 60 and name HG1 ) ( resid 61 and name HD2# ) 3.3 1.5 1.3 volume=0.901 peak=4726 ppm1=1.323 ppm2=0.769 assign ( resid 186 and name HN ) ( resid 187 and name HN ) 3.0 1.3 1.2 volume=1.553 peak=943 ppm1=7.370 ppm2=7.611 assign ( resid 4 and name HN ) ( resid 87 and name HD1# ) 3.5 1.7 1.4 volume=0.621 peak=1817 ppm1=8.190 ppm2=0.490 assign ( resid 130 and name HN ) ( resid 115 and name HG2# ) 3.9 2.2 1.6 volume=0.297 peak=1173 ppm1=7.617 ppm2=0.647 assign ( resid 14 and name HG2# ) ( resid 153 and name HN ) 3.6 1.9 1.4 volume=0.501 peak=2533 ppm1=0.758 ppm2=9.314 assign ( resid 174 and name HN ) ( resid 174 and name HG2 ) 3.2 1.5 1.3 volume=1.035 peak=850 ppm1=9.151 ppm2=2.188 assign ( resid 132 and name HG1# ) ( resid 3 and name HD1 or resid 3 and name HD2 ) 3.5 1.8 1.4 volume=0.611 peak=4119 ppm1=0.542 ppm2=7.358 assign ( resid 145 and name HG2 ) ( resid 133 and name HA ) 4.5 2.8 1.5 volume=0.122 peak=3116 ppm1=1.411 ppm2=4.662 assign ( resid 56 and name HN ) ( resid 57 and name HN ) 3.5 1.8 1.4 volume=0.549 peak=889 ppm1=8.643 ppm2=9.216 assign ( resid 145 and name HN ) ( resid 139 and name HG1 ) 3.5 1.8 1.4 volume=0.565 peak=250 ppm1=8.380 ppm2=1.793 assign ( resid 123 and name HN ) ( resid 123 and name HA ) 2.5 0.8 1.0 volume=3.932 peak=263 ppm1=8.404 ppm2=4.310 assign ( resid 95 and name HN ) ( resid 84 and name HG2# ) 3.5 1.8 1.4 volume=0.608 peak=1919 ppm1=9.128 ppm2=0.092 assign ( resid 186 and name HB2 ) ( resid 102 and name HB# ) 3.6 1.8 1.4 volume=0.530 peak=3429 ppm1=1.901 ppm2=1.291 assign ( resid 95 and name HN ) ( resid 82 and name HB1 ) 3.2 1.4 1.3 volume=1.065 peak=937 ppm1=9.125 ppm2=2.443 assign ( resid 167 and name HD1# ) ( resid 153 and name HB1 or resid 153 and name HB2 ) 3.6 1.9 1.4 volume=0.502 peak=5099 ppm1=0.763 ppm2=2.848 assign ( resid 157 and name HD2 ) ( resid 157 and name HG2 ) 3.3 1.6 1.3 volume=0.781 peak=3739 ppm1=3.627 ppm2=1.791 assign ( resid 166 and name HG2 ) ( resid 166 and name HN ) 3.9 2.2 1.6 volume=0.314 peak=3197 ppm1=1.253 ppm2=9.009 assign ( resid 159 and name HN ) ( resid 160 and name HA ) 3.7 1.9 1.5 volume=0.448 peak=1115 ppm1=9.025 ppm2=4.012 assign ( resid 41 and name HN ) ( resid 41 and name HB1 or resid 41 and name HB2 ) 3.5 1.7 1.4 volume=0.635 peak=637 ppm1=8.909 ppm2=1.934 assign ( resid 75 and name HN ) ( resid 76 and name HN ) 3.4 1.7 1.4 volume=0.642 peak=2346 ppm1=7.482 ppm2=6.690 assign ( resid 179 and name HD2# ) ( resid 179 and name HA ) 4.0 2.3 1.6 volume=0.261 peak=4818 ppm1=0.751 ppm2=3.834 assign ( resid 132 and name HN ) ( resid 132 and name HA ) 3.1 1.4 1.3 volume=1.120 peak=1953 ppm1=7.894 ppm2=4.660 assign ( resid 97 and name HG2# ) ( resid 80 and name HN ) 4.2 2.5 1.7 volume=0.183 peak=4881 ppm1=0.218 ppm2=7.560 assign ( resid 67 and name HA ) ( resid 67 and name HB1 ) 3.4 1.7 1.4 volume=0.642 peak=4544 ppm1=3.935 ppm2=2.141 assign ( resid 51 and name HN ) ( resid 51 and name HB1 or resid 51 and name HB2 ) 2.7 1.0 1.1 volume=2.528 peak=317 ppm1=8.427 ppm2=1.763 assign ( resid 197 and name HN ) ( resid 198 and name HN ) 3.3 1.6 1.3 volume=0.761 peak=1681 ppm1=7.990 ppm2=8.713 assign ( resid 41 and name HN ) ( resid 42 and name HN ) 3.6 1.9 1.4 volume=0.475 peak=905 ppm1=8.907 ppm2=8.712 assign ( resid 132 and name HG1# ) ( resid 132 and name HG2# ) 2.8 1.0 1.1 volume=2.425 peak=2471 ppm1=0.543 ppm2=0.936 assign ( resid 153 and name HB2 ) ( resid 127 and name HD1# ) 3.3 1.6 1.3 volume=0.795 peak=2875 ppm1=2.853 ppm2=0.310 assign ( resid 83 and name HN ) ( resid 82 and name HB2 ) 3.3 1.6 1.3 volume=0.808 peak=2437 ppm1=8.507 ppm2=2.441 assign ( resid 136 and name HA ) ( resid 136 and name HB2 ) 2.8 1.1 1.1 volume=2.201 peak=2655 ppm1=3.788 ppm2=1.875 assign ( resid 167 and name HA ) ( resid 168 and name HG2# ) 4.5 2.7 1.5 volume=0.136 peak=3216 ppm1=5.216 ppm2=0.187 assign ( resid 62 and name HA ) ( resid 63 and name HN ) 4.0 2.2 1.6 volume=0.279 peak=2691 ppm1=3.966 ppm2=7.325 assign ( resid 200 and name HN ) ( resid 202 and name HN ) 3.2 1.5 1.3 volume=0.976 peak=1214 ppm1=8.085 ppm2=8.564 assign ( resid 18 and name HB1 ) ( resid 18 and name HN ) 4.2 2.5 1.7 volume=0.199 peak=2661 ppm1=2.971 ppm2=7.802 assign ( resid 35 and name HN ) ( resid 30 and name HN ) 4.0 2.2 1.6 volume=0.280 peak=864 ppm1=9.430 ppm2=8.696 assign ( resid 103 and name HG2# ) ( resid 103 and name HA ) 3.9 2.2 1.6 volume=0.284 peak=2569 ppm1=0.878 ppm2=3.628 assign ( resid 167 and name HN ) ( resid 155 and name HA ) 4.1 2.3 1.6 volume=0.237 peak=1694 ppm1=8.643 ppm2=5.256 assign ( resid 205 and name HB# ) ( resid 205 and name HN ) 2.9 1.2 1.2 volume=1.653 peak=4492 ppm1=1.295 ppm2=7.177 assign ( resid 128 and name HN ) ( resid 128 and name HA ) 3.4 1.7 1.4 volume=0.705 peak=450 ppm1=9.934 ppm2=5.575 assign ( resid 72 and name HN ) ( resid 72 and name HG12 ) 3.2 1.5 1.3 volume=1.019 peak=549 ppm1=7.536 ppm2=1.011 assign ( resid 179 and name HB2 ) ( resid 179 and name HB1 ) 2.9 1.1 1.1 volume=1.942 peak=2790 ppm1=2.493 ppm2=2.752 assign ( resid 204 and name HG2 ) ( resid 204 and name HE2 ) 3.9 2.2 1.6 volume=0.309 peak=4467 ppm1=1.295 ppm2=2.840 assign ( resid 168 and name HG1# ) ( resid 51 and name HG2 ) 2.4 0.7 1.0 volume=5.104 peak=4342 ppm1=0.768 ppm2=1.947 assign ( resid 3 and name HZ ) ( resid 3 and name HD1 or resid 3 and name HD2 ) 3.8 2.1 1.5 volume=0.359 peak=145 ppm1=6.204 ppm2=7.378 assign ( resid 120 and name HN ) ( resid 119 and name HG2 or resid 119 and name HG1 ) 3.3 1.6 1.3 volume=0.764 peak=856 ppm1=8.911 ppm2=1.279 assign ( resid 204 and name HN ) ( resid 206 and name HN ) 3.9 2.2 1.6 volume=0.301 peak=2195 ppm1=6.748 ppm2=7.455 assign ( resid 72 and name HG12 ) ( resid 71 and name HD2 or resid 71 and name HD1 ) 4.1 2.3 1.6 volume=0.240 peak=3988 ppm1=1.038 ppm2=2.739 assign ( resid 112 and name HG2# ) ( resid 93 and name HD1# ) 3.5 1.8 1.4 volume=0.572 peak=3576 ppm1=0.680 ppm2=-0.268 assign ( resid 93 and name HG2# ) ( resid 113 and name HN ) 4.3 2.6 1.7 volume=0.163 peak=2727 ppm1=-0.013 ppm2=8.273 assign ( resid 147 and name HN ) ( resid 147 and name HD1 or resid 147 and name HD2 ) 3.4 1.7 1.4 volume=0.683 peak=513 ppm1=8.785 ppm2=6.219 assign ( resid 93 and name HD1# ) ( resid 85 and name HB1 or resid 85 and name HB2 ) 3.4 1.7 1.4 volume=0.653 peak=4920 ppm1=-0.273 ppm2=3.053 assign ( resid 137 and name HN ) ( resid 135 and name HA ) 3.3 1.6 1.3 volume=0.849 peak=1330 ppm1=8.051 ppm2=4.150 assign ( resid 53 and name HN ) ( resid 52 and name HA2 ) 3.0 1.2 1.2 volume=1.605 peak=1415 ppm1=8.307 ppm2=4.515 assign ( resid 130 and name HB1 ) ( resid 130 and name HA ) 4.4 2.7 1.6 volume=0.147 peak=4066 ppm1=1.887 ppm2=3.889 assign ( resid 125 and name HN ) ( resid 126 and name HN ) 3.4 1.6 1.3 volume=0.755 peak=1247 ppm1=8.772 ppm2=9.090 assign ( resid 190 and name HB2 ) ( resid 190 and name HN ) 3.6 1.8 1.4 volume=0.532 peak=3748 ppm1=3.883 ppm2=7.478 assign ( resid 142 and name HB2 ) ( resid 142 and name HB1 ) 3.5 1.8 1.4 volume=0.544 peak=3022 ppm1=1.841 ppm2=1.882 assign ( resid 100 and name HN ) ( resid 99 and name HG2 ) 4.0 2.3 1.6 volume=0.273 peak=974 ppm1=8.396 ppm2=2.449 assign ( resid 136 and name HB1 ) ( resid 134 and name HE1 or resid 134 and name HE2 ) 3.8 2.0 1.5 volume=0.384 peak=2551 ppm1=1.744 ppm2=7.141 assign ( resid 112 and name HG2# ) ( resid 134 and name HE1 or resid 134 and name HE2 ) 3.2 1.5 1.3 volume=0.975 peak=4683 ppm1=0.680 ppm2=7.155 assign ( resid 208 and name HA ) ( resid 208 and name HG2# ) 3.5 1.8 1.4 volume=0.593 peak=3448 ppm1=4.406 ppm2=1.136 assign ( resid 114 and name HD1# ) ( resid 93 and name HD1# ) 3.3 1.6 1.3 volume=0.807 peak=3274 ppm1=0.537 ppm2=-0.271 assign ( resid 90 and name HN ) ( resid 91 and name HA ) 4.0 2.2 1.6 volume=0.279 peak=2166 ppm1=8.382 ppm2=5.835 assign ( resid 17 and name HD1 or resid 17 and name HD2 ) ( resid 17 and name HN ) 3.6 1.9 1.4 volume=0.505 peak=111 ppm1=6.484 ppm2=7.627 assign ( resid 36 and name HN ) ( resid 35 and name HN ) 3.7 2.0 1.5 volume=0.420 peak=1508 ppm1=9.877 ppm2=9.353 assign ( resid 78 and name HN ) ( resid 76 and name HN ) 3.4 1.7 1.4 volume=0.709 peak=1121 ppm1=7.147 ppm2=6.738 assign ( resid 166 and name HD1 ) ( resid 166 and name HE2 ) 3.6 1.9 1.5 volume=0.465 peak=3829 ppm1=1.469 ppm2=2.708 assign ( resid 203 and name HD1# ) ( resid 203 and name HA ) 3.2 1.5 1.3 volume=0.925 peak=2642 ppm1=-0.010 ppm2=2.846 assign ( resid 210 and name HN ) ( resid 210 and name HA ) 4.0 2.2 1.6 volume=0.276 peak=2085 ppm1=8.308 ppm2=4.264 assign ( resid 153 and name HN ) ( resid 154 and name HA ) 3.8 2.0 1.5 volume=0.378 peak=203 ppm1=9.330 ppm2=4.659 assign ( resid 173 and name HN ) ( resid 171 and name HG2# ) 3.7 2.0 1.5 volume=0.389 peak=677 ppm1=8.519 ppm2=0.812 assign ( resid 40 and name HN ) ( resid 40 and name HA ) 3.3 1.6 1.3 volume=0.873 peak=1030 ppm1=8.509 ppm2=4.003 assign ( resid 146 and name HN ) ( resid 145 and name HA ) 3.3 1.6 1.3 volume=0.840 peak=1539 ppm1=8.400 ppm2=4.922 assign ( resid 91 and name HG2# ) ( resid 8 and name HN ) 3.7 2.0 1.5 volume=0.400 peak=3494 ppm1=1.017 ppm2=7.613 assign ( resid 86 and name HA ) ( resid 86 and name HG2 ) 3.1 1.4 1.2 volume=1.246 peak=3781 ppm1=4.286 ppm2=1.459 assign ( resid 205 and name HB# ) ( resid 204 and name HN ) 2.8 1.1 1.1 volume=2.309 peak=4561 ppm1=1.296 ppm2=6.772 assign ( resid 71 and name HD1 ) ( resid 96 and name HG2# ) 3.0 1.3 1.2 volume=1.535 peak=3558 ppm1=2.780 ppm2=1.155 assign ( resid 93 and name HN ) ( resid 85 and name HN ) 3.5 1.8 1.4 volume=0.550 peak=1006 ppm1=8.905 ppm2=7.147 assign ( resid 29 and name HA ) ( resid 28 and name HB1 or resid 28 and name HB2 ) 5.0 3.3 1.0 volume=0.071 peak=3323 ppm1=5.251 ppm2=1.881 assign ( resid 72 and name HG11 ) ( resid 72 and name HG12 ) 3.1 1.4 1.2 volume=1.155 peak=4769 ppm1=1.171 ppm2=1.035 assign ( resid 167 and name HD1# ) ( resid 168 and name HN ) 3.4 1.6 1.3 volume=0.745 peak=3251 ppm1=0.764 ppm2=8.647 assign ( resid 3 and name HD1 or resid 3 and name HD2 ) ( resid 93 and name HD1# ) 3.5 1.7 1.4 volume=0.624 peak=128 ppm1=7.379 ppm2=-0.268 assign ( resid 3 and name HN ) ( resid 5 and name HN ) 3.4 1.6 1.3 volume=0.745 peak=1018 ppm1=7.919 ppm2=7.445 assign ( resid 6 and name HG11 ) ( resid 6 and name HA ) 4.2 2.4 1.7 volume=0.205 peak=5159 ppm1=1.056 ppm2=3.622 assign ( resid 71 and name HN ) ( resid 78 and name HD1# ) 3.2 1.5 1.3 volume=1.043 peak=1463 ppm1=7.218 ppm2=0.496 assign ( resid 114 and name HD1# ) ( resid 93 and name HN ) 3.8 2.1 1.5 volume=0.335 peak=3488 ppm1=0.536 ppm2=8.921 assign ( resid 159 and name HB2 or resid 159 and name HB1 ) ( resid 159 and name HN ) 4.0 2.3 1.6 volume=0.250 peak=3010 ppm1=1.876 ppm2=9.018 assign ( resid 6 and name HG11 ) ( resid 6 and name HN ) 4.0 2.3 1.6 volume=0.252 peak=4897 ppm1=1.058 ppm2=7.729 assign ( resid 42 and name HA ) ( resid 42 and name HN ) 4.0 2.2 1.6 volume=0.281 peak=4770 ppm1=4.137 ppm2=8.706 assign ( resid 73 and name HN ) ( resid 73 and name HG2# ) 2.7 1.0 1.1 volume=2.637 peak=2408 ppm1=7.504 ppm2=1.200 assign ( resid 2 and name HN ) ( resid 3 and name HN ) 3.2 1.5 1.3 volume=0.948 peak=1727 ppm1=8.188 ppm2=7.910 assign ( resid 5 and name HN ) ( resid 4 and name HN ) 2.9 1.2 1.2 volume=1.689 peak=2444 ppm1=7.460 ppm2=8.175 assign ( resid 204 and name HA ) ( resid 204 and name HB1 ) 2.8 1.1 1.1 volume=2.030 peak=4171 ppm1=3.803 ppm2=1.707 assign ( resid 114 and name HD2# ) ( resid 114 and name HA ) 4.3 2.6 1.7 volume=0.164 peak=4500 ppm1=0.782 ppm2=4.449 assign ( resid 6 and name HN ) ( resid 5 and name HA ) 3.5 1.8 1.4 volume=0.553 peak=2289 ppm1=7.720 ppm2=4.025 assign ( resid 200 and name HA ) ( resid 200 and name HB1 ) 3.5 1.8 1.4 volume=0.614 peak=3929 ppm1=3.361 ppm2=1.669 assign ( resid 199 and name HN ) ( resid 199 and name HA ) 3.2 1.5 1.3 volume=0.925 peak=2114 ppm1=8.633 ppm2=2.788 assign ( resid 102 and name HB# ) ( resid 183 and name HD1# ) 2.8 1.1 1.1 volume=2.359 peak=4658 ppm1=1.279 ppm2=0.883 assign ( resid 129 and name HB1 ) ( resid 115 and name HG2# ) 3.7 2.0 1.5 volume=0.410 peak=2567 ppm1=3.366 ppm2=0.648 assign ( resid 6 and name HN ) ( resid 8 and name HG1 ) 3.8 2.1 1.5 volume=0.367 peak=1897 ppm1=7.722 ppm2=2.312 assign ( resid 12 and name HN ) ( resid 10 and name HN ) 3.3 1.6 1.3 volume=0.820 peak=2368 ppm1=7.546 ppm2=8.319 assign ( resid 98 and name HN ) ( resid 97 and name HG2# ) 3.0 1.3 1.2 volume=1.399 peak=1101 ppm1=9.356 ppm2=0.230 assign ( resid 53 and name HN ) ( resid 53 and name HG2# ) 3.0 1.3 1.2 volume=1.527 peak=1361 ppm1=8.307 ppm2=0.886 assign ( resid 213 and name HN ) ( resid 212 and name HG1 ) 4.4 2.7 1.6 volume=0.148 peak=782 ppm1=8.276 ppm2=1.534 assign ( resid 147 and name HB1 ) ( resid 147 and name HN ) 3.9 2.2 1.6 volume=0.296 peak=3260 ppm1=2.632 ppm2=8.779 assign ( resid 71 and name HG2 ) ( resid 71 and name HD1 ) 4.3 2.6 1.7 volume=0.176 peak=3904 ppm1=0.317 ppm2=2.776 assign ( resid 76 and name HA ) ( resid 76 and name HG2 ) 4.2 2.5 1.7 volume=0.188 peak=2734 ppm1=4.123 ppm2=1.370 assign ( resid 7 and name HB# ) ( resid 8 and name HB2 or resid 8 and name HB1 ) 3.6 1.8 1.4 volume=0.520 peak=4704 ppm1=0.752 ppm2=2.041 assign ( resid 64 and name HN ) ( resid 65 and name HB1 or resid 65 and name HB2 ) 3.2 1.5 1.3 volume=1.020 peak=2377 ppm1=7.878 ppm2=1.662 assign ( resid 126 and name HG11 ) ( resid 126 and name HB ) 3.6 1.9 1.5 volume=0.469 peak=3521 ppm1=1.079 ppm2=1.572 assign ( resid 13 and name HN ) ( resid 13 and name HB2 ) 2.8 1.0 1.1 volume=2.462 peak=2321 ppm1=7.727 ppm2=1.897 assign ( resid 144 and name HA ) ( resid 146 and name HN ) 4.0 2.3 1.6 volume=0.270 peak=4331 ppm1=3.987 ppm2=8.458 assign ( resid 42 and name HB2 or resid 42 and name HB1 ) ( resid 42 and name HG1 or resid 42 and name HG2 ) 2.8 1.1 1.1 volume=2.336 peak=2530 ppm1=1.666 ppm2=1.286 assign ( resid 73 and name HA ) ( resid 73 and name HN ) 4.2 2.5 1.7 volume=0.199 peak=2737 ppm1=3.920 ppm2=7.501 assign ( resid 117 and name HN ) ( resid 118 and name HB1 or resid 118 and name HB2 ) 4.0 2.3 1.6 volume=0.260 peak=2051 ppm1=8.230 ppm2=2.453 assign ( resid 154 and name HG2# ) ( resid 126 and name HB ) 2.9 1.1 1.1 volume=1.971 peak=2811 ppm1=0.836 ppm2=1.551 assign ( resid 71 and name HD2 ) ( resid 67 and name HA ) 3.9 2.2 1.6 volume=0.287 peak=5092 ppm1=2.780 ppm2=3.958 assign ( resid 112 and name HG12 ) ( resid 112 and name HG11 ) 2.4 0.7 1.0 volume=5.641 peak=3677 ppm1=1.250 ppm2=1.562 assign ( resid 4 and name HN ) ( resid 1 and name HB1 or resid 1 and name HB2 ) 2.7 0.9 1.1 volume=3.004 peak=511 ppm1=8.189 ppm2=2.046 assign ( resid 6 and name HA ) ( resid 5 and name HA ) 4.2 2.5 1.7 volume=0.192 peak=4943 ppm1=3.618 ppm2=4.013 assign ( resid 183 and name HA ) ( resid 183 and name HD1# ) 2.7 1.0 1.1 volume=2.675 peak=5155 ppm1=3.917 ppm2=0.863 assign ( resid 36 and name HN ) ( resid 49 and name HB1 ) 3.7 2.0 1.5 volume=0.420 peak=2139 ppm1=9.880 ppm2=1.764 assign ( resid 6 and name HD1# ) ( resid 132 and name HG1# ) 3.1 1.4 1.2 volume=1.246 peak=3548 ppm1=0.794 ppm2=0.528 assign ( resid 169 and name HB2 ) ( resid 169 and name HG1 ) 4.1 2.4 1.6 volume=0.218 peak=2835 ppm1=1.787 ppm2=2.003 assign ( resid 64 and name HZ ) ( resid 65 and name HD2# ) 3.2 1.5 1.3 volume=0.988 peak=137 ppm1=7.052 ppm2=0.339 assign ( resid 169 and name HN ) ( resid 154 and name HG2# ) 3.5 1.8 1.4 volume=0.566 peak=1370 ppm1=9.257 ppm2=0.871 assign ( resid 184 and name HA ) ( resid 184 and name HG2# ) 3.0 1.3 1.2 volume=1.531 peak=3042 ppm1=3.629 ppm2=1.094 assign ( resid 34 and name HB ) ( resid 35 and name HN ) 4.9 3.2 1.1 volume=0.079 peak=3541 ppm1=3.828 ppm2=9.430 assign ( resid 53 and name HD1# ) ( resid 166 and name HE1 ) 2.8 1.1 1.1 volume=2.073 peak=2824 ppm1=0.795 ppm2=2.719 assign ( resid 197 and name HN ) ( resid 197 and name HB2 ) 2.9 1.2 1.2 volume=1.820 peak=2135 ppm1=7.988 ppm2=1.792 assign ( resid 202 and name HN ) ( resid 64 and name HE1 or resid 64 and name HE2 ) 4.1 2.4 1.6 volume=0.222 peak=1163 ppm1=8.575 ppm2=6.489 assign ( resid 64 and name HA ) ( resid 64 and name HN ) 3.8 2.0 1.5 volume=0.377 peak=4372 ppm1=3.862 ppm2=7.878 assign ( resid 83 and name HG1 ) ( resid 92 and name HB1 ) 4.6 2.9 1.4 volume=0.111 peak=2668 ppm1=1.722 ppm2=3.052 assign ( resid 15 and name HA ) ( resid 15 and name HD2# ) 3.6 1.9 1.4 volume=0.479 peak=2677 ppm1=3.674 ppm2=0.682 assign ( resid 54 and name HD1# ) ( resid 52 and name HN ) 3.8 2.1 1.5 volume=0.344 peak=4503 ppm1=0.492 ppm2=8.613 assign ( resid 130 and name HN ) ( resid 10 and name HG2# ) 3.5 1.7 1.4 volume=0.616 peak=686 ppm1=7.617 ppm2=1.093 assign ( resid 106 and name HG2# ) ( resid 106 and name HG12 ) 3.0 1.3 1.2 volume=1.369 peak=4380 ppm1=0.897 ppm2=1.389 assign ( resid 34 and name HG2# ) ( resid 26 and name HG2# ) 2.3 0.6 0.9 volume=7.461 peak=4433 ppm1=1.100 ppm2=0.908 assign ( resid 86 and name HD1 ) ( resid 86 and name HA ) 3.1 1.3 1.2 volume=1.334 peak=5007 ppm1=2.928 ppm2=4.286 assign ( resid 15 and name HB1 ) ( resid 15 and name HN ) 4.0 2.3 1.6 volume=0.271 peak=2912 ppm1=1.710 ppm2=7.808 assign ( resid 124 and name HN ) ( resid 124 and name HB2 or resid 124 and name HB1 ) 2.8 1.1 1.1 volume=2.233 peak=1748 ppm1=6.472 ppm2=2.044 assign ( resid 208 and name HA ) ( resid 210 and name HB2 or resid 210 and name HB1 ) 4.1 2.4 1.6 volume=0.226 peak=5011 ppm1=4.406 ppm2=3.767 assign ( resid 43 and name HN ) ( resid 41 and name HB1 ) 3.4 1.6 1.3 volume=0.755 peak=1446 ppm1=7.302 ppm2=1.981 assign ( resid 199 and name HN ) ( resid 197 and name HA ) 3.9 2.2 1.6 volume=0.294 peak=224 ppm1=8.632 ppm2=3.743 assign ( resid 45 and name HN ) ( resid 43 and name HN ) 2.8 1.1 1.1 volume=2.256 peak=1653 ppm1=6.654 ppm2=7.325 assign ( resid 153 and name HB2 ) ( resid 153 and name HA ) 4.5 2.8 1.5 volume=0.124 peak=3539 ppm1=2.854 ppm2=5.323 assign ( resid 41 and name HG2 or resid 41 and name HG1 ) ( resid 41 and name HD2 or resid 41 and name HD1 ) 2.8 1.1 1.1 volume=2.147 peak=5115 ppm1=1.539 ppm2=3.086 assign ( resid 134 and name HN ) ( resid 133 and name HA ) 3.8 2.1 1.5 volume=0.356 peak=654 ppm1=8.745 ppm2=4.675 assign ( resid 203 and name HG12 ) ( resid 203 and name HN ) 4.4 2.7 1.6 volume=0.150 peak=3167 ppm1=0.516 ppm2=7.705 assign ( resid 83 and name HG1 ) ( resid 92 and name HE1 or resid 92 and name HE2 ) 3.8 2.1 1.5 volume=0.363 peak=4063 ppm1=1.727 ppm2=6.750 assign ( resid 72 and name HG11 ) ( resid 71 and name HD2 or resid 71 and name HD1 ) 3.8 2.1 1.5 volume=0.350 peak=3932 ppm1=1.172 ppm2=2.731 assign ( resid 187 and name HG2# ) ( resid 187 and name HA ) 3.5 1.8 1.4 volume=0.584 peak=4199 ppm1=1.057 ppm2=4.281 assign ( resid 153 and name HN ) ( resid 154 and name HB ) 3.7 2.0 1.5 volume=0.387 peak=791 ppm1=9.329 ppm2=2.186 assign ( resid 8 and name HB2 or resid 8 and name HB1 ) ( resid 8 and name HG1 or resid 8 and name HG2 ) 2.5 0.8 1.0 volume=4.394 peak=4120 ppm1=2.048 ppm2=2.324 assign ( resid 186 and name HN ) ( resid 186 and name HB2 ) 2.3 0.6 0.9 volume=6.403 peak=2183 ppm1=7.370 ppm2=1.926 assign ( resid 10 and name HG2# ) ( resid 128 and name HA ) 3.8 2.1 1.5 volume=0.335 peak=5034 ppm1=1.083 ppm2=5.612 assign ( resid 3 and name HZ ) ( resid 134 and name HE1 or resid 134 and name HE2 ) 3.8 2.1 1.5 volume=0.373 peak=44 ppm1=6.204 ppm2=7.177 assign ( resid 113 and name HN ) ( resid 112 and name HA ) 2.9 1.2 1.2 volume=1.629 peak=1985 ppm1=8.232 ppm2=4.962 assign ( resid 154 and name HN ) ( resid 153 and name HA ) 3.0 1.3 1.2 volume=1.429 peak=2205 ppm1=10.005 ppm2=5.309 assign ( resid 36 and name HN ) ( resid 36 and name HA ) 3.8 2.1 1.5 volume=0.341 peak=1321 ppm1=9.877 ppm2=5.831 assign ( resid 121 and name HB1 ) ( resid 121 and name HB2 ) 3.4 1.7 1.4 volume=0.710 peak=3359 ppm1=2.051 ppm2=1.968 assign ( resid 192 and name HN ) ( resid 189 and name HA ) 2.7 1.0 1.1 volume=2.858 peak=1706 ppm1=8.208 ppm2=4.659 assign ( resid 144 and name HN ) ( resid 110 and name HB2 ) 3.7 2.0 1.5 volume=0.422 peak=2167 ppm1=7.538 ppm2=2.965 assign ( resid 67 and name HB2 ) ( resid 67 and name HA ) 2.9 1.2 1.1 volume=1.913 peak=4464 ppm1=2.066 ppm2=3.956 assign ( resid 117 and name HB ) ( resid 117 and name HG12 ) 4.0 2.3 1.6 volume=0.254 peak=3952 ppm1=1.037 ppm2=0.650 assign ( resid 87 and name HN ) ( resid 87 and name HG11 ) 3.6 1.9 1.4 volume=0.491 peak=304 ppm1=8.039 ppm2=1.269 assign ( resid 184 and name HA ) ( resid 184 and name HN ) 3.9 2.2 1.6 volume=0.293 peak=4200 ppm1=3.628 ppm2=7.503 assign ( resid 167 and name HB2 ) ( resid 196 and name HD1# ) 3.5 1.8 1.4 volume=0.614 peak=4719 ppm1=1.678 ppm2=0.740 assign ( resid 155 and name HN ) ( resid 126 and name HB ) 3.3 1.6 1.3 volume=0.760 peak=2054 ppm1=8.976 ppm2=1.540 assign ( resid 129 and name HB1 ) ( resid 113 and name HB1 ) 4.0 2.3 1.6 volume=0.259 peak=3427 ppm1=3.369 ppm2=2.006 assign ( resid 155 and name HA ) ( resid 167 and name HD2# ) 4.3 2.5 1.7 volume=0.180 peak=3102 ppm1=5.265 ppm2=0.766 assign ( resid 110 and name HN ) ( resid 144 and name HN ) 3.4 1.7 1.4 volume=0.700 peak=1210 ppm1=8.721 ppm2=7.519 assign ( resid 193 and name HG1# ) ( resid 193 and name HN ) 4.4 2.7 1.6 volume=0.141 peak=4910 ppm1=0.788 ppm2=7.629 assign ( resid 203 and name HG2# ) ( resid 201 and name HN ) 4.3 2.5 1.7 volume=0.181 peak=3644 ppm1=0.340 ppm2=7.416 assign ( resid 21 and name HG2# ) ( resid 24 and name HH2 ) 3.8 2.0 1.5 volume=0.377 peak=4104 ppm1=1.149 ppm2=6.772 assign ( resid 84 and name HB ) ( resid 134 and name HZ ) 3.8 2.1 1.5 volume=0.358 peak=2498 ppm1=1.995 ppm2=6.632 assign ( resid 8 and name HG1 or resid 8 and name HG2 ) ( resid 8 and name HN ) 3.4 1.6 1.3 volume=0.755 peak=2709 ppm1=2.321 ppm2=7.610 assign ( resid 112 and name HB ) ( resid 112 and name HG12 ) 4.0 2.3 1.6 volume=0.270 peak=3390 ppm1=2.171 ppm2=1.238 assign ( resid 20 and name HN ) ( resid 20 and name HA ) 2.7 1.0 1.1 volume=2.500 peak=1933 ppm1=7.405 ppm2=4.661 assign ( resid 59 and name HN ) ( resid 62 and name HN ) 3.8 2.0 1.5 volume=0.381 peak=743 ppm1=8.092 ppm2=8.176 assign ( resid 81 and name HN ) ( resid 80 and name HN ) 3.6 1.9 1.5 volume=0.458 peak=1398 ppm1=8.508 ppm2=7.527 assign ( resid 34 and name HA ) ( resid 26 and name HG1# ) 4.4 2.7 1.6 volume=0.149 peak=2850 ppm1=4.966 ppm2=0.767 assign ( resid 121 and name HA ) ( resid 121 and name HB2 ) 4.2 2.5 1.7 volume=0.184 peak=3330 ppm1=4.144 ppm2=1.971 assign ( resid 132 and name HG2# ) ( resid 130 and name HD2 or resid 130 and name HD1 ) 2.9 1.2 1.2 volume=1.754 peak=4217 ppm1=0.937 ppm2=1.680 assign ( resid 47 and name HN ) ( resid 46 and name HB2 ) 4.4 2.7 1.6 volume=0.150 peak=1272 ppm1=8.702 ppm2=2.055 assign ( resid 24 and name HE1 ) ( resid 36 and name HB1 ) 4.0 2.3 1.6 volume=0.253 peak=31 ppm1=7.000 ppm2=3.858 assign ( resid 5 and name HN ) ( resid 5 and name HA ) 2.8 1.1 1.1 volume=2.116 peak=1874 ppm1=7.460 ppm2=4.002 assign ( resid 188 and name HN ) ( resid 187 and name HG2# ) 3.1 1.4 1.2 volume=1.279 peak=911 ppm1=8.441 ppm2=1.015 assign ( resid 26 and name HG1# ) ( resid 26 and name HB ) 2.5 0.8 1.0 volume=4.174 peak=4893 ppm1=0.779 ppm2=1.926 assign ( resid 180 and name HN ) ( resid 179 and name HA ) 2.9 1.2 1.2 volume=1.704 peak=1159 ppm1=8.354 ppm2=3.827 assign ( resid 193 and name HA ) ( resid 35 and name HG1# ) 3.4 1.7 1.4 volume=0.718 peak=4755 ppm1=3.462 ppm2=0.913 assign ( resid 52 and name HN ) ( resid 51 and name HG1 ) 3.1 1.4 1.2 volume=1.256 peak=2405 ppm1=8.614 ppm2=1.963 assign ( resid 191 and name HN ) ( resid 190 and name HN ) 3.0 1.2 1.2 volume=1.582 peak=1559 ppm1=7.651 ppm2=7.525 assign ( resid 84 and name HG2# ) ( resid 85 and name HB2 ) 4.0 2.3 1.6 volume=0.255 peak=4699 ppm1=0.111 ppm2=3.046 assign ( resid 78 and name HN ) ( resid 76 and name HB2 ) 3.5 1.7 1.4 volume=0.617 peak=2257 ppm1=7.148 ppm2=1.996 assign ( resid 53 and name HG2# ) ( resid 54 and name HB ) 3.2 1.4 1.3 volume=1.068 peak=3076 ppm1=0.898 ppm2=1.795 assign ( resid 204 and name HN ) ( resid 203 and name HG2# ) 2.8 1.1 1.1 volume=2.051 peak=2272 ppm1=6.744 ppm2=0.362 assign ( resid 7 and name HN ) ( resid 8 and name HG1 ) 3.4 1.7 1.4 volume=0.663 peak=2243 ppm1=8.433 ppm2=2.309 assign ( resid 188 and name HB2 ) ( resid 187 and name HG2# ) 3.1 1.3 1.2 volume=1.300 peak=2920 ppm1=1.448 ppm2=1.047 assign ( resid 106 and name HB ) ( resid 106 and name HG2# ) 3.2 1.5 1.3 volume=0.968 peak=4748 ppm1=1.793 ppm2=0.889 assign ( resid 191 and name HB2 ) ( resid 191 and name HN ) 4.0 2.3 1.6 volume=0.260 peak=5093 ppm1=2.816 ppm2=7.655 assign ( resid 202 and name HN ) ( resid 205 and name HB# ) 3.7 2.0 1.5 volume=0.423 peak=1458 ppm1=8.576 ppm2=1.267 assign ( resid 190 and name HN ) ( resid 191 and name HN ) 3.1 1.4 1.3 volume=1.122 peak=1341 ppm1=7.521 ppm2=7.655 assign ( resid 87 and name HG2# ) ( resid 87 and name HG11 ) 2.7 1.0 1.1 volume=2.931 peak=3831 ppm1=0.850 ppm2=1.266 assign ( resid 194 and name HB2 ) ( resid 193 and name HG1# ) 3.4 1.6 1.3 volume=0.748 peak=2973 ppm1=2.823 ppm2=0.778 assign ( resid 103 and name HG2# ) ( resid 103 and name HN ) 4.2 2.5 1.7 volume=0.204 peak=5010 ppm1=0.878 ppm2=8.447 assign ( resid 45 and name HN ) ( resid 45 and name HA1 ) 3.7 1.9 1.5 volume=0.453 peak=2314 ppm1=6.655 ppm2=3.631 assign ( resid 166 and name HD1 ) ( resid 166 and name HG1 ) 3.0 1.2 1.2 volume=1.608 peak=3021 ppm1=1.467 ppm2=1.231 assign ( resid 80 and name HN ) ( resid 79 and name HN ) 3.3 1.6 1.3 volume=0.836 peak=2299 ppm1=7.523 ppm2=8.828 assign ( resid 161 and name HN ) ( resid 164 and name HB2 ) 3.6 1.9 1.4 volume=0.485 peak=2427 ppm1=6.905 ppm2=2.987 assign ( resid 73 and name HA ) ( resid 72 and name HA ) 4.9 3.2 1.1 volume=0.073 peak=3432 ppm1=3.920 ppm2=3.635 assign ( resid 198 and name HN ) ( resid 195 and name HN ) 3.4 1.7 1.4 volume=0.654 peak=1385 ppm1=8.717 ppm2=7.946 assign ( resid 16 and name HN ) ( resid 15 and name HB1 ) 3.1 1.4 1.2 volume=1.185 peak=1740 ppm1=7.497 ppm2=1.698 assign ( resid 80 and name HN ) ( resid 81 and name HB1 ) 3.8 2.1 1.5 volume=0.346 peak=1223 ppm1=7.525 ppm2=2.342 assign ( resid 123 and name HN ) ( resid 124 and name HA ) 3.8 2.1 1.5 volume=0.353 peak=1326 ppm1=8.404 ppm2=5.172 assign ( resid 132 and name HG2# ) ( resid 130 and name HB1 ) 2.9 1.2 1.2 volume=1.864 peak=2894 ppm1=0.935 ppm2=1.872 assign ( resid 84 and name HB ) ( resid 134 and name HD1 or resid 134 and name HD2 ) 4.0 2.3 1.6 volume=0.250 peak=4237 ppm1=1.992 ppm2=6.857 assign ( resid 46 and name HN ) ( resid 45 and name HN ) 3.1 1.3 1.2 volume=1.332 peak=2230 ppm1=8.560 ppm2=6.674 assign ( resid 113 and name HN ) ( resid 115 and name HG1# ) 3.2 1.5 1.3 volume=0.926 peak=1890 ppm1=8.232 ppm2=0.264 assign ( resid 196 and name HG12 ) ( resid 197 and name HN ) 4.0 2.3 1.6 volume=0.246 peak=2995 ppm1=1.466 ppm2=8.005 assign ( resid 154 and name HG1# ) ( resid 126 and name HB ) 2.9 1.2 1.2 volume=1.700 peak=4558 ppm1=0.917 ppm2=1.563 assign ( resid 184 and name HB ) ( resid 184 and name HA ) 3.5 1.8 1.4 volume=0.557 peak=4003 ppm1=2.049 ppm2=3.629 assign ( resid 114 and name HD2# ) ( resid 7 and name HN ) 3.4 1.6 1.3 volume=0.734 peak=4932 ppm1=0.781 ppm2=8.460 assign ( resid 76 and name HG1 ) ( resid 76 and name HN ) 3.6 1.9 1.5 volume=0.460 peak=4123 ppm1=1.384 ppm2=6.703 assign ( resid 173 and name HN ) ( resid 171 and name HA ) 3.3 1.5 1.3 volume=0.910 peak=1473 ppm1=8.519 ppm2=4.140 assign ( resid 186 and name HG1 ) ( resid 186 and name HA ) 3.9 2.2 1.6 volume=0.290 peak=3501 ppm1=1.479 ppm2=4.211 assign ( resid 67 and name HN ) ( resid 67 and name HA ) 2.8 1.1 1.1 volume=2.071 peak=1366 ppm1=7.602 ppm2=3.923 assign ( resid 203 and name HA ) ( resid 203 and name HB ) 3.8 2.1 1.5 volume=0.365 peak=2925 ppm1=2.835 ppm2=0.126 assign ( resid 80 and name HN ) ( resid 97 and name HN ) 3.4 1.6 1.3 volume=0.743 peak=1805 ppm1=7.523 ppm2=8.361 assign ( resid 22 and name HN ) ( resid 38 and name HD2 ) 3.0 1.3 1.2 volume=1.420 peak=1659 ppm1=8.193 ppm2=1.009 assign ( resid 92 and name HE1 or resid 92 and name HE2 ) ( resid 92 and name HN ) 4.2 2.5 1.7 volume=0.186 peak=48 ppm1=6.750 ppm2=9.460 assign ( resid 132 and name HG2# ) ( resid 132 and name HG1# ) 2.7 1.0 1.1 volume=2.727 peak=4425 ppm1=0.936 ppm2=0.540 assign ( resid 159 and name HB2 or resid 159 and name HB1 ) ( resid 161 and name HN ) 4.1 2.3 1.6 volume=0.241 peak=4121 ppm1=1.877 ppm2=6.959 assign ( resid 137 and name HB2 ) ( resid 136 and name HG1 ) 4.5 2.8 1.5 volume=0.132 peak=3411 ppm1=2.575 ppm2=2.002 assign ( resid 199 and name HB# ) ( resid 203 and name HN ) 3.8 2.0 1.5 volume=0.374 peak=2537 ppm1=0.693 ppm2=7.674 assign ( resid 3 and name HD1 or resid 3 and name HD2 ) ( resid 134 and name HD1 or resid 134 and name HD2 ) 4.0 2.3 1.6 volume=0.244 peak=11 ppm1=7.379 ppm2=6.859 assign ( resid 155 and name HN ) ( resid 126 and name HG2# ) 3.0 1.3 1.2 volume=1.490 peak=1198 ppm1=8.976 ppm2=0.754 assign ( resid 72 and name HN ) ( resid 72 and name HB ) 3.3 1.6 1.3 volume=0.842 peak=1687 ppm1=7.535 ppm2=1.820 assign ( resid 93 and name HN ) ( resid 93 and name HB ) 3.5 1.8 1.4 volume=0.576 peak=2260 ppm1=8.904 ppm2=1.220 assign ( resid 147 and name HN ) ( resid 176 and name HG1 ) 3.3 1.6 1.3 volume=0.761 peak=1098 ppm1=8.783 ppm2=1.665 assign ( resid 71 and name HN ) ( resid 71 and name HD2 ) 3.4 1.7 1.4 volume=0.701 peak=748 ppm1=7.221 ppm2=2.811 assign ( resid 35 and name HG2# ) ( resid 49 and name HN ) 4.4 2.7 1.6 volume=0.142 peak=4627 ppm1=0.889 ppm2=8.916 assign ( resid 196 and name HG12 ) ( resid 196 and name HN ) 3.7 2.0 1.5 volume=0.429 peak=3181 ppm1=1.467 ppm2=7.466 assign ( resid 128 and name HA ) ( resid 116 and name HN ) 4.3 2.6 1.7 volume=0.163 peak=4345 ppm1=5.580 ppm2=8.795 assign ( resid 72 and name HG2# ) ( resid 71 and name HB2 or resid 71 and name HB1 ) 3.3 1.6 1.3 volume=0.827 peak=4201 ppm1=0.603 ppm2=1.527 assign ( resid 169 and name HN ) ( resid 168 and name HG2# ) 3.5 1.7 1.4 volume=0.630 peak=1275 ppm1=9.257 ppm2=0.228 assign ( resid 106 and name HD1# ) ( resid 179 and name HG ) 2.9 1.1 1.1 volume=1.970 peak=4964 ppm1=0.772 ppm2=1.485 assign ( resid 199 and name HN ) ( resid 195 and name HA ) 3.6 1.8 1.4 volume=0.536 peak=1088 ppm1=8.633 ppm2=4.403 assign ( resid 142 and name HN ) ( resid 141 and name HB1 ) 3.6 1.9 1.4 volume=0.505 peak=843 ppm1=7.900 ppm2=3.752 assign ( resid 187 and name HA ) ( resid 191 and name HN ) 5.2 3.5 0.8 volume=0.056 peak=4548 ppm1=4.263 ppm2=7.634 assign ( resid 15 and name HD1# ) ( resid 15 and name HN ) 3.3 1.6 1.3 volume=0.800 peak=3509 ppm1=0.439 ppm2=7.804 assign ( resid 87 and name HD1# ) ( resid 88 and name HN ) 3.8 2.1 1.5 volume=0.334 peak=3641 ppm1=0.440 ppm2=8.585 assign ( resid 195 and name HN ) ( resid 195 and name HB2 ) 3.1 1.3 1.2 volume=1.311 peak=244 ppm1=7.971 ppm2=3.222 assign ( resid 178 and name HB2 ) ( resid 178 and name HG2 ) 3.7 2.0 1.5 volume=0.431 peak=3604 ppm1=1.666 ppm2=1.295 assign ( resid 84 and name HG2# ) ( resid 136 and name HB1 ) 3.8 2.1 1.5 volume=0.351 peak=2922 ppm1=0.113 ppm2=1.801 assign ( resid 72 and name HG2# ) ( resid 70 and name HN ) 3.5 1.8 1.4 volume=0.571 peak=4274 ppm1=0.602 ppm2=8.575 assign ( resid 143 and name HB2 ) ( resid 143 and name HN ) 3.6 1.9 1.5 volume=0.469 peak=4378 ppm1=2.703 ppm2=6.902 assign ( resid 199 and name HN ) ( resid 198 and name HN ) 3.4 1.7 1.3 volume=0.727 peak=2187 ppm1=8.633 ppm2=8.708 assign ( resid 114 and name HN ) ( resid 132 and name HG1# ) 3.3 1.6 1.3 volume=0.815 peak=2212 ppm1=8.800 ppm2=0.542 assign ( resid 126 and name HG2# ) ( resid 124 and name HB1 ) 3.3 1.6 1.3 volume=0.774 peak=5040 ppm1=0.751 ppm2=2.064 assign ( resid 84 and name HG2# ) ( resid 134 and name HZ ) 3.5 1.8 1.4 volume=0.559 peak=3898 ppm1=0.112 ppm2=6.628 assign ( resid 88 and name HN ) ( resid 87 and name HG11 ) 3.0 1.2 1.2 volume=1.591 peak=2387 ppm1=8.594 ppm2=1.271 assign ( resid 190 and name HN ) ( resid 187 and name HA ) 3.4 1.7 1.4 volume=0.718 peak=374 ppm1=7.519 ppm2=4.266 assign ( resid 165 and name HA ) ( resid 158 and name HG1 ) 4.1 2.3 1.6 volume=0.243 peak=3320 ppm1=5.221 ppm2=2.409 assign ( resid 154 and name HB ) ( resid 124 and name HG2 ) 2.2 0.5 0.9 volume=9.617 peak=2993 ppm1=2.178 ppm2=2.398 assign ( resid 114 and name HD1# ) ( resid 93 and name HG2# ) 4.1 2.4 1.6 volume=0.221 peak=3455 ppm1=0.538 ppm2=-0.010 assign ( resid 57 and name HN ) ( resid 59 and name HB# ) 3.3 1.6 1.3 volume=0.826 peak=1363 ppm1=9.217 ppm2=1.256 assign ( resid 167 and name HA ) ( resid 167 and name HB2 ) 4.6 2.9 1.4 volume=0.115 peak=3938 ppm1=5.218 ppm2=1.675 assign ( resid 50 and name HN ) ( resid 48 and name HB1 ) 4.1 2.4 1.6 volume=0.231 peak=2301 ppm1=9.300 ppm2=2.686 assign ( resid 63 and name HN ) ( resid 61 and name HD2# ) 3.5 1.8 1.4 volume=0.538 peak=2366 ppm1=7.300 ppm2=0.750 assign ( resid 65 and name HA ) ( resid 65 and name HD2# ) 3.4 1.7 1.4 volume=0.715 peak=2469 ppm1=3.888 ppm2=0.320 assign ( resid 157 and name HD2 ) ( resid 122 and name HA1 ) 4.0 2.2 1.6 volume=0.279 peak=2870 ppm1=3.627 ppm2=3.757 assign ( resid 120 and name HN ) ( resid 120 and name HA ) 3.3 1.6 1.3 volume=0.857 peak=1876 ppm1=8.910 ppm2=4.486 assign ( resid 39 and name HN ) ( resid 39 and name HB# ) 2.3 0.6 0.9 volume=6.500 peak=376 ppm1=8.249 ppm2=1.144 assign ( resid 99 and name HA ) ( resid 99 and name HB2 ) 3.0 1.3 1.2 volume=1.522 peak=5049 ppm1=4.284 ppm2=1.787 assign ( resid 14 and name HN ) ( resid 14 and name HB ) 2.8 1.1 1.1 volume=2.129 peak=283 ppm1=7.793 ppm2=1.676 assign ( resid 120 and name HB2 ) ( resid 124 and name HB1 ) 3.6 1.9 1.5 volume=0.471 peak=3542 ppm1=3.001 ppm2=2.077 assign ( resid 151 and name HN ) ( resid 151 and name HA ) 3.8 2.1 1.5 volume=0.353 peak=170 ppm1=8.646 ppm2=4.920 assign ( resid 78 and name HN ) ( resid 79 and name HN ) 4.0 2.2 1.6 volume=0.280 peak=311 ppm1=7.148 ppm2=8.835 assign ( resid 26 and name HN ) ( resid 37 and name HN ) 4.2 2.4 1.7 volume=0.210 peak=1907 ppm1=8.863 ppm2=9.631 assign ( resid 206 and name HN ) ( resid 206 and name HB2 ) 3.2 1.5 1.3 volume=0.998 peak=2153 ppm1=7.464 ppm2=2.963 assign ( resid 84 and name HG1# ) ( resid 95 and name HN ) 3.7 2.0 1.5 volume=0.402 peak=4613 ppm1=0.532 ppm2=9.115 assign ( resid 134 and name HZ ) ( resid 112 and name HD1# ) 2.6 0.9 1.0 volume=3.497 peak=25 ppm1=6.644 ppm2=0.376 assign ( resid 147 and name HN ) ( resid 173 and name HG2# ) 3.6 1.9 1.4 volume=0.499 peak=2009 ppm1=8.784 ppm2=1.006 assign ( resid 159 and name HN ) ( resid 158 and name HG2 ) 3.2 1.5 1.3 volume=1.025 peak=1337 ppm1=9.024 ppm2=2.408 assign ( resid 93 and name HG2# ) ( resid 112 and name HB ) 3.6 1.8 1.4 volume=0.530 peak=3319 ppm1=-0.013 ppm2=2.156 assign ( resid 201 and name HN ) ( resid 200 and name HA ) 3.2 1.5 1.3 volume=0.996 peak=1778 ppm1=7.401 ppm2=3.358 assign ( resid 96 and name HN ) ( resid 96 and name HG2# ) 3.5 1.8 1.4 volume=0.547 peak=881 ppm1=8.473 ppm2=1.141 assign ( resid 106 and name HG12 or resid 106 and name HG11 ) ( resid 179 and name HD2# ) 3.1 1.4 1.2 volume=1.202 peak=3142 ppm1=1.408 ppm2=0.773 assign ( resid 112 and name HG11 ) ( resid 145 and name HB1 or resid 145 and name HB2 ) 3.2 1.5 1.3 volume=1.055 peak=4109 ppm1=1.602 ppm2=1.928 assign ( resid 94 and name HN ) ( resid 113 and name HB1 or resid 113 and name HB2 ) 3.4 1.7 1.4 volume=0.696 peak=394 ppm1=9.599 ppm2=2.057 assign ( resid 36 and name HN ) ( resid 50 and name HA ) 3.5 1.8 1.4 volume=0.580 peak=1262 ppm1=9.878 ppm2=5.181 assign ( resid 35 and name HN ) ( resid 34 and name HN ) 3.9 2.2 1.6 volume=0.286 peak=2097 ppm1=9.430 ppm2=8.179 assign ( resid 166 and name HB1 ) ( resid 167 and name HN ) 4.1 2.4 1.6 volume=0.218 peak=5058 ppm1=1.656 ppm2=8.698 assign ( resid 132 and name HG1# ) ( resid 132 and name HB ) 3.1 1.4 1.3 volume=1.101 peak=3184 ppm1=0.542 ppm2=2.274 assign ( resid 132 and name HN ) ( resid 114 and name HB2 ) 3.7 2.0 1.5 volume=0.391 peak=490 ppm1=7.893 ppm2=1.658 assign ( resid 158 and name HG2 ) ( resid 158 and name HA ) 3.8 2.1 1.5 volume=0.362 peak=2527 ppm1=2.439 ppm2=4.147 assign ( resid 129 and name HB1 ) ( resid 152 and name HA1 ) 4.2 2.5 1.7 volume=0.193 peak=3564 ppm1=3.368 ppm2=3.708 assign ( resid 160 and name HB2 ) ( resid 160 and name HN ) 4.5 2.7 1.5 volume=0.138 peak=4037 ppm1=2.035 ppm2=8.837 assign ( resid 146 and name HN ) ( resid 146 and name HA1 ) 3.5 1.7 1.4 volume=0.620 peak=971 ppm1=8.400 ppm2=4.008 assign ( resid 70 and name HN ) ( resid 70 and name HA ) 2.8 1.1 1.1 volume=2.077 peak=2069 ppm1=8.575 ppm2=4.847 assign ( resid 121 and name HG1 ) ( resid 121 and name HN ) 4.4 2.6 1.6 volume=0.158 peak=2941 ppm1=2.310 ppm2=8.581 assign ( resid 84 and name HB ) ( resid 84 and name HN ) 4.2 2.5 1.7 volume=0.189 peak=5105 ppm1=1.994 ppm2=8.526 assign ( resid 37 and name HB1 or resid 37 and name HB2 ) ( resid 35 and name HG2# or resid 35 and name HG1# ) 4.1 2.4 1.6 volume=0.230 peak=3268 ppm1=3.287 ppm2=0.905 assign ( resid 168 and name HN ) ( resid 156 and name HN ) 3.8 2.1 1.5 volume=0.361 peak=457 ppm1=8.694 ppm2=8.576 assign ( resid 165 and name HA ) ( resid 58 and name HG1 ) 3.6 1.9 1.4 volume=0.476 peak=2897 ppm1=5.220 ppm2=1.778 assign ( resid 49 and name HN ) ( resid 49 and name HG1 or resid 49 and name HG2 ) 3.5 1.8 1.4 volume=0.580 peak=2335 ppm1=8.914 ppm2=1.536 assign ( resid 34 and name HG2# ) ( resid 28 and name HN ) 3.5 1.7 1.4 volume=0.624 peak=3161 ppm1=1.101 ppm2=7.809 assign ( resid 106 and name HD1# ) ( resid 106 and name HB ) 2.9 1.2 1.2 volume=1.870 peak=2749 ppm1=0.768 ppm2=1.760 assign ( resid 175 and name HB1 ) ( resid 179 and name HD2# ) 2.8 1.1 1.1 volume=2.101 peak=3606 ppm1=2.450 ppm2=0.777 assign ( resid 94 and name HN ) ( resid 113 and name HN ) 4.2 2.5 1.7 volume=0.200 peak=319 ppm1=9.599 ppm2=8.232 assign ( resid 202 and name HN ) ( resid 198 and name HB1 ) 3.1 1.4 1.3 volume=1.147 peak=1025 ppm1=8.576 ppm2=3.101 assign ( resid 166 and name HD2 ) ( resid 166 and name HB1 ) 3.4 1.7 1.4 volume=0.655 peak=4158 ppm1=1.428 ppm2=1.668 assign ( resid 159 and name HN ) ( resid 158 and name HA ) 2.8 1.1 1.1 volume=2.374 peak=1534 ppm1=9.022 ppm2=4.137 assign ( resid 38 and name HN ) ( resid 46 and name HB2 ) 3.7 1.9 1.5 volume=0.448 peak=391 ppm1=8.466 ppm2=2.056 assign ( resid 61 and name HD1# ) ( resid 54 and name HB ) 2.4 0.7 1.0 volume=5.601 peak=4002 ppm1=0.746 ppm2=1.779 assign ( resid 1 and name HN# ) ( resid 2 and name HA ) 3.6 1.9 1.4 volume=0.487 peak=811 ppm1=8.201 ppm2=4.144 assign ( resid 39 and name HA ) ( resid 40 and name HN ) 3.7 2.0 1.5 volume=0.420 peak=2822 ppm1=4.141 ppm2=8.524 assign ( resid 132 and name HG1# ) ( resid 93 and name HG2# ) 3.5 1.8 1.4 volume=0.565 peak=3038 ppm1=0.544 ppm2=-0.012 assign ( resid 7 and name HB# ) ( resid 4 and name HG1 or resid 4 and name HG2 ) 3.3 1.6 1.3 volume=0.771 peak=2947 ppm1=0.752 ppm2=1.382 assign ( resid 18 and name HN ) ( resid 19 and name HD1 or resid 19 and name HD2 ) 3.0 1.3 1.2 volume=1.358 peak=1015 ppm1=7.765 ppm2=2.986 assign ( resid 94 and name HN ) ( resid 93 and name HG2# ) 3.2 1.5 1.3 volume=0.966 peak=300 ppm1=9.604 ppm2=-0.025 assign ( resid 179 and name HN ) ( resid 179 and name HA ) 2.6 0.9 1.1 volume=3.112 peak=1618 ppm1=7.303 ppm2=3.876 assign ( resid 67 and name HN ) ( resid 66 and name HB1 ) 3.1 1.4 1.2 volume=1.213 peak=1233 ppm1=7.603 ppm2=3.103 assign ( resid 54 and name HG2# ) ( resid 55 and name HD1 or resid 55 and name HD2 ) 3.2 1.5 1.3 volume=0.996 peak=3889 ppm1=0.576 ppm2=3.374 assign ( resid 123 and name HA ) ( resid 120 and name HB2 ) 3.9 2.2 1.6 volume=0.293 peak=4083 ppm1=4.351 ppm2=2.986 assign ( resid 161 and name HN ) ( resid 162 and name HD2 ) 3.2 1.5 1.3 volume=1.056 peak=2428 ppm1=6.905 ppm2=3.472 assign ( resid 190 and name HA ) ( resid 190 and name HN ) 3.6 1.9 1.4 volume=0.480 peak=5121 ppm1=3.979 ppm2=7.526 assign ( resid 60 and name HN ) ( resid 59 and name HN ) 3.5 1.8 1.4 volume=0.552 peak=1644 ppm1=7.266 ppm2=8.069 assign ( resid 187 and name HG2# ) ( resid 188 and name HE# ) 4.7 3.0 1.3 volume=0.098 peak=4768 ppm1=1.062 ppm2=1.880 assign ( resid 93 and name HN ) ( resid 87 and name HD1# ) 3.8 2.1 1.5 volume=0.363 peak=1956 ppm1=8.904 ppm2=0.440 assign ( resid 132 and name HB ) ( resid 114 and name HD2# ) 3.5 1.8 1.4 volume=0.593 peak=3864 ppm1=2.283 ppm2=0.772 assign ( resid 64 and name HA ) ( resid 63 and name HB2 or resid 63 and name HB1 ) 3.5 1.8 1.4 volume=0.608 peak=3574 ppm1=3.859 ppm2=2.663 assign ( resid 186 and name HA ) ( resid 186 and name HB1 ) 2.9 1.2 1.2 volume=1.725 peak=3031 ppm1=4.212 ppm2=1.868 assign ( resid 26 and name HG2# ) ( resid 25 and name HG2 or resid 25 and name HG1 ) 2.9 1.2 1.1 volume=1.905 peak=2778 ppm1=0.912 ppm2=1.287 assign ( resid 57 and name HN ) ( resid 56 and name HB1 ) 3.1 1.3 1.2 volume=1.322 peak=1841 ppm1=9.217 ppm2=1.802 assign ( resid 139 and name HG2 ) ( resid 139 and name HB2 ) 3.6 1.9 1.5 volume=0.470 peak=4335 ppm1=1.802 ppm2=2.197 assign ( resid 134 and name HN ) ( resid 112 and name HG12 ) 4.0 2.3 1.6 volume=0.262 peak=1495 ppm1=8.745 ppm2=1.267 assign ( resid 69 and name HN ) ( resid 69 and name HA1 ) 2.6 0.9 1.0 volume=3.320 peak=550 ppm1=8.217 ppm2=3.861 assign ( resid 160 and name HN ) ( resid 161 and name HA ) 2.9 1.2 1.2 volume=1.791 peak=2413 ppm1=8.833 ppm2=4.663 assign ( resid 129 and name HN ) ( resid 129 and name HB2 ) 3.3 1.6 1.3 volume=0.875 peak=1813 ppm1=8.718 ppm2=3.428 assign ( resid 176 and name HN ) ( resid 144 and name HD1# ) 4.0 2.3 1.6 volume=0.254 peak=946 ppm1=8.405 ppm2=0.625 assign ( resid 14 and name HG2# ) ( resid 14 and name HB ) 2.7 0.9 1.1 volume=3.054 peak=4912 ppm1=0.756 ppm2=1.710 assign ( resid 60 and name HN ) ( resid 60 and name HA ) 2.9 1.2 1.2 volume=1.869 peak=1725 ppm1=7.266 ppm2=3.879 assign ( resid 159 and name HA ) ( resid 159 and name HB2 or resid 159 and name HB1 ) 2.7 1.0 1.1 volume=2.606 peak=2978 ppm1=3.771 ppm2=1.880 assign ( resid 93 and name HG2# ) ( resid 84 and name HN ) 4.2 2.5 1.7 volume=0.185 peak=2589 ppm1=-0.015 ppm2=8.519 assign ( resid 14 and name HN ) ( resid 17 and name HD1 or resid 17 and name HD2 ) 4.1 2.4 1.6 volume=0.229 peak=1544 ppm1=7.791 ppm2=6.484 assign ( resid 168 and name HG2# ) ( resid 154 and name HB ) 3.7 2.0 1.5 volume=0.433 peak=2600 ppm1=0.200 ppm2=2.200 assign ( resid 186 and name HA ) ( resid 186 and name HD2 ) 4.1 2.4 1.7 volume=0.215 peak=3520 ppm1=4.214 ppm2=1.620 assign ( resid 201 and name HA ) ( resid 204 and name HE2 ) 4.5 2.8 1.5 volume=0.127 peak=3364 ppm1=4.334 ppm2=2.829 assign ( resid 154 and name HG1# ) ( resid 126 and name HD1# ) 3.5 1.8 1.4 volume=0.596 peak=3694 ppm1=0.914 ppm2=0.379 assign ( resid 154 and name HG1# ) ( resid 124 and name HB1 ) 2.8 1.1 1.1 volume=2.036 peak=4494 ppm1=0.916 ppm2=2.069 assign ( resid 187 and name HN ) ( resid 188 and name HN ) 3.1 1.4 1.3 volume=1.105 peak=414 ppm1=7.600 ppm2=8.437 assign ( resid 107 and name HN ) ( resid 106 and name HG2# ) 3.2 1.5 1.3 volume=0.916 peak=353 ppm1=8.396 ppm2=0.888 assign ( resid 197 and name HA ) ( resid 200 and name HB2 ) 2.9 1.2 1.2 volume=1.837 peak=4672 ppm1=3.793 ppm2=1.716 assign ( resid 164 and name HN ) ( resid 163 and name HB# ) 2.7 1.0 1.1 volume=2.501 peak=276 ppm1=7.976 ppm2=1.138 assign ( resid 9 and name HN ) ( resid 8 and name HN ) 3.0 1.3 1.2 volume=1.355 peak=1667 ppm1=7.988 ppm2=7.654 assign ( resid 26 and name HB ) ( resid 26 and name HG1# ) 2.8 1.1 1.1 volume=2.323 peak=4522 ppm1=1.924 ppm2=0.779 assign ( resid 71 and name HB1 ) ( resid 69 and name HN ) 4.1 2.4 1.6 volume=0.227 peak=3322 ppm1=1.528 ppm2=8.200 assign ( resid 66 and name HN ) ( resid 71 and name HB2 ) 3.0 1.2 1.2 volume=1.621 peak=798 ppm1=8.051 ppm2=1.506 assign ( resid 146 and name HN ) ( resid 145 and name HB1 ) 3.5 1.7 1.4 volume=0.635 peak=327 ppm1=8.401 ppm2=1.940 assign ( resid 38 and name HN ) ( resid 48 and name HA ) 3.6 1.9 1.4 volume=0.483 peak=1812 ppm1=8.467 ppm2=5.307 assign ( resid 121 and name HG2 ) ( resid 121 and name HB1 ) 2.6 0.9 1.0 volume=3.285 peak=3014 ppm1=2.310 ppm2=2.049 assign ( resid 93 and name HD1# ) ( resid 94 and name HN ) 3.8 2.1 1.5 volume=0.346 peak=4394 ppm1=-0.273 ppm2=9.628 assign ( resid 129 and name HA ) ( resid 115 and name HG1# ) 4.4 2.7 1.6 volume=0.142 peak=3559 ppm1=5.704 ppm2=0.316 assign ( resid 169 and name HA ) ( resid 154 and name HA ) 4.6 2.9 1.4 volume=0.107 peak=4610 ppm1=5.246 ppm2=4.677 assign ( resid 6 and name HA ) ( resid 6 and name HB ) 4.0 2.3 1.6 volume=0.259 peak=3296 ppm1=3.617 ppm2=1.743 assign ( resid 134 and name HZ ) ( resid 84 and name HN ) 3.6 1.9 1.4 volume=0.482 peak=107 ppm1=6.644 ppm2=8.501 assign ( resid 97 and name HN ) ( resid 80 and name HB ) 3.4 1.7 1.4 volume=0.707 peak=2091 ppm1=8.362 ppm2=1.378 assign ( resid 5 and name HB# ) ( resid 5 and name HA ) 2.9 1.2 1.2 volume=1.882 peak=3784 ppm1=1.341 ppm2=4.021 assign ( resid 157 and name HG2 ) ( resid 123 and name HN ) 4.7 2.9 1.3 volume=0.105 peak=2828 ppm1=1.791 ppm2=8.398 assign ( resid 57 and name HA ) ( resid 61 and name HD1# ) 4.3 2.5 1.7 volume=0.181 peak=4930 ppm1=4.134 ppm2=0.734 assign ( resid 71 and name HN ) ( resid 69 and name HN ) 3.7 2.0 1.5 volume=0.422 peak=582 ppm1=7.220 ppm2=8.176 assign ( resid 207 and name HA ) ( resid 208 and name HN ) 3.6 1.9 1.5 volume=0.456 peak=3730 ppm1=4.167 ppm2=8.016 assign ( resid 196 and name HN ) ( resid 196 and name HG2# ) 3.0 1.2 1.2 volume=1.582 peak=750 ppm1=7.437 ppm2=0.828 assign ( resid 130 and name HE1 ) ( resid 130 and name HD2 ) 3.3 1.5 1.3 volume=0.880 peak=3177 ppm1=2.839 ppm2=1.665 assign ( resid 114 and name HD2# ) ( resid 3 and name HN ) 3.9 2.2 1.6 volume=0.298 peak=3292 ppm1=0.782 ppm2=7.940 assign ( resid 54 and name HD1# ) ( resid 203 and name HD1# ) 3.6 1.9 1.4 volume=0.481 peak=5091 ppm1=0.490 ppm2=-0.011 assign ( resid 116 and name HN ) ( resid 115 and name HB ) 3.4 1.6 1.3 volume=0.748 peak=2226 ppm1=8.834 ppm2=0.233 assign ( resid 197 and name HN ) ( resid 198 and name HB2 ) 3.8 2.0 1.5 volume=0.383 peak=382 ppm1=7.989 ppm2=3.090 assign ( resid 199 and name HB# ) ( resid 167 and name HD2# ) 2.1 0.4 0.9 volume=11.159 peak=2674 ppm1=0.692 ppm2=0.801 assign ( resid 37 and name HN ) ( resid 26 and name HG1# ) 3.4 1.7 1.4 volume=0.717 peak=788 ppm1=9.659 ppm2=0.780 assign ( resid 179 and name HB1 ) ( resid 179 and name HG ) 2.7 1.0 1.1 volume=2.631 peak=3560 ppm1=2.752 ppm2=1.510 assign ( resid 87 and name HN ) ( resid 93 and name HN ) 4.3 2.6 1.7 volume=0.171 peak=1913 ppm1=8.040 ppm2=8.911 assign ( resid 112 and name HN ) ( resid 112 and name HG2# ) 3.5 1.8 1.4 volume=0.602 peak=1218 ppm1=8.134 ppm2=0.675 assign ( resid 34 and name HG2# ) ( resid 35 and name HN ) 4.3 2.5 1.7 volume=0.180 peak=3847 ppm1=1.101 ppm2=9.433 assign ( resid 91 and name HN ) ( resid 88 and name HN ) 3.4 1.6 1.3 volume=0.754 peak=2093 ppm1=7.219 ppm2=8.592 assign ( resid 167 and name HB1 ) ( resid 54 and name HD1# ) 4.8 3.1 1.2 volume=0.087 peak=3568 ppm1=1.678 ppm2=0.503 assign ( resid 21 and name HN ) ( resid 21 and name HG2# ) 3.3 1.6 1.3 volume=0.766 peak=406 ppm1=8.284 ppm2=1.154 assign ( resid 51 and name HG1 or resid 51 and name HG2 ) ( resid 168 and name HG2# ) 3.8 2.1 1.5 volume=0.337 peak=2620 ppm1=1.972 ppm2=0.202 assign ( resid 208 and name HG2# ) ( resid 204 and name HE2 or resid 204 and name HE1 ) 4.0 2.3 1.6 volume=0.268 peak=3746 ppm1=1.137 ppm2=2.855 assign ( resid 24 and name HD1 ) ( resid 24 and name HA ) 4.1 2.4 1.6 volume=0.232 peak=151 ppm1=6.802 ppm2=4.253 assign ( resid 93 and name HG2# ) ( resid 114 and name HB1 ) 4.0 2.3 1.6 volume=0.272 peak=4899 ppm1=-0.014 ppm2=1.060 assign ( resid 15 and name HB2 ) ( resid 15 and name HG ) 4.5 2.8 1.5 volume=0.128 peak=2626 ppm1=1.368 ppm2=1.239 assign ( resid 175 and name HG1 ) ( resid 173 and name HG2# ) 3.7 2.0 1.5 volume=0.413 peak=2627 ppm1=2.553 ppm2=1.037 assign ( resid 60 and name HN ) ( resid 61 and name HD2# ) 3.6 1.9 1.4 volume=0.519 peak=1297 ppm1=7.266 ppm2=0.750 assign ( resid 22 and name HN ) ( resid 21 and name HA ) 2.2 0.5 0.9 volume=8.398 peak=1518 ppm1=8.194 ppm2=4.660 assign ( resid 112 and name HG2# ) ( resid 112 and name HN ) 3.2 1.5 1.3 volume=0.912 peak=2535 ppm1=0.681 ppm2=8.129 assign ( resid 137 and name HN ) ( resid 112 and name HD1# ) 3.4 1.7 1.4 volume=0.703 peak=255 ppm1=8.051 ppm2=0.368 assign ( resid 60 and name HB2 ) ( resid 60 and name HA ) 3.5 1.8 1.4 volume=0.567 peak=3365 ppm1=1.715 ppm2=3.871 assign ( resid 201 and name HN ) ( resid 201 and name HB2 ) 2.6 0.9 1.0 volume=3.320 peak=1835 ppm1=7.401 ppm2=2.580 assign ( resid 80 and name HN ) ( resid 96 and name HA ) 3.6 1.8 1.4 volume=0.526 peak=1815 ppm1=7.524 ppm2=4.819 assign ( resid 27 and name HN ) ( resid 28 and name HA ) 3.3 1.6 1.3 volume=0.780 peak=1070 ppm1=9.278 ppm2=4.392 assign ( resid 97 and name HG2# ) ( resid 97 and name HN ) 3.5 1.8 1.4 volume=0.546 peak=4885 ppm1=0.213 ppm2=8.357 assign ( resid 193 and name HN ) ( resid 196 and name HB ) 3.9 2.2 1.6 volume=0.301 peak=820 ppm1=7.620 ppm2=2.255 assign ( resid 62 and name HA ) ( resid 62 and name HB2 ) 4.2 2.5 1.7 volume=0.196 peak=3950 ppm1=3.966 ppm2=3.858 assign ( resid 126 and name HN ) ( resid 126 and name HG11 or resid 126 and name HG12 ) 3.3 1.6 1.3 volume=0.869 peak=600 ppm1=9.104 ppm2=1.138 assign ( resid 65 and name HN ) ( resid 64 and name HD1 or resid 64 and name HD2 ) 4.3 2.5 1.7 volume=0.178 peak=962 ppm1=7.743 ppm2=5.965 assign ( resid 65 and name HB1 or resid 65 and name HB2 ) ( resid 127 and name HG2# ) 3.5 1.8 1.4 volume=0.588 peak=3667 ppm1=1.641 ppm2=0.844 assign ( resid 8 and name HG1 or resid 8 and name HG2 ) ( resid 10 and name HN ) 4.5 2.7 1.5 volume=0.138 peak=4843 ppm1=2.321 ppm2=8.324 assign ( resid 169 and name HN ) ( resid 169 and name HA ) 3.9 2.2 1.6 volume=0.314 peak=1374 ppm1=9.257 ppm2=5.189 assign ( resid 33 and name HD1# ) ( resid 50 and name HG1# ) 3.4 1.7 1.4 volume=0.700 peak=3590 ppm1=0.360 ppm2=0.635 assign ( resid 153 and name HA ) ( resid 169 and name HG1 ) 3.9 2.2 1.6 volume=0.283 peak=4593 ppm1=5.318 ppm2=1.938 assign ( resid 4 and name HN ) ( resid 5 and name HN ) 2.8 1.1 1.1 volume=2.023 peak=570 ppm1=8.189 ppm2=7.496 assign ( resid 65 and name HA ) ( resid 65 and name HN ) 4.2 2.4 1.7 volume=0.205 peak=3358 ppm1=3.889 ppm2=7.735 assign ( resid 93 and name HG12 ) ( resid 93 and name HD1# ) 3.8 2.1 1.5 volume=0.339 peak=4555 ppm1=0.598 ppm2=-0.271 assign ( resid 28 and name HN ) ( resid 27 and name HG1# ) 2.4 0.7 1.0 volume=5.038 peak=768 ppm1=7.808 ppm2=0.884 assign ( resid 139 and name HB1 ) ( resid 145 and name HG2 ) 4.5 2.8 1.5 volume=0.131 peak=4131 ppm1=2.195 ppm2=1.410 assign ( resid 174 and name HN ) ( resid 148 and name HA ) 3.1 1.4 1.2 volume=1.173 peak=865 ppm1=9.153 ppm2=5.035 assign ( resid 5 and name HA ) ( resid 5 and name HB# ) 2.8 1.1 1.1 volume=2.375 peak=4934 ppm1=4.024 ppm2=1.338 assign ( resid 2 and name HN ) ( resid 1 and name HA ) 3.1 1.4 1.3 volume=1.143 peak=1074 ppm1=8.186 ppm2=4.281 assign ( resid 169 and name HN ) ( resid 49 and name HA ) 3.5 1.8 1.4 volume=0.556 peak=935 ppm1=9.256 ppm2=4.899 assign ( resid 156 and name HN ) ( resid 167 and name HD2# ) 3.1 1.3 1.2 volume=1.301 peak=1754 ppm1=8.551 ppm2=0.757 assign ( resid 5 and name HN ) ( resid 5 and name HB# ) 2.5 0.8 1.0 volume=4.662 peak=1691 ppm1=7.459 ppm2=1.340 assign ( resid 132 and name HB ) ( resid 132 and name HG2# ) 3.4 1.7 1.4 volume=0.710 peak=2521 ppm1=2.284 ppm2=0.935 assign ( resid 134 and name HA ) ( resid 135 and name HG1 ) 4.4 2.7 1.6 volume=0.151 peak=4256 ppm1=5.189 ppm2=1.768 assign ( resid 136 and name HN ) ( resid 135 and name HB2 ) 3.2 1.5 1.3 volume=0.925 peak=834 ppm1=6.891 ppm2=2.200 assign ( resid 93 and name HG2# ) ( resid 85 and name HN ) 3.5 1.8 1.4 volume=0.597 peak=4812 ppm1=-0.013 ppm2=7.152 assign ( resid 50 and name HN ) ( resid 169 and name HG2 ) 3.3 1.6 1.3 volume=0.877 peak=390 ppm1=9.300 ppm2=1.928 assign ( resid 190 and name HN ) ( resid 192 and name HN ) 4.2 2.5 1.7 volume=0.202 peak=1045 ppm1=7.518 ppm2=8.171 assign ( resid 128 and name HA ) ( resid 14 and name HG2# ) 3.9 2.2 1.6 volume=0.286 peak=2679 ppm1=5.580 ppm2=0.775 assign ( resid 84 and name HN ) ( resid 95 and name HA ) 4.0 2.3 1.6 volume=0.250 peak=653 ppm1=8.505 ppm2=5.574 assign ( resid 5 and name HB# ) ( resid 2 and name HA ) 3.4 1.7 1.4 volume=0.711 peak=2662 ppm1=1.341 ppm2=4.141 assign ( resid 198 and name HB2 ) ( resid 199 and name HB# ) 4.3 2.6 1.7 volume=0.170 peak=3839 ppm1=3.088 ppm2=0.729 assign ( resid 22 and name HB2 or resid 22 and name HB1 ) ( resid 21 and name HN ) 3.7 2.0 1.5 volume=0.386 peak=4642 ppm1=3.771 ppm2=8.266 assign ( resid 35 and name HG2# ) ( resid 192 and name HD1# ) 3.6 1.8 1.4 volume=0.524 peak=2566 ppm1=0.889 ppm2=0.477 assign ( resid 126 and name HG2# ) ( resid 126 and name HD1# ) 2.8 1.1 1.1 volume=2.254 peak=3482 ppm1=0.754 ppm2=0.351 assign ( resid 45 and name HN ) ( resid 43 and name HB1 ) 3.7 1.9 1.5 volume=0.441 peak=2157 ppm1=6.656 ppm2=2.962 assign ( resid 208 and name HG2# ) ( resid 209 and name HG2 ) 3.2 1.5 1.3 volume=0.914 peak=4052 ppm1=1.137 ppm2=1.896 assign ( resid 176 and name HG1 ) ( resid 176 and name HN ) 4.1 2.4 1.7 volume=0.216 peak=3040 ppm1=1.642 ppm2=8.409 assign ( resid 68 and name HN ) ( resid 68 and name HG2# ) 3.2 1.5 1.3 volume=1.045 peak=1749 ppm1=8.021 ppm2=0.745 assign ( resid 16 and name HN ) ( resid 15 and name HD1# ) 3.4 1.6 1.3 volume=0.754 peak=1183 ppm1=7.497 ppm2=0.434 assign ( resid 153 and name HN ) ( resid 153 and name HA ) 3.5 1.8 1.4 volume=0.570 peak=774 ppm1=9.328 ppm2=5.314 assign ( resid 80 and name HN ) ( resid 80 and name HB ) 2.9 1.2 1.2 volume=1.678 peak=759 ppm1=7.523 ppm2=1.404 assign ( resid 199 and name HN ) ( resid 64 and name HZ ) 3.8 2.0 1.5 volume=0.381 peak=1634 ppm1=8.635 ppm2=7.081 assign ( resid 26 and name HN ) ( resid 27 and name HN ) 3.9 2.2 1.6 volume=0.316 peak=955 ppm1=8.862 ppm2=9.275 assign ( resid 91 and name HG2# ) ( resid 115 and name HN ) 3.5 1.8 1.4 volume=0.600 peak=2817 ppm1=1.017 ppm2=9.099 assign ( resid 173 and name HN ) ( resid 172 and name HB1 ) 3.3 1.5 1.3 volume=0.898 peak=2045 ppm1=8.519 ppm2=1.795 assign ( resid 168 and name HB ) ( resid 168 and name HG1# ) 4.4 2.7 1.6 volume=0.152 peak=2717 ppm1=1.725 ppm2=0.767 assign ( resid 171 and name HN ) ( resid 171 and name HG2# ) 3.1 1.3 1.2 volume=1.306 peak=1304 ppm1=9.063 ppm2=0.754 assign ( resid 123 and name HN ) ( resid 120 and name HB1 ) 3.1 1.3 1.2 volume=1.318 peak=1787 ppm1=8.403 ppm2=2.972 assign ( resid 20 and name HN ) ( resid 19 and name HG2 ) 3.0 1.3 1.2 volume=1.420 peak=232 ppm1=7.408 ppm2=1.663 assign ( resid 190 and name HN ) ( resid 188 and name HE# ) 3.8 2.1 1.5 volume=0.352 peak=1062 ppm1=7.519 ppm2=1.910 assign ( resid 196 and name HA ) ( resid 196 and name HD1# ) 3.0 1.2 1.2 volume=1.569 peak=2651 ppm1=3.453 ppm2=0.728 assign ( resid 114 and name HD1# ) ( resid 4 and name HA ) 3.7 2.0 1.5 volume=0.402 peak=3942 ppm1=0.537 ppm2=3.774 assign ( resid 199 and name HB# ) ( resid 196 and name HA ) 3.2 1.5 1.3 volume=0.952 peak=3132 ppm1=0.693 ppm2=3.440 assign ( resid 165 and name HN ) ( resid 158 and name HG1 ) 3.9 2.2 1.6 volume=0.293 peak=1893 ppm1=8.465 ppm2=2.446 assign ( resid 169 and name HA ) ( resid 169 and name HG1 ) 4.4 2.7 1.6 volume=0.147 peak=4520 ppm1=5.237 ppm2=1.927 assign ( resid 192 and name HD2# ) ( resid 188 and name HB1 ) 3.5 1.8 1.4 volume=0.558 peak=3540 ppm1=0.492 ppm2=1.446 assign ( resid 151 and name HN ) ( resid 152 and name HA1 ) 3.8 2.1 1.5 volume=0.364 peak=1362 ppm1=8.647 ppm2=3.616 assign ( resid 130 and name HN ) ( resid 114 and name HB1 ) 3.5 1.8 1.4 volume=0.569 peak=489 ppm1=7.615 ppm2=1.053 assign ( resid 36 and name HB1 ) ( resid 26 and name HG1# ) 5.0 3.3 1.0 volume=0.067 peak=4463 ppm1=3.858 ppm2=0.769 assign ( resid 162 and name HG2 ) ( resid 162 and name HD2 ) 2.9 1.2 1.2 volume=1.693 peak=4296 ppm1=1.919 ppm2=3.488 assign ( resid 93 and name HB ) ( resid 93 and name HG11 ) 3.9 2.2 1.6 volume=0.310 peak=5053 ppm1=1.224 ppm2=0.687 assign ( resid 94 and name HN ) ( resid 112 and name HD1# ) 3.5 1.8 1.4 volume=0.608 peak=1828 ppm1=9.602 ppm2=0.362 assign ( resid 186 and name HD1 ) ( resid 186 and name HE2 ) 3.4 1.7 1.4 volume=0.686 peak=3651 ppm1=1.676 ppm2=2.959 assign ( resid 197 and name HB2 ) ( resid 197 and name HG ) 4.6 2.9 1.4 volume=0.112 peak=4040 ppm1=1.782 ppm2=1.268 assign ( resid 168 and name HG1# ) ( resid 154 and name HB ) 2.9 1.2 1.1 volume=1.920 peak=4552 ppm1=0.768 ppm2=2.183 assign ( resid 11 and name HN ) ( resid 10 and name HA ) 2.9 1.2 1.2 volume=1.762 peak=928 ppm1=8.179 ppm2=3.621 assign ( resid 120 and name HB2 ) ( resid 124 and name HG2 ) 3.8 2.1 1.5 volume=0.333 peak=4005 ppm1=2.999 ppm2=2.401 assign ( resid 6 and name HN ) ( resid 7 and name HN ) 3.5 1.8 1.4 volume=0.595 peak=2006 ppm1=7.724 ppm2=8.436 assign ( resid 167 and name HN ) ( resid 52 and name HN ) 3.2 1.4 1.3 volume=1.092 peak=1601 ppm1=8.643 ppm2=8.610 assign ( resid 51 and name HG1 or resid 51 and name HG2 ) ( resid 51 and name HB1 or resid 51 and name HB2 ) 2.6 0.8 1.0 volume=3.860 peak=3380 ppm1=1.972 ppm2=1.763 assign ( resid 91 and name HN ) ( resid 92 and name HN ) 4.0 2.3 1.6 volume=0.274 peak=710 ppm1=7.219 ppm2=9.478 assign ( resid 115 and name HN ) ( resid 115 and name HA ) 3.3 1.6 1.3 volume=0.859 peak=893 ppm1=9.053 ppm2=4.400 assign ( resid 130 and name HD2 ) ( resid 130 and name HE1 ) 2.8 1.1 1.1 volume=2.038 peak=3573 ppm1=1.660 ppm2=2.835 assign ( resid 173 and name HN ) ( resid 173 and name HB ) 3.2 1.5 1.3 volume=0.972 peak=1032 ppm1=8.519 ppm2=3.619 assign ( resid 63 and name HN ) ( resid 63 and name HB2 ) 2.5 0.7 1.0 volume=4.962 peak=1684 ppm1=7.297 ppm2=2.707 assign ( resid 125 and name HN ) ( resid 124 and name HN ) 3.5 1.8 1.4 volume=0.585 peak=916 ppm1=8.772 ppm2=6.477 assign ( resid 117 and name HN ) ( resid 92 and name HN ) 4.4 2.6 1.6 volume=0.155 peak=1605 ppm1=8.231 ppm2=9.471 assign ( resid 25 and name HN ) ( resid 37 and name HN ) 3.4 1.7 1.4 volume=0.676 peak=719 ppm1=9.015 ppm2=9.623 assign ( resid 37 and name HA ) ( resid 38 and name HA ) 4.4 2.7 1.6 volume=0.151 peak=4603 ppm1=5.823 ppm2=4.287 assign ( resid 173 and name HN ) ( resid 172 and name HN ) 3.3 1.6 1.3 volume=0.764 peak=1414 ppm1=8.520 ppm2=8.836 assign ( resid 186 and name HB2 ) ( resid 183 and name HA ) 3.8 2.1 1.5 volume=0.336 peak=4218 ppm1=1.905 ppm2=3.897 assign ( resid 92 and name HN ) ( resid 115 and name HA ) 3.6 1.9 1.5 volume=0.466 peak=1996 ppm1=9.455 ppm2=4.404 assign ( resid 132 and name HG1# ) ( resid 3 and name HE1 or resid 3 and name HE2 ) 3.5 1.8 1.4 volume=0.545 peak=5089 ppm1=0.542 ppm2=7.219 assign ( resid 87 and name HD1# ) ( resid 87 and name HG2# ) 2.7 1.0 1.1 volume=2.931 peak=4821 ppm1=0.440 ppm2=0.838 assign ( resid 93 and name HD1# ) ( resid 84 and name HB ) 3.7 2.0 1.5 volume=0.414 peak=3511 ppm1=-0.272 ppm2=1.999 assign ( resid 168 and name HN ) ( resid 168 and name HG2# ) 3.6 1.9 1.4 volume=0.504 peak=1086 ppm1=8.694 ppm2=0.226 assign ( resid 167 and name HD1# ) ( resid 167 and name HG ) 3.1 1.4 1.3 volume=1.102 peak=4711 ppm1=0.764 ppm2=0.923 assign ( resid 1 and name HN# ) ( resid 2 and name HA ) 3.0 1.3 1.2 volume=1.377 peak=609 ppm1=8.196 ppm2=4.147 assign ( resid 191 and name HA ) ( resid 194 and name HN ) 4.2 2.4 1.7 volume=0.206 peak=3267 ppm1=4.272 ppm2=7.810 assign ( resid 116 and name HN ) ( resid 91 and name HA ) 4.0 2.2 1.6 volume=0.277 peak=2254 ppm1=8.835 ppm2=5.829 assign ( resid 37 and name HB1 or resid 37 and name HB2 ) ( resid 46 and name HB1 ) 4.0 2.3 1.6 volume=0.252 peak=4318 ppm1=3.288 ppm2=1.549 assign ( resid 201 and name HN ) ( resid 200 and name HB2 ) 2.8 1.0 1.1 volume=2.429 peak=1768 ppm1=7.403 ppm2=1.664 assign ( resid 196 and name HN ) ( resid 33 and name HD1# ) 4.0 2.3 1.6 volume=0.261 peak=1031 ppm1=7.437 ppm2=0.356 assign ( resid 92 and name HE1 or resid 92 and name HE2 ) ( resid 86 and name HD1 ) 3.3 1.6 1.3 volume=0.805 peak=105 ppm1=6.750 ppm2=2.900 assign ( resid 194 and name HN ) ( resid 33 and name HD1# ) 3.8 2.0 1.5 volume=0.378 peak=1829 ppm1=7.773 ppm2=0.357 assign ( resid 159 and name HA ) ( resid 158 and name HB1 ) 2.9 1.2 1.2 volume=1.715 peak=4008 ppm1=3.772 ppm2=2.204 assign ( resid 204 and name HB2 ) ( resid 204 and name HN ) 3.3 1.5 1.3 volume=0.883 peak=2756 ppm1=1.713 ppm2=6.757 assign ( resid 15 and name HD2# ) ( resid 15 and name HG ) 2.3 0.5 0.9 volume=8.165 peak=3200 ppm1=0.685 ppm2=1.242 assign ( resid 172 and name HN ) ( resid 173 and name HN ) 3.7 2.0 1.5 volume=0.407 peak=2184 ppm1=8.856 ppm2=8.522 assign ( resid 80 and name HG1# ) ( resid 81 and name HA ) 4.2 2.5 1.7 volume=0.194 peak=2476 ppm1=0.708 ppm2=4.680 assign ( resid 79 and name HN ) ( resid 99 and name HN ) 4.3 2.6 1.7 volume=0.162 peak=580 ppm1=8.843 ppm2=7.799 assign ( resid 91 and name HN ) ( resid 90 and name HN ) 3.0 1.2 1.2 volume=1.577 peak=362 ppm1=7.221 ppm2=8.428 assign ( resid 198 and name HB2 ) ( resid 197 and name HB2 ) 4.5 2.8 1.5 volume=0.131 peak=2972 ppm1=3.087 ppm2=1.742 assign ( resid 19 and name HN ) ( resid 21 and name HG2# ) 3.6 1.9 1.4 volume=0.499 peak=337 ppm1=7.482 ppm2=1.141 assign ( resid 74 and name HZ2 ) ( resid 74 and name HE1 ) 3.9 2.1 1.5 volume=0.325 peak=95 ppm1=6.458 ppm2=9.624 assign ( resid 105 and name HN ) ( resid 104 and name HA2 ) 3.4 1.7 1.4 volume=0.679 peak=1085 ppm1=7.944 ppm2=3.491 assign ( resid 154 and name HG1# ) ( resid 153 and name HN ) 3.2 1.4 1.3 volume=1.087 peak=2776 ppm1=0.909 ppm2=9.307 assign ( resid 135 and name HB2 or resid 135 and name HB1 ) ( resid 135 and name HG2 or resid 135 and name HG1 ) 2.2 0.4 0.9 volume=10.662 peak=3534 ppm1=2.191 ppm2=1.783 assign ( resid 37 and name HA ) ( resid 38 and name HN ) 4.1 2.3 1.6 volume=0.240 peak=4506 ppm1=5.821 ppm2=8.521 assign ( resid 202 and name HN ) ( resid 201 and name HB2 ) 3.0 1.3 1.2 volume=1.542 peak=1608 ppm1=8.575 ppm2=2.585 assign ( resid 188 and name HB2 ) ( resid 189 and name HD1 ) 3.9 2.2 1.6 volume=0.288 peak=2934 ppm1=1.447 ppm2=3.441 assign ( resid 16 and name HN ) ( resid 15 and name HD2# ) 3.3 1.6 1.3 volume=0.761 peak=1327 ppm1=7.496 ppm2=0.686 assign ( resid 146 and name HN ) ( resid 109 and name HG2 ) 3.6 1.8 1.4 volume=0.522 peak=447 ppm1=8.400 ppm2=1.530 assign ( resid 114 and name HB1 ) ( resid 114 and name HG ) 3.6 1.9 1.5 volume=0.469 peak=4880 ppm1=1.063 ppm2=0.943 assign ( resid 91 and name HN ) ( resid 87 and name HG11 ) 3.5 1.8 1.4 volume=0.552 peak=1042 ppm1=7.217 ppm2=1.260 assign ( resid 168 and name HG2# ) ( resid 51 and name HA ) 4.2 2.5 1.7 volume=0.186 peak=2996 ppm1=0.200 ppm2=5.653 assign ( resid 84 and name HG2# ) ( resid 112 and name HD1# ) 3.2 1.5 1.3 volume=0.913 peak=3946 ppm1=0.109 ppm2=0.384 assign ( resid 137 and name HN ) ( resid 134 and name HE1 or resid 134 and name HE2 ) 3.1 1.4 1.2 volume=1.241 peak=2234 ppm1=8.053 ppm2=7.126 assign ( resid 79 and name HN ) ( resid 72 and name HG2# ) 3.3 1.6 1.3 volume=0.802 peak=1864 ppm1=8.843 ppm2=0.621 assign ( resid 196 and name HN ) ( resid 198 and name HN ) 3.8 2.1 1.5 volume=0.364 peak=285 ppm1=7.438 ppm2=8.707 assign ( resid 84 and name HN ) ( resid 83 and name HG2 ) 3.2 1.5 1.3 volume=0.964 peak=1921 ppm1=8.504 ppm2=1.724 assign ( resid 204 and name HN ) ( resid 202 and name HN ) 3.7 2.0 1.5 volume=0.423 peak=2280 ppm1=6.745 ppm2=8.564 assign ( resid 173 and name HN ) ( resid 172 and name HA ) 3.8 2.0 1.5 volume=0.374 peak=1668 ppm1=8.519 ppm2=3.116 assign ( resid 54 and name HG2# ) ( resid 54 and name HD1# ) 2.3 0.6 0.9 volume=7.655 peak=3503 ppm1=0.577 ppm2=0.487 assign ( resid 102 and name HA ) ( resid 101 and name HA ) 4.2 2.5 1.7 volume=0.193 peak=3544 ppm1=4.117 ppm2=4.676 assign ( resid 114 and name HN ) ( resid 114 and name HB2 ) 3.4 1.7 1.4 volume=0.701 peak=2182 ppm1=8.799 ppm2=1.671 assign ( resid 94 and name HN ) ( resid 114 and name HA ) 3.8 2.0 1.5 volume=0.377 peak=2310 ppm1=9.601 ppm2=4.403 assign ( resid 104 and name HN ) ( resid 102 and name HN ) 3.5 1.8 1.4 volume=0.549 peak=2011 ppm1=8.051 ppm2=8.537 assign ( resid 187 and name HG2# ) ( resid 175 and name HG1 ) 3.4 1.7 1.4 volume=0.699 peak=4760 ppm1=1.060 ppm2=2.526 assign ( resid 176 and name HN ) ( resid 174 and name HB1 ) 3.1 1.4 1.2 volume=1.185 peak=1961 ppm1=8.403 ppm2=1.938 assign ( resid 26 and name HA ) ( resid 26 and name HG1# ) 4.2 2.5 1.7 volume=0.199 peak=2774 ppm1=3.980 ppm2=0.780 assign ( resid 64 and name HN ) ( resid 65 and name HD2# ) 3.6 1.9 1.4 volume=0.508 peak=1773 ppm1=7.876 ppm2=0.362 assign ( resid 72 and name HD1# ) ( resid 72 and name HB ) 2.9 1.1 1.1 volume=1.997 peak=3628 ppm1=0.588 ppm2=1.855 assign ( resid 114 and name HD1# ) ( resid 92 and name HB1 ) 3.7 2.0 1.5 volume=0.422 peak=3643 ppm1=0.538 ppm2=3.055 assign ( resid 54 and name HD1# ) ( resid 196 and name HB ) 3.9 2.2 1.6 volume=0.298 peak=3701 ppm1=0.491 ppm2=2.265 assign ( resid 51 and name HG1 or resid 51 and name HG2 ) ( resid 34 and name HG2# ) 3.3 1.6 1.3 volume=0.763 peak=4652 ppm1=1.972 ppm2=1.162 assign ( resid 114 and name HN ) ( resid 114 and name HB1 ) 3.3 1.6 1.3 volume=0.785 peak=1221 ppm1=8.800 ppm2=1.063 assign ( resid 148 and name HN ) ( resid 148 and name HA ) 4.0 2.3 1.6 volume=0.257 peak=536 ppm1=9.153 ppm2=4.994 assign ( resid 192 and name HB1 ) ( resid 50 and name HG1# ) 3.9 2.2 1.6 volume=0.298 peak=2599 ppm1=1.331 ppm2=0.650 assign ( resid 119 and name HD1 ) ( resid 119 and name HG2 ) 2.7 1.0 1.1 volume=2.651 peak=2724 ppm1=2.901 ppm2=1.269 assign ( resid 170 and name HN ) ( resid 171 and name HN ) 3.2 1.5 1.3 volume=0.990 peak=279 ppm1=9.145 ppm2=9.077 assign ( resid 54 and name HG11 ) ( resid 200 and name HN ) 3.9 2.2 1.6 volume=0.286 peak=4549 ppm1=1.184 ppm2=8.075 assign ( resid 168 and name HN ) ( resid 154 and name HB ) 3.6 1.9 1.4 volume=0.475 peak=237 ppm1=8.693 ppm2=2.181 assign ( resid 184 and name HG11 ) ( resid 184 and name HA ) 3.0 1.2 1.2 volume=1.565 peak=2965 ppm1=1.677 ppm2=3.628 assign ( resid 112 and name HB ) ( resid 112 and name HG11 ) 3.7 2.0 1.5 volume=0.396 peak=3301 ppm1=2.170 ppm2=1.604 assign ( resid 110 and name HN ) ( resid 146 and name HN ) 3.4 1.7 1.4 volume=0.655 peak=1976 ppm1=8.721 ppm2=8.442 assign ( resid 25 and name HN ) ( resid 24 and name HB2 or resid 24 and name HB1 ) 3.0 1.3 1.2 volume=1.402 peak=1093 ppm1=9.009 ppm2=2.954 assign ( resid 197 and name HN ) ( resid 197 and name HA ) 3.2 1.4 1.3 volume=1.058 peak=615 ppm1=7.990 ppm2=3.750 assign ( resid 176 and name HG1 ) ( resid 147 and name HN ) 4.1 2.3 1.6 volume=0.238 peak=5146 ppm1=1.642 ppm2=8.734 assign ( resid 180 and name HN ) ( resid 180 and name HA ) 3.5 1.8 1.4 volume=0.549 peak=1563 ppm1=8.353 ppm2=4.878 assign ( resid 102 and name HB# ) ( resid 102 and name HA ) 3.2 1.4 1.3 volume=1.074 peak=3639 ppm1=1.279 ppm2=4.114 assign ( resid 104 and name HN ) ( resid 106 and name HD1# ) 3.4 1.6 1.3 volume=0.752 peak=1765 ppm1=8.052 ppm2=0.747 assign ( resid 88 and name HN ) ( resid 87 and name HD1# ) 3.5 1.7 1.4 volume=0.631 peak=2074 ppm1=8.595 ppm2=0.434 assign ( resid 183 and name HN ) ( resid 180 and name HN ) 2.9 1.2 1.2 volume=1.841 peak=2047 ppm1=7.419 ppm2=8.347 assign ( resid 133 and name HN ) ( resid 132 and name HG2# ) 2.7 1.0 1.1 volume=2.546 peak=2430 ppm1=8.122 ppm2=0.931 assign ( resid 112 and name HG2# ) ( resid 112 and name HB ) 2.9 1.1 1.1 volume=1.976 peak=3925 ppm1=0.678 ppm2=2.163 assign ( resid 115 and name HA ) ( resid 114 and name HG ) 3.5 1.8 1.4 volume=0.560 peak=4151 ppm1=4.399 ppm2=0.967 assign ( resid 63 and name HN ) ( resid 59 and name HB# ) 3.4 1.6 1.3 volume=0.759 peak=1519 ppm1=7.298 ppm2=1.277 assign ( resid 114 and name HB2 ) ( resid 114 and name HD1# ) 3.9 2.2 1.6 volume=0.298 peak=4655 ppm1=1.701 ppm2=0.533 assign ( resid 69 and name HN ) ( resid 72 and name HG2# ) 3.6 1.9 1.4 volume=0.486 peak=968 ppm1=8.223 ppm2=0.615 assign ( resid 95 and name HN ) ( resid 96 and name HN ) 3.4 1.7 1.4 volume=0.640 peak=636 ppm1=9.125 ppm2=8.455 assign ( resid 199 and name HB# ) ( resid 197 and name HA ) 3.8 2.0 1.5 volume=0.381 peak=4618 ppm1=0.692 ppm2=3.822 assign ( resid 197 and name HN ) ( resid 196 and name HG2# ) 2.5 0.8 1.0 volume=4.416 peak=617 ppm1=7.988 ppm2=0.816 assign ( resid 116 and name HN ) ( resid 115 and name HN ) 3.1 1.4 1.2 volume=1.239 peak=205 ppm1=8.835 ppm2=9.027 assign ( resid 115 and name HN ) ( resid 93 and name HD1# ) 4.1 2.4 1.6 volume=0.229 peak=1403 ppm1=9.051 ppm2=-0.277 assign ( resid 112 and name HG2# ) ( resid 84 and name HG2# ) 3.2 1.5 1.3 volume=1.043 peak=2910 ppm1=0.680 ppm2=0.119 assign ( resid 8 and name HA ) ( resid 11 and name HN ) 3.8 2.1 1.5 volume=0.374 peak=3126 ppm1=3.839 ppm2=8.194 assign ( resid 192 and name HG ) ( resid 192 and name HB2 ) 3.7 1.9 1.5 volume=0.453 peak=3264 ppm1=1.755 ppm2=1.327 assign ( resid 41 and name HN ) ( resid 40 and name HB1 ) 3.6 1.9 1.5 volume=0.466 peak=313 ppm1=8.909 ppm2=3.351 assign ( resid 206 and name HA ) ( resid 60 and name HD2 ) 3.2 1.5 1.3 volume=0.938 peak=3912 ppm1=4.365 ppm2=1.558 assign ( resid 18 and name HB1 ) ( resid 15 and name HG ) 3.9 2.2 1.6 volume=0.289 peak=4017 ppm1=2.970 ppm2=1.223 assign ( resid 203 and name HN ) ( resid 203 and name HG11 or resid 203 and name HG12 ) 2.9 1.2 1.2 volume=1.887 peak=2349 ppm1=7.684 ppm2=0.513 assign ( resid 205 and name HB# ) ( resid 203 and name HA ) 3.3 1.5 1.3 volume=0.879 peak=3072 ppm1=1.299 ppm2=2.845 assign ( resid 67 and name HN ) ( resid 68 and name HA ) 3.3 1.5 1.3 volume=0.884 peak=407 ppm1=7.602 ppm2=4.344 assign ( resid 191 and name HB1 ) ( resid 191 and name HA ) 4.3 2.6 1.7 volume=0.174 peak=3796 ppm1=2.817 ppm2=4.275 assign ( resid 1 and name HN# ) ( resid 1 and name HB2 ) 3.5 1.8 1.4 volume=0.588 peak=2281 ppm1=8.201 ppm2=2.042 assign ( resid 11 and name HB# ) ( resid 13 and name HN ) 3.8 2.0 1.5 volume=0.374 peak=2531 ppm1=1.631 ppm2=7.735 assign ( resid 18 and name HB2 ) ( resid 18 and name HN ) 4.0 2.3 1.6 volume=0.253 peak=2692 ppm1=2.446 ppm2=7.800 assign ( resid 2 and name HN ) ( resid 2 and name HB2 or resid 2 and name HB1 ) 3.6 1.9 1.5 volume=0.468 peak=462 ppm1=8.191 ppm2=2.837 assign ( resid 6 and name HD1# ) ( resid 6 and name HG11 or resid 6 and name HG12 ) 2.6 0.9 1.0 volume=3.427 peak=4124 ppm1=0.794 ppm2=1.089 assign ( resid 180 and name HN ) ( resid 179 and name HB2 ) 3.5 1.7 1.4 volume=0.627 peak=777 ppm1=8.353 ppm2=2.489 assign ( resid 135 and name HD2 ) ( resid 134 and name HE1 or resid 134 and name HE2 ) 4.1 2.4 1.7 volume=0.211 peak=4257 ppm1=3.222 ppm2=7.150 assign ( resid 10 and name HG2# ) ( resid 10 and name HN ) 3.4 1.7 1.4 volume=0.666 peak=4209 ppm1=1.084 ppm2=8.327 assign ( resid 177 and name HN ) ( resid 176 and name HG1 ) 3.4 1.6 1.3 volume=0.748 peak=2150 ppm1=8.463 ppm2=1.663 assign ( resid 15 and name HN ) ( resid 15 and name HD1# ) 3.4 1.7 1.4 volume=0.684 peak=986 ppm1=7.809 ppm2=0.420 assign ( resid 93 and name HN ) ( resid 93 and name HD1# ) 3.8 2.1 1.5 volume=0.363 peak=2452 ppm1=8.905 ppm2=-0.288 assign ( resid 79 and name HB2 ) ( resid 99 and name HA ) 3.6 1.8 1.4 volume=0.533 peak=3428 ppm1=1.780 ppm2=4.283 assign ( resid 105 and name HB1 ) ( resid 102 and name HB# ) 3.1 1.3 1.2 volume=1.284 peak=4229 ppm1=3.869 ppm2=1.286 assign ( resid 54 and name HN ) ( resid 165 and name HN ) 3.6 1.9 1.4 volume=0.499 peak=1898 ppm1=9.021 ppm2=8.519 assign ( resid 92 and name HE1 or resid 92 and name HE2 ) ( resid 117 and name HG2# ) 3.0 1.3 1.2 volume=1.477 peak=16 ppm1=6.750 ppm2=0.366 assign ( resid 139 and name HD1 ) ( resid 139 and name HB2 ) 3.9 2.2 1.6 volume=0.296 peak=2895 ppm1=3.620 ppm2=2.197 assign ( resid 117 and name HN ) ( resid 117 and name HG11 ) 3.4 1.7 1.4 volume=0.719 peak=1259 ppm1=8.232 ppm2=0.682 assign ( resid 114 and name HB2 ) ( resid 114 and name HD2# ) 3.4 1.6 1.3 volume=0.739 peak=4225 ppm1=1.701 ppm2=0.778 assign ( resid 39 and name HN ) ( resid 38 and name HA ) 2.8 1.0 1.1 volume=2.473 peak=2100 ppm1=8.244 ppm2=4.281 assign ( resid 141 and name HN ) ( resid 141 and name HB2 or resid 141 and name HB1 ) 3.9 2.1 1.5 volume=0.326 peak=2381 ppm1=8.446 ppm2=3.742 assign ( resid 146 and name HN ) ( resid 144 and name HG11 ) 4.0 2.3 1.6 volume=0.254 peak=1246 ppm1=8.401 ppm2=1.282 assign ( resid 134 and name HN ) ( resid 134 and name HA ) 3.0 1.2 1.2 volume=1.624 peak=277 ppm1=8.746 ppm2=5.182 assign ( resid 31 and name HN ) ( resid 32 and name HA ) 3.5 1.8 1.4 volume=0.613 peak=1036 ppm1=9.253 ppm2=3.747 assign ( resid 132 and name HN ) ( resid 130 and name HN ) 3.5 1.8 1.4 volume=0.556 peak=970 ppm1=7.894 ppm2=7.659 assign ( resid 112 and name HD1# ) ( resid 84 and name HG2# ) 3.2 1.5 1.3 volume=0.916 peak=4722 ppm1=0.373 ppm2=0.116 assign ( resid 21 and name HN ) ( resid 22 and name HN ) 3.6 1.9 1.4 volume=0.477 peak=1642 ppm1=8.282 ppm2=8.174 assign ( resid 23 and name HN ) ( resid 22 and name HB1 ) 3.5 1.8 1.4 volume=0.558 peak=851 ppm1=8.630 ppm2=3.767 assign ( resid 109 and name HB1 or resid 109 and name HB2 ) ( resid 109 and name HG2 or resid 109 and name HG1 ) 3.4 1.7 1.4 volume=0.726 peak=2702 ppm1=1.721 ppm2=1.547 assign ( resid 41 and name HD2 or resid 41 and name HD1 ) ( resid 41 and name HB1 or resid 41 and name HB2 ) 2.8 1.1 1.1 volume=2.013 peak=3648 ppm1=3.096 ppm2=1.999 assign ( resid 199 and name HA ) ( resid 64 and name HD1 or resid 64 and name HD2 ) 4.6 2.9 1.4 volume=0.116 peak=4423 ppm1=2.798 ppm2=5.971 assign ( resid 137 and name HN ) ( resid 137 and name HA ) 3.0 1.2 1.2 volume=1.620 peak=2337 ppm1=8.052 ppm2=4.524 assign ( resid 42 and name HG1 ) ( resid 42 and name HD2 ) 2.1 0.4 0.9 volume=11.081 peak=4185 ppm1=1.291 ppm2=1.521 assign ( resid 106 and name HN ) ( resid 106 and name HG12 or resid 106 and name HG11 ) 3.2 1.5 1.3 volume=0.944 peak=267 ppm1=7.943 ppm2=1.408 assign ( resid 162 and name HA ) ( resid 162 and name HD1 ) 2.4 0.7 1.0 volume=5.393 peak=4470 ppm1=3.650 ppm2=3.489 assign ( resid 52 and name HN ) ( resid 169 and name HN ) 4.0 2.3 1.6 volume=0.266 peak=156 ppm1=8.614 ppm2=9.249 assign ( resid 17 and name HN ) ( resid 18 and name HN ) 3.0 1.3 1.2 volume=1.447 peak=408 ppm1=7.602 ppm2=7.775 assign ( resid 112 and name HG2# ) ( resid 113 and name HA ) 4.1 2.4 1.6 volume=0.224 peak=3002 ppm1=0.680 ppm2=5.266 assign ( resid 158 and name HN ) ( resid 158 and name HA ) 3.0 1.3 1.2 volume=1.479 peak=1536 ppm1=8.217 ppm2=4.136 assign ( resid 160 and name HB1 ) ( resid 160 and name HG2 ) 4.0 2.2 1.6 volume=0.281 peak=3615 ppm1=2.035 ppm2=2.197 assign ( resid 200 and name HA ) ( resid 200 and name HG2 ) 4.0 2.3 1.6 volume=0.264 peak=4732 ppm1=3.363 ppm2=1.134 assign ( resid 200 and name HD1 ) ( resid 196 and name HG2# ) 2.4 0.7 1.0 volume=5.821 peak=4921 ppm1=1.549 ppm2=0.818 assign ( resid 89 and name HB2 ) ( resid 89 and name HA ) 4.6 2.9 1.4 volume=0.107 peak=3836 ppm1=3.875 ppm2=4.163 assign ( resid 130 and name HN ) ( resid 115 and name HN ) 4.1 2.4 1.6 volume=0.232 peak=1016 ppm1=7.616 ppm2=9.015 assign ( resid 183 and name HG2# ) ( resid 183 and name HD1# ) 1.8 0.1 0.7 volume=31.500 peak=4686 ppm1=0.932 ppm2=0.871 assign ( resid 171 and name HN ) ( resid 47 and name HG ) 3.2 1.5 1.3 volume=0.932 peak=1678 ppm1=9.062 ppm2=0.622 assign ( resid 72 and name HB ) ( resid 72 and name HN ) 3.5 1.8 1.4 volume=0.577 peak=2955 ppm1=1.856 ppm2=7.539 assign ( resid 114 and name HG ) ( resid 7 and name HB# ) 3.5 1.8 1.4 volume=0.597 peak=4933 ppm1=0.953 ppm2=0.724 assign ( resid 3 and name HE1 or resid 3 and name HE2 ) ( resid 114 and name HB1 ) 3.0 1.3 1.2 volume=1.410 peak=52 ppm1=7.213 ppm2=1.055 assign ( resid 87 and name HD1# ) ( resid 85 and name HB1 ) 3.4 1.7 1.4 volume=0.661 peak=3314 ppm1=0.440 ppm2=3.044 assign ( resid 26 and name HA ) ( resid 26 and name HN ) 4.0 2.3 1.6 volume=0.255 peak=4162 ppm1=3.980 ppm2=8.864 assign ( resid 102 and name HB# ) ( resid 186 and name HB2 ) 3.9 2.1 1.5 volume=0.320 peak=4884 ppm1=1.279 ppm2=1.846 assign ( resid 71 and name HN ) ( resid 71 and name HA ) 3.5 1.7 1.4 volume=0.625 peak=2308 ppm1=7.218 ppm2=4.860 assign ( resid 97 and name HN ) ( resid 110 and name HA ) 4.2 2.5 1.7 volume=0.193 peak=2110 ppm1=8.364 ppm2=5.442 assign ( resid 168 and name HG2# ) ( resid 168 and name HB ) 3.0 1.3 1.2 volume=1.525 peak=3073 ppm1=0.199 ppm2=1.734 assign ( resid 37 and name HA ) ( resid 49 and name HB1 ) 3.9 2.2 1.6 volume=0.290 peak=4923 ppm1=5.823 ppm2=1.738 assign ( resid 191 and name HB2 ) ( resid 190 and name HN ) 4.1 2.4 1.7 volume=0.214 peak=3659 ppm1=2.814 ppm2=7.489 assign ( resid 71 and name HD1 ) ( resid 71 and name HG2 ) 3.8 2.1 1.5 volume=0.352 peak=3282 ppm1=2.782 ppm2=0.312 assign ( resid 120 and name HN ) ( resid 119 and name HA ) 3.3 1.6 1.3 volume=0.841 peak=1055 ppm1=8.912 ppm2=4.814 assign ( resid 8 and name HG1 or resid 8 and name HG2 ) ( resid 4 and name HG1 or resid 4 and name HG2 ) 4.1 2.4 1.6 volume=0.231 peak=3970 ppm1=2.321 ppm2=1.358 assign ( resid 50 and name HN ) ( resid 49 and name HA ) 3.2 1.5 1.3 volume=1.016 peak=1931 ppm1=9.300 ppm2=4.887 assign ( resid 135 and name HG2 ) ( resid 135 and name HB2 ) 3.0 1.3 1.2 volume=1.364 peak=2666 ppm1=1.786 ppm2=2.185 assign ( resid 117 and name HA ) ( resid 117 and name HG2# ) 4.5 2.8 1.5 volume=0.134 peak=5128 ppm1=5.016 ppm2=0.365 assign ( resid 5 and name HN ) ( resid 4 and name HA ) 3.4 1.6 1.3 volume=0.748 peak=1788 ppm1=7.457 ppm2=3.739 assign ( resid 50 and name HA ) ( resid 50 and name HB ) 3.6 1.9 1.4 volume=0.504 peak=4852 ppm1=5.176 ppm2=1.824 assign ( resid 168 and name HG1# ) ( resid 168 and name HG2# ) 2.7 1.0 1.1 volume=2.892 peak=3220 ppm1=0.767 ppm2=0.195 assign ( resid 134 and name HZ ) ( resid 84 and name HB ) 3.0 1.3 1.2 volume=1.528 peak=85 ppm1=6.644 ppm2=1.978 assign ( resid 186 and name HD1 ) ( resid 186 and name HG2 ) 2.3 0.6 0.9 volume=7.833 peak=4848 ppm1=1.674 ppm2=1.479 assign ( resid 81 and name HN ) ( resid 81 and name HA ) 3.4 1.7 1.4 volume=0.641 peak=1175 ppm1=8.507 ppm2=4.656 assign ( resid 184 and name HG12 ) ( resid 185 and name HN ) 4.6 2.9 1.4 volume=0.115 peak=4366 ppm1=1.094 ppm2=8.187 assign ( resid 96 and name HN ) ( resid 97 and name HD1# ) 3.7 2.0 1.5 volume=0.405 peak=417 ppm1=8.473 ppm2=0.099 assign ( resid 211 and name HA ) ( resid 214 and name HA ) 2.7 1.0 1.1 volume=2.507 peak=3580 ppm1=4.485 ppm2=4.414 assign ( resid 64 and name HA ) ( resid 203 and name HD1# ) 4.2 2.5 1.7 volume=0.198 peak=2858 ppm1=3.860 ppm2=-0.011 assign ( resid 115 and name HN ) ( resid 114 and name HB2 ) 3.7 2.0 1.5 volume=0.392 peak=272 ppm1=9.053 ppm2=1.660 assign ( resid 4 and name HN ) ( resid 2 and name HA ) 2.9 1.2 1.2 volume=1.707 peak=229 ppm1=8.186 ppm2=4.140 assign ( resid 115 and name HG2# ) ( resid 128 and name HN ) 4.0 2.3 1.6 volume=0.269 peak=4128 ppm1=0.660 ppm2=9.959 assign ( resid 132 and name HG1# ) ( resid 114 and name HN ) 3.8 2.1 1.5 volume=0.340 peak=4334 ppm1=0.543 ppm2=8.785 assign ( resid 92 and name HE1 or resid 92 and name HE2 ) ( resid 83 and name HG2 ) 3.6 1.9 1.4 volume=0.514 peak=6 ppm1=6.750 ppm2=1.729 assign ( resid 112 and name HN ) ( resid 112 and name HA ) 3.7 1.9 1.5 volume=0.453 peak=727 ppm1=8.136 ppm2=4.937 assign ( resid 87 and name HD1# ) ( resid 84 and name HG2# ) 3.9 2.1 1.5 volume=0.321 peak=4397 ppm1=0.441 ppm2=0.120 assign ( resid 72 and name HG2# ) ( resid 71 and name HD2 or resid 71 and name HD1 ) 4.0 2.3 1.6 volume=0.247 peak=4937 ppm1=0.603 ppm2=2.796 assign ( resid 17 and name HD1 or resid 17 and name HD2 ) ( resid 14 and name HG2# ) 3.1 1.4 1.2 volume=1.280 peak=108 ppm1=6.485 ppm2=0.740 assign ( resid 91 and name HG2# ) ( resid 4 and name HD1 ) 2.9 1.2 1.2 volume=1.654 peak=2513 ppm1=1.019 ppm2=1.566 assign ( resid 179 and name HD1# ) ( resid 179 and name HG ) 3.3 1.6 1.3 volume=0.870 peak=3433 ppm1=0.531 ppm2=1.516 assign ( resid 192 and name HN ) ( resid 192 and name HB2 ) 3.4 1.6 1.3 volume=0.758 peak=2241 ppm1=8.210 ppm2=1.282 assign ( resid 203 and name HN ) ( resid 199 and name HA ) 3.1 1.3 1.2 volume=1.300 peak=1528 ppm1=7.684 ppm2=2.754 assign ( resid 115 and name HG2# ) ( resid 115 and name HN ) 3.4 1.7 1.4 volume=0.651 peak=3869 ppm1=0.660 ppm2=9.098 assign ( resid 130 and name HB1 ) ( resid 130 and name HN ) 4.0 2.2 1.6 volume=0.275 peak=3120 ppm1=1.886 ppm2=7.618 assign ( resid 183 and name HD1# ) ( resid 183 and name HG11 ) 2.6 0.9 1.0 volume=3.564 peak=4559 ppm1=0.869 ppm2=1.268 assign ( resid 112 and name HG2# ) ( resid 134 and name HZ ) 4.1 2.4 1.6 volume=0.227 peak=2733 ppm1=0.680 ppm2=6.628 assign ( resid 66 and name HN ) ( resid 65 and name HN ) 3.4 1.7 1.4 volume=0.676 peak=814 ppm1=8.049 ppm2=7.727 assign ( resid 125 and name HN ) ( resid 124 and name HB1 ) 2.9 1.2 1.2 volume=1.698 peak=1160 ppm1=8.771 ppm2=2.067 assign ( resid 3 and name HN ) ( resid 6 and name HD1# ) 2.9 1.1 1.1 volume=1.930 peak=468 ppm1=7.913 ppm2=0.759 assign ( resid 166 and name HB1 ) ( resid 168 and name HG1# ) 3.3 1.6 1.3 volume=0.775 peak=5131 ppm1=1.654 ppm2=0.776 assign ( resid 54 and name HN ) ( resid 61 and name HD1# ) 2.7 1.0 1.1 volume=2.597 peak=1021 ppm1=9.024 ppm2=0.753 assign ( resid 84 and name HG2# ) ( resid 84 and name HB ) 3.1 1.3 1.2 volume=1.302 peak=5100 ppm1=0.111 ppm2=2.010 assign ( resid 87 and name HD1# ) ( resid 87 and name HG11 ) 3.0 1.2 1.2 volume=1.609 peak=3384 ppm1=0.441 ppm2=1.232 assign ( resid 197 and name HN ) ( resid 200 and name HN ) 3.0 1.3 1.2 volume=1.436 peak=164 ppm1=7.989 ppm2=8.084 assign ( resid 146 and name HA2 ) ( resid 147 and name HN ) 4.6 2.9 1.4 volume=0.110 peak=3621 ppm1=4.013 ppm2=8.800 assign ( resid 5 and name HB# ) ( resid 8 and name HB2 or resid 8 and name HB1 ) 3.4 1.7 1.4 volume=0.668 peak=3849 ppm1=1.343 ppm2=2.044 assign ( resid 201 and name HB2 ) ( resid 202 and name HN ) 4.0 2.3 1.6 volume=0.249 peak=4982 ppm1=2.582 ppm2=8.580 assign ( resid 201 and name HB2 ) ( resid 201 and name HN ) 3.6 1.9 1.4 volume=0.517 peak=3708 ppm1=2.580 ppm2=7.395 assign ( resid 159 and name HB1 ) ( resid 160 and name HG1 ) 3.9 2.2 1.6 volume=0.296 peak=4645 ppm1=1.876 ppm2=2.142 assign ( resid 3 and name HZ ) ( resid 93 and name HG2# ) 3.6 1.9 1.4 volume=0.504 peak=42 ppm1=6.204 ppm2=0.011 assign ( resid 85 and name HN ) ( resid 93 and name HB ) 2.9 1.2 1.2 volume=1.694 peak=707 ppm1=7.152 ppm2=1.278 assign ( resid 130 and name HA ) ( resid 130 and name HG1 ) 3.8 2.0 1.5 volume=0.385 peak=4668 ppm1=3.882 ppm2=1.308 assign ( resid 98 and name HN ) ( resid 109 and name HB2 ) 3.8 2.0 1.5 volume=0.381 peak=789 ppm1=9.355 ppm2=1.708 assign ( resid 65 and name HB1 or resid 65 and name HB2 ) ( resid 64 and name HE1 or resid 64 and name HE2 ) 4.0 2.3 1.6 volume=0.262 peak=4784 ppm1=1.641 ppm2=6.468 assign ( resid 72 and name HN ) ( resid 72 and name HG11 ) 3.0 1.3 1.2 volume=1.490 peak=1850 ppm1=7.536 ppm2=1.146 assign ( resid 67 and name HB2 ) ( resid 67 and name HN ) 3.0 1.2 1.2 volume=1.616 peak=4275 ppm1=2.065 ppm2=7.604 assign ( resid 12 and name HN ) ( resid 11 and name HN ) 3.1 1.4 1.3 volume=1.105 peak=257 ppm1=7.546 ppm2=8.172 assign ( resid 142 and name HB1 ) ( resid 143 and name HA ) 3.8 2.1 1.5 volume=0.348 peak=2861 ppm1=1.884 ppm2=4.687 assign ( resid 106 and name HN ) ( resid 104 and name HA2 ) 3.6 1.8 1.4 volume=0.521 peak=2414 ppm1=7.941 ppm2=3.491 assign ( resid 91 and name HG2# ) ( resid 91 and name HB ) 3.6 1.8 1.4 volume=0.524 peak=4508 ppm1=1.017 ppm2=3.627 assign ( resid 73 and name HG2# ) ( resid 202 and name HA2 ) 4.6 2.8 1.4 volume=0.121 peak=3188 ppm1=1.218 ppm2=3.377 assign ( resid 95 and name HN ) ( resid 95 and name HA ) 3.8 2.1 1.5 volume=0.362 peak=822 ppm1=9.127 ppm2=5.567 assign ( resid 13 and name HN ) ( resid 11 and name HN ) 3.7 2.0 1.5 volume=0.408 peak=601 ppm1=7.721 ppm2=8.170 assign ( resid 167 and name HA ) ( resid 168 and name HG1# ) 3.6 1.9 1.4 volume=0.474 peak=5054 ppm1=5.218 ppm2=0.791 assign ( resid 126 and name HN ) ( resid 126 and name HA ) 3.8 2.1 1.5 volume=0.371 peak=2224 ppm1=9.105 ppm2=5.315 assign ( resid 24 and name HZ2 ) ( resid 24 and name HZ1 ) 3.0 1.3 1.2 volume=1.442 peak=76 ppm1=7.537 ppm2=7.016 assign ( resid 10 and name HN ) ( resid 10 and name HG2# ) 3.3 1.5 1.3 volume=0.898 peak=564 ppm1=8.320 ppm2=1.078 assign ( resid 188 and name HA ) ( resid 187 and name HG2# ) 4.4 2.7 1.6 volume=0.142 peak=4266 ppm1=4.211 ppm2=1.088 assign ( resid 91 and name HA ) ( resid 91 and name HN ) 3.9 2.2 1.6 volume=0.314 peak=2998 ppm1=5.876 ppm2=7.223 assign ( resid 69 and name HN ) ( resid 68 and name HG2# ) 3.7 2.0 1.5 volume=0.402 peak=475 ppm1=8.219 ppm2=0.745 assign ( resid 81 and name HN ) ( resid 80 and name HA ) 2.9 1.2 1.2 volume=1.869 peak=2312 ppm1=8.508 ppm2=4.002 assign ( resid 184 and name HG12 ) ( resid 184 and name HB ) 4.1 2.4 1.7 volume=0.211 peak=4815 ppm1=1.095 ppm2=2.049 assign ( resid 112 and name HG2# ) ( resid 94 and name HN ) 4.3 2.6 1.7 volume=0.172 peak=2690 ppm1=0.678 ppm2=9.594 assign ( resid 44 and name HN ) ( resid 45 and name HA1 ) 3.8 2.1 1.5 volume=0.334 peak=2049 ppm1=8.371 ppm2=3.627 assign ( resid 196 and name HA ) ( resid 196 and name HG12 ) 4.4 2.7 1.6 volume=0.152 peak=3656 ppm1=3.454 ppm2=1.468 assign ( resid 116 and name HA ) ( resid 117 and name HN ) 4.6 2.9 1.4 volume=0.109 peak=4545 ppm1=6.165 ppm2=8.204 assign ( resid 179 and name HD2# ) ( resid 179 and name HB2 ) 3.7 2.0 1.5 volume=0.414 peak=3763 ppm1=0.743 ppm2=2.486 assign ( resid 194 and name HN ) ( resid 195 and name HN ) 2.9 1.2 1.2 volume=1.722 peak=1797 ppm1=7.772 ppm2=7.965 assign ( resid 190 and name HA ) ( resid 192 and name HN ) 4.2 2.5 1.7 volume=0.204 peak=3493 ppm1=3.977 ppm2=8.190 assign ( resid 203 and name HD1# ) ( resid 63 and name HB2 ) 3.4 1.6 1.3 volume=0.743 peak=5080 ppm1=-0.010 ppm2=2.664 assign ( resid 14 and name HG1# ) ( resid 14 and name HA ) 3.1 1.4 1.2 volume=1.228 peak=3334 ppm1=0.677 ppm2=2.817 assign ( resid 15 and name HD2# ) ( resid 12 and name HB2 or resid 12 and name HB1 ) 3.8 2.1 1.5 volume=0.331 peak=3581 ppm1=0.683 ppm2=2.201 assign ( resid 26 and name HG1# ) ( resid 28 and name HN ) 3.3 1.6 1.3 volume=0.866 peak=2707 ppm1=0.779 ppm2=7.811 assign ( resid 46 and name HN ) ( resid 46 and name HA ) 2.9 1.2 1.2 volume=1.664 peak=2144 ppm1=8.558 ppm2=4.937 assign ( resid 203 and name HD1# ) ( resid 54 and name HB ) 3.1 1.4 1.2 volume=1.182 peak=3450 ppm1=-0.010 ppm2=1.808 assign ( resid 14 and name HN ) ( resid 12 and name HA ) 3.2 1.5 1.3 volume=1.015 peak=999 ppm1=7.788 ppm2=3.893 assign ( resid 84 and name HG1# ) ( resid 84 and name HN ) 3.4 1.6 1.3 volume=0.754 peak=5052 ppm1=0.534 ppm2=8.519 assign ( resid 155 and name HN ) ( resid 155 and name HB1 ) 3.4 1.7 1.4 volume=0.643 peak=1673 ppm1=8.977 ppm2=2.964 assign ( resid 168 and name HN ) ( resid 155 and name HA ) 3.5 1.8 1.4 volume=0.586 peak=443 ppm1=8.694 ppm2=5.252 assign ( resid 62 and name HN ) ( resid 61 and name HN ) 3.6 1.9 1.4 volume=0.505 peak=741 ppm1=8.130 ppm2=8.707 assign ( resid 57 and name HN ) ( resid 203 and name HG11 ) 3.6 1.9 1.5 volume=0.468 peak=1371 ppm1=9.220 ppm2=0.492 assign ( resid 171 and name HN ) ( resid 48 and name HB1 ) 3.6 1.8 1.4 volume=0.532 peak=491 ppm1=9.062 ppm2=2.575 assign ( resid 112 and name HG11 ) ( resid 112 and name HG12 ) 3.3 1.6 1.3 volume=0.812 peak=2615 ppm1=1.602 ppm2=1.254 assign ( resid 129 and name HB2 ) ( resid 129 and name HN ) 4.2 2.5 1.7 volume=0.199 peak=4212 ppm1=3.367 ppm2=8.721 assign ( resid 193 and name HN ) ( resid 192 and name HN ) 3.4 1.6 1.3 volume=0.756 peak=1046 ppm1=7.621 ppm2=8.184 assign ( resid 127 and name HD1# ) ( resid 65 and name HG ) 3.3 1.6 1.3 volume=0.856 peak=4844 ppm1=0.286 ppm2=1.624 assign ( resid 134 and name HB1 ) ( resid 133 and name HA ) 4.1 2.4 1.7 volume=0.217 peak=3239 ppm1=3.050 ppm2=4.684 assign ( resid 122 and name HN ) ( resid 122 and name HA1 ) 3.4 1.7 1.4 volume=0.707 peak=2283 ppm1=8.645 ppm2=3.821 assign ( resid 149 and name HN ) ( resid 148 and name HB1 ) 4.0 2.2 1.6 volume=0.276 peak=1106 ppm1=7.757 ppm2=2.948 assign ( resid 198 and name HN ) ( resid 197 and name HN ) 3.0 1.3 1.2 volume=1.517 peak=2023 ppm1=8.717 ppm2=8.001 assign ( resid 132 and name HG2# ) ( resid 113 and name HA ) 4.0 2.3 1.6 volume=0.264 peak=2550 ppm1=0.937 ppm2=5.283 assign ( resid 184 and name HG2# ) ( resid 187 and name HB ) 3.7 2.0 1.5 volume=0.387 peak=4734 ppm1=1.093 ppm2=4.103 assign ( resid 60 and name HN ) ( resid 60 and name HD1 ) 3.9 2.2 1.6 volume=0.286 peak=1184 ppm1=7.266 ppm2=1.529 assign ( resid 98 and name HN ) ( resid 109 and name HA ) 3.7 2.0 1.5 volume=0.433 peak=2087 ppm1=9.354 ppm2=3.877 assign ( resid 188 and name HB2 ) ( resid 185 and name HA ) 3.9 2.2 1.6 volume=0.292 peak=4497 ppm1=1.446 ppm2=3.841 assign ( resid 62 and name HN ) ( resid 155 and name HB2 ) 3.8 2.1 1.5 volume=0.348 peak=760 ppm1=8.130 ppm2=2.562 assign ( resid 126 and name HD1# ) ( resid 10 and name HG2# ) 2.9 1.1 1.1 volume=2.003 peak=2650 ppm1=0.348 ppm2=1.081 assign ( resid 163 and name HN ) ( resid 162 and name HB2 ) 3.4 1.7 1.3 volume=0.730 peak=1636 ppm1=7.326 ppm2=2.184 assign ( resid 84 and name HN ) ( resid 84 and name HA ) 3.1 1.4 1.2 volume=1.203 peak=735 ppm1=8.505 ppm2=4.269 assign ( resid 68 and name HN ) ( resid 71 and name HB2 ) 4.0 2.3 1.6 volume=0.253 peak=158 ppm1=8.024 ppm2=1.536 assign ( resid 141 and name HA ) ( resid 142 and name HN ) 3.6 1.9 1.4 volume=0.475 peak=3806 ppm1=3.931 ppm2=7.872 assign ( resid 34 and name HG2# ) ( resid 34 and name HN ) 3.9 2.1 1.5 volume=0.328 peak=3934 ppm1=1.101 ppm2=8.150 assign ( resid 199 and name HB# ) ( resid 64 and name HZ ) 3.4 1.7 1.4 volume=0.698 peak=3169 ppm1=0.692 ppm2=7.095 assign ( resid 184 and name HD1# ) ( resid 185 and name HN ) 3.9 2.2 1.6 volume=0.306 peak=3391 ppm1=0.894 ppm2=8.185 assign ( resid 167 and name HN ) ( resid 166 and name HA ) 3.2 1.4 1.3 volume=1.083 peak=234 ppm1=8.643 ppm2=4.400 assign ( resid 35 and name HN ) ( resid 28 and name HB1 ) 3.8 2.1 1.5 volume=0.369 peak=2293 ppm1=9.428 ppm2=1.890 assign ( resid 126 and name HN ) ( resid 154 and name HB ) 3.3 1.6 1.3 volume=0.783 peak=2422 ppm1=9.105 ppm2=2.172 assign ( resid 22 and name HN ) ( resid 23 and name HN ) 3.8 2.1 1.5 volume=0.356 peak=1825 ppm1=8.190 ppm2=8.684 assign ( resid 207 and name HN ) ( resid 207 and name HG1 ) 3.2 1.5 1.3 volume=0.977 peak=1220 ppm1=7.833 ppm2=1.537 assign ( resid 136 and name HG2 ) ( resid 136 and name HB1 ) 2.3 0.6 0.9 volume=6.719 peak=4687 ppm1=1.948 ppm2=1.743 assign ( resid 36 and name HA ) ( resid 27 and name HN ) 4.1 2.4 1.6 volume=0.221 peak=3147 ppm1=5.851 ppm2=9.306 assign ( resid 54 and name HB ) ( resid 203 and name HG2# ) 4.2 2.5 1.7 volume=0.201 peak=4703 ppm1=1.771 ppm2=0.332 assign ( resid 121 and name HB1 ) ( resid 121 and name HA ) 3.3 1.6 1.3 volume=0.838 peak=3071 ppm1=2.053 ppm2=4.170 assign ( resid 143 and name HB2 ) ( resid 139 and name HB1 ) 3.0 1.3 1.2 volume=1.393 peak=4504 ppm1=2.705 ppm2=2.213 assign ( resid 165 and name HN ) ( resid 166 and name HA ) 3.4 1.7 1.4 volume=0.677 peak=969 ppm1=8.464 ppm2=4.521 assign ( resid 90 and name HN ) ( resid 90 and name HB2 ) 3.2 1.5 1.3 volume=0.932 peak=987 ppm1=8.383 ppm2=3.359 assign ( resid 68 and name HG2# ) ( resid 83 and name HA ) 3.9 2.2 1.6 volume=0.291 peak=4765 ppm1=0.752 ppm2=4.680 assign ( resid 154 and name HB ) ( resid 126 and name HG12 ) 3.1 1.4 1.3 volume=1.133 peak=3738 ppm1=2.180 ppm2=1.085 assign ( resid 196 and name HG2# ) ( resid 33 and name HA ) 4.9 3.2 1.1 volume=0.080 peak=2844 ppm1=0.812 ppm2=4.676 assign ( resid 184 and name HN ) ( resid 182 and name HA ) 3.7 2.0 1.5 volume=0.417 peak=1352 ppm1=7.499 ppm2=4.157 assign ( resid 89 and name HB2 ) ( resid 91 and name HN ) 4.2 2.5 1.7 volume=0.188 peak=4976 ppm1=3.877 ppm2=7.223 assign ( resid 71 and name HD2 ) ( resid 71 and name HB2 ) 2.6 0.9 1.0 volume=3.626 peak=4625 ppm1=2.780 ppm2=1.528 assign ( resid 115 and name HG1# ) ( resid 114 and name HB1 ) 3.1 1.4 1.2 volume=1.267 peak=3270 ppm1=0.301 ppm2=1.047 assign ( resid 34 and name HN ) ( resid 34 and name HB ) 3.0 1.3 1.2 volume=1.547 peak=1802 ppm1=8.136 ppm2=3.747 assign ( resid 15 and name HN ) ( resid 16 and name HN ) 3.2 1.5 1.3 volume=0.912 peak=412 ppm1=7.809 ppm2=7.525 assign ( resid 166 and name HN ) ( resid 166 and name HA ) 3.4 1.6 1.3 volume=0.735 peak=1656 ppm1=8.999 ppm2=4.477 assign ( resid 214 and name HN ) ( resid 211 and name HA ) 3.5 1.7 1.4 volume=0.632 peak=711 ppm1=7.956 ppm2=4.474 assign ( resid 128 and name HA ) ( resid 14 and name HG1# ) 4.0 2.2 1.6 volume=0.281 peak=3408 ppm1=5.581 ppm2=0.695 assign ( resid 19 and name HN ) ( resid 18 and name HN ) 3.3 1.6 1.3 volume=0.781 peak=2111 ppm1=7.481 ppm2=7.787 assign ( resid 177 and name HN ) ( resid 144 and name HD1# ) 3.5 1.8 1.4 volume=0.565 peak=894 ppm1=8.462 ppm2=0.615 assign ( resid 169 and name HA ) ( resid 153 and name HN ) 4.1 2.4 1.6 volume=0.236 peak=3550 ppm1=5.252 ppm2=9.333 assign ( resid 172 and name HG2 ) ( resid 172 and name HN ) 4.4 2.7 1.6 volume=0.149 peak=4022 ppm1=2.295 ppm2=8.854 assign ( resid 131 and name HN ) ( resid 150 and name HA ) 3.6 1.9 1.4 volume=0.480 peak=2352 ppm1=9.294 ppm2=4.000 assign ( resid 210 and name HA ) ( resid 210 and name HB1 ) 3.4 1.7 1.4 volume=0.644 peak=4654 ppm1=4.268 ppm2=3.758 assign ( resid 184 and name HA ) ( resid 186 and name HG1 or resid 186 and name HG2 ) 3.9 2.1 1.5 volume=0.320 peak=3872 ppm1=3.630 ppm2=1.490 assign ( resid 211 and name HN ) ( resid 208 and name HG2# ) 3.5 1.8 1.4 volume=0.564 peak=720 ppm1=8.307 ppm2=1.145 assign ( resid 203 and name HN ) ( resid 203 and name HB ) 2.7 1.0 1.1 volume=2.825 peak=860 ppm1=7.682 ppm2=0.122 assign ( resid 102 and name HB# ) ( resid 103 and name HA ) 3.9 2.2 1.6 volume=0.298 peak=2825 ppm1=1.279 ppm2=3.645 assign ( resid 127 and name HN ) ( resid 126 and name HG2# ) 3.2 1.5 1.3 volume=0.929 peak=178 ppm1=9.384 ppm2=0.746 assign ( resid 67 and name HA ) ( resid 67 and name HG1 ) 3.9 2.2 1.6 volume=0.312 peak=4233 ppm1=3.935 ppm2=2.634 assign ( resid 54 and name HN ) ( resid 54 and name HB ) 3.0 1.3 1.2 volume=1.395 peak=1633 ppm1=9.023 ppm2=1.744 assign ( resid 147 and name HN ) ( resid 176 and name HB2 ) 3.4 1.7 1.4 volume=0.640 peak=920 ppm1=8.784 ppm2=1.857 assign ( resid 96 and name HB ) ( resid 96 and name HG2# ) 3.6 1.9 1.4 volume=0.511 peak=3917 ppm1=3.865 ppm2=1.142 assign ( resid 166 and name HN ) ( resid 156 and name HN ) 3.2 1.5 1.3 volume=0.988 peak=2073 ppm1=9.000 ppm2=8.566 assign ( resid 69 and name HN ) ( resid 70 and name HB1 or resid 70 and name HB2 ) 3.4 1.7 1.4 volume=0.650 peak=2250 ppm1=8.219 ppm2=2.570 assign ( resid 149 and name HN ) ( resid 148 and name HA ) 3.4 1.7 1.3 volume=0.731 peak=1028 ppm1=7.760 ppm2=4.992 assign ( resid 33 and name HG11 ) ( resid 32 and name HB2 or resid 32 and name HB1 ) 2.7 0.9 1.1 volume=2.982 peak=4971 ppm1=1.886 ppm2=2.206 assign ( resid 132 and name HG2# ) ( resid 3 and name HB1 or resid 3 and name HB2 ) 3.9 2.2 1.6 volume=0.285 peak=4511 ppm1=0.935 ppm2=3.055 assign ( resid 193 and name HN ) ( resid 192 and name HB1 ) 3.4 1.6 1.3 volume=0.746 peak=847 ppm1=7.621 ppm2=1.308 assign ( resid 14 and name HN ) ( resid 12 and name HN ) 3.2 1.5 1.3 volume=0.932 peak=1808 ppm1=7.789 ppm2=7.531 assign ( resid 27 and name HN ) ( resid 27 and name HA ) 3.2 1.5 1.3 volume=0.915 peak=1957 ppm1=9.277 ppm2=4.488 assign ( resid 198 and name HN ) ( resid 197 and name HA ) 3.4 1.7 1.4 volume=0.722 peak=2322 ppm1=8.717 ppm2=3.745 assign ( resid 103 and name HN ) ( resid 102 and name HA ) 3.4 1.7 1.4 volume=0.685 peak=934 ppm1=8.452 ppm2=4.139 assign ( resid 92 and name HN ) ( resid 115 and name HG2# ) 3.2 1.5 1.3 volume=0.980 peak=1095 ppm1=9.457 ppm2=0.624 assign ( resid 160 and name HA ) ( resid 160 and name HB1 ) 2.8 1.1 1.1 volume=2.193 peak=3592 ppm1=4.009 ppm2=2.008 assign ( resid 202 and name HN ) ( resid 202 and name HA1 ) 3.1 1.4 1.2 volume=1.213 peak=631 ppm1=8.576 ppm2=3.023 assign ( resid 57 and name HN ) ( resid 56 and name HG1 ) 3.5 1.7 1.4 volume=0.628 peak=2103 ppm1=9.217 ppm2=1.989 assign ( resid 97 and name HN ) ( resid 96 and name HG2# ) 3.1 1.4 1.2 volume=1.269 peak=799 ppm1=8.363 ppm2=1.135 assign ( resid 206 and name HN ) ( resid 205 and name HB# ) 3.0 1.3 1.2 volume=1.407 peak=1782 ppm1=7.462 ppm2=1.274 assign ( resid 87 and name HG12 ) ( resid 87 and name HG2# ) 2.8 1.1 1.1 volume=2.271 peak=2503 ppm1=1.049 ppm2=0.845 assign ( resid 17 and name HD1 or resid 17 and name HD2 ) ( resid 47 and name HD1# ) 3.6 1.8 1.4 volume=0.535 peak=116 ppm1=6.485 ppm2=0.106 assign ( resid 109 and name HN ) ( resid 99 and name HA ) 3.5 1.8 1.4 volume=0.554 peak=1287 ppm1=8.168 ppm2=4.283 assign ( resid 199 and name HN ) ( resid 201 and name HN ) 3.7 2.0 1.5 volume=0.422 peak=1915 ppm1=8.634 ppm2=7.398 assign ( resid 126 and name HN ) ( resid 155 and name HN ) 3.5 1.8 1.4 volume=0.579 peak=1794 ppm1=9.105 ppm2=8.994 assign ( resid 142 and name HB1 ) ( resid 142 and name HA ) 3.8 2.1 1.5 volume=0.365 peak=4429 ppm1=1.884 ppm2=4.137 assign ( resid 176 and name HG1 ) ( resid 176 and name HB2 ) 3.8 2.1 1.5 volume=0.367 peak=2869 ppm1=1.641 ppm2=1.860 assign ( resid 92 and name HN ) ( resid 92 and name HB2 ) 3.4 1.7 1.4 volume=0.651 peak=364 ppm1=9.457 ppm2=3.102 assign ( resid 165 and name HN ) ( resid 53 and name HG2# ) 3.4 1.7 1.4 volume=0.657 peak=2298 ppm1=8.465 ppm2=0.876 assign ( resid 51 and name HG1 or resid 51 and name HG2 ) ( resid 51 and name HA ) 4.5 2.8 1.5 volume=0.123 peak=4465 ppm1=1.970 ppm2=5.613 assign ( resid 14 and name HG1# ) ( resid 11 and name HA ) 3.8 2.1 1.5 volume=0.347 peak=5153 ppm1=0.678 ppm2=3.954 assign ( resid 18 and name HN ) ( resid 18 and name HB2 ) 3.3 1.6 1.3 volume=0.775 peak=1426 ppm1=7.760 ppm2=2.451 assign ( resid 196 and name HA ) ( resid 199 and name HB# ) 3.2 1.4 1.3 volume=1.067 peak=4664 ppm1=3.454 ppm2=0.689 assign ( resid 60 and name HB1 ) ( resid 60 and name HD1 ) 2.3 0.6 0.9 volume=7.495 peak=2847 ppm1=1.718 ppm2=1.532 assign ( resid 80 and name HA ) ( resid 80 and name HN ) 3.7 1.9 1.5 volume=0.447 peak=3805 ppm1=3.985 ppm2=7.525 assign ( resid 196 and name HG12 ) ( resid 196 and name HG11 ) 2.8 1.1 1.1 volume=2.183 peak=5071 ppm1=1.476 ppm2=1.807 assign ( resid 3 and name HZ ) ( resid 3 and name HE1 or resid 3 and name HE2 ) 3.3 1.6 1.3 volume=0.794 peak=89 ppm1=6.203 ppm2=7.216 assign ( resid 51 and name HB1 or resid 51 and name HB2 ) ( resid 51 and name HA ) 4.2 2.4 1.7 volume=0.207 peak=3451 ppm1=1.781 ppm2=5.621 assign ( resid 29 and name HN ) ( resid 28 and name HG1 ) 2.9 1.2 1.2 volume=1.638 peak=2162 ppm1=8.568 ppm2=1.008 assign ( resid 158 and name HN ) ( resid 158 and name HG1 ) 2.9 1.2 1.2 volume=1.870 peak=1484 ppm1=8.216 ppm2=2.437 assign ( resid 203 and name HG2# ) ( resid 206 and name HB1 ) 3.4 1.6 1.3 volume=0.747 peak=4994 ppm1=0.339 ppm2=2.930 assign ( resid 147 and name HN ) ( resid 146 and name HA2 ) 3.2 1.5 1.3 volume=0.934 peak=2211 ppm1=8.785 ppm2=4.005 assign ( resid 28 and name HN ) ( resid 26 and name HA ) 2.9 1.2 1.2 volume=1.711 peak=1911 ppm1=7.810 ppm2=3.971 assign ( resid 136 and name HG2 ) ( resid 134 and name HZ ) 3.2 1.5 1.3 volume=1.005 peak=3013 ppm1=1.953 ppm2=6.645 assign ( resid 166 and name HG2 ) ( resid 166 and name HE1 ) 4.0 2.3 1.6 volume=0.266 peak=3099 ppm1=1.252 ppm2=2.710 assign ( resid 154 and name HG2# ) ( resid 156 and name HN ) 4.1 2.4 1.7 volume=0.217 peak=4831 ppm1=0.837 ppm2=8.518 assign ( resid 9 and name HN ) ( resid 8 and name HB2 or resid 8 and name HB1 ) 2.5 0.8 1.0 volume=4.636 peak=1522 ppm1=7.984 ppm2=2.049 assign ( resid 109 and name HG1 ) ( resid 109 and name HN ) 3.7 2.0 1.5 volume=0.414 peak=4713 ppm1=1.546 ppm2=8.168 assign ( resid 35 and name HN ) ( resid 29 and name HG2# ) 2.7 1.0 1.1 volume=2.926 peak=533 ppm1=9.427 ppm2=1.014 assign ( resid 196 and name HD1# ) ( resid 196 and name HG11 ) 2.8 1.1 1.1 volume=2.367 peak=4348 ppm1=0.727 ppm2=1.807 assign ( resid 73 and name HB ) ( resid 72 and name HD1# ) 4.1 2.4 1.7 volume=0.210 peak=4952 ppm1=4.300 ppm2=0.577 assign ( resid 69 and name HN ) ( resid 68 and name HN ) 3.0 1.2 1.2 volume=1.625 peak=1572 ppm1=8.216 ppm2=8.025 assign ( resid 90 and name HN ) ( resid 117 and name HN ) 4.1 2.4 1.6 volume=0.221 peak=879 ppm1=8.381 ppm2=8.239 assign ( resid 158 and name HA ) ( resid 166 and name HB2 ) 3.0 1.3 1.2 volume=1.433 peak=3710 ppm1=4.139 ppm2=1.677 assign ( resid 3 and name HZ ) ( resid 93 and name HD1# ) 3.1 1.3 1.2 volume=1.331 peak=135 ppm1=6.203 ppm2=-0.280 assign ( resid 127 and name HD1# ) ( resid 127 and name HN ) 4.2 2.4 1.7 volume=0.205 peak=3923 ppm1=0.285 ppm2=9.381 assign ( resid 96 and name HN ) ( resid 111 and name HN ) 3.0 1.3 1.2 volume=1.466 peak=184 ppm1=8.473 ppm2=8.632 assign ( resid 73 and name HG2# ) ( resid 72 and name HA ) 4.5 2.8 1.5 volume=0.133 peak=2797 ppm1=1.218 ppm2=3.638 assign ( resid 111 and name HN ) ( resid 146 and name HN ) 4.2 2.5 1.7 volume=0.194 peak=918 ppm1=8.631 ppm2=8.394 assign ( resid 28 and name HN ) ( resid 29 and name HG2# ) 2.6 0.9 1.0 volume=3.584 peak=1150 ppm1=7.808 ppm2=0.974 assign ( resid 112 and name HD1# ) ( resid 113 and name HN ) 3.8 2.1 1.5 volume=0.356 peak=3772 ppm1=0.373 ppm2=8.266 assign ( resid 203 and name HG11 or resid 203 and name HG12 ) ( resid 203 and name HG2# ) 3.4 1.7 1.3 volume=0.727 peak=2946 ppm1=0.516 ppm2=0.335 assign ( resid 71 and name HB2 ) ( resid 71 and name HD2 ) 4.1 2.4 1.7 volume=0.211 peak=2549 ppm1=1.527 ppm2=2.782 assign ( resid 154 and name HB ) ( resid 126 and name HB ) 3.1 1.4 1.3 volume=1.123 peak=4355 ppm1=2.180 ppm2=1.587 assign ( resid 114 and name HD2# ) ( resid 114 and name HG ) 2.4 0.7 1.0 volume=5.101 peak=3079 ppm1=0.781 ppm2=0.949 assign ( resid 75 and name HN ) ( resid 78 and name HB2 ) 3.2 1.5 1.3 volume=0.915 peak=2068 ppm1=7.480 ppm2=1.375 assign ( resid 49 and name HN ) ( resid 35 and name HG2# or resid 35 and name HG1# ) 3.2 1.5 1.3 volume=0.919 peak=1285 ppm1=8.917 ppm2=0.876 assign ( resid 2 and name HA ) ( resid 2 and name HB2 ) 4.3 2.5 1.7 volume=0.180 peak=2623 ppm1=4.146 ppm2=2.831 assign ( resid 63 and name HN ) ( resid 61 and name HN ) 3.8 2.1 1.5 volume=0.371 peak=2432 ppm1=7.294 ppm2=8.708 assign ( resid 134 and name HN ) ( resid 133 and name HN ) 3.6 1.8 1.4 volume=0.520 peak=2190 ppm1=8.745 ppm2=8.164 assign ( resid 132 and name HB ) ( resid 132 and name HG1# ) 3.5 1.8 1.4 volume=0.606 peak=3638 ppm1=2.284 ppm2=0.537 assign ( resid 168 and name HN ) ( resid 167 and name HD1# ) 2.9 1.1 1.1 volume=1.953 peak=1532 ppm1=8.694 ppm2=0.742 assign ( resid 183 and name HG11 ) ( resid 183 and name HG12 ) 2.9 1.2 1.2 volume=1.808 peak=2980 ppm1=1.269 ppm2=1.538 assign ( resid 54 and name HD1# ) ( resid 167 and name HN ) 3.6 1.9 1.4 volume=0.500 peak=3452 ppm1=0.492 ppm2=8.717 assign ( resid 212 and name HN ) ( resid 210 and name HA ) 3.3 1.5 1.3 volume=0.890 peak=1002 ppm1=8.246 ppm2=4.270 assign ( resid 93 and name HG2# ) ( resid 93 and name HG12 ) 2.8 1.1 1.1 volume=2.182 peak=2522 ppm1=-0.013 ppm2=0.597 assign ( resid 123 and name HB1 or resid 123 and name HB2 ) ( resid 123 and name HA ) 4.0 2.3 1.6 volume=0.269 peak=3049 ppm1=2.735 ppm2=4.289 assign ( resid 162 and name HB1 ) ( resid 57 and name HA ) 3.6 1.9 1.4 volume=0.479 peak=4892 ppm1=2.206 ppm2=4.160 assign ( resid 96 and name HN ) ( resid 111 and name HB2 ) 3.4 1.7 1.4 volume=0.704 peak=208 ppm1=8.473 ppm2=2.963 assign ( resid 35 and name HG2# ) ( resid 35 and name HB ) 3.0 1.3 1.2 volume=1.451 peak=2807 ppm1=0.889 ppm2=2.056 assign ( resid 14 and name HA ) ( resid 14 and name HB ) 3.9 2.2 1.6 volume=0.317 peak=2799 ppm1=2.817 ppm2=1.714 assign ( resid 35 and name HG2# ) ( resid 189 and name HA ) 3.7 2.0 1.5 volume=0.431 peak=3793 ppm1=0.890 ppm2=4.650 assign ( resid 184 and name HG2# ) ( resid 185 and name HA ) 3.7 2.0 1.5 volume=0.417 peak=2575 ppm1=1.095 ppm2=3.911 assign ( resid 193 and name HA ) ( resid 193 and name HN ) 3.9 2.2 1.6 volume=0.293 peak=3053 ppm1=3.462 ppm2=7.623 assign ( resid 160 and name HB1 ) ( resid 160 and name HA ) 3.1 1.4 1.2 volume=1.190 peak=4333 ppm1=2.034 ppm2=4.018 assign ( resid 132 and name HG1# ) ( resid 133 and name HB2 or resid 133 and name HB1 ) 3.6 1.9 1.4 volume=0.478 peak=3974 ppm1=0.544 ppm2=2.513 assign ( resid 145 and name HN ) ( resid 145 and name HA ) 3.7 2.0 1.5 volume=0.403 peak=757 ppm1=8.380 ppm2=4.927 assign ( resid 184 and name HA ) ( resid 184 and name HB ) 3.3 1.5 1.3 volume=0.908 peak=4351 ppm1=3.629 ppm2=2.070 assign ( resid 37 and name HN ) ( resid 37 and name HA ) 2.9 1.2 1.2 volume=1.751 peak=696 ppm1=9.659 ppm2=5.807 assign ( resid 169 and name HN ) ( resid 50 and name HN ) 3.4 1.7 1.4 volume=0.660 peak=1026 ppm1=9.257 ppm2=9.302 assign ( resid 72 and name HA ) ( resid 72 and name HB ) 3.3 1.6 1.3 volume=0.807 peak=4178 ppm1=3.634 ppm2=1.850 assign ( resid 130 and name HD2 ) ( resid 6 and name HG2# ) 4.2 2.5 1.7 volume=0.203 peak=3341 ppm1=1.660 ppm2=0.833 assign ( resid 176 and name HB2 ) ( resid 176 and name HA ) 4.4 2.7 1.6 volume=0.141 peak=3379 ppm1=1.851 ppm2=4.008 assign ( resid 187 and name HG2# ) ( resid 191 and name HN ) 3.8 2.1 1.5 volume=0.365 peak=3019 ppm1=1.052 ppm2=7.677 assign ( resid 41 and name HN ) ( resid 43 and name HN ) 3.9 2.2 1.5 volume=0.317 peak=1489 ppm1=8.907 ppm2=7.266 assign ( resid 168 and name HB ) ( resid 168 and name HN ) 4.4 2.7 1.6 volume=0.142 peak=2927 ppm1=1.728 ppm2=8.704 assign ( resid 73 and name HN ) ( resid 74 and name HB1 ) 4.4 2.7 1.6 volume=0.142 peak=1097 ppm1=7.507 ppm2=3.249 assign ( resid 143 and name HN ) ( resid 141 and name HN ) 3.9 2.2 1.6 volume=0.310 peak=1103 ppm1=6.900 ppm2=8.441 assign ( resid 167 and name HD2# ) ( resid 167 and name HB2 ) 4.0 2.2 1.6 volume=0.279 peak=4531 ppm1=0.763 ppm2=1.684 assign ( resid 144 and name HG2# ) ( resid 144 and name HN ) 3.6 1.9 1.4 volume=0.484 peak=4143 ppm1=0.766 ppm2=7.536 assign ( resid 64 and name HE1 or resid 64 and name HE2 ) ( resid 64 and name HD1 or resid 64 and name HD2 ) 3.5 1.8 1.4 volume=0.573 peak=90 ppm1=6.486 ppm2=5.969 assign ( resid 152 and name HN ) ( resid 152 and name HA2 ) 3.5 1.7 1.4 volume=0.615 peak=1124 ppm1=8.345 ppm2=3.879 assign ( resid 51 and name HA ) ( resid 51 and name HB1 or resid 51 and name HB2 ) 3.7 1.9 1.5 volume=0.441 peak=4859 ppm1=5.622 ppm2=1.749 assign ( resid 51 and name HG1 or resid 51 and name HG2 ) ( resid 168 and name HG1# ) 3.0 1.2 1.2 volume=1.582 peak=3963 ppm1=1.971 ppm2=0.759 assign ( resid 62 and name HN ) ( resid 59 and name HA ) 3.6 1.9 1.4 volume=0.506 peak=2000 ppm1=8.131 ppm2=4.513 assign ( resid 130 and name HN ) ( resid 114 and name HN ) 3.4 1.7 1.4 volume=0.659 peak=728 ppm1=7.616 ppm2=8.824 assign ( resid 3 and name HE1 or resid 3 and name HE2 ) ( resid 3 and name HB1 or resid 3 and name HB2 ) 3.1 1.3 1.2 volume=1.311 peak=140 ppm1=7.212 ppm2=3.041 assign ( resid 176 and name HD1 ) ( resid 176 and name HB1 ) 3.9 2.2 1.6 volume=0.309 peak=5039 ppm1=3.213 ppm2=1.869 assign ( resid 196 and name HD1# ) ( resid 195 and name HB1 ) 4.2 2.5 1.7 volume=0.187 peak=3736 ppm1=0.726 ppm2=3.189 assign ( resid 158 and name HG2 ) ( resid 160 and name HN ) 4.6 2.9 1.4 volume=0.109 peak=4382 ppm1=2.438 ppm2=8.851 assign ( resid 90 and name HN ) ( resid 92 and name HN ) 4.4 2.7 1.6 volume=0.140 peak=332 ppm1=8.382 ppm2=9.469 assign ( resid 126 and name HD1# ) ( resid 154 and name HA ) 4.8 3.1 1.2 volume=0.087 peak=2686 ppm1=0.348 ppm2=4.676 assign ( resid 132 and name HN ) ( resid 133 and name HB2 ) 3.9 2.1 1.5 volume=0.327 peak=2287 ppm1=7.894 ppm2=2.520 assign ( resid 156 and name HN ) ( resid 166 and name HD2 ) 3.3 1.5 1.3 volume=0.894 peak=762 ppm1=8.551 ppm2=1.407 assign ( resid 144 and name HG2# ) ( resid 143 and name HB1 ) 3.7 1.9 1.5 volume=0.453 peak=3513 ppm1=0.765 ppm2=2.707 assign ( resid 204 and name HA ) ( resid 203 and name HG2# ) 4.3 2.6 1.7 volume=0.164 peak=4479 ppm1=3.799 ppm2=0.324 assign ( resid 136 and name HG2 ) ( resid 137 and name HN ) 3.8 2.1 1.5 volume=0.366 peak=3649 ppm1=1.953 ppm2=8.057 assign ( resid 172 and name HN ) ( resid 151 and name HB1 ) 3.7 2.0 1.5 volume=0.421 peak=2339 ppm1=8.855 ppm2=2.963 assign ( resid 17 and name HN ) ( resid 15 and name HG ) 3.5 1.8 1.4 volume=0.551 peak=2244 ppm1=7.610 ppm2=1.263 assign ( resid 127 and name HD1# ) ( resid 127 and name HB ) 3.5 1.8 1.4 volume=0.542 peak=2939 ppm1=0.285 ppm2=2.020 assign ( resid 127 and name HN ) ( resid 153 and name HB1 ) 3.8 2.1 1.5 volume=0.372 peak=2030 ppm1=9.382 ppm2=2.843 assign ( resid 86 and name HN ) ( resid 86 and name HB2 ) 4.2 2.5 1.7 volume=0.191 peak=941 ppm1=8.619 ppm2=1.533 assign ( resid 34 and name HN ) ( resid 34 and name HA ) 3.2 1.5 1.3 volume=1.034 peak=497 ppm1=8.137 ppm2=4.940 assign ( resid 168 and name HN ) ( resid 154 and name HA ) 3.9 2.1 1.5 volume=0.324 peak=160 ppm1=8.694 ppm2=4.657 assign ( resid 122 and name HN ) ( resid 121 and name HB2 ) 3.0 1.3 1.2 volume=1.521 peak=1109 ppm1=8.646 ppm2=1.923 assign ( resid 57 and name HN ) ( resid 203 and name HG2# ) 4.0 2.3 1.6 volume=0.255 peak=2076 ppm1=9.218 ppm2=0.339 assign ( resid 200 and name HD1 ) ( resid 54 and name HD1# ) 3.2 1.5 1.3 volume=1.004 peak=3043 ppm1=1.549 ppm2=0.518 assign ( resid 146 and name HN ) ( resid 110 and name HN ) 3.4 1.7 1.4 volume=0.642 peak=373 ppm1=8.400 ppm2=8.700 assign ( resid 85 and name HN ) ( resid 84 and name HB ) 2.9 1.2 1.2 volume=1.755 peak=212 ppm1=7.152 ppm2=2.052 assign ( resid 37 and name HN ) ( resid 27 and name HN ) 3.7 2.0 1.5 volume=0.431 peak=1017 ppm1=9.660 ppm2=9.301 assign ( resid 171 and name HA ) ( resid 171 and name HG1# ) 3.8 2.1 1.5 volume=0.363 peak=4049 ppm1=4.148 ppm2=0.871 assign ( resid 10 and name HN ) ( resid 10 and name HA ) 3.1 1.4 1.2 volume=1.277 peak=1235 ppm1=8.320 ppm2=3.622 assign ( resid 146 and name HN ) ( resid 111 and name HA ) 3.3 1.6 1.3 volume=0.840 peak=2033 ppm1=8.400 ppm2=4.776 assign ( resid 126 and name HG12 ) ( resid 14 and name HG1# ) 4.0 2.2 1.6 volume=0.275 peak=4665 ppm1=1.077 ppm2=0.639 assign ( resid 159 and name HA ) ( resid 159 and name HN ) 3.9 2.2 1.6 volume=0.289 peak=4659 ppm1=3.772 ppm2=9.031 assign ( resid 169 and name HA ) ( resid 170 and name HN ) 4.0 2.3 1.6 volume=0.270 peak=3686 ppm1=5.252 ppm2=9.171 assign ( resid 66 and name HB1 or resid 66 and name HB2 ) ( resid 66 and name HD1 or resid 66 and name HD2 ) 3.7 2.0 1.5 volume=0.388 peak=3981 ppm1=3.104 ppm2=7.040 assign ( resid 166 and name HG2 ) ( resid 51 and name HG2 ) 3.0 1.3 1.2 volume=1.404 peak=4127 ppm1=1.253 ppm2=1.996 assign ( resid 125 and name HN ) ( resid 125 and name HB2 ) 3.0 1.3 1.2 volume=1.336 peak=2441 ppm1=8.771 ppm2=2.449 assign ( resid 8 and name HB2 or resid 8 and name HB1 ) ( resid 118 and name HE1 or resid 118 and name HE2 ) 3.8 2.0 1.5 volume=0.377 peak=3537 ppm1=2.048 ppm2=2.983 assign ( resid 43 and name HN ) ( resid 42 and name HN ) 2.8 1.1 1.1 volume=2.036 peak=736 ppm1=7.304 ppm2=8.702 assign ( resid 71 and name HN ) ( resid 72 and name HD1# ) 3.2 1.5 1.3 volume=0.980 peak=587 ppm1=7.220 ppm2=0.619 assign ( resid 137 and name HN ) ( resid 135 and name HB2 ) 3.3 1.6 1.3 volume=0.762 peak=1925 ppm1=8.050 ppm2=2.139 assign ( resid 96 and name HG2# ) ( resid 96 and name HB ) 4.3 2.6 1.7 volume=0.165 peak=2906 ppm1=1.141 ppm2=3.862 assign ( resid 197 and name HD1# ) ( resid 194 and name HA ) 3.2 1.5 1.3 volume=0.931 peak=3164 ppm1=0.756 ppm2=4.352 assign ( resid 143 and name HN ) ( resid 144 and name HG2# ) 3.6 1.9 1.4 volume=0.515 peak=784 ppm1=6.900 ppm2=0.749 assign ( resid 17 and name HN ) ( resid 17 and name HE1 or resid 17 and name HE2 ) 3.5 1.7 1.4 volume=0.631 peak=1292 ppm1=7.609 ppm2=6.747 assign ( resid 28 and name HB1 or resid 28 and name HB2 ) ( resid 28 and name HN ) 3.4 1.6 1.3 volume=0.741 peak=4488 ppm1=1.912 ppm2=7.806 assign ( resid 160 and name HG2 ) ( resid 160 and name HB1 ) 2.6 0.9 1.0 volume=3.283 peak=2613 ppm1=2.201 ppm2=2.037 assign ( resid 10 and name HN ) ( resid 10 and name HB ) 3.5 1.7 1.4 volume=0.631 peak=2456 ppm1=8.320 ppm2=3.680 assign ( resid 88 and name HN ) ( resid 86 and name HA ) 3.5 1.8 1.4 volume=0.546 peak=1999 ppm1=8.595 ppm2=4.284 assign ( resid 168 and name HN ) ( resid 168 and name HB ) 3.2 1.5 1.3 volume=1.023 peak=551 ppm1=8.693 ppm2=1.665 assign ( resid 114 and name HD2# ) ( resid 132 and name HB ) 3.6 1.9 1.5 volume=0.467 peak=4027 ppm1=0.782 ppm2=2.275 assign ( resid 204 and name HB2 ) ( resid 205 and name HN ) 3.6 1.9 1.4 volume=0.505 peak=2489 ppm1=1.712 ppm2=7.212 assign ( resid 3 and name HE1 or resid 3 and name HE2 ) ( resid 3 and name HN ) 3.5 1.8 1.4 volume=0.612 peak=148 ppm1=7.212 ppm2=7.921 assign ( resid 28 and name HN ) ( resid 26 and name HB ) 3.1 1.3 1.2 volume=1.325 peak=1067 ppm1=7.808 ppm2=1.918 assign ( resid 170 and name HN ) ( resid 168 and name HG2# ) 4.3 2.6 1.7 volume=0.165 peak=2392 ppm1=9.145 ppm2=0.223 assign ( resid 152 and name HN ) ( resid 151 and name HA ) 3.5 1.8 1.4 volume=0.573 peak=2197 ppm1=8.344 ppm2=4.921 assign ( resid 162 and name HA ) ( resid 162 and name HB1 ) 4.0 2.3 1.6 volume=0.246 peak=3460 ppm1=3.651 ppm2=2.145 assign ( resid 42 and name HD1 ) ( resid 42 and name HA ) 3.8 2.1 1.5 volume=0.353 peak=4916 ppm1=1.529 ppm2=4.145 assign ( resid 137 and name HB1 ) ( resid 112 and name HG11 ) 3.5 1.8 1.4 volume=0.541 peak=4443 ppm1=2.809 ppm2=1.607 assign ( resid 196 and name HG2# ) ( resid 33 and name HD1# ) 3.0 1.2 1.2 volume=1.605 peak=3524 ppm1=0.812 ppm2=0.366 assign ( resid 112 and name HG2# ) ( resid 134 and name HB1 ) 3.2 1.4 1.3 volume=1.076 peak=3947 ppm1=0.680 ppm2=3.046 assign ( resid 157 and name HD2 ) ( resid 125 and name HN ) 4.6 2.8 1.4 volume=0.119 peak=5072 ppm1=3.627 ppm2=8.770 assign ( resid 64 and name HN ) ( resid 63 and name HN ) 3.5 1.8 1.4 volume=0.609 peak=983 ppm1=7.879 ppm2=7.300 assign ( resid 56 and name HN ) ( resid 61 and name HD1# ) 3.2 1.4 1.3 volume=1.080 peak=453 ppm1=8.639 ppm2=0.747 assign ( resid 51 and name HN ) ( resid 50 and name HA ) 3.0 1.3 1.2 volume=1.393 peak=2379 ppm1=8.424 ppm2=5.177 assign ( resid 132 and name HG2# ) ( resid 134 and name HD1 or resid 134 and name HD2 ) 3.5 1.8 1.4 volume=0.545 peak=3447 ppm1=0.935 ppm2=6.831 assign ( resid 93 and name HG2# ) ( resid 94 and name HN ) 4.1 2.4 1.7 volume=0.218 peak=3812 ppm1=-0.013 ppm2=9.573 assign ( resid 148 and name HN ) ( resid 148 and name HB1 or resid 148 and name HB2 ) 4.3 2.6 1.7 volume=0.162 peak=1512 ppm1=9.152 ppm2=2.902 assign ( resid 114 and name HD1# ) ( resid 3 and name HE1 or resid 3 and name HE2 ) 3.5 1.8 1.4 volume=0.569 peak=4537 ppm1=0.537 ppm2=7.220 assign ( resid 17 and name HN ) ( resid 18 and name HB2 ) 3.6 1.9 1.4 volume=0.494 peak=1793 ppm1=7.610 ppm2=2.435 assign ( resid 192 and name HN ) ( resid 192 and name HG ) 2.9 1.2 1.2 volume=1.828 peak=688 ppm1=8.210 ppm2=1.677 assign ( resid 15 and name HD1# ) ( resid 15 and name HA ) 3.3 1.6 1.3 volume=0.852 peak=2985 ppm1=0.440 ppm2=3.655 assign ( resid 3 and name HN ) ( resid 1 and name HB1 or resid 1 and name HB2 ) 3.6 1.9 1.4 volume=0.485 peak=1265 ppm1=7.918 ppm2=2.053 assign ( resid 171 and name HN ) ( resid 170 and name HA ) 3.3 1.6 1.3 volume=0.824 peak=957 ppm1=9.061 ppm2=5.832 assign ( resid 183 and name HN ) ( resid 179 and name HB1 ) 4.1 2.4 1.7 volume=0.212 peak=1543 ppm1=7.420 ppm2=2.708 assign ( resid 196 and name HG12 ) ( resid 193 and name HA ) 3.9 2.2 1.6 volume=0.289 peak=4612 ppm1=1.468 ppm2=3.455 assign ( resid 75 and name HN ) ( resid 74 and name HN ) 2.8 1.1 1.1 volume=2.112 peak=2240 ppm1=7.480 ppm2=6.488 assign ( resid 53 and name HD1# ) ( resid 53 and name HG12 ) 2.5 0.8 1.0 volume=4.261 peak=5009 ppm1=0.797 ppm2=1.413 assign ( resid 204 and name HG2 ) ( resid 204 and name HA ) 3.5 1.8 1.4 volume=0.591 peak=4090 ppm1=1.302 ppm2=3.816 assign ( resid 119 and name HN ) ( resid 118 and name HB1 or resid 118 and name HB2 ) 3.9 2.2 1.6 volume=0.290 peak=2279 ppm1=8.055 ppm2=2.431 assign ( resid 132 and name HN ) ( resid 114 and name HN ) 3.8 2.0 1.5 volume=0.385 peak=1466 ppm1=7.894 ppm2=8.824 assign ( resid 162 and name HA ) ( resid 161 and name HA ) 4.5 2.8 1.5 volume=0.129 peak=4527 ppm1=3.650 ppm2=4.680 assign ( resid 121 and name HN ) ( resid 121 and name HA ) 3.0 1.3 1.2 volume=1.392 peak=1162 ppm1=8.586 ppm2=4.146 assign ( resid 88 and name HN ) ( resid 87 and name HN ) 3.2 1.5 1.3 volume=0.922 peak=469 ppm1=8.596 ppm2=8.043 assign ( resid 184 and name HA ) ( resid 184 and name HD1# ) 3.0 1.3 1.2 volume=1.463 peak=3655 ppm1=3.629 ppm2=0.898 assign ( resid 113 and name HA ) ( resid 114 and name HN ) 4.1 2.4 1.6 volume=0.232 peak=3060 ppm1=5.306 ppm2=8.794 assign ( resid 26 and name HG2# ) ( resid 27 and name HA ) 3.1 1.4 1.2 volume=1.252 peak=3563 ppm1=0.912 ppm2=4.401 assign ( resid 26 and name HN ) ( resid 26 and name HG2# ) 2.6 0.8 1.0 volume=3.899 peak=540 ppm1=8.862 ppm2=0.901 assign ( resid 96 and name HG2# ) ( resid 72 and name HG12 ) 3.7 2.0 1.5 volume=0.436 peak=3528 ppm1=1.142 ppm2=1.010 assign ( resid 63 and name HN ) ( resid 62 and name HN ) 3.1 1.4 1.2 volume=1.186 peak=1439 ppm1=7.301 ppm2=8.169 assign ( resid 167 and name HD2# ) ( resid 155 and name HN ) 4.6 2.9 1.4 volume=0.116 peak=3173 ppm1=0.763 ppm2=8.925 assign ( resid 137 and name HN ) ( resid 93 and name HG2# ) 4.0 2.2 1.6 volume=0.279 peak=1182 ppm1=8.052 ppm2=-0.027 assign ( resid 142 and name HN ) ( resid 142 and name HB2 ) 3.2 1.4 1.3 volume=1.097 peak=771 ppm1=7.899 ppm2=1.800 assign ( resid 10 and name HB ) ( resid 10 and name HG2# ) 3.9 2.2 1.6 volume=0.309 peak=5124 ppm1=3.687 ppm2=1.091 assign ( resid 144 and name HG12 ) ( resid 109 and name HG2 ) 3.4 1.7 1.4 volume=0.692 peak=2974 ppm1=1.272 ppm2=1.491 assign ( resid 15 and name HG ) ( resid 15 and name HD1# ) 3.0 1.3 1.2 volume=1.432 peak=2516 ppm1=1.242 ppm2=0.441 assign ( resid 98 and name HN ) ( resid 80 and name HN ) 4.3 2.6 1.7 volume=0.169 peak=951 ppm1=9.353 ppm2=7.529 assign ( resid 144 and name HG2# ) ( resid 109 and name HD2 ) 3.2 1.5 1.3 volume=1.017 peak=4766 ppm1=0.766 ppm2=3.110 assign ( resid 53 and name HG2# ) ( resid 54 and name HD1# ) 4.2 2.5 1.7 volume=0.189 peak=4062 ppm1=0.903 ppm2=0.440 assign ( resid 199 and name HB# ) ( resid 199 and name HN ) 3.0 1.3 1.2 volume=1.336 peak=4592 ppm1=0.693 ppm2=8.654 assign ( resid 173 and name HA ) ( resid 172 and name HB1 ) 3.8 2.1 1.5 volume=0.369 peak=2703 ppm1=3.612 ppm2=1.807 assign ( resid 120 and name HN ) ( resid 124 and name HN ) 3.5 1.7 1.4 volume=0.621 peak=769 ppm1=8.909 ppm2=6.482 assign ( resid 84 and name HG1# ) ( resid 84 and name HA ) 4.2 2.4 1.7 volume=0.208 peak=3545 ppm1=0.532 ppm2=4.381 assign ( resid 114 and name HN ) ( resid 113 and name HB1 ) 3.3 1.6 1.3 volume=0.793 peak=2284 ppm1=8.798 ppm2=2.058 assign ( resid 184 and name HG2# ) ( resid 187 and name HN ) 3.9 2.2 1.6 volume=0.295 peak=4168 ppm1=1.093 ppm2=7.592 assign ( resid 136 and name HN ) ( resid 137 and name HB2 ) 3.4 1.6 1.3 volume=0.738 peak=230 ppm1=6.893 ppm2=2.576 assign ( resid 113 and name HN ) ( resid 95 and name HA ) 3.6 1.9 1.5 volume=0.457 peak=1349 ppm1=8.233 ppm2=5.554 assign ( resid 145 and name HN ) ( resid 145 and name HD1 ) 4.1 2.3 1.6 volume=0.242 peak=1059 ppm1=8.379 ppm2=3.480 assign ( resid 173 and name HN ) ( resid 174 and name HN ) 3.7 2.0 1.5 volume=0.436 peak=683 ppm1=8.519 ppm2=9.162 assign ( resid 176 and name HB2 ) ( resid 176 and name HD1 ) 3.7 2.0 1.5 volume=0.394 peak=5076 ppm1=1.850 ppm2=3.205 assign ( resid 60 and name HN ) ( resid 203 and name HD1# ) 4.1 2.4 1.6 volume=0.218 peak=1823 ppm1=7.265 ppm2=-0.008 assign ( resid 186 and name HB2 ) ( resid 186 and name HE1 ) 3.9 2.1 1.5 volume=0.327 peak=2649 ppm1=1.899 ppm2=2.924 assign ( resid 4 and name HN ) ( resid 3 and name HN ) 3.2 1.5 1.3 volume=0.919 peak=2203 ppm1=8.190 ppm2=7.915 assign ( resid 169 and name HN ) ( resid 49 and name HG2 ) 3.9 2.1 1.5 volume=0.325 peak=871 ppm1=9.256 ppm2=1.580 assign ( resid 73 and name HN ) ( resid 72 and name HB ) 4.0 2.2 1.6 volume=0.278 peak=1319 ppm1=7.510 ppm2=1.798 assign ( resid 54 and name HG11 ) ( resid 54 and name HG2# ) 2.8 1.1 1.1 volume=2.233 peak=2660 ppm1=1.188 ppm2=0.577 assign ( resid 139 and name HG1 ) ( resid 139 and name HD1 ) 3.4 1.7 1.4 volume=0.684 peak=5061 ppm1=1.802 ppm2=3.619 assign ( resid 77 and name HN ) ( resid 78 and name HN ) 3.3 1.6 1.3 volume=0.859 peak=1118 ppm1=8.056 ppm2=7.131 assign ( resid 200 and name HA ) ( resid 200 and name HN ) 4.2 2.5 1.7 volume=0.184 peak=4231 ppm1=3.362 ppm2=8.081 assign ( resid 144 and name HN ) ( resid 144 and name HG2# ) 3.2 1.5 1.3 volume=0.983 peak=594 ppm1=7.536 ppm2=0.750 assign ( resid 84 and name HG2# ) ( resid 134 and name HE1 or resid 134 and name HE2 ) 3.3 1.5 1.3 volume=0.892 peak=3700 ppm1=0.111 ppm2=7.152 assign ( resid 64 and name HN ) ( resid 62 and name HN ) 3.8 2.0 1.5 volume=0.375 peak=419 ppm1=7.880 ppm2=8.152 assign ( resid 145 and name HG1 ) ( resid 112 and name HG12 ) 3.2 1.4 1.3 volume=1.058 peak=4721 ppm1=1.410 ppm2=1.291 assign ( resid 11 and name HN ) ( resid 10 and name HG2# ) 2.9 1.2 1.2 volume=1.703 peak=1468 ppm1=8.182 ppm2=1.077 assign ( resid 151 and name HN ) ( resid 14 and name HG2# ) 3.9 2.2 1.6 volume=0.303 peak=310 ppm1=8.646 ppm2=0.753 assign ( resid 155 and name HN ) ( resid 126 and name HG12 ) 3.4 1.7 1.4 volume=0.680 peak=1196 ppm1=8.977 ppm2=1.073 assign ( resid 42 and name HN ) ( resid 40 and name HB1 ) 3.8 2.1 1.5 volume=0.352 peak=2004 ppm1=8.698 ppm2=3.353 assign ( resid 82 and name HN ) ( resid 83 and name HN ) 3.1 1.4 1.2 volume=1.277 peak=1697 ppm1=8.562 ppm2=8.448 assign ( resid 51 and name HA ) ( resid 52 and name HN ) 3.8 2.1 1.5 volume=0.337 peak=3212 ppm1=5.621 ppm2=8.594 assign ( resid 109 and name HN ) ( resid 98 and name HB ) 3.5 1.8 1.4 volume=0.587 peak=2117 ppm1=8.165 ppm2=4.656 assign ( resid 92 and name HN ) ( resid 92 and name HA ) 3.5 1.8 1.4 volume=0.573 peak=292 ppm1=9.456 ppm2=4.926 assign ( resid 203 and name HN ) ( resid 204 and name HN ) 3.2 1.5 1.3 volume=0.921 peak=2228 ppm1=7.684 ppm2=6.734 assign ( resid 207 and name HG2 ) ( resid 207 and name HD1 ) 2.6 0.9 1.1 volume=3.144 peak=3553 ppm1=1.469 ppm2=3.044 assign ( resid 184 and name HN ) ( resid 184 and name HB ) 2.7 0.9 1.1 volume=2.969 peak=393 ppm1=7.499 ppm2=2.064 assign ( resid 64 and name HN ) ( resid 203 and name HD1# ) 3.4 1.7 1.4 volume=0.663 peak=1027 ppm1=7.878 ppm2=-0.026 assign ( resid 126 and name HD1# ) ( resid 126 and name HG2# ) 3.6 1.9 1.4 volume=0.515 peak=4135 ppm1=0.348 ppm2=0.747 assign ( resid 192 and name HN ) ( resid 193 and name HG1# ) 3.0 1.2 1.2 volume=1.606 peak=1375 ppm1=8.210 ppm2=0.768 assign ( resid 36 and name HN ) ( resid 36 and name HB1 ) 3.5 1.8 1.4 volume=0.551 peak=2027 ppm1=9.878 ppm2=3.880 assign ( resid 114 and name HD2# ) ( resid 115 and name HN ) 3.8 2.1 1.5 volume=0.336 peak=4389 ppm1=0.781 ppm2=9.054 assign ( resid 122 and name HN ) ( resid 120 and name HN ) 4.4 2.7 1.6 volume=0.153 peak=2303 ppm1=8.646 ppm2=8.939 assign ( resid 130 and name HB1 ) ( resid 132 and name HG1# ) 3.6 1.9 1.4 volume=0.481 peak=2843 ppm1=1.887 ppm2=0.574 assign ( resid 176 and name HB2 ) ( resid 176 and name HG1 ) 3.0 1.3 1.2 volume=1.397 peak=3419 ppm1=1.850 ppm2=1.637 assign ( resid 205 and name HN ) ( resid 206 and name HN ) 3.0 1.3 1.2 volume=1.369 peak=264 ppm1=7.185 ppm2=7.510 assign ( resid 92 and name HN ) ( resid 87 and name HG11 ) 3.4 1.7 1.4 volume=0.645 peak=2013 ppm1=9.456 ppm2=1.266 assign ( resid 200 and name HG2 ) ( resid 197 and name HA ) 4.5 2.8 1.5 volume=0.122 peak=3498 ppm1=1.129 ppm2=3.757 assign ( resid 90 and name HN ) ( resid 89 and name HB2 ) 3.1 1.4 1.2 volume=1.215 peak=1969 ppm1=8.380 ppm2=3.880 assign ( resid 84 and name HG2# ) ( resid 84 and name HN ) 3.5 1.8 1.4 volume=0.596 peak=4451 ppm1=0.111 ppm2=8.517 assign ( resid 158 and name HN ) ( resid 158 and name HB2 ) 2.7 1.0 1.1 volume=2.711 peak=1511 ppm1=8.216 ppm2=2.213 assign ( resid 63 and name HB2 or resid 63 and name HB1 ) ( resid 63 and name HA ) 4.0 2.2 1.6 volume=0.276 peak=2944 ppm1=2.688 ppm2=4.395 assign ( resid 208 and name HA ) ( resid 209 and name HD2 or resid 209 and name HD1 ) 3.5 1.8 1.4 volume=0.573 peak=2803 ppm1=4.406 ppm2=3.574 assign ( resid 8 and name HG1 or resid 8 and name HG2 ) ( resid 7 and name HA ) 4.2 2.5 1.7 volume=0.193 peak=4305 ppm1=2.322 ppm2=3.636 assign ( resid 60 and name HE1 ) ( resid 60 and name HG2 ) 2.7 1.0 1.1 volume=2.725 peak=3991 ppm1=2.834 ppm2=1.323 assign ( resid 3 and name HD1 or resid 3 and name HD2 ) ( resid 3 and name HB1 or resid 3 and name HB2 ) 4.1 2.3 1.6 volume=0.240 peak=122 ppm1=7.379 ppm2=2.937 assign ( resid 197 and name HG ) ( resid 33 and name HD1# ) 3.7 2.0 1.5 volume=0.405 peak=4651 ppm1=1.279 ppm2=0.384 assign ( resid 134 and name HB1 ) ( resid 112 and name HG2# ) 3.8 2.0 1.5 volume=0.374 peak=2881 ppm1=3.047 ppm2=0.596 assign ( resid 203 and name HN ) ( resid 205 and name HB# ) 3.6 1.9 1.4 volume=0.485 peak=2247 ppm1=7.684 ppm2=1.268 assign ( resid 127 and name HD1# ) ( resid 127 and name HG11 or resid 127 and name HG12 ) 3.0 1.3 1.2 volume=1.378 peak=2621 ppm1=0.286 ppm2=1.037 assign ( resid 124 and name HN ) ( resid 119 and name HA ) 3.0 1.3 1.2 volume=1.350 peak=1450 ppm1=6.472 ppm2=4.798 assign ( resid 28 and name HB1 or resid 28 and name HB2 ) ( resid 28 and name HD2 or resid 28 and name HD1 ) 3.1 1.4 1.2 volume=1.217 peak=2969 ppm1=1.912 ppm2=1.387 assign ( resid 116 and name HN ) ( resid 7 and name HB# ) 2.9 1.2 1.2 volume=1.845 peak=1212 ppm1=8.834 ppm2=0.752 assign ( resid 130 and name HN ) ( resid 114 and name HD2# ) 3.3 1.6 1.3 volume=0.761 peak=1171 ppm1=7.617 ppm2=0.762 assign ( resid 199 and name HB# ) ( resid 201 and name HN ) 3.6 1.9 1.4 volume=0.493 peak=2539 ppm1=0.692 ppm2=7.413 assign ( resid 101 and name HN ) ( resid 106 and name HG2# ) 4.3 2.6 1.7 volume=0.161 peak=1301 ppm1=8.477 ppm2=0.890 assign ( resid 61 and name HG ) ( resid 57 and name HA ) 3.4 1.7 1.4 volume=0.687 peak=4677 ppm1=1.715 ppm2=4.156 assign ( resid 179 and name HB2 ) ( resid 183 and name HB ) 3.8 2.1 1.5 volume=0.340 peak=4089 ppm1=2.493 ppm2=1.945 assign ( resid 99 and name HA ) ( resid 99 and name HG1 ) 3.8 2.1 1.5 volume=0.365 peak=4607 ppm1=4.285 ppm2=2.444 assign ( resid 63 and name HB2 ) ( resid 63 and name HN ) 3.4 1.7 1.4 volume=0.686 peak=5101 ppm1=2.687 ppm2=7.294 assign ( resid 191 and name HN ) ( resid 188 and name HE# ) 3.3 1.6 1.3 volume=0.814 peak=1987 ppm1=7.651 ppm2=1.908 assign ( resid 33 and name HN ) ( resid 31 and name HN ) 2.8 1.1 1.1 volume=2.037 peak=2112 ppm1=8.170 ppm2=9.256 assign ( resid 15 and name HB1 ) ( resid 15 and name HG ) 4.0 2.2 1.6 volume=0.275 peak=3571 ppm1=1.712 ppm2=1.231 assign ( resid 134 and name HB1 ) ( resid 93 and name HD1# ) 5.5 3.8 0.5 volume=0.039 peak=3297 ppm1=3.049 ppm2=-0.281 assign ( resid 52 and name HN ) ( resid 167 and name HN ) 3.6 1.9 1.5 volume=0.462 peak=1970 ppm1=8.619 ppm2=8.647 assign ( resid 93 and name HD1# ) ( resid 134 and name HZ ) 4.0 2.3 1.6 volume=0.257 peak=3920 ppm1=-0.278 ppm2=6.639 assign ( resid 87 and name HG2# ) ( resid 93 and name HD1# ) 4.1 2.4 1.7 volume=0.214 peak=4577 ppm1=0.852 ppm2=-0.275 assign ( resid 69 and name HN ) ( resid 68 and name HA ) 3.6 1.9 1.4 volume=0.485 peak=1040 ppm1=8.217 ppm2=4.274 assign ( resid 134 and name HE1 or resid 134 and name HE2 ) ( resid 84 and name HG1# ) 2.9 1.1 1.1 volume=1.944 peak=80 ppm1=7.141 ppm2=0.567 assign ( resid 204 and name HA ) ( resid 204 and name HD1 ) 2.9 1.2 1.2 volume=1.688 peak=5144 ppm1=3.799 ppm2=1.491 assign ( resid 198 and name HN ) ( resid 200 and name HN ) 3.4 1.6 1.3 volume=0.753 peak=1470 ppm1=8.717 ppm2=8.054 assign ( resid 72 and name HA ) ( resid 71 and name HB1 ) 3.6 1.9 1.5 volume=0.459 peak=4599 ppm1=3.631 ppm2=1.541 assign ( resid 160 and name HB2 ) ( resid 164 and name HB2 ) 4.1 2.3 1.6 volume=0.243 peak=4181 ppm1=2.035 ppm2=2.988 assign ( resid 15 and name HD2# ) ( resid 12 and name HN ) 3.8 2.1 1.5 volume=0.333 peak=4449 ppm1=0.682 ppm2=7.609 assign ( resid 168 and name HN ) ( resid 166 and name HD1 ) 3.6 1.9 1.5 volume=0.471 peak=1882 ppm1=8.694 ppm2=1.400 assign ( resid 22 and name HN ) ( resid 24 and name HB2 ) 3.5 1.8 1.4 volume=0.581 peak=872 ppm1=8.193 ppm2=2.955 assign ( resid 184 and name HA ) ( resid 184 and name HG11 ) 3.2 1.4 1.3 volume=1.099 peak=4476 ppm1=3.629 ppm2=1.680 assign ( resid 117 and name HN ) ( resid 116 and name HB1 ) 3.5 1.7 1.4 volume=0.618 peak=1353 ppm1=8.232 ppm2=2.839 assign ( resid 186 and name HB2 ) ( resid 186 and name HN ) 3.2 1.5 1.3 volume=0.921 peak=3034 ppm1=1.900 ppm2=7.390 assign ( resid 86 and name HA ) ( resid 83 and name HG2 ) 4.0 2.3 1.6 volume=0.247 peak=3107 ppm1=4.287 ppm2=1.722 assign ( resid 6 and name HG12 ) ( resid 6 and name HG2# ) 3.0 1.3 1.2 volume=1.498 peak=5043 ppm1=1.060 ppm2=0.835 assign ( resid 159 and name HA ) ( resid 158 and name HG1 or resid 158 and name HG2 ) 4.0 2.3 1.6 volume=0.245 peak=4426 ppm1=3.773 ppm2=2.398 assign ( resid 33 and name HN ) ( resid 30 and name HN ) 3.1 1.4 1.2 volume=1.218 peak=1143 ppm1=8.169 ppm2=8.697 assign ( resid 24 and name HD1 ) ( resid 36 and name HB2 ) 3.9 2.2 1.6 volume=0.311 peak=10 ppm1=6.801 ppm2=3.486 assign ( resid 203 and name HG2# ) ( resid 204 and name HG1 ) 3.4 1.6 1.3 volume=0.750 peak=3907 ppm1=0.339 ppm2=1.420 assign ( resid 26 and name HN ) ( resid 36 and name HA ) 3.6 1.9 1.5 volume=0.469 peak=344 ppm1=8.860 ppm2=5.830 assign ( resid 124 and name HN ) ( resid 123 and name HN ) 2.8 1.1 1.1 volume=2.139 peak=2356 ppm1=6.472 ppm2=8.443 assign ( resid 37 and name HA ) ( resid 48 and name HN ) 4.0 2.3 1.6 volume=0.264 peak=4878 ppm1=5.823 ppm2=9.305 assign ( resid 209 and name HG1 ) ( resid 209 and name HD1 ) 3.1 1.4 1.2 volume=1.243 peak=3061 ppm1=1.896 ppm2=3.588 assign ( resid 24 and name HN ) ( resid 23 and name HA1 or resid 23 and name HA2 ) 2.6 0.9 1.1 volume=3.241 peak=1047 ppm1=7.833 ppm2=3.620 assign ( resid 43 and name HN ) ( resid 41 and name HA ) 3.4 1.7 1.4 volume=0.700 peak=1417 ppm1=7.303 ppm2=4.333 assign ( resid 200 and name HG2 ) ( resid 196 and name HG2# ) 3.8 2.1 1.5 volume=0.365 peak=2682 ppm1=1.133 ppm2=0.786 assign ( resid 179 and name HD2# ) ( resid 179 and name HG ) 3.1 1.3 1.2 volume=1.311 peak=4525 ppm1=0.745 ppm2=1.512 assign ( resid 35 and name HB ) ( resid 28 and name HN ) 3.8 2.0 1.5 volume=0.376 peak=4532 ppm1=2.052 ppm2=7.819 assign ( resid 53 and name HD1# ) ( resid 53 and name HB ) 2.9 1.2 1.2 volume=1.765 peak=5120 ppm1=0.796 ppm2=1.607 assign ( resid 120 and name HN ) ( resid 119 and name HD1 ) 3.7 2.0 1.5 volume=0.433 peak=2044 ppm1=8.911 ppm2=2.896 assign ( resid 100 and name HN ) ( resid 108 and name HB1 ) 4.1 2.4 1.6 volume=0.234 peak=624 ppm1=8.396 ppm2=2.324 assign ( resid 92 and name HB2 ) ( resid 92 and name HE1 or resid 92 and name HE2 ) 4.1 2.3 1.6 volume=0.243 peak=2684 ppm1=3.103 ppm2=6.752 assign ( resid 126 and name HG12 ) ( resid 126 and name HG2# ) 3.5 1.8 1.4 volume=0.596 peak=3903 ppm1=1.079 ppm2=0.755 assign ( resid 196 and name HB ) ( resid 196 and name HG2# ) 3.1 1.4 1.3 volume=1.105 peak=3512 ppm1=2.252 ppm2=0.822 assign ( resid 53 and name HG2# ) ( resid 53 and name HG11 ) 3.0 1.3 1.2 volume=1.355 peak=3250 ppm1=0.901 ppm2=1.284 assign ( resid 154 and name HG2# ) ( resid 126 and name HD1# ) 3.2 1.5 1.3 volume=0.939 peak=3834 ppm1=0.840 ppm2=0.377 assign ( resid 76 and name HE1 ) ( resid 76 and name HB2 ) 2.9 1.2 1.2 volume=1.735 peak=5036 ppm1=2.861 ppm2=2.032 assign ( resid 144 and name HN ) ( resid 144 and name HG11 ) 3.5 1.8 1.4 volume=0.557 peak=1557 ppm1=7.536 ppm2=1.230 assign ( resid 86 and name HB1 ) ( resid 92 and name HE1 or resid 92 and name HE2 ) 3.4 1.7 1.4 volume=0.639 peak=2886 ppm1=1.563 ppm2=6.750 assign ( resid 162 and name HG2 ) ( resid 162 and name HB2 ) 2.8 1.1 1.1 volume=2.073 peak=4767 ppm1=1.920 ppm2=2.206 assign ( resid 208 and name HB ) ( resid 208 and name HG2# ) 2.7 0.9 1.1 volume=3.049 peak=3389 ppm1=4.031 ppm2=1.138 assign ( resid 136 and name HA ) ( resid 134 and name HE1 or resid 134 and name HE2 ) 4.4 2.7 1.6 volume=0.152 peak=3562 ppm1=3.784 ppm2=7.141 assign ( resid 114 and name HD1# ) ( resid 87 and name HG2# ) 2.7 0.9 1.1 volume=3.033 peak=4314 ppm1=0.536 ppm2=0.847 assign ( resid 191 and name HA ) ( resid 190 and name HB1 ) 3.8 2.1 1.5 volume=0.363 peak=2715 ppm1=4.273 ppm2=3.843 assign ( resid 121 and name HA ) ( resid 121 and name HG1 ) 3.4 1.7 1.4 volume=0.670 peak=2718 ppm1=4.143 ppm2=2.283 assign ( resid 71 and name HN ) ( resid 71 and name HB2 ) 2.9 1.2 1.2 volume=1.869 peak=1583 ppm1=7.217 ppm2=1.534 assign ( resid 120 and name HN ) ( resid 126 and name HN ) 3.2 1.5 1.3 volume=0.983 peak=633 ppm1=8.912 ppm2=9.102 assign ( resid 80 and name HN ) ( resid 79 and name HB2 ) 3.1 1.4 1.2 volume=1.281 peak=1379 ppm1=7.525 ppm2=1.802 assign ( resid 146 and name HN ) ( resid 110 and name HB1 ) 3.5 1.8 1.4 volume=0.543 peak=1783 ppm1=8.401 ppm2=2.965 assign ( resid 37 and name HA ) ( resid 36 and name HB2 ) 4.5 2.8 1.5 volume=0.125 peak=3253 ppm1=5.823 ppm2=3.443 assign ( resid 129 and name HN ) ( resid 129 and name HA ) 3.3 1.6 1.3 volume=0.820 peak=2082 ppm1=8.719 ppm2=5.684 assign ( resid 8 and name HN ) ( resid 7 and name HA ) 2.7 1.0 1.1 volume=2.607 peak=1566 ppm1=7.610 ppm2=3.693 assign ( resid 96 and name HN ) ( resid 95 and name HA ) 3.2 1.5 1.3 volume=0.953 peak=297 ppm1=8.474 ppm2=5.569 assign ( resid 204 and name HB1 ) ( resid 208 and name HB ) 3.4 1.7 1.4 volume=0.721 peak=4114 ppm1=1.713 ppm2=4.027 assign ( resid 65 and name HD2# ) ( resid 65 and name HA ) 3.4 1.6 1.3 volume=0.733 peak=4014 ppm1=0.322 ppm2=3.886 assign ( resid 130 and name HN ) ( resid 131 and name HN ) 4.0 2.3 1.6 volume=0.270 peak=1444 ppm1=7.620 ppm2=9.332 assign ( resid 124 and name HN ) ( resid 123 and name HA ) 2.7 1.0 1.1 volume=2.605 peak=817 ppm1=6.473 ppm2=4.269 assign ( resid 166 and name HB1 ) ( resid 166 and name HE1 ) 4.6 2.8 1.4 volume=0.121 peak=3124 ppm1=1.654 ppm2=2.785 assign ( resid 111 and name HN ) ( resid 110 and name HA ) 3.3 1.6 1.3 volume=0.783 peak=1227 ppm1=8.631 ppm2=5.453 assign ( resid 91 and name HG2# ) ( resid 116 and name HN ) 3.3 1.6 1.3 volume=0.760 peak=4832 ppm1=1.019 ppm2=8.849 assign ( resid 112 and name HG12 ) ( resid 112 and name HD1# ) 3.8 2.1 1.5 volume=0.361 peak=4617 ppm1=1.249 ppm2=0.376 assign ( resid 142 and name HA ) ( resid 142 and name HB2 ) 3.0 1.3 1.2 volume=1.484 peak=2849 ppm1=4.137 ppm2=1.837 assign ( resid 10 and name HB ) ( resid 11 and name HA ) 3.9 2.1 1.5 volume=0.329 peak=3808 ppm1=3.688 ppm2=3.958 assign ( resid 112 and name HG2# ) ( resid 95 and name HN ) 4.4 2.6 1.6 volume=0.154 peak=2764 ppm1=0.677 ppm2=9.044 assign ( resid 54 and name HG2# ) ( resid 200 and name HN ) 4.1 2.4 1.6 volume=0.223 peak=2860 ppm1=0.578 ppm2=8.129 assign ( resid 92 and name HN ) ( resid 93 and name HN ) 3.5 1.8 1.4 volume=0.605 peak=827 ppm1=9.455 ppm2=8.948 assign ( resid 205 and name HB# ) ( resid 74 and name HD1 ) 3.7 2.0 1.5 volume=0.393 peak=3406 ppm1=1.296 ppm2=6.944 assign ( resid 24 and name HD1 ) ( resid 22 and name HN ) 4.0 2.2 1.6 volume=0.275 peak=47 ppm1=6.802 ppm2=8.184 assign ( resid 49 and name HN ) ( resid 36 and name HB1 ) 4.1 2.4 1.6 volume=0.218 peak=1998 ppm1=8.912 ppm2=3.880 assign ( resid 155 and name HN ) ( resid 168 and name HN ) 4.0 2.3 1.6 volume=0.261 peak=1710 ppm1=8.977 ppm2=8.687 assign ( resid 184 and name HG2# ) ( resid 184 and name HG11 ) 3.0 1.3 1.2 volume=1.463 peak=3377 ppm1=1.095 ppm2=1.674 assign ( resid 8 and name HB2 or resid 8 and name HB1 ) ( resid 8 and name HA ) 3.1 1.3 1.2 volume=1.306 peak=4025 ppm1=2.048 ppm2=3.833 assign ( resid 153 and name HN ) ( resid 154 and name HG1# ) 3.3 1.6 1.3 volume=0.849 peak=1971 ppm1=9.329 ppm2=0.878 assign ( resid 92 and name HN ) ( resid 115 and name HN ) 3.5 1.8 1.4 volume=0.561 peak=1779 ppm1=9.456 ppm2=9.056 assign ( resid 61 and name HN ) ( resid 63 and name HB2 ) 3.5 1.8 1.4 volume=0.595 peak=387 ppm1=8.714 ppm2=2.709 assign ( resid 117 and name HB ) ( resid 117 and name HG2# ) 3.6 1.9 1.4 volume=0.478 peak=3141 ppm1=1.036 ppm2=0.366 assign ( resid 159 and name HN ) ( resid 161 and name HN ) 4.1 2.4 1.7 volume=0.217 peak=2393 ppm1=9.023 ppm2=6.922 assign ( resid 167 and name HN ) ( resid 51 and name HA ) 4.2 2.5 1.7 volume=0.187 peak=1202 ppm1=8.642 ppm2=5.569 assign ( resid 197 and name HA ) ( resid 196 and name HG2# ) 3.9 2.2 1.6 volume=0.312 peak=4519 ppm1=3.794 ppm2=0.811 assign ( resid 172 and name HN ) ( resid 172 and name HG2 ) 3.7 2.0 1.5 volume=0.429 peak=2264 ppm1=8.856 ppm2=2.198 assign ( resid 179 and name HB2 ) ( resid 179 and name HG ) 3.4 1.6 1.3 volume=0.748 peak=4326 ppm1=2.492 ppm2=1.515 assign ( resid 77 and name HN ) ( resid 76 and name HB2 ) 3.6 1.9 1.5 volume=0.470 peak=1575 ppm1=8.057 ppm2=1.942 assign ( resid 159 and name HB2 or resid 159 and name HB1 ) ( resid 160 and name HA ) 3.6 1.8 1.4 volume=0.530 peak=3826 ppm1=1.880 ppm2=4.025 assign ( resid 140 and name HN ) ( resid 142 and name HN ) 4.2 2.4 1.7 volume=0.210 peak=724 ppm1=9.581 ppm2=7.921 assign ( resid 91 and name HA ) ( resid 7 and name HB# ) 4.3 2.5 1.7 volume=0.177 peak=2953 ppm1=5.876 ppm2=0.755 assign ( resid 128 and name HN ) ( resid 116 and name HN ) 3.6 1.9 1.4 volume=0.483 peak=989 ppm1=9.931 ppm2=8.826 assign ( resid 147 and name HB2 ) ( resid 174 and name HG2 ) 3.9 2.1 1.5 volume=0.324 peak=5136 ppm1=2.705 ppm2=2.207 assign ( resid 194 and name HA ) ( resid 194 and name HN ) 3.8 2.0 1.5 volume=0.382 peak=3362 ppm1=4.334 ppm2=7.772 assign ( resid 154 and name HG1# ) ( resid 18 and name HB1 ) 3.7 1.9 1.5 volume=0.454 peak=4196 ppm1=0.914 ppm2=2.976 assign ( resid 174 and name HN ) ( resid 173 and name HA ) 3.2 1.5 1.3 volume=0.961 peak=1282 ppm1=9.153 ppm2=3.614 assign ( resid 17 and name HD1 or resid 17 and name HD2 ) ( resid 17 and name HE1 or resid 17 and name HE2 ) 3.1 1.4 1.3 volume=1.138 peak=77 ppm1=6.486 ppm2=6.730 assign ( resid 167 and name HB2 ) ( resid 54 and name HG2# ) 3.8 2.1 1.5 volume=0.342 peak=5102 ppm1=1.679 ppm2=0.567 assign ( resid 210 and name HN ) ( resid 208 and name HG2# ) 3.6 1.9 1.4 volume=0.487 peak=1980 ppm1=8.308 ppm2=1.139 assign ( resid 11 and name HN ) ( resid 8 and name HA ) 2.9 1.2 1.2 volume=1.644 peak=1155 ppm1=8.178 ppm2=3.837 assign ( resid 65 and name HD2# ) ( resid 63 and name HB2 or resid 63 and name HB1 ) 3.8 2.1 1.5 volume=0.344 peak=3976 ppm1=0.320 ppm2=2.657 assign ( resid 106 and name HB ) ( resid 106 and name HD1# ) 3.2 1.4 1.3 volume=1.082 peak=2942 ppm1=1.795 ppm2=0.768 assign ( resid 180 and name HB2 ) ( resid 183 and name HG12 ) 3.0 1.3 1.2 volume=1.448 peak=3549 ppm1=3.906 ppm2=1.548 assign ( resid 196 and name HA ) ( resid 197 and name HN ) 4.8 3.1 1.2 volume=0.087 peak=4804 ppm1=3.453 ppm2=7.999 assign ( resid 144 and name HG2# ) ( resid 144 and name HA ) 3.9 2.2 1.6 volume=0.312 peak=2538 ppm1=0.766 ppm2=3.980 assign ( resid 128 and name HN ) ( resid 126 and name HD1# ) 3.6 1.9 1.5 volume=0.456 peak=1792 ppm1=9.933 ppm2=0.359 assign ( resid 36 and name HA ) ( resid 24 and name HE1 ) 4.5 2.8 1.5 volume=0.127 peak=4018 ppm1=5.852 ppm2=6.994 assign ( resid 196 and name HD1# ) ( resid 53 and name HN ) 4.1 2.4 1.6 volume=0.221 peak=2823 ppm1=0.728 ppm2=8.326 assign ( resid 11 and name HA ) ( resid 11 and name HB# ) 3.4 1.7 1.4 volume=0.690 peak=4568 ppm1=3.956 ppm2=1.635 assign ( resid 33 and name HN ) ( resid 32 and name HB2 or resid 32 and name HB1 ) 2.5 0.8 1.0 volume=4.471 peak=1615 ppm1=8.163 ppm2=2.196 assign ( resid 167 and name HA ) ( resid 51 and name HA ) 4.9 3.2 1.1 volume=0.076 peak=4872 ppm1=5.217 ppm2=5.592 assign ( resid 92 and name HE1 or resid 92 and name HE2 ) ( resid 86 and name HB1 ) 3.5 1.8 1.4 volume=0.567 peak=54 ppm1=6.750 ppm2=1.603 assign ( resid 54 and name HN ) ( resid 54 and name HD1# ) 3.4 1.6 1.3 volume=0.745 peak=806 ppm1=9.029 ppm2=0.482 assign ( resid 29 and name HB ) ( resid 33 and name HG11 ) 4.1 2.4 1.6 volume=0.227 peak=3052 ppm1=3.930 ppm2=1.873 assign ( resid 160 and name HG1 ) ( resid 159 and name HA ) 4.3 2.5 1.7 volume=0.181 peak=2793 ppm1=2.200 ppm2=3.767 assign ( resid 87 and name HG11 ) ( resid 87 and name HD1# ) 3.7 1.9 1.5 volume=0.443 peak=4080 ppm1=1.265 ppm2=0.439 assign ( resid 151 and name HN ) ( resid 129 and name HN ) 3.3 1.5 1.3 volume=0.881 peak=349 ppm1=8.646 ppm2=8.728 assign ( resid 208 and name HG2# ) ( resid 208 and name HB ) 2.8 1.1 1.1 volume=2.362 peak=4972 ppm1=1.137 ppm2=4.033 assign ( resid 16 and name HN ) ( resid 15 and name HG ) 3.3 1.6 1.3 volume=0.772 peak=1141 ppm1=7.497 ppm2=1.242 assign ( resid 127 and name HN ) ( resid 126 and name HB ) 4.1 2.4 1.7 volume=0.217 peak=1232 ppm1=9.384 ppm2=1.609 assign ( resid 124 and name HN ) ( resid 126 and name HG2# ) 3.6 1.9 1.5 volume=0.461 peak=648 ppm1=6.473 ppm2=0.749 assign ( resid 127 and name HG12 ) ( resid 127 and name HG2# ) 3.2 1.4 1.3 volume=1.077 peak=4399 ppm1=1.042 ppm2=0.801 assign ( resid 87 and name HG2# ) ( resid 88 and name HN ) 3.5 1.8 1.4 volume=0.604 peak=4272 ppm1=0.852 ppm2=8.593 assign ( resid 162 and name HA ) ( resid 163 and name HB# ) 3.5 1.8 1.4 volume=0.540 peak=4343 ppm1=3.652 ppm2=1.096 assign ( resid 87 and name HD1# ) ( resid 3 and name HB1 or resid 3 and name HB2 ) 3.5 1.8 1.4 volume=0.574 peak=4874 ppm1=0.440 ppm2=2.919 assign ( resid 25 and name HN ) ( resid 25 and name HB1 ) 2.7 1.0 1.1 volume=2.790 peak=401 ppm1=9.009 ppm2=1.727 assign ( resid 132 and name HG2# ) ( resid 132 and name HB ) 3.0 1.3 1.2 volume=1.382 peak=3139 ppm1=0.935 ppm2=2.284 assign ( resid 197 and name HN ) ( resid 196 and name HN ) 3.4 1.7 1.4 volume=0.692 peak=772 ppm1=7.990 ppm2=7.439 assign ( resid 54 and name HD1# ) ( resid 54 and name HA ) 4.5 2.8 1.5 volume=0.131 peak=3510 ppm1=0.490 ppm2=4.555 assign ( resid 77 and name HB1 ) ( resid 78 and name HA ) 3.9 2.2 1.6 volume=0.299 peak=3933 ppm1=3.887 ppm2=4.675 assign ( resid 197 and name HN ) ( resid 196 and name HG12 ) 3.2 1.4 1.3 volume=1.079 peak=888 ppm1=7.989 ppm2=1.402 assign ( resid 51 and name HN ) ( resid 34 and name HN ) 3.6 1.8 1.4 volume=0.528 peak=1167 ppm1=8.425 ppm2=8.136 assign ( resid 67 and name HG2 ) ( resid 67 and name HG1 ) 2.8 1.1 1.1 volume=2.244 peak=2959 ppm1=2.568 ppm2=2.655 assign ( resid 15 and name HG ) ( resid 15 and name HB1 ) 2.8 1.1 1.1 volume=2.112 peak=3822 ppm1=1.243 ppm2=1.708 assign ( resid 114 and name HD1# ) ( resid 87 and name HB ) 3.3 1.6 1.3 volume=0.866 peak=5075 ppm1=0.537 ppm2=1.366 assign ( resid 137 and name HN ) ( resid 137 and name HB1 ) 3.0 1.3 1.2 volume=1.387 peak=1377 ppm1=8.052 ppm2=2.841 assign ( resid 175 and name HN ) ( resid 174 and name HB1 ) 3.0 1.3 1.2 volume=1.398 peak=2373 ppm1=8.804 ppm2=1.922 assign ( resid 132 and name HG1# ) ( resid 114 and name HD2# ) 2.7 1.0 1.1 volume=2.804 peak=3496 ppm1=0.543 ppm2=0.783 assign ( resid 100 and name HN ) ( resid 100 and name HA ) 4.0 2.2 1.6 volume=0.282 peak=1105 ppm1=8.396 ppm2=4.159 assign ( resid 167 and name HG ) ( resid 199 and name HB# ) 3.3 1.6 1.3 volume=0.855 peak=5127 ppm1=0.922 ppm2=0.680 assign ( resid 3 and name HD1 or resid 3 and name HD2 ) ( resid 114 and name HB2 ) 3.4 1.7 1.4 volume=0.660 peak=143 ppm1=7.378 ppm2=1.636 assign ( resid 136 and name HN ) ( resid 135 and name HD2 ) 3.4 1.7 1.4 volume=0.657 peak=2133 ppm1=6.891 ppm2=3.224 assign ( resid 187 and name HG2# ) ( resid 179 and name HD1# ) 3.2 1.5 1.3 volume=0.995 peak=3317 ppm1=1.062 ppm2=0.545 assign ( resid 15 and name HB1 ) ( resid 15 and name HD1# ) 4.2 2.4 1.7 volume=0.210 peak=3637 ppm1=1.713 ppm2=0.435 assign ( resid 87 and name HN ) ( resid 87 and name HG2# ) 3.9 2.2 1.6 volume=0.315 peak=1003 ppm1=8.041 ppm2=0.853 assign ( resid 48 and name HN ) ( resid 48 and name HA ) 4.0 2.3 1.6 volume=0.252 peak=1310 ppm1=9.291 ppm2=5.306 assign ( resid 170 and name HN ) ( resid 169 and name HA ) 3.2 1.4 1.3 volume=1.087 peak=512 ppm1=9.146 ppm2=5.183 assign ( resid 35 and name HN ) ( resid 28 and name HN ) 3.9 2.2 1.6 volume=0.294 peak=695 ppm1=9.428 ppm2=7.790 assign ( resid 135 and name HD2 ) ( resid 135 and name HB2 ) 4.2 2.4 1.7 volume=0.210 peak=3610 ppm1=3.226 ppm2=2.169 assign ( resid 203 and name HD1# ) ( resid 199 and name HB# ) 2.7 1.0 1.1 volume=2.855 peak=4789 ppm1=-0.009 ppm2=0.638 assign ( resid 134 and name HB1 ) ( resid 93 and name HG2# ) 4.3 2.6 1.7 volume=0.166 peak=4042 ppm1=3.049 ppm2=-0.011 assign ( resid 75 and name HA ) ( resid 76 and name HN ) 3.8 2.1 1.5 volume=0.351 peak=3650 ppm1=4.151 ppm2=6.704 assign ( resid 64 and name HE1 or resid 64 and name HE2 ) ( resid 64 and name HZ ) 3.3 1.6 1.3 volume=0.778 peak=141 ppm1=6.485 ppm2=7.049 assign ( resid 155 and name HN ) ( resid 154 and name HN ) 4.4 2.6 1.6 volume=0.155 peak=1320 ppm1=8.977 ppm2=9.998 assign ( resid 133 and name HB2 ) ( resid 132 and name HG1# ) 3.5 1.8 1.4 volume=0.538 peak=4989 ppm1=2.559 ppm2=0.517 assign ( resid 65 and name HG ) ( resid 65 and name HA ) 4.1 2.3 1.6 volume=0.243 peak=4746 ppm1=1.641 ppm2=3.885 assign ( resid 113 and name HN ) ( resid 111 and name HB1 ) 3.6 1.9 1.5 volume=0.457 peak=1643 ppm1=8.232 ppm2=2.909 assign ( resid 134 and name HN ) ( resid 134 and name HE1 or resid 134 and name HE2 ) 3.2 1.5 1.3 volume=0.922 peak=1154 ppm1=8.747 ppm2=7.134 assign ( resid 168 and name HN ) ( resid 155 and name HB2 ) 4.0 2.3 1.6 volume=0.256 peak=458 ppm1=8.693 ppm2=2.572 assign ( resid 87 and name HB ) ( resid 87 and name HG11 ) 4.4 2.7 1.6 volume=0.152 peak=3015 ppm1=1.370 ppm2=1.273 assign ( resid 1 and name HN# ) ( resid 2 and name HB2 or resid 2 and name HB1 ) 3.8 2.1 1.5 volume=0.350 peak=1243 ppm1=8.196 ppm2=2.829 assign ( resid 8 and name HB2 or resid 8 and name HB1 ) ( resid 91 and name HG2# ) 3.5 1.7 1.4 volume=0.633 peak=3211 ppm1=2.048 ppm2=1.031 assign ( resid 29 and name HA ) ( resid 193 and name HG1# ) 3.5 1.8 1.4 volume=0.568 peak=3961 ppm1=5.251 ppm2=0.772 assign ( resid 15 and name HB1 ) ( resid 15 and name HB2 ) 4.1 2.4 1.6 volume=0.226 peak=4453 ppm1=1.712 ppm2=1.364 assign ( resid 192 and name HN ) ( resid 190 and name HA ) 3.3 1.6 1.3 volume=0.775 peak=1903 ppm1=8.209 ppm2=3.969 assign ( resid 114 and name HD2# ) ( resid 4 and name HN ) 3.8 2.1 1.5 volume=0.338 peak=4496 ppm1=0.783 ppm2=8.190 assign ( resid 15 and name HB2 ) ( resid 15 and name HB1 ) 3.9 2.1 1.5 volume=0.327 peak=3552 ppm1=1.368 ppm2=1.714 assign ( resid 73 and name HA ) ( resid 72 and name HB ) 3.8 2.1 1.5 volume=0.369 peak=5031 ppm1=3.919 ppm2=1.842 assign ( resid 71 and name HN ) ( resid 68 and name HA ) 3.3 1.5 1.3 volume=0.907 peak=945 ppm1=7.218 ppm2=4.265 assign ( resid 188 and name HA ) ( resid 191 and name HB2 ) 4.0 2.2 1.6 volume=0.281 peak=2725 ppm1=4.220 ppm2=2.836 assign ( resid 96 and name HN ) ( resid 112 and name HG2# ) 3.7 2.0 1.5 volume=0.429 peak=1827 ppm1=8.473 ppm2=0.636 assign ( resid 130 and name HB2 ) ( resid 130 and name HE2 ) 4.3 2.6 1.7 volume=0.160 peak=3902 ppm1=1.833 ppm2=2.837 assign ( resid 115 and name HG2# ) ( resid 127 and name HG11 ) 2.9 1.1 1.1 volume=1.968 peak=5032 ppm1=0.659 ppm2=1.027 assign ( resid 190 and name HN ) ( resid 189 and name HD2 ) 3.7 2.0 1.5 volume=0.427 peak=1007 ppm1=7.521 ppm2=3.476 assign ( resid 74 and name HH2 ) ( resid 64 and name HB2 or resid 64 and name HB1 ) 3.4 1.7 1.4 volume=0.710 peak=98 ppm1=6.509 ppm2=3.050 assign ( resid 36 and name HB2 ) ( resid 37 and name HN ) 4.1 2.4 1.7 volume=0.214 peak=3046 ppm1=3.520 ppm2=9.690 assign ( resid 183 and name HN ) ( resid 183 and name HB ) 2.6 0.8 1.0 volume=3.833 peak=831 ppm1=7.420 ppm2=1.924 assign ( resid 115 and name HG1# ) ( resid 113 and name HB1 ) 3.1 1.4 1.2 volume=1.267 peak=3671 ppm1=0.303 ppm2=2.014 assign ( resid 8 and name HG1 or resid 8 and name HG2 ) ( resid 11 and name HN ) 3.7 1.9 1.5 volume=0.441 peak=3689 ppm1=2.321 ppm2=8.196 assign ( resid 42 and name HA ) ( resid 42 and name HB1 ) 4.2 2.5 1.7 volume=0.191 peak=4853 ppm1=4.138 ppm2=1.663 assign ( resid 201 and name HN ) ( resid 199 and name HA ) 2.9 1.2 1.2 volume=1.799 peak=682 ppm1=7.400 ppm2=2.755 assign ( resid 73 and name HB ) ( resid 70 and name HB2 ) 4.4 2.7 1.6 volume=0.151 peak=4466 ppm1=4.300 ppm2=2.594 assign ( resid 142 and name HN ) ( resid 142 and name HB1 ) 3.3 1.6 1.3 volume=0.767 peak=1464 ppm1=7.898 ppm2=1.933 assign ( resid 51 and name HA ) ( resid 168 and name HG2# ) 3.6 1.9 1.4 volume=0.488 peak=4761 ppm1=5.622 ppm2=0.200 assign ( resid 6 and name HG11 ) ( resid 6 and name HD1# ) 3.0 1.3 1.2 volume=1.412 peak=2800 ppm1=1.038 ppm2=0.777 assign ( resid 179 and name HN ) ( resid 180 and name HN ) 3.7 2.0 1.5 volume=0.429 peak=1462 ppm1=7.303 ppm2=8.325 assign ( resid 51 and name HB1 or resid 51 and name HB2 ) ( resid 52 and name HN ) 4.1 2.3 1.6 volume=0.240 peak=4542 ppm1=1.780 ppm2=8.617 assign ( resid 27 and name HN ) ( resid 26 and name HB ) 3.5 1.8 1.4 volume=0.606 peak=180 ppm1=9.277 ppm2=1.920 assign ( resid 187 and name HA ) ( resid 188 and name HN ) 5.1 3.4 0.9 volume=0.061 peak=4188 ppm1=4.262 ppm2=8.458 assign ( resid 194 and name HB2 ) ( resid 193 and name HN ) 3.8 2.1 1.5 volume=0.365 peak=3466 ppm1=2.824 ppm2=7.679 assign ( resid 6 and name HG12 ) ( resid 6 and name HD1# ) 3.0 1.3 1.2 volume=1.547 peak=4833 ppm1=1.060 ppm2=0.772 assign ( resid 159 and name HG1 or resid 159 and name HG2 ) ( resid 159 and name HB2 or resid 159 and name HB1 ) 2.3 0.6 0.9 volume=6.567 peak=3305 ppm1=2.239 ppm2=1.883 assign ( resid 84 and name HN ) ( resid 93 and name HN ) 3.5 1.8 1.4 volume=0.564 peak=586 ppm1=8.504 ppm2=8.836 assign ( resid 109 and name HB1 ) ( resid 144 and name HG2# ) 3.6 1.9 1.4 volume=0.501 peak=3556 ppm1=1.719 ppm2=0.775 assign ( resid 61 and name HD2# ) ( resid 64 and name HN ) 3.9 2.2 1.6 volume=0.291 peak=5059 ppm1=0.748 ppm2=7.864 assign ( resid 117 and name HN ) ( resid 117 and name HD1# ) 2.9 1.1 1.1 volume=1.926 peak=869 ppm1=8.234 ppm2=0.231 assign ( resid 57 and name HN ) ( resid 203 and name HD1# ) 3.7 2.0 1.5 volume=0.392 peak=1847 ppm1=9.218 ppm2=-0.030 assign ( resid 19 and name HN ) ( resid 16 and name HA2 ) 3.2 1.5 1.3 volume=0.940 peak=2025 ppm1=7.482 ppm2=3.614 assign ( resid 37 and name HA ) ( resid 47 and name HB1 ) 4.2 2.4 1.7 volume=0.210 peak=3517 ppm1=5.823 ppm2=0.748 assign ( resid 37 and name HN ) ( resid 38 and name HN ) 3.9 2.1 1.5 volume=0.328 peak=1632 ppm1=9.662 ppm2=8.439 assign ( resid 117 and name HD1# ) ( resid 116 and name HA ) 4.3 2.5 1.7 volume=0.180 peak=2491 ppm1=0.243 ppm2=6.172 assign ( resid 87 and name HB ) ( resid 87 and name HD1# ) 4.2 2.4 1.7 volume=0.208 peak=4958 ppm1=1.369 ppm2=0.439 assign ( resid 79 and name HB2 ) ( resid 99 and name HN ) 3.7 2.0 1.5 volume=0.411 peak=2794 ppm1=1.779 ppm2=7.803 assign ( resid 167 and name HN ) ( resid 53 and name HA ) 3.7 2.0 1.5 volume=0.409 peak=1314 ppm1=8.642 ppm2=4.922 assign ( resid 61 and name HD1# ) ( resid 56 and name HN ) 3.1 1.4 1.2 volume=1.227 peak=2901 ppm1=0.747 ppm2=8.699 assign ( resid 165 and name HN ) ( resid 164 and name HN ) 4.0 2.3 1.6 volume=0.266 peak=2220 ppm1=8.464 ppm2=7.984 assign ( resid 134 and name HD1 or resid 134 and name HD2 ) ( resid 84 and name HG2# ) 3.6 1.9 1.5 volume=0.462 peak=68 ppm1=6.862 ppm2=0.141 assign ( resid 26 and name HN ) ( resid 25 and name HG2 ) 3.1 1.4 1.3 volume=1.124 peak=588 ppm1=8.863 ppm2=1.267 assign ( resid 86 and name HA ) ( resid 92 and name HE1 or resid 92 and name HE2 ) 3.9 2.2 1.6 volume=0.293 peak=3696 ppm1=4.252 ppm2=6.756 assign ( resid 42 and name HB2 ) ( resid 42 and name HN ) 3.4 1.7 1.4 volume=0.723 peak=4142 ppm1=1.666 ppm2=8.709 assign ( resid 185 and name HN ) ( resid 184 and name HD1# ) 3.1 1.4 1.2 volume=1.215 peak=1428 ppm1=8.185 ppm2=0.894 assign ( resid 41 and name HD2 or resid 41 and name HD1 ) ( resid 41 and name HG2 or resid 41 and name HG1 ) 2.3 0.5 0.9 volume=7.857 peak=3485 ppm1=3.093 ppm2=1.559 assign ( resid 73 and name HN ) ( resid 72 and name HG2# ) 3.1 1.4 1.2 volume=1.239 peak=274 ppm1=7.504 ppm2=0.619 assign ( resid 15 and name HA ) ( resid 15 and name HN ) 4.0 2.3 1.6 volume=0.274 peak=2812 ppm1=3.674 ppm2=7.811 assign ( resid 166 and name HN ) ( resid 165 and name HB1 ) 3.1 1.4 1.2 volume=1.177 peak=870 ppm1=8.998 ppm2=2.963 assign ( resid 77 and name HN ) ( resid 99 and name HN ) 3.8 2.1 1.5 volume=0.330 peak=177 ppm1=8.057 ppm2=7.789 assign ( resid 200 and name HB2 ) ( resid 200 and name HN ) 4.3 2.6 1.7 volume=0.166 peak=2915 ppm1=1.668 ppm2=8.098 assign ( resid 168 and name HG1# ) ( resid 168 and name HN ) 3.9 2.1 1.5 volume=0.329 peak=3918 ppm1=0.768 ppm2=8.703 assign ( resid 184 and name HG12 ) ( resid 184 and name HN ) 3.7 1.9 1.5 volume=0.441 peak=2738 ppm1=1.093 ppm2=7.504 assign ( resid 114 and name HD1# ) ( resid 87 and name HN ) 4.1 2.4 1.7 volume=0.217 peak=3859 ppm1=0.537 ppm2=8.065 assign ( resid 196 and name HA ) ( resid 196 and name HG2# ) 3.4 1.7 1.4 volume=0.689 peak=4674 ppm1=3.453 ppm2=0.809 assign ( resid 208 and name HG2# ) ( resid 207 and name HD1 or resid 207 and name HD2 ) 3.7 2.0 1.5 volume=0.388 peak=3218 ppm1=1.137 ppm2=3.012 assign ( resid 153 and name HN ) ( resid 14 and name HG2# ) 3.1 1.4 1.3 volume=1.150 peak=1753 ppm1=9.329 ppm2=0.753 assign ( resid 76 and name HN ) ( resid 77 and name HB1 ) 4.1 2.4 1.7 volume=0.217 peak=1959 ppm1=6.701 ppm2=3.876 assign ( resid 159 and name HN ) ( resid 159 and name HB1 ) 2.7 1.0 1.1 volume=2.682 peak=1670 ppm1=9.023 ppm2=1.793 assign ( resid 205 and name HN ) ( resid 203 and name HA ) 3.2 1.5 1.3 volume=1.051 peak=703 ppm1=7.178 ppm2=2.832 assign ( resid 159 and name HB2 ) ( resid 158 and name HA ) 4.6 2.9 1.4 volume=0.117 peak=4661 ppm1=1.876 ppm2=4.139 assign ( resid 196 and name HN ) ( resid 195 and name HB2 ) 3.3 1.6 1.3 volume=0.842 peak=737 ppm1=7.438 ppm2=3.246 assign ( resid 122 and name HN ) ( resid 120 and name HB1 ) 4.2 2.5 1.7 volume=0.184 peak=1488 ppm1=8.645 ppm2=2.967 assign ( resid 101 and name HB1 ) ( resid 106 and name HD1# ) 4.1 2.4 1.6 volume=0.236 peak=2937 ppm1=2.987 ppm2=0.789 assign ( resid 95 and name HN ) ( resid 94 and name HA ) 3.0 1.3 1.2 volume=1.443 peak=1419 ppm1=9.129 ppm2=5.038 assign ( resid 212 and name HA ) ( resid 212 and name HN ) 4.1 2.4 1.6 volume=0.229 peak=4992 ppm1=4.140 ppm2=8.248 assign ( resid 35 and name HB ) ( resid 28 and name HB1 ) 3.2 1.4 1.3 volume=1.068 peak=4822 ppm1=2.053 ppm2=1.898 assign ( resid 196 and name HG11 ) ( resid 196 and name HN ) 3.7 2.0 1.5 volume=0.388 peak=3112 ppm1=1.806 ppm2=7.473 assign ( resid 187 and name HA ) ( resid 187 and name HG2# ) 3.7 2.0 1.5 volume=0.437 peak=2505 ppm1=4.270 ppm2=1.091 assign ( resid 96 and name HG2# ) ( resid 111 and name HN ) 3.8 2.1 1.5 volume=0.335 peak=2669 ppm1=1.141 ppm2=8.617 assign ( resid 179 and name HD1# ) ( resid 179 and name HD2# ) 2.6 0.9 1.0 volume=3.528 peak=3519 ppm1=0.529 ppm2=0.739 assign ( resid 109 and name HG2 ) ( resid 109 and name HA ) 3.8 2.1 1.5 volume=0.339 peak=5079 ppm1=1.547 ppm2=3.878 assign ( resid 176 and name HN ) ( resid 176 and name HG1 ) 3.0 1.3 1.2 volume=1.381 peak=685 ppm1=8.404 ppm2=1.660 assign ( resid 52 and name HN ) ( resid 167 and name HD1# ) 3.0 1.3 1.2 volume=1.563 peak=167 ppm1=8.612 ppm2=0.752 assign ( resid 79 and name HG2 ) ( resid 99 and name HN ) 4.0 2.3 1.6 volume=0.261 peak=4478 ppm1=1.916 ppm2=7.759 assign ( resid 154 and name HG2# ) ( resid 153 and name HN ) 3.7 2.0 1.5 volume=0.403 peak=2495 ppm1=0.841 ppm2=9.360 assign ( resid 159 and name HN ) ( resid 158 and name HB1 ) 2.8 1.1 1.1 volume=2.115 peak=1448 ppm1=9.024 ppm2=2.179 assign ( resid 42 and name HN ) ( resid 41 and name HN ) 3.8 2.0 1.5 volume=0.383 peak=775 ppm1=8.699 ppm2=8.903 assign ( resid 173 and name HG2# ) ( resid 174 and name HN ) 3.5 1.8 1.4 volume=0.581 peak=4809 ppm1=1.034 ppm2=9.155 assign ( resid 184 and name HB ) ( resid 185 and name HN ) 3.8 2.1 1.5 volume=0.340 peak=3473 ppm1=2.045 ppm2=8.186 assign ( resid 5 and name HB# ) ( resid 4 and name HB2 ) 2.9 1.2 1.2 volume=1.656 peak=3035 ppm1=1.339 ppm2=1.736 assign ( resid 76 and name HN ) ( resid 78 and name HN ) 3.9 2.1 1.5 volume=0.327 peak=2208 ppm1=6.700 ppm2=7.135 assign ( resid 102 and name HB# ) ( resid 102 and name HN ) 4.1 2.4 1.6 volume=0.235 peak=3892 ppm1=1.279 ppm2=8.520 assign ( resid 167 and name HN ) ( resid 54 and name HN ) 3.6 1.9 1.5 volume=0.455 peak=1300 ppm1=8.642 ppm2=9.083 assign ( resid 38 and name HN ) ( resid 46 and name HA ) 3.5 1.8 1.4 volume=0.572 peak=1483 ppm1=8.467 ppm2=4.929 assign ( resid 145 and name HN ) ( resid 145 and name HB1 or resid 145 and name HB2 ) 3.0 1.3 1.2 volume=1.345 peak=1786 ppm1=8.379 ppm2=1.923 assign ( resid 35 and name HG2# ) ( resid 36 and name HA ) 4.2 2.5 1.7 volume=0.187 peak=3777 ppm1=0.889 ppm2=5.847 assign ( resid 29 and name HB ) ( resid 29 and name HA ) 4.4 2.6 1.6 volume=0.155 peak=3249 ppm1=3.929 ppm2=5.269 assign ( resid 137 and name HN ) ( resid 136 and name HB1 ) 2.8 1.1 1.1 volume=2.012 peak=1111 ppm1=8.051 ppm2=1.857 assign ( resid 67 and name HB2 ) ( resid 68 and name HN ) 3.1 1.4 1.3 volume=1.145 peak=3567 ppm1=2.064 ppm2=7.999 assign ( resid 83 and name HN ) ( resid 82 and name HN ) 2.9 1.2 1.2 volume=1.877 peak=1384 ppm1=8.503 ppm2=8.568 assign ( resid 80 and name HB ) ( resid 80 and name HN ) 4.0 2.3 1.6 volume=0.247 peak=4628 ppm1=1.395 ppm2=7.545 assign ( resid 202 and name HA1 ) ( resid 201 and name HB2 ) 4.8 3.1 1.2 volume=0.089 peak=3446 ppm1=3.063 ppm2=2.594 assign ( resid 11 and name HB# ) ( resid 12 and name HG1 or resid 12 and name HG2 ) 3.4 1.7 1.4 volume=0.668 peak=3027 ppm1=1.630 ppm2=2.401 assign ( resid 11 and name HA ) ( resid 11 and name HN ) 3.9 2.2 1.6 volume=0.316 peak=4294 ppm1=3.956 ppm2=8.181 assign ( resid 177 and name HN ) ( resid 176 and name HB2 or resid 176 and name HB1 ) 3.2 1.5 1.3 volume=0.944 peak=428 ppm1=8.463 ppm2=1.911 assign ( resid 186 and name HE1 ) ( resid 186 and name HB2 ) 3.8 2.1 1.5 volume=0.359 peak=3801 ppm1=2.958 ppm2=1.877 assign ( resid 121 and name HA ) ( resid 121 and name HN ) 4.4 2.7 1.6 volume=0.140 peak=4388 ppm1=4.144 ppm2=8.584 assign ( resid 114 and name HN ) ( resid 132 and name HB ) 4.1 2.4 1.6 volume=0.225 peak=2056 ppm1=8.799 ppm2=2.265 assign ( resid 192 and name HB1 ) ( resid 192 and name HG ) 3.9 2.2 1.6 volume=0.299 peak=2740 ppm1=1.331 ppm2=1.753 assign ( resid 109 and name HN ) ( resid 98 and name HN ) 3.9 2.2 1.6 volume=0.285 peak=2420 ppm1=8.166 ppm2=9.349 assign ( resid 87 and name HN ) ( resid 87 and name HG12 ) 3.6 1.9 1.5 volume=0.463 peak=1078 ppm1=8.039 ppm2=1.008 assign ( resid 57 and name HA ) ( resid 162 and name HB1 ) 3.9 2.1 1.5 volume=0.330 peak=3152 ppm1=4.135 ppm2=2.267 assign ( resid 18 and name HN ) ( resid 15 and name HB2 ) 3.2 1.5 1.3 volume=1.055 peak=1671 ppm1=7.766 ppm2=1.367 assign ( resid 7 and name HA ) ( resid 114 and name HD2# ) 3.2 1.4 1.3 volume=1.088 peak=4657 ppm1=3.710 ppm2=0.777 assign ( resid 180 and name HB1 ) ( resid 183 and name HG11 ) 2.9 1.2 1.2 volume=1.861 peak=4448 ppm1=3.907 ppm2=1.267 assign ( resid 8 and name HB2 or resid 8 and name HB1 ) ( resid 7 and name HB# ) 3.3 1.6 1.3 volume=0.796 peak=2486 ppm1=2.050 ppm2=0.769 assign ( resid 67 and name HG2 ) ( resid 67 and name HN ) 3.8 2.1 1.5 volume=0.353 peak=2470 ppm1=2.570 ppm2=7.605 assign ( resid 38 and name HN ) ( resid 46 and name HB1 ) 3.2 1.4 1.3 volume=1.058 peak=1934 ppm1=8.467 ppm2=1.534 assign ( resid 15 and name HA ) ( resid 15 and name HG ) 3.5 1.8 1.4 volume=0.545 peak=5138 ppm1=3.674 ppm2=1.243 assign ( resid 97 and name HG2# ) ( resid 96 and name HG2# ) 3.8 2.1 1.5 volume=0.340 peak=4215 ppm1=0.218 ppm2=1.074 assign ( resid 129 and name HN ) ( resid 10 and name HG2# ) 3.2 1.5 1.3 volume=0.933 peak=1050 ppm1=8.719 ppm2=1.079 assign ( resid 198 and name HN ) ( resid 199 and name HN ) 3.4 1.6 1.3 volume=0.753 peak=1631 ppm1=8.718 ppm2=8.620 assign ( resid 153 and name HN ) ( resid 153 and name HB1 or resid 153 and name HB2 ) 3.4 1.7 1.4 volume=0.715 peak=2067 ppm1=9.329 ppm2=2.845 assign ( resid 48 and name HN ) ( resid 171 and name HN ) 3.4 1.6 1.3 volume=0.750 peak=910 ppm1=9.294 ppm2=9.061 assign ( resid 24 and name HD1 ) ( resid 38 and name HG1 ) 4.0 2.3 1.6 volume=0.251 peak=39 ppm1=6.802 ppm2=0.512 assign ( resid 60 and name HN ) ( resid 59 and name HB# ) 2.7 0.9 1.1 volume=3.028 peak=1389 ppm1=7.271 ppm2=1.267 assign ( resid 179 and name HB1 ) ( resid 183 and name HN ) 4.2 2.4 1.7 volume=0.205 peak=2552 ppm1=2.754 ppm2=7.479 assign ( resid 96 and name HG2# ) ( resid 111 and name HB2 ) 3.8 2.1 1.5 volume=0.360 peak=2625 ppm1=1.144 ppm2=2.902 assign ( resid 134 and name HZ ) ( resid 136 and name HB1 ) 3.0 1.2 1.2 volume=1.617 peak=14 ppm1=6.641 ppm2=1.750 assign ( resid 15 and name HA ) ( resid 15 and name HD1# ) 3.5 1.8 1.4 volume=0.544 peak=4960 ppm1=3.674 ppm2=0.442 assign ( resid 87 and name HG2# ) ( resid 91 and name HB ) 3.5 1.8 1.4 volume=0.543 peak=4579 ppm1=0.850 ppm2=3.633 assign ( resid 60 and name HG2 ) ( resid 60 and name HD2 ) 2.1 0.4 0.8 volume=11.926 peak=3937 ppm1=1.325 ppm2=1.542 assign ( resid 15 and name HD1# ) ( resid 12 and name HN ) 3.8 2.1 1.5 volume=0.362 peak=4644 ppm1=0.440 ppm2=7.575 assign ( resid 6 and name HD1# ) ( resid 3 and name HB1 or resid 3 and name HB2 ) 3.9 2.2 1.6 volume=0.313 peak=4107 ppm1=0.794 ppm2=3.039 assign ( resid 192 and name HN ) ( resid 188 and name HA ) 3.1 1.4 1.3 volume=1.125 peak=185 ppm1=8.209 ppm2=4.205 assign ( resid 116 and name HN ) ( resid 114 and name HG ) 3.0 1.3 1.2 volume=1.480 peak=1752 ppm1=8.835 ppm2=0.957 assign ( resid 185 and name HG2 ) ( resid 185 and name HB1 ) 2.6 0.9 1.0 volume=3.342 peak=3867 ppm1=2.343 ppm2=2.151 assign ( resid 184 and name HB ) ( resid 184 and name HD1# ) 3.0 1.3 1.2 volume=1.399 peak=2586 ppm1=2.045 ppm2=0.893 assign ( resid 117 and name HD1# ) ( resid 117 and name HG11 or resid 117 and name HG12 ) 3.1 1.3 1.2 volume=1.294 peak=3393 ppm1=0.245 ppm2=0.646 assign ( resid 90 and name HN ) ( resid 91 and name HN ) 2.8 1.1 1.1 volume=2.111 peak=2154 ppm1=8.381 ppm2=7.219 assign ( resid 132 and name HN ) ( resid 132 and name HG1# ) 3.1 1.4 1.3 volume=1.150 peak=965 ppm1=7.894 ppm2=0.502 assign ( resid 116 and name HN ) ( resid 115 and name HG1# ) 3.5 1.8 1.4 volume=0.598 peak=1064 ppm1=8.834 ppm2=0.306 assign ( resid 67 and name HG2 ) ( resid 67 and name HB1 ) 3.3 1.6 1.3 volume=0.811 peak=3114 ppm1=2.568 ppm2=2.145 assign ( resid 48 and name HN ) ( resid 47 and name HB1 ) 3.1 1.4 1.2 volume=1.173 peak=1383 ppm1=9.293 ppm2=0.747 assign ( resid 10 and name HN ) ( resid 9 and name HA ) 3.3 1.6 1.3 volume=0.787 peak=2213 ppm1=8.317 ppm2=3.984 assign ( resid 199 and name HB# ) ( resid 200 and name HN ) 3.2 1.5 1.3 volume=0.912 peak=3992 ppm1=0.692 ppm2=8.128 assign ( resid 34 and name HN ) ( resid 34 and name HG2# ) 3.1 1.4 1.2 volume=1.187 peak=2332 ppm1=8.137 ppm2=1.103 assign ( resid 98 and name HG2# ) ( resid 109 and name HA ) 4.4 2.7 1.6 volume=0.140 peak=3020 ppm1=1.318 ppm2=3.898 assign ( resid 47 and name HN ) ( resid 47 and name HA ) 3.2 1.5 1.3 volume=0.969 peak=444 ppm1=8.699 ppm2=4.805 assign ( resid 129 and name HN ) ( resid 152 and name HA2 ) 3.1 1.4 1.2 volume=1.222 peak=1043 ppm1=8.719 ppm2=3.879 assign ( resid 154 and name HB ) ( resid 126 and name HG2# ) 4.5 2.8 1.5 volume=0.124 peak=2997 ppm1=2.182 ppm2=0.759 assign ( resid 184 and name HN ) ( resid 180 and name HN ) 3.4 1.7 1.4 volume=0.692 peak=1954 ppm1=7.500 ppm2=8.344 assign ( resid 158 and name HG1 ) ( resid 166 and name HN ) 4.0 2.3 1.6 volume=0.247 peak=4736 ppm1=2.439 ppm2=9.015 assign ( resid 194 and name HN ) ( resid 190 and name HA ) 3.2 1.4 1.3 volume=1.077 peak=307 ppm1=7.775 ppm2=4.002 assign ( resid 8 and name HA ) ( resid 8 and name HG1 or resid 8 and name HG2 ) 3.3 1.5 1.3 volume=0.901 peak=5014 ppm1=3.839 ppm2=2.326 assign ( resid 180 and name HB2 ) ( resid 183 and name HN ) 4.5 2.8 1.5 volume=0.135 peak=3092 ppm1=3.912 ppm2=7.474 assign ( resid 170 and name HN ) ( resid 49 and name HG1 ) 4.2 2.5 1.7 volume=0.204 peak=1474 ppm1=9.145 ppm2=1.589 assign ( resid 184 and name HG2# ) ( resid 184 and name HD1# ) 3.0 1.3 1.2 volume=1.407 peak=2572 ppm1=1.096 ppm2=0.887 assign ( resid 57 and name HA ) ( resid 58 and name HG1 ) 3.3 1.5 1.3 volume=0.896 peak=4973 ppm1=4.135 ppm2=1.745 assign ( resid 184 and name HB ) ( resid 184 and name HG11 ) 3.4 1.6 1.3 volume=0.753 peak=3820 ppm1=2.045 ppm2=1.679 assign ( resid 199 and name HA ) ( resid 199 and name HN ) 3.9 2.2 1.6 volume=0.297 peak=3449 ppm1=2.796 ppm2=8.658 assign ( resid 160 and name HN ) ( resid 159 and name HA ) 3.0 1.3 1.2 volume=1.523 peak=2165 ppm1=8.832 ppm2=3.751 assign ( resid 67 and name HB1 ) ( resid 67 and name HN ) 3.4 1.7 1.4 volume=0.652 peak=3789 ppm1=2.151 ppm2=7.609 assign ( resid 54 and name HG2# ) ( resid 203 and name HD1# ) 3.4 1.6 1.3 volume=0.744 peak=3492 ppm1=0.576 ppm2=-0.009 assign ( resid 167 and name HN ) ( resid 168 and name HA ) 4.0 2.3 1.6 volume=0.266 peak=1378 ppm1=8.641 ppm2=4.791 assign ( resid 162 and name HA ) ( resid 57 and name HA ) 3.0 1.3 1.2 volume=1.475 peak=4471 ppm1=3.650 ppm2=4.199 assign ( resid 121 and name HN ) ( resid 120 and name HN ) 3.4 1.7 1.4 volume=0.693 peak=1910 ppm1=8.585 ppm2=8.923 assign ( resid 184 and name HA ) ( resid 188 and name HE# ) 4.3 2.5 1.7 volume=0.181 peak=3605 ppm1=3.626 ppm2=1.894 assign ( resid 157 and name HG1 ) ( resid 58 and name HB1 or resid 58 and name HB2 ) 4.0 2.3 1.6 volume=0.249 peak=3159 ppm1=1.790 ppm2=2.136 assign ( resid 193 and name HG1# ) ( resid 193 and name HB ) 2.8 1.1 1.1 volume=2.147 peak=3702 ppm1=0.792 ppm2=2.052 assign ( resid 99 and name HG2 ) ( resid 99 and name HB1 ) 3.7 2.0 1.5 volume=0.434 peak=3908 ppm1=2.439 ppm2=1.760 assign ( resid 152 and name HA1 ) ( resid 153 and name HB2 ) 3.6 1.8 1.4 volume=0.525 peak=3790 ppm1=3.710 ppm2=2.868 assign ( resid 114 and name HN ) ( resid 93 and name HD1# ) 4.2 2.5 1.7 volume=0.196 peak=1594 ppm1=8.799 ppm2=-0.289 assign ( resid 169 and name HA ) ( resid 169 and name HN ) 4.4 2.7 1.6 volume=0.152 peak=3715 ppm1=5.252 ppm2=9.258 assign ( resid 85 and name HB2 ) ( resid 84 and name HG1# ) 4.4 2.7 1.6 volume=0.141 peak=4238 ppm1=3.052 ppm2=0.543 assign ( resid 203 and name HG11 ) ( resid 56 and name HB2 ) 3.5 1.8 1.4 volume=0.573 peak=2507 ppm1=0.517 ppm2=1.746 assign ( resid 3 and name HE1 or resid 3 and name HE2 ) ( resid 134 and name HD1 or resid 134 and name HD2 ) 3.1 1.4 1.2 volume=1.183 peak=133 ppm1=7.211 ppm2=6.882 assign ( resid 184 and name HD1# ) ( resid 179 and name HD1# ) 3.0 1.3 1.2 volume=1.510 peak=2611 ppm1=0.890 ppm2=0.573 assign ( resid 66 and name HB1 ) ( resid 66 and name HN ) 4.0 2.3 1.6 volume=0.272 peak=4846 ppm1=3.101 ppm2=8.030 assign ( resid 145 and name HG2 ) ( resid 145 and name HB1 ) 3.2 1.4 1.3 volume=1.081 peak=4032 ppm1=1.409 ppm2=1.912 assign ( resid 120 and name HN ) ( resid 126 and name HG2# ) 3.7 2.0 1.5 volume=0.422 peak=2035 ppm1=8.910 ppm2=0.753 assign ( resid 66 and name HN ) ( resid 65 and name HD1# ) 3.4 1.6 1.3 volume=0.753 peak=1977 ppm1=8.049 ppm2=0.176 assign ( resid 126 and name HD1# ) ( resid 15 and name HD1# ) 3.9 2.1 1.5 volume=0.323 peak=4883 ppm1=0.348 ppm2=0.431 assign ( resid 133 and name HN ) ( resid 134 and name HN ) 3.6 1.9 1.4 volume=0.500 peak=1192 ppm1=8.115 ppm2=8.698 assign ( resid 79 and name HB1 ) ( resid 80 and name HG2# ) 2.8 1.1 1.1 volume=2.047 peak=3115 ppm1=1.779 ppm2=0.699 assign ( resid 168 and name HG1# ) ( resid 166 and name HE1 ) 3.2 1.5 1.3 volume=0.979 peak=2943 ppm1=0.766 ppm2=2.708 assign ( resid 169 and name HA ) ( resid 169 and name HB2 ) 3.6 1.9 1.4 volume=0.489 peak=4098 ppm1=5.237 ppm2=1.786 assign ( resid 120 and name HN ) ( resid 118 and name HA ) 3.9 2.1 1.5 volume=0.329 peak=667 ppm1=8.911 ppm2=3.802 assign ( resid 190 and name HB2 ) ( resid 186 and name HA ) 4.4 2.6 1.6 volume=0.155 peak=3343 ppm1=3.881 ppm2=4.142 assign ( resid 167 and name HN ) ( resid 52 and name HA2 ) 3.5 1.8 1.4 volume=0.580 peak=1610 ppm1=8.642 ppm2=4.526 assign ( resid 192 and name HB2 ) ( resid 193 and name HN ) 4.5 2.8 1.5 volume=0.133 peak=3425 ppm1=1.331 ppm2=7.644 assign ( resid 113 and name HN ) ( resid 112 and name HG2# ) 3.0 1.3 1.2 volume=1.557 peak=1938 ppm1=8.232 ppm2=0.612 assign ( resid 45 and name HN ) ( resid 46 and name HN ) 3.4 1.7 1.4 volume=0.717 peak=557 ppm1=6.653 ppm2=8.565 assign ( resid 173 and name HG2# ) ( resid 175 and name HN ) 3.6 1.9 1.5 volume=0.463 peak=3782 ppm1=1.026 ppm2=8.816 assign ( resid 37 and name HB1 or resid 37 and name HB2 ) ( resid 37 and name HA ) 4.2 2.5 1.7 volume=0.190 peak=4255 ppm1=3.288 ppm2=5.819 assign ( resid 87 and name HG12 ) ( resid 87 and name HG11 ) 3.4 1.7 1.4 volume=0.661 peak=4720 ppm1=1.049 ppm2=1.262 assign ( resid 204 and name HN ) ( resid 203 and name HD1# ) 3.7 2.0 1.5 volume=0.422 peak=2397 ppm1=6.743 ppm2=-0.008 assign ( resid 26 and name HG1# ) ( resid 27 and name HN ) 4.0 2.3 1.6 volume=0.264 peak=3595 ppm1=0.778 ppm2=9.304 assign ( resid 188 and name HN ) ( resid 189 and name HD2 ) 3.3 1.6 1.3 volume=0.777 peak=2168 ppm1=8.442 ppm2=3.459 assign ( resid 203 and name HG2# ) ( resid 207 and name HN ) 3.2 1.5 1.3 volume=1.040 peak=4744 ppm1=0.338 ppm2=7.750 assign ( resid 95 and name HN ) ( resid 112 and name HG2# ) 3.3 1.6 1.3 volume=0.805 peak=1190 ppm1=9.124 ppm2=0.625 assign ( resid 99 and name HN ) ( resid 109 and name HN ) 3.2 1.4 1.3 volume=1.092 peak=2341 ppm1=7.799 ppm2=8.172 assign ( resid 186 and name HB2 ) ( resid 186 and name HD2 ) 4.2 2.5 1.7 volume=0.199 peak=4587 ppm1=1.903 ppm2=1.612 assign ( resid 50 and name HN ) ( resid 50 and name HA ) 3.7 2.0 1.5 volume=0.396 peak=372 ppm1=9.302 ppm2=5.183 assign ( resid 109 and name HN ) ( resid 109 and name HB2 ) 2.8 1.1 1.1 volume=2.292 peak=1715 ppm1=8.165 ppm2=1.723 assign ( resid 92 and name HE1 or resid 92 and name HE2 ) ( resid 117 and name HN ) 3.5 1.7 1.4 volume=0.618 peak=36 ppm1=6.750 ppm2=8.244 assign ( resid 114 and name HD1# ) ( resid 114 and name HA ) 4.4 2.7 1.6 volume=0.149 peak=3439 ppm1=0.538 ppm2=4.445 assign ( resid 15 and name HN ) ( resid 12 and name HG1 or resid 12 and name HG2 ) 3.6 1.9 1.5 volume=0.464 peak=1746 ppm1=7.812 ppm2=2.438 assign ( resid 201 and name HN ) ( resid 197 and name HA ) 3.4 1.7 1.4 volume=0.672 peak=2236 ppm1=7.402 ppm2=3.747 assign ( resid 87 and name HN ) ( resid 86 and name HB1 ) 3.5 1.8 1.4 volume=0.594 peak=1758 ppm1=8.039 ppm2=1.530 assign ( resid 195 and name HN ) ( resid 192 and name HA ) 3.5 1.8 1.4 volume=0.612 peak=923 ppm1=7.971 ppm2=4.140 assign ( resid 130 and name HE2 ) ( resid 10 and name HG2# ) 2.8 1.0 1.1 volume=2.423 peak=2871 ppm1=2.835 ppm2=1.072 assign ( resid 167 and name HD1# ) ( resid 167 and name HB1 ) 3.6 1.9 1.5 volume=0.469 peak=4170 ppm1=0.763 ppm2=1.678 assign ( resid 4 and name HN ) ( resid 4 and name HG1 or resid 4 and name HG2 ) 2.6 0.9 1.1 volume=3.220 peak=1877 ppm1=8.190 ppm2=1.399 assign ( resid 204 and name HB2 ) ( resid 203 and name HG2# ) 3.5 1.8 1.4 volume=0.545 peak=3426 ppm1=1.712 ppm2=0.322 assign ( resid 54 and name HN ) ( resid 54 and name HA ) 3.3 1.6 1.3 volume=0.763 peak=976 ppm1=9.024 ppm2=4.533 assign ( resid 77 and name HN ) ( resid 75 and name HN ) 4.2 2.5 1.7 volume=0.204 peak=2022 ppm1=8.056 ppm2=7.504 assign ( resid 28 and name HN ) ( resid 27 and name HN ) 3.7 2.0 1.5 volume=0.413 peak=2300 ppm1=7.809 ppm2=9.276 assign ( resid 90 and name HN ) ( resid 91 and name HG2# ) 3.4 1.6 1.3 volume=0.750 peak=2156 ppm1=8.382 ppm2=1.013 assign ( resid 167 and name HA ) ( resid 154 and name HG2# ) 3.5 1.7 1.4 volume=0.617 peak=3146 ppm1=5.218 ppm2=0.853 assign ( resid 114 and name HB2 ) ( resid 114 and name HB1 ) 3.8 2.1 1.5 volume=0.356 peak=4157 ppm1=1.701 ppm2=1.062 assign ( resid 64 and name HN ) ( resid 61 and name HN ) 4.2 2.5 1.7 volume=0.191 peak=2380 ppm1=7.881 ppm2=8.700 assign ( resid 196 and name HG11 ) ( resid 196 and name HG12 ) 2.8 1.1 1.1 volume=2.330 peak=3629 ppm1=1.806 ppm2=1.478 assign ( resid 56 and name HN ) ( resid 165 and name HA ) 3.7 2.0 1.5 volume=0.410 peak=1336 ppm1=8.640 ppm2=5.186 assign ( resid 79 and name HB2 ) ( resid 99 and name HG1 ) 3.0 1.2 1.2 volume=1.607 peak=5152 ppm1=1.780 ppm2=2.460 assign ( resid 143 and name HN ) ( resid 140 and name HN ) 4.0 2.3 1.6 volume=0.257 peak=1912 ppm1=6.903 ppm2=9.607 assign ( resid 61 and name HN ) ( resid 203 and name HD1# ) 3.8 2.1 1.5 volume=0.332 peak=1456 ppm1=8.712 ppm2=-0.036 assign ( resid 115 and name HG1# ) ( resid 114 and name HG ) 3.1 1.4 1.2 volume=1.267 peak=5098 ppm1=0.302 ppm2=0.968 assign ( resid 54 and name HD1# ) ( resid 203 and name HB ) 3.5 1.8 1.4 volume=0.604 peak=4890 ppm1=0.490 ppm2=0.120 assign ( resid 154 and name HG2# ) ( resid 155 and name HN ) 3.6 1.9 1.4 volume=0.478 peak=4915 ppm1=0.838 ppm2=8.988 assign ( resid 154 and name HG2# ) ( resid 154 and name HN ) 3.7 1.9 1.5 volume=0.449 peak=2751 ppm1=0.844 ppm2=10.009 assign ( resid 34 and name HN ) ( resid 50 and name HA ) 3.6 1.8 1.4 volume=0.526 peak=1260 ppm1=8.136 ppm2=5.180 assign ( resid 10 and name HB ) ( resid 11 and name HB# ) 4.4 2.7 1.6 volume=0.153 peak=4224 ppm1=3.687 ppm2=1.680 assign ( resid 16 and name HN ) ( resid 19 and name HD1 ) 3.8 2.1 1.5 volume=0.336 peak=2259 ppm1=7.496 ppm2=2.966 assign ( resid 11 and name HA ) ( resid 10 and name HG2# ) 3.8 2.0 1.5 volume=0.385 peak=4221 ppm1=3.956 ppm2=1.100 assign ( resid 160 and name HB1 ) ( resid 163 and name HB# ) 2.7 1.0 1.1 volume=2.520 peak=3857 ppm1=2.036 ppm2=1.109 assign ( resid 114 and name HD2# ) ( resid 6 and name HN ) 3.6 1.9 1.4 volume=0.476 peak=5081 ppm1=0.781 ppm2=7.735 assign ( resid 60 and name HB2 ) ( resid 203 and name HG2# ) 3.4 1.7 1.4 volume=0.665 peak=2467 ppm1=1.720 ppm2=0.336 assign ( resid 63 and name HN ) ( resid 63 and name HA ) 2.9 1.2 1.2 volume=1.877 peak=1057 ppm1=7.294 ppm2=4.395 assign ( resid 6 and name HB ) ( resid 6 and name HN ) 4.5 2.7 1.5 volume=0.138 peak=3533 ppm1=1.727 ppm2=7.725 assign ( resid 54 and name HG2# ) ( resid 54 and name HN ) 4.1 2.4 1.6 volume=0.227 peak=4191 ppm1=0.577 ppm2=9.035 assign ( resid 200 and name HA ) ( resid 200 and name HD1 ) 3.5 1.8 1.4 volume=0.566 peak=4422 ppm1=3.361 ppm2=1.550 assign ( resid 199 and name HA ) ( resid 202 and name HN ) 4.5 2.8 1.5 volume=0.133 peak=4312 ppm1=2.796 ppm2=8.545 assign ( resid 159 and name HN ) ( resid 160 and name HN ) 4.0 2.2 1.6 volume=0.281 peak=2128 ppm1=9.024 ppm2=8.832 assign ( resid 40 and name HN ) ( resid 40 and name HB2 ) 3.1 1.4 1.3 volume=1.148 peak=2081 ppm1=8.509 ppm2=3.354 assign ( resid 59 and name HN ) ( resid 58 and name HD2 ) 3.5 1.8 1.4 volume=0.603 peak=1920 ppm1=8.089 ppm2=3.872 assign ( resid 40 and name HN ) ( resid 45 and name HA1 ) 3.3 1.6 1.3 volume=0.806 peak=938 ppm1=8.510 ppm2=3.237 assign ( resid 147 and name HB1 ) ( resid 148 and name HN ) 4.3 2.6 1.7 volume=0.169 peak=3198 ppm1=2.632 ppm2=9.132 assign ( resid 71 and name HB2 ) ( resid 65 and name HD1# ) 4.3 2.6 1.7 volume=0.173 peak=4353 ppm1=1.529 ppm2=0.193 assign ( resid 117 and name HD1# ) ( resid 116 and name HN ) 4.1 2.4 1.7 volume=0.217 peak=4564 ppm1=0.244 ppm2=8.818 assign ( resid 99 and name HA ) ( resid 79 and name HG1 ) 3.1 1.4 1.2 volume=1.266 peak=3284 ppm1=4.283 ppm2=1.885 assign ( resid 26 and name HG1# ) ( resid 34 and name HG2# ) 2.5 0.7 1.0 volume=4.817 peak=4048 ppm1=0.778 ppm2=1.096 assign ( resid 179 and name HD1# ) ( resid 179 and name HB2 ) 3.8 2.1 1.5 volume=0.352 peak=3835 ppm1=0.530 ppm2=2.493 assign ( resid 132 and name HG2# ) ( resid 130 and name HN ) 3.5 1.8 1.4 volume=0.558 peak=4723 ppm1=0.936 ppm2=7.673 assign ( resid 76 and name HD2 ) ( resid 77 and name HN ) 3.6 1.9 1.5 volume=0.455 peak=4621 ppm1=1.550 ppm2=8.103 assign ( resid 203 and name HG2# ) ( resid 203 and name HD1# ) 2.8 1.0 1.1 volume=2.404 peak=4688 ppm1=0.340 ppm2=-0.009 assign ( resid 1 and name HA ) ( resid 4 and name HB1 ) 3.5 1.8 1.4 volume=0.608 peak=2954 ppm1=4.282 ppm2=1.806 assign ( resid 87 and name HD1# ) ( resid 91 and name HB ) 4.0 2.3 1.6 volume=0.247 peak=3312 ppm1=0.440 ppm2=3.632 assign ( resid 192 and name HD2# ) ( resid 50 and name HG1# ) 3.0 1.3 1.2 volume=1.419 peak=2987 ppm1=0.494 ppm2=0.704 assign ( resid 200 and name HB1 ) ( resid 200 and name HE1 ) 3.7 2.0 1.5 volume=0.397 peak=2929 ppm1=1.670 ppm2=2.738 assign ( resid 73 and name HB ) ( resid 73 and name HN ) 3.7 2.0 1.5 volume=0.433 peak=5097 ppm1=4.302 ppm2=7.547 assign ( resid 26 and name HN ) ( resid 26 and name HA ) 3.4 1.7 1.4 volume=0.642 peak=2440 ppm1=8.861 ppm2=3.977 assign ( resid 143 and name HN ) ( resid 142 and name HB2 ) 2.8 1.1 1.1 volume=2.263 peak=697 ppm1=6.899 ppm2=1.803 assign ( resid 15 and name HD1# ) ( resid 12 and name HA ) 4.0 2.3 1.6 volume=0.271 peak=2696 ppm1=0.438 ppm2=3.921 assign ( resid 154 and name HG2# ) ( resid 18 and name HB1 ) 3.6 1.9 1.5 volume=0.472 peak=4362 ppm1=0.837 ppm2=2.985 assign ( resid 113 and name HN ) ( resid 113 and name HB2 ) 3.0 1.3 1.2 volume=1.439 peak=1216 ppm1=8.233 ppm2=2.059 assign ( resid 87 and name HG2# ) ( resid 87 and name HB ) 2.7 1.0 1.1 volume=2.960 peak=2714 ppm1=0.850 ppm2=1.368 assign ( resid 61 and name HN ) ( resid 59 and name HN ) 2.9 1.1 1.1 volume=1.983 peak=1165 ppm1=8.715 ppm2=8.021 assign ( resid 33 and name HD1# ) ( resid 197 and name HA ) 4.5 2.8 1.5 volume=0.122 peak=5074 ppm1=0.361 ppm2=3.769 assign ( resid 36 and name HA ) ( resid 24 and name HA ) 4.5 2.8 1.5 volume=0.128 peak=3670 ppm1=5.851 ppm2=4.291 assign ( resid 184 and name HN ) ( resid 185 and name HG1 ) 3.6 1.9 1.5 volume=0.466 peak=2450 ppm1=7.499 ppm2=2.358 assign ( resid 129 and name HN ) ( resid 115 and name HG2# ) 3.5 1.8 1.4 volume=0.550 peak=1110 ppm1=8.719 ppm2=0.644 assign ( resid 6 and name HA ) ( resid 6 and name HG2# ) 2.9 1.2 1.2 volume=1.815 peak=2639 ppm1=3.616 ppm2=0.858 assign ( resid 172 and name HN ) ( resid 172 and name HB1 ) 4.0 2.3 1.6 volume=0.268 peak=666 ppm1=8.854 ppm2=1.794 assign ( resid 130 and name HB1 ) ( resid 114 and name HB1 ) 3.1 1.4 1.2 volume=1.255 peak=4608 ppm1=1.886 ppm2=1.027 assign ( resid 157 and name HB2 ) ( resid 157 and name HG2 ) 2.8 1.1 1.1 volume=2.116 peak=3097 ppm1=2.308 ppm2=1.792 assign ( resid 164 and name HN ) ( resid 164 and name HB2 ) 3.0 1.3 1.2 volume=1.370 peak=1724 ppm1=7.977 ppm2=2.990 assign ( resid 130 and name HB2 ) ( resid 130 and name HD2 ) 3.1 1.4 1.2 volume=1.242 peak=4715 ppm1=1.833 ppm2=1.659 assign ( resid 54 and name HD1# ) ( resid 54 and name HB ) 2.7 0.9 1.1 volume=2.971 peak=3456 ppm1=0.490 ppm2=1.777 assign ( resid 145 and name HG1 ) ( resid 112 and name HB ) 3.5 1.8 1.4 volume=0.613 peak=4347 ppm1=1.408 ppm2=2.068 assign ( resid 166 and name HN ) ( resid 61 and name HD1# ) 3.0 1.3 1.2 volume=1.422 peak=347 ppm1=9.001 ppm2=0.750 assign ( resid 10 and name HG2# ) ( resid 116 and name HN ) 4.3 2.6 1.7 volume=0.162 peak=2990 ppm1=1.084 ppm2=8.843 assign ( resid 26 and name HG2# ) ( resid 25 and name HE1 or resid 25 and name HE2 ) 3.4 1.7 1.4 volume=0.661 peak=4367 ppm1=0.913 ppm2=2.865 assign ( resid 87 and name HN ) ( resid 88 and name HN ) 3.9 2.1 1.5 volume=0.328 peak=612 ppm1=8.040 ppm2=8.568 assign ( resid 175 and name HN ) ( resid 173 and name HB ) 3.1 1.4 1.3 volume=1.102 peak=416 ppm1=8.803 ppm2=3.620 assign ( resid 173 and name HB ) ( resid 173 and name HG2# ) 2.9 1.2 1.2 volume=1.702 peak=3084 ppm1=3.613 ppm2=1.032 assign ( resid 158 and name HA ) ( resid 158 and name HN ) 4.4 2.7 1.6 volume=0.154 peak=3353 ppm1=4.138 ppm2=8.202 assign ( resid 162 and name HD1 ) ( resid 162 and name HA ) 3.6 1.8 1.4 volume=0.534 peak=4175 ppm1=3.488 ppm2=3.647 assign ( resid 4 and name HN ) ( resid 3 and name HA ) 3.2 1.4 1.3 volume=1.064 peak=1558 ppm1=8.189 ppm2=4.312 assign ( resid 164 and name HB2 ) ( resid 164 and name HN ) 4.3 2.5 1.7 volume=0.179 peak=3728 ppm1=2.997 ppm2=7.973 assign ( resid 31 and name HN ) ( resid 31 and name HA ) 4.0 2.3 1.6 volume=0.260 peak=573 ppm1=9.253 ppm2=4.402 assign ( resid 117 and name HN ) ( resid 117 and name HG2# ) 3.2 1.5 1.3 volume=1.041 peak=1504 ppm1=8.234 ppm2=0.372 assign ( resid 74 and name HD1 ) ( resid 74 and name HN ) 3.1 1.4 1.3 volume=1.118 peak=112 ppm1=6.939 ppm2=6.509 assign ( resid 39 and name HB# ) ( resid 40 and name HN ) 3.1 1.4 1.3 volume=1.103 peak=3378 ppm1=1.175 ppm2=8.517 assign ( resid 96 and name HN ) ( resid 112 and name HA ) 3.4 1.7 1.4 volume=0.715 peak=1123 ppm1=8.473 ppm2=4.919 assign ( resid 64 and name HN ) ( resid 63 and name HB2 or resid 63 and name HB1 ) 2.7 1.0 1.1 volume=2.596 peak=1906 ppm1=7.879 ppm2=2.703 assign ( resid 199 and name HN ) ( resid 54 and name HD1# ) 2.7 1.0 1.1 volume=2.825 peak=1567 ppm1=8.634 ppm2=0.495 assign ( resid 124 and name HN ) ( resid 122 and name HA1 ) 3.1 1.4 1.3 volume=1.122 peak=678 ppm1=6.472 ppm2=3.876 assign ( resid 211 and name HA ) ( resid 211 and name HD2 ) 3.1 1.4 1.2 volume=1.233 peak=4383 ppm1=4.485 ppm2=2.983 assign ( resid 128 and name HN ) ( resid 127 and name HG2# ) 3.3 1.6 1.3 volume=0.772 peak=501 ppm1=9.933 ppm2=0.750 assign ( resid 187 and name HN ) ( resid 184 and name HG2# ) 3.2 1.5 1.3 volume=0.933 peak=1991 ppm1=7.601 ppm2=1.099 assign ( resid 126 and name HB ) ( resid 126 and name HG2# ) 3.2 1.5 1.3 volume=0.986 peak=2748 ppm1=1.596 ppm2=0.762 assign ( resid 24 and name HD1 ) ( resid 24 and name HZ2 ) 3.7 1.9 1.5 volume=0.442 peak=61 ppm1=6.801 ppm2=7.537 assign ( resid 79 and name HN ) ( resid 79 and name HA ) 3.7 2.0 1.5 volume=0.397 peak=2277 ppm1=8.844 ppm2=4.404 assign ( resid 153 and name HN ) ( resid 170 and name HN ) 3.8 2.1 1.5 volume=0.364 peak=979 ppm1=9.328 ppm2=9.152 assign ( resid 34 and name HB ) ( resid 34 and name HG2# ) 3.1 1.3 1.2 volume=1.283 peak=4865 ppm1=3.828 ppm2=1.103 assign ( resid 179 and name HD1# ) ( resid 180 and name HN ) 4.2 2.5 1.7 volume=0.202 peak=3045 ppm1=0.530 ppm2=8.259 assign ( resid 112 and name HN ) ( resid 96 and name HB ) 3.9 2.1 1.5 volume=0.324 peak=1020 ppm1=8.134 ppm2=3.877 assign ( resid 183 and name HD1# ) ( resid 183 and name HN ) 3.4 1.7 1.4 volume=0.656 peak=3383 ppm1=0.871 ppm2=7.471 assign ( resid 196 and name HG2# ) ( resid 196 and name HB ) 3.5 1.8 1.4 volume=0.561 peak=4322 ppm1=0.813 ppm2=2.244 assign ( resid 68 and name HG2# ) ( resid 69 and name HA1 ) 2.5 0.8 1.0 volume=4.572 peak=3128 ppm1=0.751 ppm2=3.768 assign ( resid 27 and name HN ) ( resid 28 and name HN ) 3.8 2.1 1.5 volume=0.349 peak=1211 ppm1=9.278 ppm2=7.784 assign ( resid 204 and name HD1 ) ( resid 204 and name HA ) 3.7 1.9 1.5 volume=0.445 peak=3529 ppm1=1.485 ppm2=3.801 assign ( resid 164 and name HN ) ( resid 164 and name HA ) 3.3 1.6 1.3 volume=0.854 peak=1649 ppm1=7.977 ppm2=4.901 assign ( resid 127 and name HN ) ( resid 153 and name HN ) 3.7 2.0 1.5 volume=0.431 peak=402 ppm1=9.383 ppm2=9.317 assign ( resid 72 and name HD1# ) ( resid 70 and name HN ) 3.6 1.9 1.4 volume=0.493 peak=3733 ppm1=0.588 ppm2=8.521 assign ( resid 88 and name HN ) ( resid 86 and name HB2 ) 3.1 1.4 1.2 volume=1.220 peak=2290 ppm1=8.595 ppm2=1.526 assign ( resid 167 and name HB2 ) ( resid 54 and name HG12 ) 4.1 2.4 1.6 volume=0.226 peak=4147 ppm1=1.680 ppm2=1.216 assign ( resid 140 and name HN ) ( resid 139 and name HB1 ) 3.2 1.5 1.3 volume=0.967 peak=885 ppm1=9.582 ppm2=2.180 assign ( resid 174 and name HN ) ( resid 173 and name HB ) 4.1 2.3 1.6 volume=0.237 peak=2113 ppm1=9.152 ppm2=3.550 assign ( resid 73 and name HB ) ( resid 73 and name HA ) 4.4 2.6 1.6 volume=0.155 peak=4452 ppm1=4.300 ppm2=3.919 assign ( resid 33 and name HD1# ) ( resid 33 and name HN ) 2.9 1.2 1.2 volume=1.780 peak=4281 ppm1=0.358 ppm2=8.185 assign ( resid 28 and name HN ) ( resid 28 and name HD2 ) 3.0 1.3 1.2 volume=1.501 peak=1054 ppm1=7.809 ppm2=1.398 assign ( resid 76 and name HG2 ) ( resid 76 and name HD1 ) 2.2 0.5 0.9 volume=8.795 peak=4752 ppm1=1.384 ppm2=1.551 assign ( resid 126 and name HD1# ) ( resid 118 and name HB2 ) 4.3 2.6 1.7 volume=0.169 peak=4313 ppm1=0.349 ppm2=2.520 assign ( resid 69 and name HN ) ( resid 70 and name HA ) 3.5 1.8 1.4 volume=0.593 peak=1818 ppm1=8.216 ppm2=4.852 assign ( resid 180 and name HN ) ( resid 180 and name HB2 ) 3.8 2.1 1.5 volume=0.368 peak=792 ppm1=8.353 ppm2=3.883 assign ( resid 208 and name HN ) ( resid 208 and name HG2# ) 3.7 2.0 1.5 volume=0.416 peak=2191 ppm1=8.011 ppm2=1.133 assign ( resid 99 and name HB1 ) ( resid 99 and name HN ) 3.4 1.7 1.4 volume=0.672 peak=3958 ppm1=1.790 ppm2=7.777 assign ( resid 202 and name HN ) ( resid 203 and name HG2# ) 3.5 1.7 1.4 volume=0.627 peak=599 ppm1=8.576 ppm2=0.352 assign ( resid 51 and name HA ) ( resid 51 and name HG1 or resid 51 and name HG2 ) 3.7 2.0 1.5 volume=0.406 peak=3050 ppm1=5.622 ppm2=1.943 assign ( resid 153 and name HA ) ( resid 152 and name HA1 ) 4.1 2.4 1.6 volume=0.221 peak=2596 ppm1=5.319 ppm2=3.694 assign ( resid 66 and name HN ) ( resid 66 and name HB1 or resid 66 and name HB2 ) 3.0 1.3 1.2 volume=1.450 peak=352 ppm1=8.050 ppm2=3.101 assign ( resid 183 and name HA ) ( resid 183 and name HG12 ) 3.0 1.2 1.2 volume=1.614 peak=4350 ppm1=3.919 ppm2=1.549 assign ( resid 184 and name HN ) ( resid 183 and name HN ) 2.7 1.0 1.1 volume=2.553 peak=1621 ppm1=7.499 ppm2=7.421 assign ( resid 203 and name HD1# ) ( resid 65 and name HN ) 3.7 2.0 1.5 volume=0.406 peak=4472 ppm1=-0.009 ppm2=7.737 assign ( resid 76 and name HN ) ( resid 198 and name HN ) 4.3 2.6 1.7 volume=0.172 peak=591 ppm1=6.699 ppm2=8.702 assign ( resid 201 and name HN ) ( resid 203 and name HG2# ) 3.5 1.8 1.4 volume=0.593 peak=569 ppm1=7.405 ppm2=0.361 assign ( resid 175 and name HG1 ) ( resid 175 and name HN ) 4.8 3.1 1.2 volume=0.083 peak=3749 ppm1=2.553 ppm2=8.802 assign ( resid 6 and name HN ) ( resid 7 and name HB# ) 2.6 0.9 1.0 volume=3.659 peak=1238 ppm1=7.723 ppm2=0.751 assign ( resid 39 and name HB# ) ( resid 47 and name HN ) 3.8 2.1 1.5 volume=0.342 peak=3614 ppm1=1.175 ppm2=8.715 assign ( resid 179 and name HA ) ( resid 179 and name HD1# ) 4.1 2.4 1.7 volume=0.211 peak=2813 ppm1=3.821 ppm2=0.513 assign ( resid 106 and name HB ) ( resid 102 and name HB# ) 3.8 2.1 1.5 volume=0.343 peak=3682 ppm1=1.795 ppm2=1.287 assign ( resid 110 and name HN ) ( resid 109 and name HB1 ) 3.1 1.4 1.2 volume=1.262 peak=2163 ppm1=8.722 ppm2=1.735 assign ( resid 112 and name HN ) ( resid 146 and name HN ) 3.4 1.6 1.3 volume=0.746 peak=1280 ppm1=8.134 ppm2=8.401 assign ( resid 113 and name HN ) ( resid 94 and name HN ) 3.8 2.0 1.5 volume=0.380 peak=1696 ppm1=8.233 ppm2=9.602 assign ( resid 162 and name HB2 ) ( resid 163 and name HB# ) 3.2 1.4 1.3 volume=1.087 peak=2631 ppm1=2.206 ppm2=1.094 assign ( resid 198 and name HN ) ( resid 194 and name HB1 ) 3.4 1.7 1.4 volume=0.666 peak=1137 ppm1=8.717 ppm2=2.814 assign ( resid 53 and name HG2# ) ( resid 32 and name HE1 ) 3.9 2.2 1.6 volume=0.294 peak=3335 ppm1=0.902 ppm2=2.862 assign ( resid 74 and name HZ2 ) ( resid 74 and name HD1 ) 3.6 1.9 1.5 volume=0.468 peak=150 ppm1=6.458 ppm2=6.939 assign ( resid 190 and name HB2 ) ( resid 190 and name HA ) 2.3 0.6 0.9 volume=6.396 peak=3155 ppm1=3.880 ppm2=3.976 assign ( resid 51 and name HA ) ( resid 51 and name HN ) 4.1 2.4 1.6 volume=0.230 peak=2609 ppm1=5.621 ppm2=8.459 assign ( resid 16 and name HA2 or resid 16 and name HA1 ) ( resid 19 and name HB1 ) 4.0 2.3 1.6 volume=0.266 peak=4913 ppm1=3.651 ppm2=1.737 assign ( resid 91 and name HN ) ( resid 87 and name HD1# ) 3.7 2.0 1.5 volume=0.421 peak=1524 ppm1=7.218 ppm2=0.408 assign ( resid 134 and name HB1 ) ( resid 132 and name HB ) 3.2 1.5 1.3 volume=1.050 peak=4741 ppm1=3.047 ppm2=2.271 assign ( resid 35 and name HG2# ) ( resid 37 and name HN ) 3.8 2.1 1.5 volume=0.351 peak=2519 ppm1=0.890 ppm2=9.690 assign ( resid 130 and name HN ) ( resid 129 and name HN ) 3.7 2.0 1.5 volume=0.431 peak=389 ppm1=7.617 ppm2=8.718 assign ( resid 187 and name HG2# ) ( resid 188 and name HN ) 3.3 1.6 1.3 volume=0.815 peak=3895 ppm1=1.051 ppm2=8.449 assign ( resid 126 and name HD1# ) ( resid 154 and name HB ) 4.0 2.3 1.6 volume=0.249 peak=2496 ppm1=0.348 ppm2=2.148 assign ( resid 124 and name HN ) ( resid 125 and name HA ) 4.0 2.3 1.6 volume=0.249 peak=481 ppm1=6.472 ppm2=5.571 assign ( resid 184 and name HN ) ( resid 186 and name HE1 ) 3.6 1.9 1.5 volume=0.466 peak=228 ppm1=7.500 ppm2=2.974 assign ( resid 184 and name HN ) ( resid 187 and name HN ) 2.9 1.2 1.2 volume=1.692 peak=1781 ppm1=7.501 ppm2=7.617 assign ( resid 6 and name HD1# ) ( resid 5 and name HN ) 3.6 1.9 1.4 volume=0.478 peak=2678 ppm1=0.795 ppm2=7.481 assign ( resid 177 and name HA2 ) ( resid 178 and name HB1 or resid 178 and name HB2 ) 4.0 2.3 1.6 volume=0.257 peak=4945 ppm1=3.743 ppm2=1.685 assign ( resid 144 and name HG2# ) ( resid 144 and name HG12 ) 2.9 1.2 1.2 volume=1.856 peak=3557 ppm1=0.766 ppm2=1.269 assign ( resid 192 and name HB1 ) ( resid 50 and name HB ) 4.0 2.3 1.6 volume=0.264 peak=2846 ppm1=1.330 ppm2=1.828 assign ( resid 114 and name HN ) ( resid 129 and name HA ) 3.6 1.9 1.4 volume=0.489 peak=1869 ppm1=8.799 ppm2=5.693 assign ( resid 171 and name HA ) ( resid 151 and name HB2 ) 4.6 2.8 1.4 volume=0.118 peak=3658 ppm1=4.148 ppm2=2.993 assign ( resid 68 and name HG2# ) ( resid 68 and name HN ) 3.8 2.1 1.5 volume=0.363 peak=2747 ppm1=0.751 ppm2=8.010 assign ( resid 137 and name HB1 ) ( resid 112 and name HG12 ) 4.0 2.3 1.6 volume=0.244 peak=3851 ppm1=2.806 ppm2=1.271 assign ( resid 203 and name HN ) ( resid 200 and name HN ) 3.9 2.2 1.6 volume=0.289 peak=226 ppm1=7.683 ppm2=8.071 assign ( resid 14 and name HA ) ( resid 14 and name HG1# ) 3.3 1.5 1.3 volume=0.904 peak=4498 ppm1=2.818 ppm2=0.678 assign ( resid 87 and name HG12 ) ( resid 87 and name HA ) 3.9 2.2 1.6 volume=0.301 peak=3467 ppm1=1.050 ppm2=3.873 assign ( resid 143 and name HN ) ( resid 143 and name HB2 ) 3.2 1.4 1.3 volume=1.090 peak=1729 ppm1=6.900 ppm2=2.702 assign ( resid 11 and name HN ) ( resid 12 and name HN ) 3.6 1.9 1.4 volume=0.479 peak=953 ppm1=8.180 ppm2=7.542 assign ( resid 9 and name HN ) ( resid 9 and name HA ) 3.5 1.8 1.4 volume=0.575 peak=752 ppm1=7.984 ppm2=4.003 assign ( resid 200 and name HB2 ) ( resid 200 and name HG1 ) 3.5 1.8 1.4 volume=0.613 peak=4589 ppm1=1.670 ppm2=1.130 assign ( resid 120 and name HB2 ) ( resid 126 and name HG2# ) 3.7 2.0 1.5 volume=0.429 peak=3166 ppm1=3.000 ppm2=0.747 assign ( resid 186 and name HN ) ( resid 106 and name HD1# ) 3.7 2.0 1.5 volume=0.394 peak=2359 ppm1=7.370 ppm2=0.757 assign ( resid 145 and name HB2 ) ( resid 139 and name HB1 ) 2.7 1.0 1.1 volume=2.713 peak=2583 ppm1=1.929 ppm2=2.197 assign ( resid 115 and name HG1# ) ( resid 129 and name HB2 or resid 129 and name HB1 ) 3.8 2.1 1.5 volume=0.372 peak=3409 ppm1=0.303 ppm2=3.374 assign ( resid 130 and name HE2 ) ( resid 130 and name HB2 ) 3.0 1.3 1.2 volume=1.554 peak=4406 ppm1=2.839 ppm2=1.856 assign ( resid 38 and name HN ) ( resid 47 and name HD2# ) 3.3 1.6 1.3 volume=0.766 peak=1622 ppm1=8.465 ppm2=0.117 assign ( resid 75 and name HA ) ( resid 77 and name HN ) 3.5 1.7 1.4 volume=0.628 peak=4670 ppm1=4.153 ppm2=8.003 assign ( resid 126 and name HA ) ( resid 126 and name HD1# ) 4.5 2.8 1.5 volume=0.123 peak=4029 ppm1=5.426 ppm2=0.326 assign ( resid 149 and name HN ) ( resid 173 and name HA ) 3.9 2.2 1.6 volume=0.298 peak=2425 ppm1=7.758 ppm2=3.611 assign ( resid 11 and name HB# ) ( resid 11 and name HA ) 3.4 1.7 1.4 volume=0.718 peak=3192 ppm1=1.632 ppm2=3.956 assign ( resid 166 and name HN ) ( resid 167 and name HN ) 3.4 1.7 1.4 volume=0.660 peak=1125 ppm1=9.000 ppm2=8.686 assign ( resid 24 and name HH2 ) ( resid 36 and name HB1 ) 3.5 1.8 1.4 volume=0.571 peak=71 ppm1=6.802 ppm2=3.891 assign ( resid 131 and name HN ) ( resid 132 and name HA ) 3.4 1.7 1.4 volume=0.654 peak=2149 ppm1=9.292 ppm2=4.659 assign ( resid 82 and name HN ) ( resid 83 and name HB2 ) 3.8 2.0 1.5 volume=0.381 peak=1316 ppm1=8.563 ppm2=1.021 assign ( resid 37 and name HB1 or resid 37 and name HB2 ) ( resid 36 and name HB2 ) 4.2 2.4 1.7 volume=0.207 peak=3616 ppm1=3.288 ppm2=3.442 assign ( resid 196 and name HD1# ) ( resid 169 and name HN ) 4.5 2.8 1.5 volume=0.134 peak=3259 ppm1=0.730 ppm2=9.235 assign ( resid 162 and name HB1 ) ( resid 162 and name HG1 ) 2.8 1.1 1.1 volume=2.337 peak=5048 ppm1=2.209 ppm2=1.918 assign ( resid 121 and name HN ) ( resid 124 and name HN ) 3.5 1.8 1.4 volume=0.557 peak=2227 ppm1=8.586 ppm2=6.488 assign ( resid 72 and name HG2# ) ( resid 73 and name HA ) 3.6 1.9 1.4 volume=0.477 peak=3290 ppm1=0.603 ppm2=3.963 assign ( resid 64 and name HD1 or resid 64 and name HD2 ) ( resid 199 and name HN ) 4.2 2.5 1.7 volume=0.202 peak=84 ppm1=5.973 ppm2=8.640 assign ( resid 35 and name HN ) ( resid 27 and name HN ) 3.2 1.5 1.3 volume=1.017 peak=596 ppm1=9.428 ppm2=9.337 assign ( resid 75 and name HN ) ( resid 71 and name HA ) 4.1 2.3 1.6 volume=0.242 peak=477 ppm1=7.480 ppm2=4.872 assign ( resid 144 and name HG2# ) ( resid 143 and name HA ) 4.5 2.7 1.5 volume=0.138 peak=3371 ppm1=0.766 ppm2=4.674 assign ( resid 56 and name HN ) ( resid 165 and name HB1 ) 3.4 1.7 1.4 volume=0.655 peak=427 ppm1=8.638 ppm2=2.961 assign ( resid 61 and name HG ) ( resid 61 and name HD1# ) 2.7 1.0 1.1 volume=2.562 peak=4601 ppm1=1.718 ppm2=0.761 assign ( resid 193 and name HA ) ( resid 33 and name HD1# ) 3.8 2.0 1.5 volume=0.379 peak=2841 ppm1=3.460 ppm2=0.324 assign ( resid 65 and name HD1# ) ( resid 153 and name HB1 or resid 153 and name HB2 ) 4.0 2.3 1.6 volume=0.254 peak=4243 ppm1=0.175 ppm2=2.861 assign ( resid 84 and name HA ) ( resid 84 and name HG1# ) 3.7 2.0 1.5 volume=0.399 peak=4308 ppm1=4.391 ppm2=0.513 assign ( resid 129 and name HA ) ( resid 130 and name HN ) 4.4 2.7 1.6 volume=0.153 peak=4208 ppm1=5.702 ppm2=7.641 assign ( resid 29 and name HG2# ) ( resid 28 and name HN ) 4.1 2.3 1.6 volume=0.237 peak=3193 ppm1=1.066 ppm2=7.807 assign ( resid 136 and name HN ) ( resid 134 and name HA ) 3.9 2.1 1.5 volume=0.329 peak=1208 ppm1=6.891 ppm2=5.184 assign ( resid 186 and name HB2 ) ( resid 187 and name HN ) 4.0 2.2 1.6 volume=0.278 peak=3624 ppm1=1.900 ppm2=7.604 assign ( resid 97 and name HN ) ( resid 79 and name HB2 ) 4.1 2.4 1.7 volume=0.211 peak=1628 ppm1=8.363 ppm2=1.790 assign ( resid 173 and name HB ) ( resid 188 and name HE# ) 3.8 2.0 1.5 volume=0.376 peak=2473 ppm1=3.613 ppm2=1.878 assign ( resid 115 and name HG1# ) ( resid 115 and name HG2# ) 2.7 0.9 1.1 volume=3.041 peak=4277 ppm1=0.303 ppm2=0.660 assign ( resid 151 and name HN ) ( resid 128 and name HA ) 4.3 2.6 1.7 volume=0.174 peak=603 ppm1=8.647 ppm2=5.577 assign ( resid 191 and name HN ) ( resid 190 and name HB2 ) 2.8 1.1 1.1 volume=2.120 peak=1695 ppm1=7.651 ppm2=3.880 assign ( resid 144 and name HG2# ) ( resid 177 and name HN ) 3.2 1.4 1.3 volume=1.070 peak=4641 ppm1=0.767 ppm2=8.469 assign ( resid 10 and name HN ) ( resid 9 and name HG2 or resid 9 and name HG1 ) 3.4 1.7 1.4 volume=0.725 peak=1197 ppm1=8.318 ppm2=2.396 assign ( resid 128 and name HA ) ( resid 10 and name HG2# ) 4.2 2.4 1.7 volume=0.207 peak=4588 ppm1=5.580 ppm2=1.093 assign ( resid 133 and name HN ) ( resid 133 and name HB2 or resid 133 and name HB1 ) 2.7 0.9 1.1 volume=3.090 peak=1685 ppm1=8.121 ppm2=2.574 assign ( resid 13 and name HN ) ( resid 13 and name HG2 ) 2.5 0.8 1.0 volume=4.079 peak=838 ppm1=7.728 ppm2=2.056 assign ( resid 179 and name HA ) ( resid 106 and name HG12 ) 3.7 2.0 1.5 volume=0.421 peak=2930 ppm1=3.821 ppm2=1.417 assign ( resid 82 and name HN ) ( resid 82 and name HA ) 3.2 1.4 1.3 volume=1.083 peak=745 ppm1=8.563 ppm2=5.048 assign ( resid 77 and name HN ) ( resid 76 and name HD2 ) 3.5 1.7 1.4 volume=0.618 peak=2457 ppm1=8.056 ppm2=1.551 assign ( resid 64 and name HN ) ( resid 65 and name HN ) 3.2 1.5 1.3 volume=0.960 peak=1412 ppm1=7.878 ppm2=7.724 assign ( resid 67 and name HA ) ( resid 68 and name HN ) 4.0 2.3 1.6 volume=0.254 peak=3756 ppm1=3.940 ppm2=8.066 assign ( resid 77 and name HN ) ( resid 77 and name HA ) 3.0 1.3 1.2 volume=1.491 peak=179 ppm1=8.056 ppm2=4.267 assign ( resid 142 and name HN ) ( resid 143 and name HB2 ) 4.0 2.3 1.6 volume=0.258 peak=460 ppm1=7.898 ppm2=2.702 assign ( resid 145 and name HG1 ) ( resid 112 and name HD1# ) 3.9 2.2 1.6 volume=0.311 peak=4375 ppm1=1.412 ppm2=0.441 assign ( resid 137 and name HN ) ( resid 136 and name HG1 ) 3.2 1.5 1.3 volume=0.982 peak=2042 ppm1=8.050 ppm2=2.030 assign ( resid 114 and name HD2# ) ( resid 114 and name HN ) 3.5 1.8 1.4 volume=0.612 peak=4827 ppm1=0.783 ppm2=8.800 assign ( resid 43 and name HN ) ( resid 41 and name HN ) 3.4 1.7 1.4 volume=0.682 peak=608 ppm1=7.303 ppm2=8.905 assign ( resid 196 and name HD1# ) ( resid 192 and name HB1 ) 3.1 1.3 1.2 volume=1.286 peak=4437 ppm1=0.727 ppm2=1.308 assign ( resid 174 and name HN ) ( resid 174 and name HB1 ) 3.4 1.7 1.4 volume=0.709 peak=663 ppm1=9.152 ppm2=1.925 assign ( resid 99 and name HA ) ( resid 98 and name HA ) 4.0 2.2 1.6 volume=0.279 peak=4236 ppm1=4.284 ppm2=4.639 assign ( resid 52 and name HN ) ( resid 168 and name HA ) 3.5 1.8 1.4 volume=0.594 peak=908 ppm1=8.617 ppm2=4.790 assign ( resid 87 and name HG2# ) ( resid 87 and name HD1# ) 2.7 1.0 1.1 volume=2.878 peak=4957 ppm1=0.853 ppm2=0.439 assign ( resid 8 and name HN ) ( resid 7 and name HN ) 3.1 1.3 1.2 volume=1.315 peak=2062 ppm1=7.615 ppm2=8.434 assign ( resid 73 and name HG2# ) ( resid 74 and name HN ) 3.4 1.7 1.4 volume=0.675 peak=3012 ppm1=1.218 ppm2=6.504 assign ( resid 36 and name HN ) ( resid 26 and name HA ) 4.0 2.3 1.6 volume=0.265 peak=2324 ppm1=9.882 ppm2=3.965 assign ( resid 179 and name HB1 ) ( resid 180 and name HB2 ) 4.2 2.5 1.7 volume=0.204 peak=4149 ppm1=2.753 ppm2=3.964 assign ( resid 106 and name HG2# ) ( resid 106 and name HD1# ) 2.2 0.4 0.9 volume=10.293 peak=2770 ppm1=0.897 ppm2=0.769 assign ( resid 54 and name HD1# ) ( resid 200 and name HN ) 3.8 2.1 1.5 volume=0.348 peak=3236 ppm1=0.492 ppm2=8.127 assign ( resid 54 and name HD1# ) ( resid 203 and name HG2# ) 2.8 1.1 1.1 volume=2.336 peak=3582 ppm1=0.490 ppm2=0.321 assign ( resid 188 and name HN ) ( resid 188 and name HB2 or resid 188 and name HB1 ) 3.1 1.4 1.2 volume=1.172 peak=1133 ppm1=8.442 ppm2=1.406 assign ( resid 17 and name HN ) ( resid 16 and name HA2 or resid 16 and name HA1 ) 2.9 1.2 1.2 volume=1.821 peak=1189 ppm1=7.609 ppm2=3.641 assign ( resid 205 and name HB# ) ( resid 202 and name HA1 ) 3.5 1.8 1.4 volume=0.551 peak=4167 ppm1=1.299 ppm2=3.068 assign ( resid 72 and name HD1# ) ( resid 80 and name HA ) 3.7 1.9 1.5 volume=0.440 peak=3026 ppm1=0.589 ppm2=3.961 assign ( resid 86 and name HG1 ) ( resid 86 and name HB2 ) 2.5 0.7 1.0 volume=4.753 peak=4095 ppm1=1.460 ppm2=1.554 assign ( resid 10 and name HG2# ) ( resid 11 and name HA ) 2.9 1.2 1.2 volume=1.769 peak=3381 ppm1=1.085 ppm2=3.961 assign ( resid 196 and name HN ) ( resid 196 and name HB ) 3.3 1.5 1.3 volume=0.910 peak=1132 ppm1=7.440 ppm2=2.181 assign ( resid 134 and name HZ ) ( resid 93 and name HD1# ) 2.9 1.2 1.2 volume=1.663 peak=3 ppm1=6.644 ppm2=-0.277 assign ( resid 36 and name HN ) ( resid 36 and name HB2 ) 3.6 1.9 1.5 volume=0.469 peak=488 ppm1=9.880 ppm2=3.489 assign ( resid 14 and name HN ) ( resid 14 and name HA ) 3.3 1.6 1.3 volume=0.824 peak=446 ppm1=7.790 ppm2=2.819 assign ( resid 69 and name HN ) ( resid 67 and name HB1 ) 3.6 1.9 1.5 volume=0.470 peak=2233 ppm1=8.218 ppm2=2.130 assign ( resid 117 and name HD1# ) ( resid 92 and name HE1 or resid 92 and name HE2 ) 3.6 1.9 1.5 volume=0.470 peak=4291 ppm1=0.243 ppm2=6.750 assign ( resid 158 and name HN ) ( resid 161 and name HA ) 2.7 0.9 1.1 volume=3.068 peak=1855 ppm1=8.217 ppm2=4.662 assign ( resid 10 and name HG2# ) ( resid 128 and name HN ) 4.0 2.2 1.6 volume=0.281 peak=3476 ppm1=1.085 ppm2=9.929 assign ( resid 146 and name HN ) ( resid 109 and name HA ) 4.1 2.3 1.6 volume=0.239 peak=2334 ppm1=8.400 ppm2=3.895 assign ( resid 72 and name HG2# ) ( resid 81 and name HN ) 3.7 1.9 1.5 volume=0.441 peak=4415 ppm1=0.602 ppm2=8.491 assign ( resid 41 and name HN ) ( resid 41 and name HA ) 3.3 1.6 1.3 volume=0.818 peak=1928 ppm1=8.907 ppm2=4.341 assign ( resid 87 and name HD1# ) ( resid 93 and name HN ) 3.9 2.1 1.5 volume=0.321 peak=4250 ppm1=0.439 ppm2=8.912 assign ( resid 125 and name HN ) ( resid 124 and name HA ) 2.9 1.2 1.2 volume=1.833 peak=933 ppm1=8.771 ppm2=5.180 assign ( resid 64 and name HZ ) ( resid 64 and name HD1 or resid 64 and name HD2 ) 3.9 2.2 1.6 volume=0.317 peak=22 ppm1=7.052 ppm2=5.970 assign ( resid 200 and name HN ) ( resid 197 and name HN ) 3.6 1.8 1.4 volume=0.532 peak=1763 ppm1=8.084 ppm2=8.000 assign ( resid 120 and name HN ) ( resid 125 and name HA ) 3.6 1.9 1.4 volume=0.492 peak=1804 ppm1=8.910 ppm2=5.583 assign ( resid 196 and name HG11 ) ( resid 197 and name HN ) 4.0 2.2 1.6 volume=0.276 peak=4828 ppm1=1.807 ppm2=8.003 assign ( resid 54 and name HG11 ) ( resid 54 and name HB ) 3.0 1.3 1.2 volume=1.464 peak=3245 ppm1=1.188 ppm2=1.774 assign ( resid 27 and name HN ) ( resid 26 and name HG1# ) 3.4 1.7 1.4 volume=0.640 peak=1134 ppm1=9.277 ppm2=0.766 assign ( resid 168 and name HB ) ( resid 167 and name HD1# ) 4.4 2.7 1.6 volume=0.152 peak=4799 ppm1=1.724 ppm2=0.744 assign ( resid 124 and name HN ) ( resid 123 and name HB1 or resid 123 and name HB2 ) 3.4 1.7 1.4 volume=0.669 peak=1591 ppm1=6.471 ppm2=2.782 assign ( resid 174 and name HG2 ) ( resid 174 and name HB1 ) 2.6 0.9 1.0 volume=3.715 peak=3410 ppm1=2.181 ppm2=1.924 assign ( resid 93 and name HN ) ( resid 84 and name HG2# ) 3.8 2.0 1.5 volume=0.377 peak=1087 ppm1=8.905 ppm2=0.109 assign ( resid 66 and name HN ) ( resid 65 and name HA ) 3.2 1.5 1.3 volume=0.965 peak=215 ppm1=8.050 ppm2=3.880 assign ( resid 149 and name HN ) ( resid 174 and name HN ) 3.7 2.0 1.5 volume=0.410 peak=1256 ppm1=7.756 ppm2=9.210 assign ( resid 65 and name HN ) ( resid 66 and name HA ) 3.1 1.4 1.2 volume=1.271 peak=2249 ppm1=7.746 ppm2=4.267 assign ( resid 126 and name HA ) ( resid 126 and name HG11 ) 4.0 2.2 1.6 volume=0.275 peak=3745 ppm1=5.430 ppm2=1.079 assign ( resid 54 and name HG2# ) ( resid 203 and name HG2# ) 3.0 1.3 1.2 volume=1.518 peak=2510 ppm1=0.577 ppm2=0.317 assign ( resid 197 and name HD1# ) ( resid 193 and name HA ) 3.7 1.9 1.5 volume=0.443 peak=2504 ppm1=0.757 ppm2=3.440 assign ( resid 60 and name HN ) ( resid 57 and name HA ) 3.5 1.8 1.4 volume=0.549 peak=186 ppm1=7.265 ppm2=4.180 assign ( resid 179 and name HA ) ( resid 179 and name HD2# ) 3.9 2.2 1.6 volume=0.292 peak=5116 ppm1=3.821 ppm2=0.747 assign ( resid 33 and name HD1# ) ( resid 196 and name HB ) 4.0 2.3 1.6 volume=0.254 peak=3088 ppm1=0.360 ppm2=2.210 assign ( resid 170 and name HN ) ( resid 47 and name HD2# ) 4.3 2.6 1.7 volume=0.165 peak=183 ppm1=9.146 ppm2=0.103 assign ( resid 168 and name HA ) ( resid 168 and name HB ) 4.2 2.5 1.7 volume=0.187 peak=5083 ppm1=4.808 ppm2=1.727 assign ( resid 117 and name HN ) ( resid 116 and name HA ) 3.3 1.6 1.3 volume=0.764 peak=625 ppm1=8.233 ppm2=6.144 assign ( resid 50 and name HN ) ( resid 168 and name HA ) 3.3 1.5 1.3 volume=0.904 peak=1149 ppm1=9.300 ppm2=4.796 assign ( resid 8 and name HB2 or resid 8 and name HB1 ) ( resid 6 and name HN ) 3.2 1.5 1.3 volume=0.983 peak=4115 ppm1=2.048 ppm2=7.726 assign ( resid 61 and name HN ) ( resid 56 and name HG2 ) 3.4 1.7 1.3 volume=0.728 peak=669 ppm1=8.716 ppm2=1.992 assign ( resid 34 and name HN ) ( resid 51 and name HA ) 4.1 2.4 1.6 volume=0.222 peak=1769 ppm1=8.137 ppm2=5.643 assign ( resid 43 and name HN ) ( resid 42 and name HA ) 3.0 1.3 1.2 volume=1.468 peak=1586 ppm1=7.302 ppm2=4.133 assign ( resid 63 and name HN ) ( resid 62 and name HA ) 3.0 1.3 1.2 volume=1.441 peak=604 ppm1=7.296 ppm2=3.969 assign ( resid 186 and name HD2 ) ( resid 186 and name HB1 ) 3.4 1.7 1.4 volume=0.679 peak=3207 ppm1=1.674 ppm2=1.874 assign ( resid 136 and name HG2 ) ( resid 134 and name HE1 or resid 134 and name HE2 ) 3.2 1.4 1.3 volume=1.068 peak=4690 ppm1=1.949 ppm2=7.141 assign ( resid 35 and name HN ) ( resid 36 and name HN ) 4.1 2.4 1.7 volume=0.211 peak=558 ppm1=9.428 ppm2=9.879 assign ( resid 136 and name HA ) ( resid 136 and name HN ) 3.5 1.8 1.4 volume=0.575 peak=4673 ppm1=3.788 ppm2=6.892 assign ( resid 60 and name HG2 or resid 60 and name HG1 ) ( resid 60 and name HN ) 4.0 2.3 1.6 volume=0.263 peak=4743 ppm1=1.323 ppm2=7.268 assign ( resid 106 and name HA ) ( resid 183 and name HG2# ) 3.6 1.9 1.4 volume=0.489 peak=2883 ppm1=4.143 ppm2=0.997 assign ( resid 119 and name HN ) ( resid 118 and name HG2 ) 3.3 1.6 1.3 volume=0.866 peak=2189 ppm1=8.055 ppm2=0.629 assign ( resid 7 and name HA ) ( resid 7 and name HB# ) 3.2 1.4 1.3 volume=1.088 peak=2711 ppm1=3.709 ppm2=0.750 assign ( resid 80 and name HG2# ) ( resid 79 and name HG1 ) 2.6 0.9 1.1 volume=3.248 peak=4509 ppm1=0.708 ppm2=1.884 assign ( resid 61 and name HD2# ) ( resid 199 and name HA ) 2.9 1.2 1.2 volume=1.764 peak=3998 ppm1=0.748 ppm2=2.796 assign ( resid 197 and name HD1# ) ( resid 197 and name HB1 ) 3.0 1.3 1.2 volume=1.418 peak=4330 ppm1=0.758 ppm2=1.754 assign ( resid 53 and name HN ) ( resid 54 and name HN ) 3.8 2.1 1.5 volume=0.336 peak=807 ppm1=8.310 ppm2=9.076 assign ( resid 6 and name HN ) ( resid 6 and name HG11 ) 3.2 1.5 1.3 volume=0.977 peak=204 ppm1=7.724 ppm2=1.004 assign ( resid 126 and name HB ) ( resid 126 and name HD1# ) 3.6 1.9 1.5 volume=0.464 peak=4757 ppm1=1.593 ppm2=0.350 assign ( resid 136 and name HB1 ) ( resid 136 and name HA ) 3.3 1.6 1.3 volume=0.866 peak=4727 ppm1=1.747 ppm2=3.764 assign ( resid 180 and name HN ) ( resid 179 and name HN ) 3.0 1.3 1.2 volume=1.342 peak=295 ppm1=8.353 ppm2=7.262 assign ( resid 176 and name HA ) ( resid 175 and name HN ) 4.0 2.3 1.6 volume=0.259 peak=4796 ppm1=3.997 ppm2=8.781 assign ( resid 26 and name HG2# ) ( resid 28 and name HN ) 3.4 1.7 1.4 volume=0.650 peak=3468 ppm1=0.913 ppm2=7.832 assign ( resid 134 and name HB1 ) ( resid 132 and name HG2# ) 3.0 1.3 1.2 volume=1.421 peak=2581 ppm1=3.046 ppm2=0.972 assign ( resid 121 and name HN ) ( resid 121 and name HG1 ) 3.0 1.3 1.2 volume=1.543 peak=396 ppm1=8.586 ppm2=2.309 assign ( resid 112 and name HD1# ) ( resid 134 and name HN ) 4.0 2.3 1.6 volume=0.253 peak=4573 ppm1=0.371 ppm2=8.764 assign ( resid 204 and name HN ) ( resid 205 and name HB# ) 2.7 1.0 1.1 volume=2.524 peak=1878 ppm1=6.743 ppm2=1.271 assign ( resid 154 and name HN ) ( resid 169 and name HN ) 3.8 2.1 1.5 volume=0.336 peak=286 ppm1=10.007 ppm2=9.244 assign ( resid 175 and name HB2 ) ( resid 184 and name HD1# ) 3.8 2.0 1.5 volume=0.375 peak=4598 ppm1=2.450 ppm2=0.846 assign ( resid 66 and name HN ) ( resid 67 and name HN ) 3.1 1.4 1.2 volume=1.243 peak=172 ppm1=8.053 ppm2=7.652 assign ( resid 54 and name HG12 ) ( resid 61 and name HD2# ) 2.7 1.0 1.1 volume=2.746 peak=3125 ppm1=1.236 ppm2=0.738 assign ( resid 47 and name HN ) ( resid 37 and name HA ) 4.2 2.5 1.7 volume=0.192 peak=1139 ppm1=8.707 ppm2=5.824 assign ( resid 92 and name HN ) ( resid 91 and name HB ) 4.0 2.3 1.6 volume=0.263 peak=1490 ppm1=9.456 ppm2=3.613 assign ( resid 160 and name HN ) ( resid 158 and name HB1 ) 2.8 1.1 1.1 volume=2.364 peak=796 ppm1=8.832 ppm2=2.220 assign ( resid 122 and name HN ) ( resid 123 and name HN ) 3.6 1.8 1.4 volume=0.529 peak=713 ppm1=8.645 ppm2=8.401 assign ( resid 186 and name HE2 ) ( resid 183 and name HN ) 4.1 2.4 1.6 volume=0.218 peak=2788 ppm1=2.957 ppm2=7.461 assign ( resid 37 and name HN ) ( resid 24 and name HA ) 3.4 1.7 1.4 volume=0.719 peak=1502 ppm1=9.658 ppm2=4.273 assign ( resid 132 and name HG1# ) ( resid 84 and name HG2# ) 3.9 2.2 1.6 volume=0.295 peak=4869 ppm1=0.543 ppm2=0.121 assign ( resid 67 and name HA ) ( resid 71 and name HG1 ) 3.6 1.9 1.4 volume=0.485 peak=3862 ppm1=3.928 ppm2=0.317 assign ( resid 170 and name HA ) ( resid 49 and name HN ) 4.8 3.1 1.2 volume=0.087 peak=3663 ppm1=5.822 ppm2=8.926 assign ( resid 197 and name HD2# ) ( resid 197 and name HB1 ) 3.9 2.2 1.6 volume=0.285 peak=3222 ppm1=0.756 ppm2=1.783 assign ( resid 64 and name HD1 or resid 64 and name HD2 ) ( resid 199 and name HA ) 4.2 2.4 1.7 volume=0.210 peak=18 ppm1=5.970 ppm2=2.785 assign ( resid 9 and name HN ) ( resid 8 and name HG1 or resid 8 and name HG2 ) 2.9 1.2 1.2 volume=1.858 peak=1382 ppm1=7.985 ppm2=2.314 assign ( resid 56 and name HN ) ( resid 55 and name HD2 ) 3.3 1.6 1.3 volume=0.772 peak=1263 ppm1=8.635 ppm2=3.365 assign ( resid 123 and name HN ) ( resid 122 and name HA2 ) 3.0 1.3 1.2 volume=1.393 peak=2267 ppm1=8.405 ppm2=3.615 assign ( resid 184 and name HG11 ) ( resid 185 and name HN ) 3.7 2.0 1.5 volume=0.389 peak=2604 ppm1=1.677 ppm2=8.191 assign ( resid 112 and name HG11 ) ( resid 112 and name HD1# ) 4.2 2.5 1.7 volume=0.190 peak=3325 ppm1=1.602 ppm2=0.375 assign ( resid 53 and name HD1# ) ( resid 158 and name HB2 or resid 158 and name HB1 ) 3.5 1.8 1.4 volume=0.592 peak=4264 ppm1=0.796 ppm2=2.205 assign ( resid 103 and name HB ) ( resid 102 and name HN ) 4.4 2.7 1.6 volume=0.147 peak=4043 ppm1=2.588 ppm2=8.575 assign ( resid 158 and name HG1 ) ( resid 158 and name HN ) 3.8 2.1 1.5 volume=0.373 peak=3308 ppm1=2.437 ppm2=8.216 assign ( resid 57 and name HA ) ( resid 165 and name HN ) 3.9 2.2 1.6 volume=0.294 peak=2802 ppm1=4.133 ppm2=8.513 assign ( resid 78 and name HN ) ( resid 78 and name HD2# ) 2.9 1.2 1.2 volume=1.832 peak=1641 ppm1=7.148 ppm2=0.494 assign ( resid 42 and name HD2 ) ( resid 42 and name HE1 ) 2.6 0.8 1.0 volume=3.896 peak=3386 ppm1=1.529 ppm2=2.970 assign ( resid 62 and name HN ) ( resid 58 and name HB1 ) 4.0 2.3 1.6 volume=0.262 peak=852 ppm1=8.131 ppm2=2.118 assign ( resid 153 and name HN ) ( resid 14 and name HB ) 3.8 2.0 1.5 volume=0.376 peak=2357 ppm1=9.329 ppm2=1.664 assign ( resid 40 and name HA ) ( resid 47 and name HB1 or resid 47 and name HB2 ) 3.6 1.9 1.4 volume=0.503 peak=3602 ppm1=3.988 ppm2=0.722 assign ( resid 3 and name HN ) ( resid 4 and name HA ) 3.4 1.7 1.4 volume=0.643 peak=1405 ppm1=7.918 ppm2=3.776 assign ( resid 145 and name HN ) ( resid 139 and name HB1 ) 3.4 1.7 1.4 volume=0.672 peak=318 ppm1=8.380 ppm2=2.187 assign ( resid 193 and name HN ) ( resid 194 and name HB2 ) 3.4 1.7 1.4 volume=0.702 peak=2434 ppm1=7.621 ppm2=2.838 assign ( resid 187 and name HN ) ( resid 186 and name HB2 ) 3.2 1.5 1.3 volume=0.966 peak=2402 ppm1=7.600 ppm2=1.926 assign ( resid 167 and name HA ) ( resid 168 and name HB ) 4.2 2.5 1.7 volume=0.193 peak=3798 ppm1=5.217 ppm2=1.732 assign ( resid 201 and name HA ) ( resid 200 and name HN ) 4.1 2.4 1.7 volume=0.218 peak=3894 ppm1=4.332 ppm2=8.001 assign ( resid 74 and name HH2 ) ( resid 199 and name HA ) 3.7 2.0 1.5 volume=0.438 peak=62 ppm1=6.508 ppm2=2.787 assign ( resid 115 and name HG2# ) ( resid 92 and name HN ) 3.6 1.8 1.4 volume=0.529 peak=4566 ppm1=0.658 ppm2=9.465 assign ( resid 39 and name HN ) ( resid 38 and name HN ) 3.2 1.5 1.3 volume=0.960 peak=187 ppm1=8.247 ppm2=8.478 assign ( resid 113 and name HB2 ) ( resid 115 and name HG1# ) 4.3 2.6 1.7 volume=0.173 peak=4432 ppm1=2.045 ppm2=0.294 assign ( resid 54 and name HG12 ) ( resid 200 and name HN ) 4.0 2.2 1.6 volume=0.280 peak=4044 ppm1=1.236 ppm2=8.073 assign ( resid 168 and name HG2# ) ( resid 154 and name HN ) 4.2 2.5 1.7 volume=0.203 peak=3254 ppm1=0.200 ppm2=10.083 assign ( resid 113 and name HN ) ( resid 114 and name HN ) 3.9 2.2 1.6 volume=0.313 peak=380 ppm1=8.232 ppm2=8.838 assign ( resid 126 and name HN ) ( resid 124 and name HB1 ) 3.5 1.7 1.4 volume=0.616 peak=1408 ppm1=9.105 ppm2=2.030 assign ( resid 204 and name HN ) ( resid 201 and name HB1 ) 4.1 2.3 1.6 volume=0.237 peak=2032 ppm1=6.747 ppm2=2.559 assign ( resid 105 and name HN ) ( resid 104 and name HN ) 3.2 1.5 1.3 volume=0.959 peak=907 ppm1=7.944 ppm2=8.051 assign ( resid 8 and name HN ) ( resid 11 and name HN ) 3.1 1.4 1.2 volume=1.172 peak=2367 ppm1=7.614 ppm2=8.183 assign ( resid 190 and name HB1 ) ( resid 191 and name HN ) 3.5 1.8 1.4 volume=0.554 peak=2745 ppm1=3.880 ppm2=7.668 assign ( resid 130 and name HB2 ) ( resid 130 and name HG1 ) 3.3 1.6 1.3 volume=0.774 peak=3795 ppm1=1.833 ppm2=1.360 assign ( resid 130 and name HN ) ( resid 115 and name HA ) 3.7 2.0 1.5 volume=0.425 peak=563 ppm1=7.617 ppm2=4.407 assign ( resid 67 and name HA ) ( resid 67 and name HB2 ) 3.6 1.8 1.4 volume=0.522 peak=3464 ppm1=3.933 ppm2=2.021 assign ( resid 93 and name HN ) ( resid 86 and name HG1 ) 3.8 2.1 1.5 volume=0.336 peak=2358 ppm1=8.904 ppm2=1.543 assign ( resid 26 and name HG2# ) ( resid 26 and name HG1# ) 2.0 0.3 0.8 volume=18.237 peak=3579 ppm1=0.912 ppm2=0.780 assign ( resid 8 and name HG1 or resid 8 and name HG2 ) ( resid 9 and name HN ) 3.7 1.9 1.5 volume=0.443 peak=3752 ppm1=2.321 ppm2=7.999 assign ( resid 158 and name HB2 ) ( resid 161 and name HN ) 4.4 2.7 1.6 volume=0.153 peak=2698 ppm1=2.218 ppm2=6.893 assign ( resid 197 and name HD1# ) ( resid 197 and name HG ) 2.7 0.9 1.1 volume=2.973 peak=4145 ppm1=0.756 ppm2=1.282 assign ( resid 128 and name HN ) ( resid 129 and name HA ) 3.8 2.1 1.5 volume=0.355 peak=883 ppm1=9.932 ppm2=5.696 assign ( resid 48 and name HN ) ( resid 170 and name HB1 ) 3.4 1.7 1.4 volume=0.666 peak=783 ppm1=9.291 ppm2=1.796 assign ( resid 113 and name HN ) ( resid 112 and name HD1# ) 2.9 1.2 1.2 volume=1.691 peak=192 ppm1=8.233 ppm2=0.365 assign ( resid 120 and name HN ) ( resid 119 and name HN ) 3.8 2.1 1.5 volume=0.335 peak=1496 ppm1=8.912 ppm2=8.054 assign ( resid 15 and name HB1 ) ( resid 15 and name HD2# ) 3.4 1.7 1.4 volume=0.662 peak=3516 ppm1=1.713 ppm2=0.683 assign ( resid 122 and name HN ) ( resid 122 and name HA2 ) 3.1 1.3 1.2 volume=1.316 peak=2375 ppm1=8.646 ppm2=3.619 assign ( resid 54 and name HD1# ) ( resid 54 and name HG11 ) 2.6 0.9 1.0 volume=3.398 peak=3237 ppm1=0.491 ppm2=1.159 assign ( resid 179 and name HB1 ) ( resid 179 and name HN ) 3.8 2.1 1.5 volume=0.363 peak=4785 ppm1=2.752 ppm2=7.316 assign ( resid 134 and name HD1 or resid 134 and name HD2 ) ( resid 84 and name HG1# ) 3.4 1.7 1.4 volume=0.682 peak=147 ppm1=6.862 ppm2=0.543 assign ( resid 126 and name HA ) ( resid 126 and name HN ) 4.6 2.9 1.4 volume=0.115 peak=2791 ppm1=5.436 ppm2=9.092 assign ( resid 8 and name HG1 or resid 8 and name HG2 ) ( resid 5 and name HA ) 3.7 1.9 1.5 volume=0.451 peak=3266 ppm1=2.322 ppm2=4.026 assign ( resid 179 and name HG ) ( resid 179 and name HB1 ) 2.7 1.0 1.1 volume=2.797 peak=2460 ppm1=1.516 ppm2=2.752 assign ( resid 183 and name HN ) ( resid 185 and name HG2 ) 3.7 2.0 1.5 volume=0.418 peak=836 ppm1=7.420 ppm2=2.318 assign ( resid 14 and name HB ) ( resid 14 and name HN ) 3.7 2.0 1.5 volume=0.438 peak=2458 ppm1=1.712 ppm2=7.794 assign ( resid 84 and name HN ) ( resid 83 and name HA ) 3.2 1.4 1.3 volume=1.085 peak=348 ppm1=8.504 ppm2=4.663 assign ( resid 42 and name HG1 or resid 42 and name HG2 ) ( resid 42 and name HN ) 3.4 1.7 1.4 volume=0.711 peak=4737 ppm1=1.290 ppm2=8.697 assign ( resid 87 and name HA ) ( resid 87 and name HG2# ) 2.7 1.0 1.1 volume=2.828 peak=3943 ppm1=3.871 ppm2=0.850 assign ( resid 168 and name HN ) ( resid 154 and name HN ) 3.7 2.0 1.5 volume=0.418 peak=1420 ppm1=8.695 ppm2=10.006 assign ( resid 6 and name HA ) ( resid 6 and name HG11 ) 3.0 1.3 1.2 volume=1.533 peak=3356 ppm1=3.617 ppm2=1.039 assign ( resid 36 and name HN ) ( resid 49 and name HG2 ) 3.9 2.2 1.6 volume=0.297 peak=271 ppm1=9.881 ppm2=1.589 assign ( resid 84 and name HG2# ) ( resid 134 and name HD1 or resid 134 and name HD2 ) 3.8 2.1 1.5 volume=0.349 peak=3665 ppm1=0.112 ppm2=6.888 assign ( resid 101 and name HN ) ( resid 101 and name HA ) 2.9 1.2 1.2 volume=1.898 peak=1307 ppm1=8.477 ppm2=4.663 assign ( resid 114 and name HB1 ) ( resid 93 and name HB ) 3.9 2.1 1.5 volume=0.324 peak=4317 ppm1=1.063 ppm2=1.168 assign ( resid 60 and name HD1 ) ( resid 60 and name HA ) 3.0 1.3 1.2 volume=1.355 peak=4539 ppm1=1.542 ppm2=3.868 assign ( resid 11 and name HB# ) ( resid 126 and name HG11 or resid 126 and name HG12 ) 3.5 1.8 1.4 volume=0.558 peak=4316 ppm1=1.629 ppm2=1.099 assign ( resid 76 and name HE1 ) ( resid 76 and name HG1 ) 2.2 0.5 0.9 volume=9.224 peak=5156 ppm1=2.862 ppm2=1.386 assign ( resid 114 and name HN ) ( resid 130 and name HB1 ) 3.3 1.5 1.3 volume=0.906 peak=2410 ppm1=8.800 ppm2=1.931 assign ( resid 140 and name HN ) ( resid 139 and name HA ) 3.0 1.3 1.2 volume=1.431 peak=2338 ppm1=9.581 ppm2=4.270 assign ( resid 24 and name HN ) ( resid 24 and name HB2 or resid 24 and name HB1 ) 2.5 0.8 1.0 volume=4.314 peak=1905 ppm1=7.833 ppm2=2.963 assign ( resid 115 and name HG1# ) ( resid 93 and name HG2# ) 3.6 1.8 1.4 volume=0.526 peak=2541 ppm1=0.301 ppm2=-0.019 assign ( resid 139 and name HB1 ) ( resid 139 and name HA ) 3.5 1.8 1.4 volume=0.574 peak=5106 ppm1=2.195 ppm2=4.286 assign ( resid 34 and name HN ) ( resid 35 and name HG2# or resid 35 and name HG1# ) 2.6 0.9 1.1 volume=3.123 peak=1789 ppm1=8.137 ppm2=0.887 assign ( resid 15 and name HD2# ) ( resid 15 and name HA ) 3.7 1.9 1.5 volume=0.440 peak=3627 ppm1=0.683 ppm2=3.655 assign ( resid 41 and name HN ) ( resid 41 and name HG2 or resid 41 and name HG1 ) 2.9 1.2 1.1 volume=1.902 peak=940 ppm1=8.907 ppm2=1.534 assign ( resid 113 and name HN ) ( resid 113 and name HA ) 3.7 2.0 1.5 volume=0.402 peak=583 ppm1=8.233 ppm2=5.309 assign ( resid 186 and name HE1 ) ( resid 183 and name HA ) 3.6 1.8 1.4 volume=0.534 peak=4232 ppm1=2.957 ppm2=3.883 assign ( resid 71 and name HN ) ( resid 74 and name HE1 ) 4.1 2.4 1.6 volume=0.229 peak=1442 ppm1=7.220 ppm2=9.604 assign ( resid 18 and name HB1 ) ( resid 18 and name HB2 ) 3.8 2.1 1.5 volume=0.358 peak=2742 ppm1=2.972 ppm2=2.449 assign ( resid 143 and name HB1 ) ( resid 110 and name HN ) 3.9 2.2 1.6 volume=0.290 peak=5025 ppm1=2.707 ppm2=8.763 assign ( resid 72 and name HD1# ) ( resid 72 and name HA ) 3.4 1.7 1.4 volume=0.723 peak=4370 ppm1=0.588 ppm2=3.636 assign ( resid 186 and name HN ) ( resid 188 and name HN ) 3.9 2.2 1.6 volume=0.313 peak=818 ppm1=7.370 ppm2=8.448 assign ( resid 34 and name HG2# ) ( resid 26 and name HA ) 3.0 1.3 1.2 volume=1.507 peak=4007 ppm1=1.100 ppm2=3.961 assign ( resid 204 and name HA ) ( resid 204 and name HG2 ) 3.1 1.4 1.3 volume=1.130 peak=3716 ppm1=3.799 ppm2=1.320 assign ( resid 137 and name HN ) ( resid 134 and name HZ ) 2.8 1.0 1.1 volume=2.439 peak=381 ppm1=8.051 ppm2=6.611 assign ( resid 112 and name HG2# ) ( resid 145 and name HG1 or resid 145 and name HG2 ) 2.7 1.0 1.1 volume=2.843 peak=4079 ppm1=0.680 ppm2=1.430 assign ( resid 84 and name HG1# ) ( resid 84 and name HB ) 2.9 1.2 1.2 volume=1.822 peak=3119 ppm1=0.533 ppm2=2.004 assign ( resid 179 and name HB2 ) ( resid 179 and name HD1# ) 3.4 1.7 1.4 volume=0.685 peak=3059 ppm1=2.493 ppm2=0.525 assign ( resid 54 and name HD1# ) ( resid 200 and name HD1 or resid 200 and name HD2 ) 2.7 1.0 1.1 volume=2.705 peak=4995 ppm1=0.490 ppm2=1.554 assign ( resid 134 and name HA ) ( resid 132 and name HG2# ) 4.4 2.7 1.6 volume=0.152 peak=4798 ppm1=5.189 ppm2=0.902 assign ( resid 82 and name HB2 ) ( resid 83 and name HN ) 5.1 3.4 0.9 volume=0.062 peak=2960 ppm1=2.456 ppm2=8.565 assign ( resid 37 and name HB1 or resid 37 and name HB2 ) ( resid 38 and name HN ) 4.4 2.7 1.6 volume=0.147 peak=2904 ppm1=3.288 ppm2=8.522 assign ( resid 66 and name HN ) ( resid 65 and name HD2# ) 3.5 1.7 1.4 volume=0.634 peak=1445 ppm1=8.049 ppm2=0.322 assign ( resid 165 and name HN ) ( resid 164 and name HA ) 3.1 1.4 1.2 volume=1.210 peak=222 ppm1=8.465 ppm2=4.923 assign ( resid 128 and name HN ) ( resid 127 and name HA ) 3.0 1.3 1.2 volume=1.522 peak=341 ppm1=9.933 ppm2=5.046 assign ( resid 196 and name HA ) ( resid 196 and name HG11 ) 4.1 2.4 1.7 volume=0.213 peak=3209 ppm1=3.453 ppm2=1.803 assign ( resid 73 and name HA ) ( resid 73 and name HB ) 3.9 2.2 1.6 volume=0.285 peak=4961 ppm1=3.921 ppm2=4.298 assign ( resid 5 and name HA ) ( resid 6 and name HN ) 3.8 2.1 1.5 volume=0.350 peak=4172 ppm1=4.023 ppm2=7.738 assign ( resid 72 and name HN ) ( resid 73 and name HA ) 4.2 2.5 1.7 volume=0.203 peak=153 ppm1=7.543 ppm2=4.009 assign ( resid 36 and name HB2 ) ( resid 25 and name HN ) 4.4 2.7 1.6 volume=0.152 peak=4059 ppm1=3.521 ppm2=9.030 assign ( resid 180 and name HN ) ( resid 183 and name HG12 ) 3.0 1.3 1.2 volume=1.435 peak=887 ppm1=8.353 ppm2=1.529 assign ( resid 144 and name HA ) ( resid 144 and name HN ) 4.0 2.3 1.6 volume=0.249 peak=2576 ppm1=3.987 ppm2=7.540 assign ( resid 103 and name HN ) ( resid 103 and name HG2# ) 2.9 1.1 1.1 volume=1.931 peak=1299 ppm1=8.451 ppm2=0.884 assign ( resid 47 and name HN ) ( resid 38 and name HN ) 3.5 1.7 1.4 volume=0.617 peak=1500 ppm1=8.698 ppm2=8.466 assign ( resid 155 and name HA ) ( resid 154 and name HG2# ) 4.5 2.7 1.5 volume=0.136 peak=4324 ppm1=5.267 ppm2=0.896 assign ( resid 171 and name HN ) ( resid 48 and name HB2 ) 3.6 1.8 1.4 volume=0.532 peak=1351 ppm1=9.063 ppm2=2.704 assign ( resid 166 and name HN ) ( resid 158 and name HN ) 3.9 2.1 1.5 volume=0.326 peak=1112 ppm1=9.000 ppm2=8.177 assign ( resid 157 and name HG2 ) ( resid 157 and name HB2 ) 3.4 1.7 1.4 volume=0.677 peak=2644 ppm1=1.790 ppm2=2.305 assign ( resid 65 and name HD1# ) ( resid 65 and name HN ) 3.9 2.2 1.5 volume=0.318 peak=3705 ppm1=0.175 ppm2=7.732 assign ( resid 83 and name HG1 ) ( resid 83 and name HA ) 3.4 1.6 1.3 volume=0.759 peak=3607 ppm1=1.723 ppm2=4.680 assign ( resid 153 and name HN ) ( resid 129 and name HN ) 4.2 2.4 1.7 volume=0.209 peak=1071 ppm1=9.329 ppm2=8.698 assign ( resid 191 and name HN ) ( resid 193 and name HG1# ) 3.2 1.4 1.3 volume=1.062 peak=1269 ppm1=7.652 ppm2=0.741 assign ( resid 38 and name HN ) ( resid 38 and name HG2 ) 3.3 1.6 1.3 volume=0.766 peak=764 ppm1=8.465 ppm2=0.496 assign ( resid 203 and name HD1# ) ( resid 203 and name HG2# ) 2.6 0.9 1.1 volume=3.124 peak=4907 ppm1=-0.009 ppm2=0.331 assign ( resid 97 and name HN ) ( resid 96 and name HA ) 3.0 1.3 1.2 volume=1.528 peak=437 ppm1=8.362 ppm2=4.791 assign ( resid 25 and name HN ) ( resid 25 and name HB2 ) 2.7 0.9 1.1 volume=3.087 peak=2242 ppm1=9.010 ppm2=1.788 assign ( resid 42 and name HN ) ( resid 41 and name HA ) 3.5 1.8 1.4 volume=0.599 peak=2222 ppm1=8.698 ppm2=4.330 assign ( resid 126 and name HD1# ) ( resid 11 and name HN ) 4.3 2.5 1.7 volume=0.180 peak=2602 ppm1=0.350 ppm2=8.137 assign ( resid 132 and name HG1# ) ( resid 134 and name HE1 or resid 134 and name HE2 ) 3.6 1.8 1.4 volume=0.527 peak=4842 ppm1=0.540 ppm2=7.138 assign ( resid 205 and name HN ) ( resid 205 and name HB# ) 2.3 0.6 0.9 volume=7.845 peak=1178 ppm1=7.174 ppm2=1.275 assign ( resid 24 and name HN ) ( resid 25 and name HN ) 3.2 1.5 1.3 volume=0.934 peak=474 ppm1=7.830 ppm2=8.974 assign ( resid 168 and name HG2# ) ( resid 168 and name HG1# ) 2.7 1.0 1.1 volume=2.825 peak=3440 ppm1=0.198 ppm2=0.771 assign ( resid 28 and name HN ) ( resid 35 and name HN ) 3.1 1.4 1.2 volume=1.279 peak=1324 ppm1=7.808 ppm2=9.359 assign ( resid 164 and name HN ) ( resid 161 and name HA ) 2.9 1.2 1.2 volume=1.651 peak=1571 ppm1=7.976 ppm2=4.656 assign ( resid 93 and name HG11 ) ( resid 93 and name HG12 ) 2.8 1.1 1.1 volume=2.080 peak=2815 ppm1=0.690 ppm2=0.593 assign ( resid 54 and name HN ) ( resid 165 and name HA ) 4.0 2.3 1.6 volume=0.250 peak=1365 ppm1=9.022 ppm2=5.150 assign ( resid 48 and name HN ) ( resid 47 and name HD1# ) 4.0 2.3 1.6 volume=0.255 peak=2003 ppm1=9.298 ppm2=0.102 assign ( resid 126 and name HN ) ( resid 126 and name HG2# ) 3.1 1.4 1.3 volume=1.147 peak=1138 ppm1=9.105 ppm2=0.750 assign ( resid 184 and name HG12 ) ( resid 184 and name HD1# ) 2.8 1.1 1.1 volume=2.046 peak=3375 ppm1=1.093 ppm2=0.898 assign ( resid 96 and name HN ) ( resid 96 and name HA ) 3.8 2.0 1.5 volume=0.386 peak=1076 ppm1=8.473 ppm2=4.831 assign ( resid 154 and name HG1# ) ( resid 154 and name HN ) 3.6 1.9 1.4 volume=0.501 peak=3617 ppm1=0.909 ppm2=10.005 assign ( resid 8 and name HB2 or resid 8 and name HB1 ) ( resid 7 and name HN ) 3.6 1.9 1.5 volume=0.467 peak=3786 ppm1=2.048 ppm2=8.432 assign ( resid 111 and name HN ) ( resid 96 and name HG2# ) 3.7 2.0 1.5 volume=0.413 peak=717 ppm1=8.631 ppm2=1.126 assign ( resid 86 and name HG2 ) ( resid 86 and name HA ) 3.8 2.1 1.5 volume=0.341 peak=4130 ppm1=1.459 ppm2=4.287 assign ( resid 176 and name HA ) ( resid 175 and name HB2 ) 3.7 2.0 1.5 volume=0.391 peak=4299 ppm1=3.997 ppm2=2.415 assign ( resid 28 and name HN ) ( resid 29 and name HN ) 3.6 1.8 1.4 volume=0.529 peak=825 ppm1=7.809 ppm2=8.570 assign ( resid 169 and name HN ) ( resid 169 and name HB1 ) 3.5 1.8 1.4 volume=0.597 peak=492 ppm1=9.255 ppm2=1.794 assign ( resid 112 and name HD1# ) ( resid 112 and name HA ) 4.4 2.7 1.6 volume=0.144 peak=2565 ppm1=0.373 ppm2=4.959 assign ( resid 115 and name HG1# ) ( resid 115 and name HB ) 2.2 0.5 0.9 volume=9.561 peak=3876 ppm1=0.303 ppm2=0.231 assign ( resid 63 and name HN ) ( resid 64 and name HN ) 3.2 1.4 1.3 volume=1.075 peak=1629 ppm1=7.298 ppm2=7.871 assign ( resid 110 and name HN ) ( resid 109 and name HD1 ) 3.6 1.9 1.4 volume=0.513 peak=618 ppm1=8.721 ppm2=3.106 assign ( resid 151 and name HN ) ( resid 149 and name HN ) 4.4 2.7 1.6 volume=0.149 peak=1174 ppm1=8.646 ppm2=7.783 assign ( resid 81 and name HN ) ( resid 72 and name HB ) 3.7 1.9 1.5 volume=0.449 peak=1510 ppm1=8.512 ppm2=1.818 assign ( resid 152 and name HN ) ( resid 170 and name HN ) 3.8 2.0 1.5 volume=0.385 peak=2094 ppm1=8.345 ppm2=9.151 assign ( resid 165 and name HN ) ( resid 56 and name HN ) 3.3 1.6 1.3 volume=0.760 peak=1909 ppm1=8.465 ppm2=8.679 assign ( resid 149 and name HN ) ( resid 149 and name HB2 ) 3.5 1.8 1.4 volume=0.572 peak=1164 ppm1=7.758 ppm2=2.834 assign ( resid 167 and name HD2# ) ( resid 167 and name HG ) 3.1 1.4 1.2 volume=1.195 peak=3809 ppm1=0.764 ppm2=0.922 assign ( resid 198 and name HN ) ( resid 195 and name HA ) 3.1 1.4 1.2 volume=1.236 peak=709 ppm1=8.719 ppm2=4.425 assign ( resid 65 and name HD1# ) ( resid 65 and name HD2# ) 2.9 1.2 1.2 volume=1.872 peak=4793 ppm1=0.175 ppm2=0.319 assign ( resid 188 and name HN ) ( resid 190 and name HN ) 3.3 1.6 1.3 volume=0.833 peak=523 ppm1=8.443 ppm2=7.538 assign ( resid 31 and name HN ) ( resid 31 and name HA ) 3.6 1.9 1.4 volume=0.517 peak=2248 ppm1=9.253 ppm2=4.399 assign ( resid 34 and name HG2# ) ( resid 34 and name HA ) 4.1 2.4 1.6 volume=0.221 peak=4834 ppm1=1.100 ppm2=4.965 assign ( resid 49 and name HN ) ( resid 48 and name HB1 ) 4.1 2.3 1.6 volume=0.242 peak=656 ppm1=8.917 ppm2=2.623 assign ( resid 99 and name HN ) ( resid 79 and name HN ) 3.9 2.2 1.6 volume=0.301 peak=157 ppm1=7.801 ppm2=8.831 assign ( resid 72 and name HG11 ) ( resid 72 and name HN ) 3.9 2.2 1.6 volume=0.287 peak=4126 ppm1=1.171 ppm2=7.535 assign ( resid 73 and name HB ) ( resid 73 and name HG2# ) 3.0 1.3 1.2 volume=1.388 peak=3086 ppm1=4.300 ppm2=1.218 assign ( resid 117 and name HB ) ( resid 117 and name HD1# ) 3.4 1.7 1.4 volume=0.708 peak=4450 ppm1=1.035 ppm2=0.243 assign ( resid 54 and name HB ) ( resid 55 and name HD1 ) 3.3 1.6 1.3 volume=0.779 peak=5085 ppm1=1.771 ppm2=3.390 assign ( resid 54 and name HG11 ) ( resid 200 and name HD1 or resid 200 and name HD2 ) 2.9 1.2 1.2 volume=1.828 peak=2772 ppm1=1.188 ppm2=1.554 assign ( resid 109 and name HG2 ) ( resid 144 and name HG12 ) 3.7 2.0 1.5 volume=0.386 peak=4860 ppm1=1.546 ppm2=1.274 assign ( resid 20 and name HN ) ( resid 19 and name HA ) 3.2 1.5 1.3 volume=1.032 peak=1065 ppm1=7.405 ppm2=4.142 assign ( resid 6 and name HN ) ( resid 8 and name HB2 ) 3.4 1.7 1.4 volume=0.668 peak=2421 ppm1=7.723 ppm2=2.055 assign ( resid 133 and name HN ) ( resid 132 and name HB ) 3.0 1.3 1.2 volume=1.524 peak=1894 ppm1=8.123 ppm2=2.279 assign ( resid 5 and name HA ) ( resid 8 and name HG1 ) 3.2 1.5 1.3 volume=0.923 peak=3989 ppm1=4.024 ppm2=2.401 assign ( resid 11 and name HN ) ( resid 13 and name HN ) 3.3 1.6 1.3 volume=0.792 peak=483 ppm1=8.179 ppm2=7.689 assign ( resid 147 and name HN ) ( resid 144 and name HD1# ) 3.9 2.2 1.6 volume=0.313 peak=1308 ppm1=8.785 ppm2=0.626 assign ( resid 85 and name HN ) ( resid 93 and name HG2# ) 3.2 1.5 1.3 volume=0.975 peak=2064 ppm1=7.153 ppm2=-0.017 assign ( resid 30 and name HN ) ( resid 30 and name HB2 ) 3.1 1.4 1.2 volume=1.241 peak=634 ppm1=8.722 ppm2=3.485 assign ( resid 192 and name HD2# ) ( resid 169 and name HG2 ) 4.1 2.4 1.6 volume=0.220 peak=3718 ppm1=0.491 ppm2=1.940 assign ( resid 203 and name HN ) ( resid 61 and name HD2# ) 3.3 1.6 1.3 volume=0.872 peak=2328 ppm1=7.683 ppm2=0.758 assign ( resid 5 and name HB# ) ( resid 4 and name HA ) 3.5 1.7 1.4 volume=0.626 peak=3586 ppm1=1.342 ppm2=3.831 assign ( resid 152 and name HA2 ) ( resid 127 and name HG11 ) 3.5 1.8 1.4 volume=0.561 peak=3369 ppm1=3.843 ppm2=1.001 assign ( resid 173 and name HG2# ) ( resid 188 and name HE# ) 2.6 0.9 1.1 volume=3.200 peak=4716 ppm1=1.035 ppm2=1.876 assign ( resid 123 and name HA ) ( resid 123 and name HN ) 3.9 2.2 1.6 volume=0.310 peak=3499 ppm1=4.346 ppm2=8.402 assign ( resid 121 and name HB1 ) ( resid 122 and name HA1 ) 4.3 2.6 1.7 volume=0.159 peak=3215 ppm1=2.053 ppm2=3.838 assign ( resid 165 and name HN ) ( resid 54 and name HB ) 3.2 1.5 1.3 volume=1.026 peak=794 ppm1=8.464 ppm2=1.796 assign ( resid 112 and name HN ) ( resid 112 and name HG11 ) 3.5 1.8 1.4 volume=0.546 peak=1799 ppm1=8.134 ppm2=1.535 assign ( resid 184 and name HA ) ( resid 188 and name HN ) 4.2 2.5 1.7 volume=0.190 peak=4764 ppm1=3.627 ppm2=8.457 assign ( resid 123 and name HA ) ( resid 157 and name HG1 ) 3.7 2.0 1.5 volume=0.393 peak=3403 ppm1=4.352 ppm2=1.784 assign ( resid 112 and name HG2# ) ( resid 132 and name HB ) 3.1 1.4 1.2 volume=1.192 peak=4280 ppm1=0.678 ppm2=2.240 assign ( resid 166 and name HB1 ) ( resid 51 and name HG1 ) 4.3 2.6 1.7 volume=0.164 peak=3404 ppm1=1.652 ppm2=1.988 assign ( resid 72 and name HD1# ) ( resid 71 and name HN ) 3.9 2.2 1.6 volume=0.307 peak=3957 ppm1=0.589 ppm2=7.215 assign ( resid 137 and name HN ) ( resid 84 and name HG2# ) 4.0 2.3 1.6 volume=0.251 peak=1589 ppm1=8.049 ppm2=0.125 assign ( resid 41 and name HN ) ( resid 41 and name HD2 ) 3.7 2.0 1.5 volume=0.438 peak=1251 ppm1=8.908 ppm2=3.081 assign ( resid 192 and name HD1# ) ( resid 35 and name HB ) 3.5 1.8 1.4 volume=0.578 peak=4461 ppm1=0.493 ppm2=2.023 assign ( resid 97 and name HG2# ) ( resid 99 and name HG1 ) 3.9 2.2 1.6 volume=0.313 peak=4077 ppm1=0.219 ppm2=2.418 assign ( resid 209 and name HD2 ) ( resid 208 and name HB ) 3.3 1.5 1.3 volume=0.895 peak=2854 ppm1=3.605 ppm2=4.028 assign ( resid 33 and name HD1# ) ( resid 34 and name HN ) 4.0 2.3 1.6 volume=0.248 peak=4263 ppm1=0.360 ppm2=8.128 assign ( resid 24 and name HD1 ) ( resid 24 and name HN ) 3.1 1.4 1.2 volume=1.199 peak=130 ppm1=6.802 ppm2=7.848 assign ( resid 114 and name HD2# ) ( resid 93 and name HG2# ) 3.7 2.0 1.5 volume=0.417 peak=2681 ppm1=0.781 ppm2=-0.010 assign ( resid 115 and name HN ) ( resid 115 and name HG2# ) 3.1 1.4 1.3 volume=1.105 peak=463 ppm1=9.053 ppm2=0.631 assign ( resid 144 and name HG2# ) ( resid 109 and name HA ) 3.7 2.0 1.5 volume=0.409 peak=5066 ppm1=0.767 ppm2=3.899 assign ( resid 34 and name HB ) ( resid 51 and name HG1 ) 4.1 2.4 1.7 volume=0.214 peak=4955 ppm1=3.827 ppm2=1.942 assign ( resid 130 and name HN ) ( resid 148 and name HB1 ) 4.1 2.4 1.6 volume=0.226 peak=912 ppm1=7.618 ppm2=2.960 assign ( resid 188 and name HN ) ( resid 187 and name HA ) 3.1 1.4 1.2 volume=1.246 peak=1465 ppm1=8.441 ppm2=4.270 assign ( resid 166 and name HN ) ( resid 156 and name HB1 ) 3.2 1.5 1.3 volume=1.055 peak=992 ppm1=9.000 ppm2=3.361 assign ( resid 190 and name HN ) ( resid 189 and name HA ) 3.8 2.1 1.5 volume=0.341 peak=611 ppm1=7.520 ppm2=4.656 assign ( resid 102 and name HA ) ( resid 103 and name HG2# ) 3.3 1.6 1.3 volume=0.820 peak=3885 ppm1=4.116 ppm2=0.831 assign ( resid 115 and name HN ) ( resid 114 and name HB1 ) 3.5 1.8 1.4 volume=0.586 peak=2017 ppm1=9.053 ppm2=1.008 assign ( resid 42 and name HD2 ) ( resid 42 and name HN ) 3.9 2.2 1.6 volume=0.296 peak=2629 ppm1=1.530 ppm2=8.706 assign ( resid 92 and name HE1 or resid 92 and name HE2 ) ( resid 86 and name HG2 ) 3.6 1.8 1.4 volume=0.534 peak=101 ppm1=6.751 ppm2=1.475 assign ( resid 139 and name HD2 ) ( resid 139 and name HG2 ) 3.5 1.8 1.4 volume=0.548 peak=4780 ppm1=3.623 ppm2=1.804 assign ( resid 76 and name HD2 ) ( resid 76 and name HG1 ) 2.5 0.7 1.0 volume=4.813 peak=4808 ppm1=1.550 ppm2=1.379 assign ( resid 134 and name HD1 or resid 134 and name HD2 ) ( resid 134 and name HB1 ) 3.4 1.7 1.4 volume=0.653 peak=106 ppm1=6.862 ppm2=3.063 assign ( resid 121 and name HA ) ( resid 121 and name HB1 ) 3.0 1.3 1.2 volume=1.504 peak=2919 ppm1=4.144 ppm2=2.026 assign ( resid 124 and name HN ) ( resid 120 and name HB2 ) 2.9 1.2 1.2 volume=1.767 peak=333 ppm1=6.471 ppm2=2.967 assign ( resid 4 and name HN ) ( resid 91 and name HG2# ) 3.0 1.3 1.2 volume=1.341 peak=1168 ppm1=8.189 ppm2=1.016 assign ( resid 141 and name HN ) ( resid 140 and name HB2 ) 3.8 2.1 1.5 volume=0.367 peak=1096 ppm1=8.453 ppm2=4.140 assign ( resid 142 and name HN ) ( resid 140 and name HB2 or resid 140 and name HB1 ) 3.1 1.4 1.2 volume=1.158 peak=579 ppm1=7.898 ppm2=4.079 assign ( resid 57 and name HA ) ( resid 162 and name HA ) 4.1 2.3 1.6 volume=0.239 peak=4338 ppm1=4.135 ppm2=3.633 assign ( resid 72 and name HN ) ( resid 70 and name HN ) 4.2 2.5 1.7 volume=0.204 peak=1107 ppm1=7.538 ppm2=8.571 assign ( resid 132 and name HN ) ( resid 112 and name HB ) 3.4 1.6 1.3 volume=0.742 peak=479 ppm1=7.894 ppm2=2.190 assign ( resid 91 and name HN ) ( resid 89 and name HA ) 3.7 1.9 1.5 volume=0.440 peak=803 ppm1=7.215 ppm2=4.145 assign ( resid 107 and name HN ) ( resid 144 and name HG2# ) 3.3 1.5 1.3 volume=0.893 peak=2029 ppm1=8.396 ppm2=0.764 assign ( resid 97 and name HN ) ( resid 96 and name HN ) 3.1 1.4 1.2 volume=1.267 peak=505 ppm1=8.362 ppm2=8.429 assign ( resid 75 and name HN ) ( resid 74 and name HA ) 3.3 1.5 1.3 volume=0.904 peak=369 ppm1=7.481 ppm2=4.792 assign ( resid 88 and name HN ) ( resid 91 and name HA ) 4.0 2.3 1.6 volume=0.249 peak=1069 ppm1=8.595 ppm2=5.837 assign ( resid 174 and name HN ) ( resid 149 and name HN ) 3.9 2.2 1.6 volume=0.284 peak=290 ppm1=9.153 ppm2=7.788 assign ( resid 172 and name HN ) ( resid 173 and name HG2# ) 3.6 1.8 1.4 volume=0.530 peak=1916 ppm1=8.857 ppm2=1.016 assign ( resid 93 and name HG2# ) ( resid 95 and name HB2 ) 4.1 2.4 1.6 volume=0.218 peak=3382 ppm1=-0.013 ppm2=2.605 assign ( resid 150 and name HB1 ) ( resid 130 and name HG1 ) 4.5 2.7 1.5 volume=0.136 peak=4988 ppm1=2.330 ppm2=1.348 assign ( resid 7 and name HB# ) ( resid 11 and name HN ) 3.7 1.9 1.5 volume=0.440 peak=4146 ppm1=0.754 ppm2=8.262 assign ( resid 171 and name HN ) ( resid 172 and name HA ) 3.9 2.2 1.6 volume=0.310 peak=2219 ppm1=9.062 ppm2=3.095 assign ( resid 12 and name HN ) ( resid 10 and name HA ) 3.4 1.7 1.3 volume=0.728 peak=1431 ppm1=7.547 ppm2=3.631 assign ( resid 106 and name HG11 ) ( resid 183 and name HB ) 3.9 2.2 1.6 volume=0.303 peak=4058 ppm1=1.410 ppm2=2.061 assign ( resid 48 and name HN ) ( resid 37 and name HA ) 4.0 2.3 1.6 volume=0.252 peak=2333 ppm1=9.291 ppm2=5.834 assign ( resid 203 and name HB ) ( resid 203 and name HN ) 4.4 2.7 1.6 volume=0.145 peak=3535 ppm1=0.123 ppm2=7.690 assign ( resid 185 and name HG2 ) ( resid 182 and name HA ) 4.1 2.4 1.6 volume=0.226 peak=2968 ppm1=2.345 ppm2=4.036 assign ( resid 34 and name HB ) ( resid 51 and name HB2 ) 4.5 2.8 1.5 volume=0.128 peak=4728 ppm1=3.828 ppm2=1.816 assign ( resid 202 and name HN ) ( resid 203 and name HN ) 3.4 1.7 1.4 volume=0.708 peak=1553 ppm1=8.575 ppm2=7.657 assign ( resid 72 and name HG2# ) ( resid 71 and name HG2 or resid 71 and name HG1 ) 3.5 1.8 1.4 volume=0.573 peak=4065 ppm1=0.603 ppm2=0.278 assign ( resid 147 and name HN ) ( resid 147 and name HB1 ) 3.5 1.8 1.4 volume=0.586 peak=2252 ppm1=8.785 ppm2=2.565 assign ( resid 101 and name HN ) ( resid 100 and name HA ) 2.8 1.1 1.1 volume=2.005 peak=826 ppm1=8.477 ppm2=4.264 assign ( resid 11 and name HB# ) ( resid 126 and name HD1# ) 4.4 2.7 1.6 volume=0.140 peak=4402 ppm1=1.631 ppm2=0.325 assign ( resid 205 and name HB# ) ( resid 206 and name HB2 ) 4.1 2.4 1.6 volume=0.218 peak=2746 ppm1=1.299 ppm2=2.978 assign ( resid 165 and name HN ) ( resid 54 and name HG2# ) 3.7 2.0 1.5 volume=0.401 peak=1708 ppm1=8.464 ppm2=0.575 assign ( resid 65 and name HN ) ( resid 65 and name HD1# ) 3.2 1.4 1.3 volume=1.086 peak=1964 ppm1=7.744 ppm2=0.227 assign ( resid 183 and name HN ) ( resid 179 and name HB2 ) 3.8 2.0 1.5 volume=0.378 peak=1776 ppm1=7.420 ppm2=2.436 assign ( resid 18 and name HB2 ) ( resid 17 and name HB1 ) 3.3 1.6 1.3 volume=0.799 peak=2713 ppm1=2.446 ppm2=2.802 assign ( resid 114 and name HD1# ) ( resid 7 and name HN ) 4.2 2.5 1.7 volume=0.196 peak=3140 ppm1=0.535 ppm2=8.460 assign ( resid 7 and name HN ) ( resid 6 and name HA ) 3.1 1.4 1.2 volume=1.160 peak=2070 ppm1=8.431 ppm2=3.609 assign ( resid 123 and name HN ) ( resid 124 and name HB2 ) 3.5 1.8 1.4 volume=0.601 peak=538 ppm1=8.404 ppm2=2.046 assign ( resid 126 and name HN ) ( resid 154 and name HA ) 3.2 1.5 1.3 volume=0.932 peak=2263 ppm1=9.104 ppm2=4.659 assign ( resid 72 and name HG12 ) ( resid 72 and name HB ) 3.4 1.7 1.4 volume=0.670 peak=4444 ppm1=1.038 ppm2=1.856 assign ( resid 23 and name HN ) ( resid 23 and name HA1 or resid 23 and name HA2 ) 3.2 1.5 1.3 volume=1.026 peak=1108 ppm1=8.630 ppm2=3.622 assign ( resid 203 and name HD1# ) ( resid 203 and name HN ) 3.7 2.0 1.5 volume=0.389 peak=3182 ppm1=-0.009 ppm2=7.680 assign ( resid 200 and name HA ) ( resid 203 and name HG12 ) 3.7 1.9 1.5 volume=0.442 peak=3303 ppm1=3.360 ppm2=0.517 assign ( resid 177 and name HN ) ( resid 176 and name HA ) 3.6 1.8 1.4 volume=0.526 peak=988 ppm1=8.464 ppm2=4.002 assign ( resid 159 and name HG1 or resid 159 and name HG2 ) ( resid 160 and name HN ) 4.1 2.4 1.6 volume=0.226 peak=3089 ppm1=2.240 ppm2=8.841 assign ( resid 203 and name HG2# ) ( resid 57 and name HN ) 4.9 3.2 1.1 volume=0.075 peak=4405 ppm1=0.339 ppm2=9.228 assign ( resid 119 and name HN ) ( resid 117 and name HG2# ) 3.5 1.8 1.4 volume=0.547 peak=432 ppm1=8.054 ppm2=0.364 assign ( resid 161 and name HN ) ( resid 158 and name HN ) 3.3 1.6 1.3 volume=0.865 peak=1743 ppm1=6.904 ppm2=8.174 assign ( resid 175 and name HG1 ) ( resid 175 and name HB2 ) 2.8 1.0 1.1 volume=2.388 peak=5104 ppm1=2.553 ppm2=2.438 assign ( resid 179 and name HD1# ) ( resid 179 and name HA ) 3.8 2.1 1.5 volume=0.344 peak=2637 ppm1=0.531 ppm2=3.817 assign ( resid 7 and name HN ) ( resid 5 and name HB# ) 3.3 1.6 1.3 volume=0.788 peak=1153 ppm1=8.433 ppm2=1.314 assign ( resid 70 and name HN ) ( resid 69 and name HN ) 3.3 1.5 1.3 volume=0.893 peak=614 ppm1=8.574 ppm2=8.182 assign ( resid 168 and name HN ) ( resid 168 and name HA ) 3.8 2.1 1.5 volume=0.370 peak=1717 ppm1=8.694 ppm2=4.793 assign ( resid 123 and name HA ) ( resid 123 and name HB1 ) 3.8 2.1 1.5 volume=0.349 peak=3717 ppm1=4.349 ppm2=2.732 assign ( resid 51 and name HG1 or resid 51 and name HG2 ) ( resid 52 and name HA2 ) 4.7 3.0 1.3 volume=0.103 peak=3584 ppm1=1.971 ppm2=4.484 assign ( resid 190 and name HN ) ( resid 189 and name HG2 ) 3.5 1.8 1.4 volume=0.591 peak=1941 ppm1=7.521 ppm2=1.792 assign ( resid 37 and name HA ) ( resid 48 and name HA ) 4.7 3.0 1.3 volume=0.098 peak=3396 ppm1=5.823 ppm2=5.332 assign ( resid 24 and name HN ) ( resid 24 and name HD1 ) 3.6 1.9 1.4 volume=0.500 peak=1918 ppm1=7.835 ppm2=6.750 assign ( resid 167 and name HN ) ( resid 51 and name HG1 ) 4.0 2.3 1.6 volume=0.273 peak=2433 ppm1=8.642 ppm2=1.999 assign ( resid 51 and name HN ) ( resid 36 and name HN ) 4.1 2.4 1.7 volume=0.213 peak=1356 ppm1=8.428 ppm2=9.882 assign ( resid 193 and name HG2# ) ( resid 193 and name HA ) 3.3 1.6 1.3 volume=0.878 peak=3666 ppm1=0.796 ppm2=3.457 assign ( resid 6 and name HB ) ( resid 6 and name HG11 ) 4.0 2.3 1.6 volume=0.252 peak=4249 ppm1=1.722 ppm2=1.030 assign ( resid 56 and name HN ) ( resid 56 and name HG1 ) 3.3 1.6 1.3 volume=0.836 peak=1858 ppm1=8.640 ppm2=1.986 assign ( resid 116 and name HB2 ) ( resid 7 and name HB# ) 3.5 1.8 1.4 volume=0.561 peak=5095 ppm1=2.845 ppm2=0.754 assign ( resid 3 and name HE1 or resid 3 and name HE2 ) ( resid 93 and name HG12 ) 2.9 1.2 1.2 volume=1.793 peak=102 ppm1=7.214 ppm2=0.585 assign ( resid 93 and name HG2# ) ( resid 84 and name HB ) 3.7 1.9 1.5 volume=0.454 peak=3774 ppm1=-0.013 ppm2=1.999 assign ( resid 168 and name HG1# ) ( resid 166 and name HG1 ) 2.4 0.7 1.0 volume=5.022 peak=4304 ppm1=0.767 ppm2=1.210 assign ( resid 38 and name HN ) ( resid 37 and name HB2 ) 3.2 1.5 1.3 volume=0.997 peak=207 ppm1=8.467 ppm2=3.300 assign ( resid 18 and name HB1 ) ( resid 17 and name HN ) 3.9 2.2 1.6 volume=0.312 peak=4551 ppm1=2.969 ppm2=7.623 assign ( resid 130 and name HB1 ) ( resid 130 and name HD2 ) 3.2 1.4 1.3 volume=1.084 peak=4247 ppm1=1.887 ppm2=1.661 assign ( resid 214 and name HN ) ( resid 214 and name HA ) 3.6 1.9 1.4 volume=0.478 peak=2176 ppm1=7.956 ppm2=4.396 assign ( resid 45 and name HN ) ( resid 45 and name HA1 ) 3.7 2.0 1.5 volume=0.414 peak=2127 ppm1=6.653 ppm2=3.225 assign ( resid 36 and name HN ) ( resid 49 and name HN ) 3.9 2.2 1.6 volume=0.286 peak=315 ppm1=9.878 ppm2=8.954 assign ( resid 127 and name HB ) ( resid 127 and name HG2# ) 4.0 2.3 1.6 volume=0.261 peak=4371 ppm1=2.058 ppm2=0.804 assign ( resid 115 and name HA ) ( resid 114 and name HD1# ) 4.1 2.4 1.7 volume=0.218 peak=2580 ppm1=4.399 ppm2=0.539 assign ( resid 14 and name HA ) ( resid 13 and name HG2 or resid 13 and name HG1 ) 4.6 2.9 1.4 volume=0.111 peak=4332 ppm1=2.818 ppm2=2.144 assign ( resid 29 and name HG2# ) ( resid 29 and name HB ) 4.0 2.3 1.6 volume=0.249 peak=2873 ppm1=1.068 ppm2=3.930 assign ( resid 208 and name HN ) ( resid 204 and name HB1 ) 3.1 1.4 1.2 volume=1.252 peak=1880 ppm1=8.012 ppm2=1.677 assign ( resid 130 and name HG1 ) ( resid 10 and name HG2# ) 3.6 1.9 1.5 volume=0.472 peak=4269 ppm1=1.307 ppm2=1.079 assign ( resid 72 and name HB ) ( resid 78 and name HB1 ) 3.2 1.5 1.3 volume=0.947 peak=3611 ppm1=1.853 ppm2=1.362 assign ( resid 121 and name HN ) ( resid 120 and name HB1 ) 2.9 1.1 1.1 volume=1.988 peak=508 ppm1=8.583 ppm2=3.008 assign ( resid 147 and name HA ) ( resid 147 and name HB1 ) 4.4 2.7 1.6 volume=0.141 peak=2838 ppm1=4.262 ppm2=2.648 assign ( resid 79 and name HA ) ( resid 79 and name HB1 ) 3.9 2.2 1.6 volume=0.292 peak=3025 ppm1=4.396 ppm2=1.774 assign ( resid 155 and name HA ) ( resid 155 and name HB2 ) 4.3 2.6 1.7 volume=0.160 peak=4725 ppm1=5.254 ppm2=2.573 assign ( resid 11 and name HN ) ( resid 10 and name HN ) 2.8 1.0 1.1 volume=2.436 peak=863 ppm1=8.180 ppm2=8.325 assign ( resid 72 and name HG11 ) ( resid 72 and name HB ) 3.2 1.5 1.3 volume=0.916 peak=2570 ppm1=1.172 ppm2=1.853 assign ( resid 92 and name HN ) ( resid 114 and name HD1# ) 3.2 1.4 1.3 volume=1.087 peak=1660 ppm1=9.456 ppm2=0.528 assign ( resid 64 and name HN ) ( resid 61 and name HD2# ) 3.7 2.0 1.5 volume=0.422 peak=1693 ppm1=7.876 ppm2=0.755 assign ( resid 109 and name HG2 ) ( resid 144 and name HG2# ) 2.7 1.0 1.1 volume=2.823 peak=3664 ppm1=1.541 ppm2=0.778 assign ( resid 188 and name HA ) ( resid 188 and name HB1 ) 4.2 2.5 1.7 volume=0.199 peak=3497 ppm1=4.214 ppm2=1.486 assign ( resid 170 and name HN ) ( resid 151 and name HB2 ) 3.6 1.9 1.4 volume=0.509 peak=1873 ppm1=9.147 ppm2=2.963 assign ( resid 84 and name HN ) ( resid 93 and name HG2# ) 3.5 1.8 1.4 volume=0.564 peak=2059 ppm1=8.504 ppm2=-0.011 assign ( resid 15 and name HA ) ( resid 15 and name HB2 ) 4.2 2.5 1.7 volume=0.198 peak=4754 ppm1=3.673 ppm2=1.364 assign ( resid 217 and name HN ) ( resid 216 and name HB1 ) 3.6 1.8 1.4 volume=0.526 peak=1322 ppm1=8.146 ppm2=2.964 assign ( resid 33 and name HN ) ( resid 32 and name HA ) 2.7 1.0 1.1 volume=2.566 peak=1927 ppm1=8.167 ppm2=3.754 assign ( resid 71 and name HN ) ( resid 70 and name HB1 ) 3.7 2.0 1.5 volume=0.400 peak=366 ppm1=7.220 ppm2=2.599 assign ( resid 203 and name HG2# ) ( resid 205 and name HN ) 4.0 2.3 1.6 volume=0.247 peak=2499 ppm1=0.341 ppm2=7.216 assign ( resid 139 and name HB2 ) ( resid 143 and name HN ) 4.3 2.6 1.7 volume=0.175 peak=3453 ppm1=2.197 ppm2=6.900 assign ( resid 168 and name HG2# ) ( resid 50 and name HN ) 3.5 1.8 1.4 volume=0.587 peak=2755 ppm1=0.199 ppm2=9.360 assign ( resid 190 and name HN ) ( resid 189 and name HB2 ) 3.8 2.1 1.5 volume=0.352 peak=530 ppm1=7.519 ppm2=2.049 assign ( resid 47 and name HN ) ( resid 39 and name HB# ) 3.9 2.1 1.5 volume=0.328 peak=368 ppm1=8.703 ppm2=1.136 assign ( resid 185 and name HB1 ) ( resid 185 and name HN ) 3.5 1.7 1.4 volume=0.635 peak=4240 ppm1=2.151 ppm2=8.179 assign ( resid 203 and name HD1# ) ( resid 199 and name HA ) 3.2 1.5 1.3 volume=1.015 peak=4230 ppm1=-0.011 ppm2=2.781 assign ( resid 152 and name HN ) ( resid 153 and name HB2 ) 3.8 2.0 1.5 volume=0.382 peak=1896 ppm1=8.345 ppm2=2.806 assign ( resid 105 and name HB1 ) ( resid 183 and name HD1# ) 2.8 1.0 1.1 volume=2.447 peak=4845 ppm1=3.870 ppm2=0.869 assign ( resid 24 and name HH2 ) ( resid 49 and name HG2 ) 3.4 1.7 1.4 volume=0.642 peak=126 ppm1=6.801 ppm2=1.589 assign ( resid 91 and name HB ) ( resid 87 and name HD1# ) 4.3 2.6 1.7 volume=0.165 peak=2805 ppm1=3.641 ppm2=0.442 assign ( resid 34 and name HN ) ( resid 196 and name HD1# ) 2.6 0.9 1.0 volume=3.638 peak=973 ppm1=8.137 ppm2=0.756 assign ( resid 11 and name HN ) ( resid 9 and name HN ) 3.3 1.6 1.3 volume=0.772 peak=1157 ppm1=8.179 ppm2=7.982 assign ( resid 155 and name HN ) ( resid 125 and name HN ) 3.6 1.9 1.4 volume=0.477 peak=571 ppm1=8.978 ppm2=8.774 assign ( resid 15 and name HG ) ( resid 15 and name HN ) 3.9 2.2 1.6 volume=0.284 peak=4475 ppm1=1.242 ppm2=7.808 assign ( resid 146 and name HN ) ( resid 145 and name HD2 or resid 145 and name HD1 ) 3.9 2.2 1.5 volume=0.318 peak=2307 ppm1=8.399 ppm2=3.490 assign ( resid 93 and name HB ) ( resid 93 and name HD1# ) 4.1 2.4 1.7 volume=0.215 peak=3732 ppm1=1.224 ppm2=-0.273 assign ( resid 102 and name HA ) ( resid 102 and name HB# ) 2.5 0.8 1.0 volume=4.056 peak=4311 ppm1=4.117 ppm2=1.280 assign ( resid 33 and name HN ) ( resid 33 and name HD1# ) 3.8 2.1 1.5 volume=0.337 peak=265 ppm1=8.161 ppm2=0.363 assign ( resid 15 and name HG ) ( resid 15 and name HD2# ) 2.8 1.0 1.1 volume=2.398 peak=4856 ppm1=1.242 ppm2=0.685 assign ( resid 10 and name HB ) ( resid 10 and name HN ) 4.4 2.7 1.6 volume=0.154 peak=3417 ppm1=3.686 ppm2=8.328 assign ( resid 72 and name HG2# ) ( resid 72 and name HN ) 3.1 1.3 1.2 volume=1.326 peak=3783 ppm1=0.602 ppm2=7.537 assign ( resid 27 and name HN ) ( resid 36 and name HB2 ) 3.3 1.6 1.3 volume=0.814 peak=944 ppm1=9.279 ppm2=3.494 assign ( resid 203 and name HN ) ( resid 205 and name HN ) 3.6 1.9 1.4 volume=0.516 peak=1204 ppm1=7.683 ppm2=7.135 assign ( resid 3 and name HD1 or resid 3 and name HD2 ) ( resid 114 and name HD1# ) 3.1 1.3 1.2 volume=1.303 peak=59 ppm1=7.380 ppm2=0.529 assign ( resid 35 and name HG2# ) ( resid 192 and name HB2 ) 4.4 2.6 1.6 volume=0.158 peak=3168 ppm1=0.889 ppm2=1.331 assign ( resid 60 and name HB2 ) ( resid 60 and name HE2 ) 2.8 1.1 1.1 volume=2.130 peak=5028 ppm1=1.718 ppm2=2.833 assign ( resid 132 and name HG1# ) ( resid 132 and name HN ) 3.8 2.1 1.5 volume=0.364 peak=3287 ppm1=0.542 ppm2=7.886 assign ( resid 26 and name HG1# ) ( resid 36 and name HA ) 3.5 1.8 1.4 volume=0.599 peak=3055 ppm1=0.778 ppm2=5.850 assign ( resid 169 and name HN ) ( resid 170 and name HN ) 3.2 1.5 1.3 volume=0.952 peak=378 ppm1=9.256 ppm2=9.157 assign ( resid 162 and name HG2 ) ( resid 163 and name HB# ) 3.8 2.1 1.5 volume=0.356 peak=3597 ppm1=1.920 ppm2=1.160 assign ( resid 54 and name HG2# ) ( resid 200 and name HE1 ) 3.6 1.9 1.4 volume=0.504 peak=4501 ppm1=0.577 ppm2=2.797 assign ( resid 56 and name HN ) ( resid 164 and name HA ) 2.9 1.2 1.2 volume=1.751 peak=302 ppm1=8.640 ppm2=4.916 assign ( resid 135 and name HG2 ) ( resid 135 and name HD2 ) 3.5 1.8 1.4 volume=0.605 peak=4759 ppm1=1.787 ppm2=3.232 assign ( resid 86 and name HA ) ( resid 87 and name HG2# ) 3.6 1.8 1.4 volume=0.529 peak=2956 ppm1=4.286 ppm2=0.865 assign ( resid 13 and name HN ) ( resid 12 and name HN ) 3.1 1.4 1.2 volume=1.233 peak=2255 ppm1=7.721 ppm2=7.548 assign ( resid 72 and name HG11 ) ( resid 70 and name HN ) 3.9 2.1 1.5 volume=0.320 peak=3848 ppm1=1.171 ppm2=8.580 assign ( resid 154 and name HG1# ) ( resid 14 and name HG1# ) 3.3 1.6 1.3 volume=0.815 peak=2879 ppm1=0.914 ppm2=0.677 assign ( resid 19 and name HN ) ( resid 17 and name HD1 or resid 17 and name HD2 ) 3.8 2.0 1.5 volume=0.380 peak=400 ppm1=7.482 ppm2=6.513 assign ( resid 5 and name HB# ) ( resid 5 and name HN ) 3.0 1.2 1.2 volume=1.623 peak=2542 ppm1=1.341 ppm2=7.479 assign ( resid 184 and name HN ) ( resid 183 and name HA ) 3.0 1.3 1.2 volume=1.359 peak=700 ppm1=7.498 ppm2=3.882 assign ( resid 179 and name HB1 ) ( resid 179 and name HA ) 3.8 2.1 1.5 volume=0.369 peak=3032 ppm1=2.752 ppm2=3.824 assign ( resid 170 and name HN ) ( resid 151 and name HA ) 4.1 2.4 1.6 volume=0.228 peak=2309 ppm1=9.146 ppm2=4.916 assign ( resid 145 and name HN ) ( resid 144 and name HG11 ) 4.0 2.3 1.6 volume=0.245 peak=2151 ppm1=8.379 ppm2=1.247 assign ( resid 36 and name HN ) ( resid 51 and name HN ) 3.8 2.1 1.5 volume=0.336 peak=1845 ppm1=9.882 ppm2=8.446 assign ( resid 106 and name HN ) ( resid 105 and name HB1 or resid 105 and name HB2 ) 3.1 1.4 1.2 volume=1.188 peak=2026 ppm1=7.942 ppm2=3.880 assign ( resid 163 and name HN ) ( resid 161 and name HA ) 3.1 1.4 1.2 volume=1.154 peak=1053 ppm1=7.324 ppm2=4.656 assign ( resid 173 and name HN ) ( resid 173 and name HG2# ) 2.8 1.1 1.1 volume=2.195 peak=1357 ppm1=8.518 ppm2=1.016 assign ( resid 172 and name HN ) ( resid 171 and name HA ) 3.5 1.8 1.4 volume=0.614 peak=2384 ppm1=8.857 ppm2=4.134 assign ( resid 3 and name HN ) ( resid 2 and name HB2 or resid 2 and name HB1 ) 2.9 1.1 1.1 volume=1.980 peak=1609 ppm1=7.915 ppm2=2.834 assign ( resid 154 and name HN ) ( resid 153 and name HB2 ) 3.8 2.1 1.5 volume=0.367 peak=1068 ppm1=10.006 ppm2=2.909 assign ( resid 72 and name HG2# ) ( resid 72 and name HG12 ) 2.9 1.1 1.1 volume=2.002 peak=4636 ppm1=0.603 ppm2=1.039 assign ( resid 171 and name HN ) ( resid 48 and name HN ) 3.7 2.0 1.5 volume=0.436 peak=1682 ppm1=9.064 ppm2=9.290 assign ( resid 7 and name HB# ) ( resid 6 and name HN ) 3.5 1.8 1.4 volume=0.577 peak=3221 ppm1=0.753 ppm2=7.725 assign ( resid 122 and name HN ) ( resid 121 and name HN ) 2.9 1.2 1.2 volume=1.635 peak=960 ppm1=8.645 ppm2=8.584 assign ( resid 5 and name HA ) ( resid 6 and name HD1# ) 4.3 2.6 1.7 volume=0.159 peak=3951 ppm1=4.024 ppm2=0.771 assign ( resid 159 and name HN ) ( resid 159 and name HB2 ) 2.6 0.9 1.1 volume=3.181 peak=590 ppm1=9.022 ppm2=1.924 assign ( resid 183 and name HN ) ( resid 184 and name HB ) 2.6 0.8 1.0 volume=3.833 peak=1435 ppm1=7.421 ppm2=2.043 assign ( resid 133 and name HN ) ( resid 134 and name HN ) 3.6 1.9 1.4 volume=0.508 peak=1423 ppm1=8.125 ppm2=8.745 assign ( resid 19 and name HN ) ( resid 17 and name HA ) 3.5 1.8 1.4 volume=0.569 peak=2050 ppm1=7.478 ppm2=4.605 assign ( resid 132 and name HG2# ) ( resid 132 and name HA ) 4.2 2.5 1.7 volume=0.200 peak=2810 ppm1=0.936 ppm2=4.677 assign ( resid 85 and name HN ) ( resid 134 and name HD1 or resid 134 and name HD2 ) 4.1 2.4 1.6 volume=0.221 peak=1790 ppm1=7.153 ppm2=6.865 assign ( resid 153 and name HB2 ) ( resid 152 and name HA1 ) 3.4 1.7 1.4 volume=0.721 peak=4626 ppm1=2.853 ppm2=3.714 assign ( resid 97 and name HN ) ( resid 97 and name HA ) 3.3 1.6 1.3 volume=0.869 peak=524 ppm1=8.363 ppm2=4.514 assign ( resid 36 and name HA ) ( resid 37 and name HA ) 4.0 2.2 1.6 volume=0.280 peak=4705 ppm1=5.851 ppm2=5.810 assign ( resid 130 and name HN ) ( resid 130 and name HB1 ) 3.2 1.5 1.3 volume=0.955 peak=527 ppm1=7.617 ppm2=1.912 assign ( resid 21 and name HN ) ( resid 20 and name HB1 or resid 20 and name HB2 ) 3.8 2.1 1.5 volume=0.340 peak=388 ppm1=8.288 ppm2=2.731 assign ( resid 11 and name HB# ) ( resid 15 and name HD1# ) 4.1 2.4 1.6 volume=0.226 peak=3487 ppm1=1.630 ppm2=0.451 assign ( resid 26 and name HG2# ) ( resid 36 and name HA ) 4.3 2.5 1.7 volume=0.178 peak=3064 ppm1=0.911 ppm2=5.840 assign ( resid 175 and name HN ) ( resid 175 and name HB2 ) 3.1 1.4 1.3 volume=1.140 peak=343 ppm1=8.803 ppm2=2.447 assign ( resid 145 and name HN ) ( resid 143 and name HA ) 3.8 2.0 1.5 volume=0.380 peak=1541 ppm1=8.380 ppm2=4.673 assign ( resid 126 and name HG2# ) ( resid 15 and name HA ) 3.8 2.1 1.5 volume=0.339 peak=3776 ppm1=0.752 ppm2=3.698 assign ( resid 92 and name HE1 or resid 92 and name HE2 ) ( resid 116 and name HA ) 4.0 2.3 1.6 volume=0.263 peak=65 ppm1=6.750 ppm2=6.173 assign ( resid 34 and name HA ) ( resid 34 and name HB ) 3.7 2.0 1.5 volume=0.394 peak=3828 ppm1=4.965 ppm2=3.829 assign ( resid 51 and name HN ) ( resid 168 and name HA ) 3.4 1.7 1.3 volume=0.729 peak=2276 ppm1=8.424 ppm2=4.788 assign ( resid 179 and name HN ) ( resid 179 and name HD2# ) 2.9 1.2 1.2 volume=1.714 peak=2317 ppm1=7.303 ppm2=0.754 assign ( resid 202 and name HN ) ( resid 64 and name HD1 or resid 64 and name HD2 ) 3.8 2.1 1.5 volume=0.339 peak=805 ppm1=8.576 ppm2=5.968 assign ( resid 134 and name HB2 ) ( resid 135 and name HA ) 3.8 2.1 1.5 volume=0.359 peak=3241 ppm1=2.953 ppm2=4.168 assign ( resid 112 and name HD1# ) ( resid 95 and name HA ) 3.6 1.8 1.4 volume=0.522 peak=3269 ppm1=0.372 ppm2=5.585 assign ( resid 77 and name HN ) ( resid 76 and name HG1 ) 3.3 1.5 1.3 volume=0.898 peak=1023 ppm1=8.056 ppm2=1.409 assign ( resid 100 and name HB1 ) ( resid 101 and name HN ) 4.1 2.4 1.6 volume=0.230 peak=3387 ppm1=3.735 ppm2=8.525 assign ( resid 151 and name HN ) ( resid 10 and name HG2# ) 3.5 1.8 1.4 volume=0.602 peak=163 ppm1=8.646 ppm2=1.016 assign ( resid 168 and name HG2# ) ( resid 51 and name HB1 ) 3.1 1.4 1.3 volume=1.153 peak=4944 ppm1=0.200 ppm2=1.799 assign ( resid 54 and name HN ) ( resid 53 and name HA ) 3.1 1.4 1.2 volume=1.185 peak=542 ppm1=9.020 ppm2=4.917 assign ( resid 210 and name HN ) ( resid 211 and name HN ) 2.6 0.8 1.0 volume=3.727 peak=2354 ppm1=8.306 ppm2=8.268 assign ( resid 42 and name HD1 ) ( resid 42 and name HB1 ) 2.1 0.4 0.8 volume=13.167 peak=5050 ppm1=1.530 ppm2=1.666 assign ( resid 130 and name HD2 ) ( resid 130 and name HB1 or resid 130 and name HB2 ) 2.7 1.0 1.1 volume=2.639 peak=3058 ppm1=1.660 ppm2=1.858 assign ( resid 18 and name HA ) ( resid 18 and name HB1 ) 3.0 1.2 1.2 volume=1.576 peak=3707 ppm1=4.478 ppm2=2.970 assign ( resid 34 and name HG2# ) ( resid 51 and name HN ) 3.5 1.8 1.4 volume=0.582 peak=5148 ppm1=1.099 ppm2=8.451 assign ( resid 98 and name HN ) ( resid 79 and name HB2 ) 3.6 1.9 1.5 volume=0.461 peak=705 ppm1=9.354 ppm2=1.795 assign ( resid 186 and name HN ) ( resid 185 and name HG1 ) 3.4 1.7 1.4 volume=0.686 peak=1577 ppm1=7.370 ppm2=2.334 assign ( resid 112 and name HN ) ( resid 112 and name HB ) 3.4 1.7 1.4 volume=0.683 peak=778 ppm1=8.137 ppm2=2.189 assign ( resid 27 and name HN ) ( resid 27 and name HG1# ) 2.9 1.1 1.1 volume=1.939 peak=790 ppm1=9.276 ppm2=0.879 assign ( resid 204 and name HN ) ( resid 205 and name HN ) 3.0 1.3 1.2 volume=1.466 peak=1981 ppm1=6.746 ppm2=7.145 assign ( resid 13 and name HN ) ( resid 12 and name HA ) 3.0 1.3 1.2 volume=1.378 peak=1848 ppm1=7.720 ppm2=3.900 assign ( resid 41 and name HB1 or resid 41 and name HB2 ) ( resid 40 and name HA ) 3.3 1.6 1.3 volume=0.867 peak=4922 ppm1=1.979 ppm2=4.028 assign ( resid 191 and name HB1 ) ( resid 194 and name HN ) 4.3 2.6 1.7 volume=0.176 peak=4051 ppm1=2.816 ppm2=7.795 assign ( resid 204 and name HB1 ) ( resid 207 and name HN ) 3.6 1.9 1.4 volume=0.502 peak=3248 ppm1=1.713 ppm2=7.810 assign ( resid 6 and name HG11 ) ( resid 5 and name HB# ) 4.3 2.6 1.7 volume=0.177 peak=2752 ppm1=1.038 ppm2=1.298 assign ( resid 207 and name HN ) ( resid 207 and name HD2 ) 4.0 2.2 1.6 volume=0.280 peak=1926 ppm1=7.833 ppm2=3.053 assign ( resid 139 and name HA ) ( resid 139 and name HB1 ) 3.0 1.3 1.2 volume=1.423 peak=5019 ppm1=4.304 ppm2=2.197 assign ( resid 167 and name HN ) ( resid 166 and name HD1 ) 3.2 1.5 1.3 volume=1.019 peak=2204 ppm1=8.642 ppm2=1.464 assign ( resid 130 and name HB2 ) ( resid 130 and name HN ) 4.4 2.7 1.6 volume=0.147 peak=5090 ppm1=1.833 ppm2=7.617 assign ( resid 54 and name HN ) ( resid 200 and name HE1 ) 4.2 2.4 1.7 volume=0.205 peak=824 ppm1=9.020 ppm2=2.827 assign ( resid 207 and name HN ) ( resid 204 and name HB1 ) 3.2 1.5 1.3 volume=1.006 peak=602 ppm1=7.834 ppm2=1.679 assign ( resid 175 and name HN ) ( resid 173 and name HG2# ) 3.4 1.7 1.4 volume=0.655 peak=439 ppm1=8.804 ppm2=1.012 assign ( resid 127 and name HD1# ) ( resid 65 and name HD1# ) 2.7 1.0 1.1 volume=2.869 peak=4235 ppm1=0.287 ppm2=0.152 assign ( resid 68 and name HN ) ( resid 67 and name HN ) 3.7 2.0 1.5 volume=0.418 peak=1900 ppm1=8.023 ppm2=7.652 assign ( resid 17 and name HD1 or resid 17 and name HD2 ) ( resid 38 and name HE2 ) 3.5 1.7 1.4 volume=0.631 peak=73 ppm1=6.486 ppm2=2.173 assign ( resid 72 and name HA ) ( resid 75 and name HN ) 3.9 2.2 1.6 volume=0.290 peak=5078 ppm1=3.633 ppm2=7.480 assign ( resid 48 and name HN ) ( resid 47 and name HA ) 3.5 1.7 1.4 volume=0.631 peak=1723 ppm1=9.286 ppm2=4.782 assign ( resid 115 and name HA ) ( resid 116 and name HN ) 3.7 2.0 1.5 volume=0.404 peak=2783 ppm1=4.401 ppm2=8.839 assign ( resid 153 and name HN ) ( resid 154 and name HN ) 3.9 2.1 1.5 volume=0.328 peak=424 ppm1=9.329 ppm2=10.003 assign ( resid 65 and name HD1# ) ( resid 64 and name HD1 or resid 64 and name HD2 ) 4.5 2.8 1.5 volume=0.133 peak=2512 ppm1=0.177 ppm2=5.987 assign ( resid 148 and name HN ) ( resid 147 and name HD1 or resid 147 and name HD2 ) 4.1 2.4 1.7 volume=0.215 peak=1350 ppm1=9.151 ppm2=6.226 assign ( resid 19 and name HN ) ( resid 19 and name HB1 or resid 19 and name HB2 ) 3.1 1.4 1.2 volume=1.162 peak=1560 ppm1=7.481 ppm2=1.774 assign ( resid 162 and name HA ) ( resid 58 and name HG2 ) 3.4 1.7 1.4 volume=0.646 peak=2814 ppm1=3.651 ppm2=1.749 assign ( resid 14 and name HA ) ( resid 17 and name HN ) 4.2 2.5 1.7 volume=0.201 peak=4246 ppm1=2.819 ppm2=7.673 assign ( resid 131 and name HN ) ( resid 130 and name HB1 ) 3.4 1.6 1.3 volume=0.753 peak=1701 ppm1=9.293 ppm2=1.901 assign ( resid 115 and name HG2# ) ( resid 115 and name HG1# ) 2.4 0.7 1.0 volume=5.163 peak=3856 ppm1=0.659 ppm2=0.305 assign ( resid 114 and name HD2# ) ( resid 93 and name HD1# ) 3.8 2.1 1.5 volume=0.340 peak=2708 ppm1=0.780 ppm2=-0.272 assign ( resid 114 and name HD2# ) ( resid 92 and name HN ) 4.2 2.5 1.7 volume=0.199 peak=3471 ppm1=0.781 ppm2=9.442 assign ( resid 25 and name HN ) ( resid 37 and name HA ) 3.5 1.7 1.4 volume=0.626 peak=890 ppm1=9.014 ppm2=5.829 assign ( resid 184 and name HD1# ) ( resid 179 and name HB2 ) 3.4 1.7 1.4 volume=0.701 peak=4619 ppm1=0.894 ppm2=2.531 assign ( resid 175 and name HN ) ( resid 175 and name HA ) 3.4 1.7 1.4 volume=0.678 peak=1616 ppm1=8.803 ppm2=5.186 assign ( resid 165 and name HN ) ( resid 54 and name HN ) 3.6 1.9 1.4 volume=0.502 peak=1249 ppm1=8.464 ppm2=8.958 assign ( resid 67 and name HG2 ) ( resid 67 and name HB2 ) 3.3 1.6 1.3 volume=0.842 peak=2836 ppm1=2.567 ppm2=2.056 assign ( resid 96 and name HN ) ( resid 81 and name HA ) 3.4 1.7 1.4 volume=0.681 peak=1604 ppm1=8.473 ppm2=4.658 assign ( resid 79 and name HN ) ( resid 72 and name HG12 ) 3.5 1.8 1.4 volume=0.539 peak=425 ppm1=8.842 ppm2=1.013 assign ( resid 196 and name HD1# ) ( resid 193 and name HB ) 3.6 1.8 1.4 volume=0.519 peak=4777 ppm1=0.727 ppm2=2.070 assign ( resid 24 and name HZ2 ) ( resid 24 and name HE1 ) 3.5 1.8 1.4 volume=0.592 peak=21 ppm1=7.537 ppm2=10.147 assign ( resid 60 and name HN ) ( resid 60 and name HB2 or resid 60 and name HB1 ) 2.7 0.9 1.1 volume=3.076 peak=258 ppm1=7.265 ppm2=1.670 assign ( resid 208 and name HG2# ) ( resid 210 and name HB2 or resid 210 and name HB1 ) 3.3 1.6 1.3 volume=0.813 peak=2525 ppm1=1.137 ppm2=3.765 assign ( resid 68 and name HN ) ( resid 67 and name HA ) 2.9 1.2 1.2 volume=1.876 peak=1267 ppm1=8.024 ppm2=3.884 assign ( resid 202 and name HA1 ) ( resid 203 and name HA ) 4.7 3.0 1.3 volume=0.095 peak=5062 ppm1=3.062 ppm2=2.885 assign ( resid 40 and name HN ) ( resid 47 and name HA ) 3.6 1.9 1.4 volume=0.493 peak=2036 ppm1=8.507 ppm2=4.791 assign ( resid 98 and name HG2# ) ( resid 109 and name HG1 ) 3.5 1.8 1.4 volume=0.613 peak=4360 ppm1=1.325 ppm2=1.596 assign ( resid 185 and name HN ) ( resid 186 and name HE1 or resid 186 and name HE2 ) 3.4 1.7 1.4 volume=0.651 peak=1509 ppm1=8.184 ppm2=2.953 assign ( resid 15 and name HD1# ) ( resid 15 and name HB2 ) 2.9 1.2 1.2 volume=1.680 peak=4590 ppm1=0.440 ppm2=1.366 assign ( resid 126 and name HG2# ) ( resid 124 and name HG2 ) 3.3 1.6 1.3 volume=0.789 peak=3243 ppm1=0.754 ppm2=2.364 assign ( resid 179 and name HD1# ) ( resid 178 and name HB1 or resid 178 and name HB2 ) 3.3 1.6 1.3 volume=0.770 peak=3619 ppm1=0.530 ppm2=1.689 assign ( resid 124 and name HG1 ) ( resid 154 and name HG2# ) 3.6 1.9 1.5 volume=0.458 peak=4234 ppm1=2.386 ppm2=0.892 assign ( resid 137 and name HN ) ( resid 134 and name HA ) 3.9 2.1 1.5 volume=0.322 peak=561 ppm1=8.051 ppm2=5.180 assign ( resid 207 and name HA ) ( resid 206 and name HN ) 3.7 2.0 1.5 volume=0.405 peak=4980 ppm1=4.168 ppm2=7.476 assign ( resid 144 and name HN ) ( resid 143 and name HN ) 3.6 1.8 1.4 volume=0.528 peak=2271 ppm1=7.537 ppm2=6.892 assign ( resid 117 and name HD1# ) ( resid 91 and name HN ) 4.1 2.4 1.6 volume=0.223 peak=5140 ppm1=0.244 ppm2=7.217 assign ( resid 196 and name HD1# ) ( resid 200 and name HE1 ) 4.4 2.7 1.6 volume=0.152 peak=2743 ppm1=0.727 ppm2=2.802 assign ( resid 15 and name HN ) ( resid 15 and name HA ) 3.1 1.4 1.2 volume=1.251 peak=956 ppm1=7.812 ppm2=3.626 assign ( resid 200 and name HG2 ) ( resid 200 and name HD1 ) 3.2 1.5 1.3 volume=0.938 peak=3351 ppm1=1.131 ppm2=1.554 assign ( resid 34 and name HB ) ( resid 34 and name HN ) 3.9 2.2 1.6 volume=0.287 peak=4219 ppm1=3.827 ppm2=8.137 assign ( resid 65 and name HG ) ( resid 65 and name HD1# ) 3.8 2.1 1.5 volume=0.342 peak=3458 ppm1=1.640 ppm2=0.174 assign ( resid 14 and name HA ) ( resid 14 and name HG2# ) 3.3 1.6 1.3 volume=0.801 peak=3799 ppm1=2.818 ppm2=0.759 assign ( resid 184 and name HG2# ) ( resid 179 and name HD2# ) 3.3 1.6 1.3 volume=0.863 peak=2617 ppm1=1.092 ppm2=0.727 assign ( resid 3 and name HN ) ( resid 3 and name HB1 or resid 3 and name HB2 ) 3.1 1.4 1.2 volume=1.187 peak=1627 ppm1=7.918 ppm2=2.988 assign ( resid 99 and name HA ) ( resid 98 and name HG2# ) 3.6 1.9 1.4 volume=0.498 peak=3372 ppm1=4.283 ppm2=1.335 assign ( resid 200 and name HB2 ) ( resid 197 and name HA ) 3.5 1.8 1.4 volume=0.583 peak=2562 ppm1=1.670 ppm2=3.842 assign ( resid 209 and name HD1 ) ( resid 208 and name HA ) 3.9 2.2 1.6 volume=0.303 peak=4510 ppm1=3.606 ppm2=4.417 assign ( resid 116 and name HA ) ( resid 7 and name HB# ) 4.2 2.5 1.7 volume=0.193 peak=3436 ppm1=6.164 ppm2=0.739 assign ( resid 165 and name HA ) ( resid 165 and name HN ) 4.3 2.6 1.7 volume=0.162 peak=4894 ppm1=5.242 ppm2=8.458 assign ( resid 28 and name HN ) ( resid 37 and name HN ) 3.6 1.9 1.5 volume=0.458 peak=1895 ppm1=7.809 ppm2=9.647 assign ( resid 183 and name HG2# ) ( resid 183 and name HG11 ) 2.8 1.0 1.1 volume=2.427 peak=3149 ppm1=0.933 ppm2=1.267 assign ( resid 93 and name HG11 ) ( resid 93 and name HG2# ) 3.9 2.2 1.6 volume=0.291 peak=3887 ppm1=0.690 ppm2=-0.016 assign ( resid 39 and name HA ) ( resid 39 and name HN ) 3.6 1.9 1.5 volume=0.461 peak=3261 ppm1=4.139 ppm2=8.252 assign ( resid 40 and name HN ) ( resid 46 and name HA ) 3.6 1.9 1.4 volume=0.517 peak=2217 ppm1=8.508 ppm2=4.916 assign ( resid 203 and name HG11 or resid 203 and name HG12 ) ( resid 203 and name HD1# ) 3.8 2.0 1.5 volume=0.384 peak=4302 ppm1=0.515 ppm2=-0.006 assign ( resid 91 and name HG2# ) ( resid 91 and name HN ) 4.1 2.4 1.7 volume=0.211 peak=4791 ppm1=1.017 ppm2=7.206 assign ( resid 18 and name HN ) ( resid 17 and name HB1 ) 2.8 1.1 1.1 volume=2.214 peak=659 ppm1=7.766 ppm2=2.841 assign ( resid 5 and name HB# ) ( resid 6 and name HN ) 3.2 1.5 1.3 volume=1.040 peak=3594 ppm1=1.341 ppm2=7.739 assign ( resid 147 and name HN ) ( resid 131 and name HB2 ) 3.9 2.2 1.6 volume=0.293 peak=1381 ppm1=8.785 ppm2=3.488 assign ( resid 74 and name HN ) ( resid 75 and name HN ) 3.1 1.4 1.2 volume=1.266 peak=1551 ppm1=6.492 ppm2=7.394 assign ( resid 162 and name HG2 ) ( resid 163 and name HN ) 3.3 1.6 1.3 volume=0.776 peak=2935 ppm1=1.919 ppm2=7.352 assign ( resid 72 and name HN ) ( resid 78 and name HD1# ) 2.7 1.0 1.1 volume=2.672 peak=931 ppm1=7.535 ppm2=0.490 assign ( resid 72 and name HD1# ) ( resid 72 and name HG12 ) 2.6 0.9 1.1 volume=3.122 peak=3819 ppm1=0.589 ppm2=1.036 assign ( resid 8 and name HB2 or resid 8 and name HB1 ) ( resid 5 and name HA ) 3.0 1.3 1.2 volume=1.436 peak=3543 ppm1=2.047 ppm2=3.971 assign ( resid 112 and name HN ) ( resid 112 and name HG11 ) 3.5 1.8 1.4 volume=0.571 peak=2158 ppm1=8.136 ppm2=1.614 assign ( resid 90 and name HN ) ( resid 89 and name HA ) 3.1 1.4 1.2 volume=1.177 peak=1704 ppm1=8.379 ppm2=4.188 assign ( resid 203 and name HG2# ) ( resid 199 and name HA ) 3.7 2.0 1.5 volume=0.398 peak=2633 ppm1=0.339 ppm2=2.769 assign ( resid 65 and name HD2# ) ( resid 127 and name HG11 or resid 127 and name HG12 ) 3.0 1.3 1.2 volume=1.441 peak=4417 ppm1=0.320 ppm2=1.031 assign ( resid 53 and name HD1# ) ( resid 166 and name HA ) 4.3 2.5 1.7 volume=0.178 peak=2773 ppm1=0.796 ppm2=4.457 assign ( resid 121 and name HN ) ( resid 122 and name HN ) 2.9 1.1 1.1 volume=1.941 peak=1770 ppm1=8.585 ppm2=8.673 assign ( resid 129 and name HN ) ( resid 128 and name HN ) 3.9 2.2 1.6 volume=0.308 peak=2245 ppm1=8.723 ppm2=9.964 assign ( resid 200 and name HN ) ( resid 200 and name HA ) 2.8 1.1 1.1 volume=2.160 peak=1145 ppm1=8.085 ppm2=3.359 assign ( resid 35 and name HG2# ) ( resid 28 and name HN ) 3.6 1.9 1.5 volume=0.464 peak=4911 ppm1=0.888 ppm2=7.808 assign ( resid 99 and name HB2 ) ( resid 99 and name HG1 ) 3.1 1.4 1.2 volume=1.160 peak=3502 ppm1=1.791 ppm2=2.439 assign ( resid 20 and name HN ) ( resid 20 and name HB1 ) 2.7 1.0 1.1 volume=2.653 peak=2351 ppm1=7.404 ppm2=2.708 assign ( resid 208 and name HG2# ) ( resid 212 and name HN ) 4.4 2.6 1.6 volume=0.157 peak=4662 ppm1=1.137 ppm2=8.236 assign ( resid 166 and name HE2 ) ( resid 168 and name HG1# ) 3.3 1.6 1.3 volume=0.810 peak=4352 ppm1=2.710 ppm2=0.762 assign ( resid 71 and name HB2 ) ( resid 71 and name HN ) 4.8 3.1 1.2 volume=0.090 peak=2722 ppm1=1.528 ppm2=7.217 assign ( resid 113 and name HB2 ) ( resid 113 and name HN ) 4.2 2.4 1.7 volume=0.204 peak=4775 ppm1=2.040 ppm2=8.256 assign ( resid 53 and name HN ) ( resid 52 and name HN ) 3.3 1.5 1.3 volume=0.887 peak=242 ppm1=8.309 ppm2=8.620 assign ( resid 188 and name HB1 ) ( resid 188 and name HA ) 4.0 2.3 1.6 volume=0.258 peak=5112 ppm1=1.447 ppm2=4.190 assign ( resid 198 and name HN ) ( resid 74 and name HZ1 ) 4.0 2.3 1.6 volume=0.245 peak=1935 ppm1=8.717 ppm2=5.962 assign ( resid 158 and name HN ) ( resid 161 and name HN ) 4.1 2.4 1.7 volume=0.212 peak=1811 ppm1=8.215 ppm2=6.869 assign ( resid 10 and name HB ) ( resid 13 and name HG2 or resid 13 and name HG1 ) 3.7 2.0 1.5 volume=0.426 peak=3766 ppm1=3.687 ppm2=2.069 assign ( resid 91 and name HN ) ( resid 90 and name HB2 ) 3.5 1.8 1.4 volume=0.581 peak=466 ppm1=7.215 ppm2=3.349 assign ( resid 134 and name HZ ) ( resid 137 and name HN ) 3.3 1.6 1.3 volume=0.797 peak=37 ppm1=6.644 ppm2=8.060 assign ( resid 99 and name HG1 ) ( resid 97 and name HG2# ) 3.9 2.2 1.6 volume=0.308 peak=2632 ppm1=2.439 ppm2=0.249 assign ( resid 214 and name HA ) ( resid 214 and name HB2 ) 3.0 1.2 1.2 volume=1.583 peak=3238 ppm1=4.434 ppm2=2.860 assign ( resid 203 and name HA ) ( resid 203 and name HN ) 4.7 2.9 1.3 volume=0.106 peak=3919 ppm1=2.831 ppm2=7.684 assign ( resid 191 and name HN ) ( resid 192 and name HN ) 3.3 1.5 1.3 volume=0.891 peak=1397 ppm1=7.652 ppm2=8.178 assign ( resid 208 and name HB ) ( resid 209 and name HD2 or resid 209 and name HD1 ) 3.2 1.5 1.3 volume=0.941 peak=3928 ppm1=4.031 ppm2=3.571 assign ( resid 144 and name HN ) ( resid 109 and name HG2 ) 3.1 1.4 1.3 volume=1.118 peak=1554 ppm1=7.536 ppm2=1.534 assign ( resid 116 and name HN ) ( resid 11 and name HB# ) 3.5 1.8 1.4 volume=0.537 peak=2096 ppm1=8.835 ppm2=1.636 assign ( resid 200 and name HN ) ( resid 198 and name HN ) 3.2 1.4 1.3 volume=1.067 peak=243 ppm1=8.085 ppm2=8.735 assign ( resid 142 and name HN ) ( resid 140 and name HA ) 3.7 2.0 1.5 volume=0.425 peak=1831 ppm1=7.898 ppm2=4.803 assign ( resid 10 and name HG2# ) ( resid 11 and name HB# ) 3.7 1.9 1.5 volume=0.445 peak=4468 ppm1=1.085 ppm2=1.618 assign ( resid 91 and name HN ) ( resid 87 and name HB ) 3.5 1.8 1.4 volume=0.574 peak=2395 ppm1=7.218 ppm2=1.377 assign ( resid 72 and name HD1# ) ( resid 81 and name HB1 or resid 81 and name HB2 ) 3.8 2.1 1.5 volume=0.373 peak=3807 ppm1=0.589 ppm2=2.337 assign ( resid 34 and name HG2# ) ( resid 33 and name HA ) 3.6 1.9 1.4 volume=0.474 peak=5041 ppm1=1.102 ppm2=4.673 assign ( resid 6 and name HN ) ( resid 5 and name HB# ) 3.0 1.3 1.2 volume=1.398 peak=1080 ppm1=7.723 ppm2=1.339 assign ( resid 161 and name HN ) ( resid 159 and name HA ) 3.0 1.2 1.2 volume=1.579 peak=996 ppm1=6.904 ppm2=3.748 assign ( resid 130 and name HN ) ( resid 129 and name HA ) 3.0 1.3 1.2 volume=1.515 peak=507 ppm1=7.616 ppm2=5.705 assign ( resid 10 and name HG2# ) ( resid 13 and name HB2 or resid 13 and name HB1 ) 2.6 0.9 1.1 volume=3.194 peak=4730 ppm1=1.084 ppm2=1.878 assign ( resid 81 and name HN ) ( resid 68 and name HA ) 3.7 2.0 1.5 volume=0.403 peak=200 ppm1=8.509 ppm2=4.269 assign ( resid 88 and name HN ) ( resid 91 and name HG2# ) 3.1 1.4 1.2 volume=1.191 peak=225 ppm1=8.595 ppm2=1.004 assign ( resid 164 and name HN ) ( resid 158 and name HB2 ) 3.3 1.5 1.3 volume=0.906 peak=1400 ppm1=7.976 ppm2=2.184 assign ( resid 183 and name HB ) ( resid 183 and name HG12 ) 2.8 1.1 1.1 volume=2.169 peak=3737 ppm1=1.977 ppm2=1.542 assign ( resid 80 and name HA ) ( resid 80 and name HG1# ) 2.8 1.1 1.1 volume=2.318 peak=5006 ppm1=3.984 ppm2=0.706 assign ( resid 18 and name HN ) ( resid 168 and name HG2# ) 3.3 1.6 1.3 volume=0.866 peak=260 ppm1=7.766 ppm2=0.200 assign ( resid 117 and name HB ) ( resid 117 and name HG11 ) 4.1 2.4 1.6 volume=0.223 peak=4076 ppm1=1.037 ppm2=0.710 assign ( resid 126 and name HD1# ) ( resid 126 and name HB ) 3.6 1.8 1.4 volume=0.526 peak=3291 ppm1=0.348 ppm2=1.594 assign ( resid 120 and name HN ) ( resid 124 and name HB1 ) 3.7 2.0 1.5 volume=0.413 peak=2435 ppm1=8.916 ppm2=2.079 assign ( resid 169 and name HG1 ) ( resid 153 and name HN ) 4.4 2.6 1.6 volume=0.158 peak=5082 ppm1=1.933 ppm2=9.362 assign ( resid 168 and name HG2# ) ( resid 166 and name HG1 ) 3.8 2.1 1.5 volume=0.340 peak=4939 ppm1=0.200 ppm2=1.158 assign ( resid 196 and name HN ) ( resid 196 and name HG12 ) 3.0 1.2 1.2 volume=1.575 peak=1478 ppm1=7.438 ppm2=1.402 assign ( resid 87 and name HG12 ) ( resid 93 and name HD1# ) 4.1 2.4 1.7 volume=0.214 peak=3442 ppm1=1.050 ppm2=-0.279 assign ( resid 24 and name HZ1 ) ( resid 49 and name HN ) 3.8 2.1 1.5 volume=0.352 peak=91 ppm1=6.998 ppm2=9.001 assign ( resid 107 and name HN ) ( resid 106 and name HA ) 3.3 1.6 1.3 volume=0.813 peak=1514 ppm1=8.395 ppm2=4.134 assign ( resid 151 and name HN ) ( resid 149 and name HA ) 3.3 1.6 1.3 volume=0.788 peak=2181 ppm1=8.646 ppm2=4.518 assign ( resid 154 and name HG1# ) ( resid 127 and name HN ) 3.2 1.5 1.3 volume=1.010 peak=3190 ppm1=0.910 ppm2=9.377 assign ( resid 3 and name HE1 or resid 3 and name HE2 ) ( resid 93 and name HD1# ) 3.4 1.7 1.4 volume=0.707 peak=46 ppm1=7.213 ppm2=-0.281 assign ( resid 93 and name HG12 ) ( resid 93 and name HG2# ) 3.9 2.1 1.5 volume=0.325 peak=3345 ppm1=0.598 ppm2=-0.014 assign ( resid 15 and name HN ) ( resid 15 and name HB1 ) 2.8 1.1 1.1 volume=2.012 peak=1487 ppm1=7.811 ppm2=1.718 assign ( resid 26 and name HA ) ( resid 27 and name HN ) 4.3 2.6 1.7 volume=0.160 peak=2475 ppm1=3.979 ppm2=9.303 assign ( resid 79 and name HN ) ( resid 80 and name HN ) 3.6 1.9 1.5 volume=0.473 peak=1962 ppm1=8.843 ppm2=7.528 assign ( resid 37 and name HA ) ( resid 49 and name HN ) 4.0 2.3 1.6 volume=0.257 peak=3861 ppm1=5.822 ppm2=8.928 assign ( resid 183 and name HG11 ) ( resid 183 and name HN ) 3.9 2.2 1.6 volume=0.304 peak=3413 ppm1=1.267 ppm2=7.457 assign ( resid 192 and name HD2# ) ( resid 171 and name HG2# ) 3.1 1.3 1.2 volume=1.334 peak=4319 ppm1=0.492 ppm2=0.802 assign ( resid 195 and name HN ) ( resid 195 and name HA ) 3.0 1.3 1.2 volume=1.448 peak=900 ppm1=7.971 ppm2=4.442 assign ( resid 154 and name HG2# ) ( resid 168 and name HN ) 3.7 2.0 1.5 volume=0.393 peak=4638 ppm1=0.838 ppm2=8.711 assign ( resid 72 and name HN ) ( resid 71 and name HG2 ) 3.8 2.1 1.5 volume=0.369 peak=1688 ppm1=7.535 ppm2=0.273 assign ( resid 199 and name HA ) ( resid 64 and name HE1 or resid 64 and name HE2 ) 4.2 2.5 1.7 volume=0.193 peak=2789 ppm1=2.796 ppm2=6.508 assign ( resid 29 and name HA ) ( resid 29 and name HG2# ) 4.6 2.9 1.4 volume=0.117 peak=4524 ppm1=5.248 ppm2=1.072 assign ( resid 176 and name HN ) ( resid 144 and name HG2# ) 4.0 2.3 1.6 volume=0.254 peak=1573 ppm1=8.404 ppm2=0.755 assign ( resid 187 and name HN ) ( resid 106 and name HD1# ) 3.7 2.0 1.5 volume=0.410 peak=730 ppm1=7.600 ppm2=0.785 assign ( resid 53 and name HD1# ) ( resid 53 and name HG11 ) 2.6 0.9 1.0 volume=3.311 peak=4837 ppm1=0.796 ppm2=1.268 assign ( resid 3 and name HD1 or resid 3 and name HD2 ) ( resid 87 and name HD1# ) 3.5 1.7 1.4 volume=0.625 peak=136 ppm1=7.380 ppm2=0.435 assign ( resid 132 and name HG2# ) ( resid 134 and name HN ) 3.5 1.8 1.4 volume=0.584 peak=3483 ppm1=0.936 ppm2=8.784 assign ( resid 29 and name HN ) ( resid 29 and name HB ) 3.5 1.7 1.4 volume=0.625 peak=514 ppm1=8.568 ppm2=3.879 assign ( resid 84 and name HG1# ) ( resid 84 and name HG2# ) 2.8 1.0 1.1 volume=2.422 peak=3788 ppm1=0.534 ppm2=0.109 assign ( resid 92 and name HE1 or resid 92 and name HE2 ) ( resid 117 and name HD1# ) 2.9 1.2 1.1 volume=1.913 peak=41 ppm1=6.750 ppm2=0.257 assign ( resid 175 and name HB2 ) ( resid 174 and name HG1 ) 4.0 2.2 1.6 volume=0.279 peak=3057 ppm1=2.450 ppm2=2.201 assign ( resid 114 and name HN ) ( resid 132 and name HG2# ) 3.2 1.5 1.3 volume=0.913 peak=1151 ppm1=8.799 ppm2=0.904 assign ( resid 107 and name HN ) ( resid 107 and name HB1 ) 3.3 1.6 1.3 volume=0.794 peak=849 ppm1=8.396 ppm2=3.876 assign ( resid 169 and name HN ) ( resid 50 and name HG1# ) 3.5 1.8 1.4 volume=0.566 peak=2237 ppm1=9.256 ppm2=0.675 assign ( resid 193 and name HB ) ( resid 193 and name HA ) 4.3 2.6 1.7 volume=0.160 peak=3915 ppm1=2.056 ppm2=3.462 assign ( resid 187 and name HG2# ) ( resid 191 and name HB2 ) 3.5 1.7 1.4 volume=0.629 peak=3646 ppm1=1.061 ppm2=2.845 assign ( resid 77 and name HB1 ) ( resid 78 and name HG ) 2.9 1.2 1.2 volume=1.774 peak=4421 ppm1=3.888 ppm2=1.234 assign ( resid 60 and name HG1 ) ( resid 60 and name HA ) 4.0 2.3 1.6 volume=0.269 peak=4016 ppm1=1.324 ppm2=3.878 assign ( resid 43 and name HN ) ( resid 43 and name HB2 ) 3.0 1.2 1.2 volume=1.592 peak=246 ppm1=7.303 ppm2=2.838 assign ( resid 195 and name HN ) ( resid 194 and name HN ) 3.2 1.5 1.3 volume=0.963 peak=2078 ppm1=7.971 ppm2=7.787 assign ( resid 40 and name HA ) ( resid 172 and name HG1 ) 3.1 1.4 1.3 volume=1.112 peak=3418 ppm1=3.988 ppm2=2.395 assign ( resid 198 and name HN ) ( resid 197 and name HB2 ) 3.0 1.3 1.2 volume=1.467 peak=1024 ppm1=8.718 ppm2=1.794 assign ( resid 8 and name HN ) ( resid 91 and name HG2# ) 3.1 1.4 1.2 volume=1.260 peak=2400 ppm1=7.611 ppm2=1.009 assign ( resid 76 and name HN ) ( resid 76 and name HG1 ) 2.8 1.1 1.1 volume=2.004 peak=1531 ppm1=6.699 ppm2=1.403 assign ( resid 170 and name HN ) ( resid 171 and name HG1# ) 3.9 2.2 1.6 volume=0.284 peak=1117 ppm1=9.145 ppm2=0.873 assign ( resid 74 and name HN ) ( resid 75 and name HB1 ) 3.0 1.3 1.2 volume=1.424 peak=1593 ppm1=6.493 ppm2=2.835 assign ( resid 203 and name HG2# ) ( resid 56 and name HG2 or resid 56 and name HG1 ) 3.6 1.9 1.4 volume=0.503 peak=4001 ppm1=0.340 ppm2=1.984 assign ( resid 93 and name HD1# ) ( resid 132 and name HB ) 3.4 1.7 1.4 volume=0.720 peak=4841 ppm1=-0.272 ppm2=2.216 assign ( resid 85 and name HN ) ( resid 93 and name HN ) 3.5 1.8 1.4 volume=0.597 peak=2345 ppm1=7.153 ppm2=8.958 assign ( resid 134 and name HE1 or resid 134 and name HE2 ) ( resid 112 and name HB ) 2.7 1.0 1.1 volume=2.491 peak=120 ppm1=7.140 ppm2=2.171 assign ( resid 73 and name HN ) ( resid 74 and name HD1 ) 3.7 2.0 1.5 volume=0.432 peak=1784 ppm1=7.505 ppm2=6.902 assign ( resid 136 and name HN ) ( resid 136 and name HB2 ) 2.8 1.0 1.1 volume=2.447 peak=1738 ppm1=6.890 ppm2=1.917 assign ( resid 91 and name HN ) ( resid 86 and name HA ) 3.8 2.1 1.5 volume=0.369 peak=2172 ppm1=7.218 ppm2=4.274 assign ( resid 128 and name HN ) ( resid 127 and name HN ) 4.1 2.4 1.6 volume=0.236 peak=296 ppm1=9.933 ppm2=9.374 assign ( resid 102 and name HB# ) ( resid 104 and name HA2 ) 4.4 2.6 1.6 volume=0.156 peak=3863 ppm1=1.278 ppm2=3.504 assign ( resid 183 and name HA ) ( resid 183 and name HG2# ) 2.7 0.9 1.1 volume=3.003 peak=3444 ppm1=3.919 ppm2=0.923 assign ( resid 36 and name HN ) ( resid 35 and name HG2# or resid 35 and name HG1# ) 2.7 1.0 1.1 volume=2.568 peak=1677 ppm1=9.878 ppm2=0.886 assign ( resid 132 and name HN ) ( resid 131 and name HB1 or resid 131 and name HB2 ) 3.5 1.8 1.4 volume=0.590 peak=1761 ppm1=7.893 ppm2=3.484 assign ( resid 134 and name HE1 or resid 134 and name HE2 ) ( resid 112 and name HD1# ) 3.1 1.4 1.2 volume=1.282 peak=97 ppm1=7.140 ppm2=0.368 assign ( resid 99 and name HG2 ) ( resid 99 and name HA ) 3.1 1.4 1.2 volume=1.262 peak=3415 ppm1=2.437 ppm2=4.286 assign ( resid 54 and name HN ) ( resid 166 and name HA ) 3.3 1.6 1.3 volume=0.808 peak=329 ppm1=9.023 ppm2=4.448 assign ( resid 193 and name HG2# ) ( resid 33 and name HD1# ) 2.6 0.9 1.0 volume=3.510 peak=4491 ppm1=0.783 ppm2=0.389 assign ( resid 167 and name HD2# ) ( resid 168 and name HN ) 3.9 2.2 1.6 volume=0.287 peak=2587 ppm1=0.764 ppm2=8.717 assign ( resid 130 and name HD2 ) ( resid 10 and name HN ) 3.6 1.9 1.4 volume=0.507 peak=4363 ppm1=1.659 ppm2=8.326 assign ( resid 145 and name HN ) ( resid 110 and name HN ) 4.0 2.3 1.6 volume=0.247 peak=2302 ppm1=8.381 ppm2=8.703 assign ( resid 79 and name HB2 ) ( resid 97 and name HG2# ) 3.1 1.3 1.2 volume=1.317 peak=3495 ppm1=1.779 ppm2=0.240 assign ( resid 3 and name HN ) ( resid 5 and name HB# ) 3.3 1.6 1.3 volume=0.769 peak=781 ppm1=7.913 ppm2=1.291 assign ( resid 3 and name HE1 or resid 3 and name HE2 ) ( resid 2 and name HB1 ) 3.3 1.6 1.3 volume=0.775 peak=131 ppm1=7.212 ppm2=2.853 assign ( resid 144 and name HN ) ( resid 110 and name HA ) 3.7 1.9 1.5 volume=0.445 peak=833 ppm1=7.536 ppm2=5.438 assign ( resid 198 and name HN ) ( resid 198 and name HA ) 2.9 1.2 1.2 volume=1.735 peak=1493 ppm1=8.716 ppm2=4.530 assign ( resid 182 and name HB2 ) ( resid 182 and name HA ) 3.7 2.0 1.5 volume=0.403 peak=3104 ppm1=3.880 ppm2=4.131 assign ( resid 203 and name HD1# ) ( resid 203 and name HB ) 2.7 0.9 1.1 volume=2.982 peak=5069 ppm1=-0.010 ppm2=0.125 assign ( resid 197 and name HA ) ( resid 197 and name HG ) 3.3 1.6 1.3 volume=0.802 peak=3385 ppm1=3.793 ppm2=1.276 assign ( resid 192 and name HN ) ( resid 190 and name HN ) 3.4 1.7 1.4 volume=0.677 peak=546 ppm1=8.209 ppm2=7.517 assign ( resid 166 and name HG2 ) ( resid 166 and name HB2 ) 2.6 0.8 1.0 volume=3.848 peak=4252 ppm1=1.253 ppm2=1.657 assign ( resid 166 and name HD1 ) ( resid 168 and name HG1# ) 3.8 2.0 1.5 volume=0.377 peak=3993 ppm1=1.468 ppm2=0.771 assign ( resid 50 and name HN ) ( resid 35 and name HG2# or resid 35 and name HG1# ) 3.1 1.3 1.2 volume=1.288 peak=2193 ppm1=9.302 ppm2=0.881 assign ( resid 11 and name HN ) ( resid 11 and name HB# ) 2.7 0.9 1.1 volume=3.090 peak=1857 ppm1=8.181 ppm2=1.662 assign ( resid 87 and name HG2# ) ( resid 87 and name HG12 ) 2.9 1.1 1.1 volume=1.996 peak=3145 ppm1=0.852 ppm2=1.047 assign ( resid 164 and name HN ) ( resid 160 and name HA ) 3.3 1.5 1.3 volume=0.908 peak=1434 ppm1=7.977 ppm2=4.015 assign ( resid 96 and name HN ) ( resid 95 and name HN ) 4.1 2.4 1.6 volume=0.223 peak=2362 ppm1=8.473 ppm2=9.149 assign ( resid 80 and name HG1# ) ( resid 80 and name HB ) 2.7 1.0 1.1 volume=2.575 peak=2648 ppm1=0.707 ppm2=1.397 assign ( resid 140 and name HN ) ( resid 141 and name HA ) 3.3 1.6 1.3 volume=0.858 peak=2214 ppm1=9.582 ppm2=3.875 assign ( resid 75 and name HA ) ( resid 78 and name HN ) 3.5 1.8 1.4 volume=0.556 peak=3005 ppm1=4.153 ppm2=7.154 assign ( resid 7 and name HB# ) ( resid 114 and name HD1# ) 3.0 1.3 1.2 volume=1.464 peak=4751 ppm1=0.751 ppm2=0.544 assign ( resid 187 and name HA ) ( resid 187 and name HN ) 5.2 3.5 0.8 volume=0.056 peak=4414 ppm1=4.263 ppm2=7.600 assign ( resid 203 and name HD1# ) ( resid 56 and name HG2 ) 3.4 1.7 1.4 volume=0.683 peak=4216 ppm1=-0.010 ppm2=2.004 assign ( resid 29 and name HG2# ) ( resid 29 and name HA ) 4.1 2.4 1.6 volume=0.223 peak=3309 ppm1=1.067 ppm2=5.251 assign ( resid 8 and name HB2 or resid 8 and name HB1 ) ( resid 9 and name HG2 or resid 9 and name HG1 ) 2.5 0.8 1.0 volume=4.485 peak=4039 ppm1=2.046 ppm2=2.405 assign ( resid 134 and name HZ ) ( resid 93 and name HB ) 3.0 1.3 1.2 volume=1.430 peak=43 ppm1=6.644 ppm2=1.215 assign ( resid 203 and name HN ) ( resid 203 and name HA ) 2.8 1.1 1.1 volume=2.229 peak=335 ppm1=7.685 ppm2=2.840 assign ( resid 130 and name HD2 ) ( resid 130 and name HG2 ) 2.6 0.9 1.0 volume=3.414 peak=4533 ppm1=1.658 ppm2=1.314 assign ( resid 75 and name HA ) ( resid 75 and name HB2 ) 4.2 2.5 1.7 volume=0.199 peak=2948 ppm1=4.152 ppm2=2.845 assign ( resid 145 and name HN ) ( resid 144 and name HG2# ) 3.1 1.4 1.2 volume=1.189 peak=325 ppm1=8.380 ppm2=0.748 assign ( resid 168 and name HA ) ( resid 51 and name HB2 ) 4.3 2.6 1.7 volume=0.170 peak=2863 ppm1=4.810 ppm2=1.811 assign ( resid 38 and name HN ) ( resid 39 and name HN ) 3.9 2.2 1.6 volume=0.292 peak=454 ppm1=8.467 ppm2=8.206 assign ( resid 143 and name HN ) ( resid 142 and name HA ) 2.7 1.0 1.1 volume=2.522 peak=1505 ppm1=6.899 ppm2=4.135 assign ( resid 70 and name HN ) ( resid 70 and name HB2 ) 3.0 1.2 1.2 volume=1.610 peak=168 ppm1=8.575 ppm2=2.572 assign ( resid 96 and name HN ) ( resid 110 and name HA ) 3.9 2.2 1.6 volume=0.298 peak=2340 ppm1=8.473 ppm2=5.447 assign ( resid 114 and name HB1 ) ( resid 114 and name HD2# ) 3.3 1.6 1.3 volume=0.770 peak=3827 ppm1=1.063 ppm2=0.778 assign ( resid 200 and name HD1 ) ( resid 200 and name HN ) 3.5 1.8 1.4 volume=0.555 peak=4594 ppm1=1.547 ppm2=8.085 assign ( resid 201 and name HB2 ) ( resid 201 and name HA ) 3.9 2.2 1.5 volume=0.320 peak=2545 ppm1=2.581 ppm2=4.330 assign ( resid 207 and name HG1 ) ( resid 207 and name HA ) 3.3 1.6 1.3 volume=0.767 peak=3911 ppm1=1.471 ppm2=4.187 assign ( resid 125 and name HN ) ( resid 156 and name HN ) 3.4 1.7 1.4 volume=0.639 peak=321 ppm1=8.772 ppm2=8.551 assign ( resid 183 and name HN ) ( resid 184 and name HN ) 2.6 0.9 1.0 volume=3.347 peak=410 ppm1=7.418 ppm2=7.517 assign ( resid 203 and name HG2# ) ( resid 56 and name HN ) 3.8 2.1 1.5 volume=0.339 peak=3841 ppm1=0.338 ppm2=8.637 assign ( resid 100 and name HN ) ( resid 100 and name HB2 ) 3.4 1.7 1.4 volume=0.658 peak=1538 ppm1=8.397 ppm2=3.735 assign ( resid 196 and name HB ) ( resid 196 and name HN ) 4.1 2.4 1.6 volume=0.231 peak=4265 ppm1=2.253 ppm2=7.475 assign ( resid 70 and name HN ) ( resid 72 and name HN ) 3.5 1.8 1.4 volume=0.557 peak=630 ppm1=8.575 ppm2=7.516 assign ( resid 105 and name HB2 ) ( resid 183 and name HG2# ) 3.2 1.5 1.3 volume=1.023 peak=4460 ppm1=3.871 ppm2=1.019 assign ( resid 166 and name HN ) ( resid 166 and name HG2 ) 3.1 1.4 1.2 volume=1.235 peak=383 ppm1=9.000 ppm2=1.211 assign ( resid 72 and name HG2# ) ( resid 71 and name HN ) 3.9 2.2 1.6 volume=0.298 peak=2671 ppm1=0.602 ppm2=7.209 assign ( resid 186 and name HE2 ) ( resid 186 and name HG1 ) 2.3 0.6 0.9 volume=6.617 peak=3489 ppm1=2.955 ppm2=1.478 assign ( resid 167 and name HB1 ) ( resid 168 and name HN ) 4.6 2.9 1.4 volume=0.117 peak=4557 ppm1=1.680 ppm2=8.759 assign ( resid 22 and name HB2 or resid 22 and name HB1 ) ( resid 22 and name HN ) 3.7 2.0 1.5 volume=0.429 peak=3299 ppm1=3.770 ppm2=8.194 assign ( resid 166 and name HD2 ) ( resid 166 and name HE2 ) 3.9 2.2 1.6 volume=0.290 peak=2958 ppm1=1.426 ppm2=2.712 assign ( resid 91 and name HG2# ) ( resid 93 and name HG2# ) 4.3 2.6 1.7 volume=0.162 peak=3622 ppm1=1.017 ppm2=-0.011 assign ( resid 166 and name HG1 ) ( resid 166 and name HN ) 3.7 2.0 1.5 volume=0.411 peak=4012 ppm1=1.212 ppm2=9.005 assign ( resid 125 and name HN ) ( resid 155 and name HN ) 3.4 1.6 1.3 volume=0.755 peak=2445 ppm1=8.772 ppm2=8.979 assign ( resid 124 and name HN ) ( resid 120 and name HN ) 3.5 1.8 1.4 volume=0.575 peak=2361 ppm1=6.472 ppm2=8.917 assign ( resid 86 and name HA ) ( resid 92 and name HB1 ) 3.7 2.0 1.5 volume=0.433 peak=2880 ppm1=4.287 ppm2=3.051 assign ( resid 112 and name HD1# ) ( resid 112 and name HB ) 4.0 2.3 1.6 volume=0.248 peak=2891 ppm1=0.372 ppm2=2.143 assign ( resid 100 and name HN ) ( resid 99 and name HA ) 3.1 1.4 1.2 volume=1.264 peak=1648 ppm1=8.396 ppm2=4.269 assign ( resid 123 and name HB1 or resid 123 and name HB2 ) ( resid 119 and name HD1 ) 4.1 2.4 1.6 volume=0.228 peak=4647 ppm1=2.740 ppm2=2.986 assign ( resid 62 and name HA ) ( resid 65 and name HD1# ) 3.4 1.7 1.4 volume=0.662 peak=4781 ppm1=3.965 ppm2=0.201 assign ( resid 72 and name HB ) ( resid 72 and name HD1# ) 2.8 1.1 1.1 volume=2.282 peak=3593 ppm1=1.855 ppm2=0.588 assign ( resid 76 and name HN ) ( resid 76 and name HE2 ) 3.7 2.0 1.5 volume=0.419 peak=2288 ppm1=6.699 ppm2=2.961 assign ( resid 31 and name HN ) ( resid 30 and name HA ) 3.7 2.0 1.5 volume=0.401 peak=1443 ppm1=9.252 ppm2=4.654 assign ( resid 35 and name HN ) ( resid 28 and name HA ) 4.2 2.5 1.7 volume=0.197 peak=785 ppm1=9.431 ppm2=4.399 assign ( resid 87 and name HN ) ( resid 88 and name HN ) 4.0 2.3 1.6 volume=0.245 peak=195 ppm1=8.039 ppm2=8.660 assign ( resid 85 and name HN ) ( resid 84 and name HG1# ) 2.9 1.2 1.2 volume=1.687 peak=1497 ppm1=7.153 ppm2=0.518 assign ( resid 183 and name HG11 ) ( resid 183 and name HB ) 3.5 1.8 1.4 volume=0.567 peak=4486 ppm1=1.267 ppm2=1.977 assign ( resid 102 and name HA ) ( resid 105 and name HN ) 3.7 1.9 1.5 volume=0.450 peak=2777 ppm1=4.117 ppm2=7.997 assign ( resid 183 and name HN ) ( resid 183 and name HG11 ) 2.8 1.1 1.1 volume=2.323 peak=555 ppm1=7.419 ppm2=1.277 assign ( resid 70 and name HN ) ( resid 71 and name HB2 ) 2.9 1.1 1.1 volume=1.999 peak=1834 ppm1=8.574 ppm2=1.526 assign ( resid 3 and name HE1 or resid 3 and name HE2 ) ( resid 85 and name HB1 ) 3.3 1.6 1.3 volume=0.789 peak=149 ppm1=7.213 ppm2=3.137 assign ( resid 152 and name HN ) ( resid 151 and name HB2 ) 3.1 1.4 1.2 volume=1.194 peak=2199 ppm1=8.345 ppm2=2.972 assign ( resid 176 and name HA ) ( resid 177 and name HN ) 3.7 2.0 1.5 volume=0.430 peak=5000 ppm1=3.996 ppm2=8.482 assign ( resid 111 and name HN ) ( resid 95 and name HA ) 3.4 1.6 1.3 volume=0.740 peak=1726 ppm1=8.632 ppm2=5.578 assign ( resid 26 and name HB ) ( resid 26 and name HG2# ) 2.7 1.0 1.1 volume=2.795 peak=3223 ppm1=1.924 ppm2=0.908 assign ( resid 115 and name HG1# ) ( resid 114 and name HB2 ) 3.6 1.9 1.4 volume=0.486 peak=4512 ppm1=0.303 ppm2=1.686 assign ( resid 134 and name HN ) ( resid 112 and name HG2# ) 3.1 1.4 1.2 volume=1.190 peak=963 ppm1=8.745 ppm2=0.682 assign ( resid 74 and name HH2 ) ( resid 74 and name HZ1 ) 3.3 1.5 1.3 volume=0.882 peak=70 ppm1=6.509 ppm2=5.952 assign ( resid 54 and name HG2# ) ( resid 56 and name HG2 ) 3.6 1.9 1.4 volume=0.495 peak=4346 ppm1=0.576 ppm2=2.003 assign ( resid 192 and name HD1# ) ( resid 192 and name HG ) 3.4 1.7 1.4 volume=0.659 peak=2779 ppm1=0.493 ppm2=1.754 assign ( resid 54 and name HG2# ) ( resid 54 and name HG11 or resid 54 and name HG12 ) 2.8 1.1 1.1 volume=2.035 peak=4550 ppm1=0.577 ppm2=1.161 assign ( resid 119 and name HN ) ( resid 119 and name HD2 ) 3.5 1.7 1.4 volume=0.617 peak=562 ppm1=8.056 ppm2=2.964 assign ( resid 127 and name HN ) ( resid 127 and name HA ) 4.1 2.3 1.6 volume=0.243 peak=288 ppm1=9.383 ppm2=5.057 assign ( resid 76 and name HD2 ) ( resid 76 and name HE2 ) 4.1 2.3 1.6 volume=0.242 peak=4534 ppm1=1.551 ppm2=2.917 assign ( resid 204 and name HA ) ( resid 203 and name HA ) 3.7 2.0 1.5 volume=0.438 peak=3256 ppm1=3.800 ppm2=2.839 assign ( resid 152 and name HN ) ( resid 14 and name HG2# ) 3.3 1.6 1.3 volume=0.839 peak=1102 ppm1=8.344 ppm2=0.752 assign ( resid 183 and name HG12 ) ( resid 183 and name HG11 ) 2.1 0.4 0.9 volume=11.549 peak=4679 ppm1=1.541 ppm2=1.270 assign ( resid 35 and name HG2# ) ( resid 27 and name HN ) 3.6 1.8 1.4 volume=0.528 peak=3676 ppm1=0.889 ppm2=9.297 assign ( resid 203 and name HG2# ) ( resid 61 and name HN ) 4.2 2.5 1.7 volume=0.201 peak=4152 ppm1=0.340 ppm2=8.707 assign ( resid 115 and name HG2# ) ( resid 127 and name HA ) 3.2 1.5 1.3 volume=0.945 peak=2768 ppm1=0.659 ppm2=5.073 assign ( resid 207 and name HD2 ) ( resid 207 and name HA ) 3.4 1.6 1.3 volume=0.746 peak=4487 ppm1=3.047 ppm2=4.179 assign ( resid 126 and name HN ) ( resid 155 and name HB2 ) 3.7 2.0 1.5 volume=0.420 peak=1135 ppm1=9.104 ppm2=2.567 assign ( resid 135 and name HB2 ) ( resid 136 and name HA ) 3.2 1.5 1.3 volume=0.949 peak=3600 ppm1=2.188 ppm2=3.760 assign ( resid 135 and name HG1 ) ( resid 134 and name HA ) 4.6 2.9 1.4 volume=0.116 peak=2643 ppm1=1.787 ppm2=5.223 assign ( resid 168 and name HN ) ( resid 169 and name HN ) 4.2 2.4 1.7 volume=0.204 peak=2142 ppm1=8.694 ppm2=9.268 assign ( resid 65 and name HN ) ( resid 65 and name HB1 or resid 65 and name HB2 ) 3.1 1.4 1.2 volume=1.236 peak=1033 ppm1=7.744 ppm2=1.650 assign ( resid 166 and name HN ) ( resid 158 and name HA ) 3.4 1.7 1.4 volume=0.724 peak=832 ppm1=9.000 ppm2=4.137 assign ( resid 192 and name HG ) ( resid 192 and name HA ) 2.9 1.2 1.2 volume=1.632 peak=4858 ppm1=1.754 ppm2=4.148 assign ( resid 72 and name HA ) ( resid 72 and name HN ) 3.8 2.1 1.5 volume=0.361 peak=5008 ppm1=3.631 ppm2=7.537 assign ( resid 186 and name HN ) ( resid 186 and name HG1 ) 2.7 0.9 1.1 volume=3.077 peak=1372 ppm1=7.370 ppm2=1.533 assign ( resid 51 and name HN ) ( resid 196 and name HD1# ) 2.2 0.5 0.9 volume=8.677 peak=776 ppm1=8.432 ppm2=0.751 assign ( resid 99 and name HN ) ( resid 99 and name HB2 or resid 99 and name HB1 ) 3.1 1.4 1.2 volume=1.196 peak=819 ppm1=7.803 ppm2=1.787 assign ( resid 42 and name HG1 ) ( resid 42 and name HE2 ) 2.7 1.0 1.1 volume=2.682 peak=3244 ppm1=1.290 ppm2=2.969 assign ( resid 158 and name HG2 ) ( resid 159 and name HN ) 4.0 2.3 1.6 volume=0.247 peak=2885 ppm1=2.439 ppm2=9.044 assign ( resid 145 and name HB1 ) ( resid 145 and name HG2 ) 5.3 3.6 0.7 volume=0.048 peak=4631 ppm1=1.928 ppm2=1.441 assign ( resid 40 and name HN ) ( resid 43 and name HN ) 3.9 2.1 1.5 volume=0.325 peak=2031 ppm1=8.512 ppm2=7.270 assign ( resid 36 and name HN ) ( resid 35 and name HA ) 3.1 1.4 1.2 volume=1.213 peak=2305 ppm1=9.876 ppm2=4.916 assign ( resid 65 and name HD2# ) ( resid 65 and name HN ) 3.6 1.9 1.5 volume=0.468 peak=5163 ppm1=0.319 ppm2=7.740 assign ( resid 193 and name HG1# ) ( resid 194 and name HB2 ) 3.5 1.7 1.4 volume=0.632 peak=3853 ppm1=0.796 ppm2=2.789 assign ( resid 11 and name HA ) ( resid 12 and name HN ) 3.3 1.6 1.3 volume=0.774 peak=4928 ppm1=3.957 ppm2=7.614 assign ( resid 115 and name HG1# ) ( resid 116 and name HN ) 3.7 2.0 1.5 volume=0.412 peak=3344 ppm1=0.303 ppm2=8.837 assign ( resid 197 and name HN ) ( resid 194 and name HB1 ) 3.6 1.8 1.4 volume=0.519 peak=1737 ppm1=7.988 ppm2=2.835 assign ( resid 153 and name HA ) ( resid 154 and name HN ) 4.0 2.3 1.6 volume=0.244 peak=4069 ppm1=5.316 ppm2=10.030 assign ( resid 14 and name HN ) ( resid 14 and name HG1# ) 2.9 1.2 1.2 volume=1.873 peak=284 ppm1=7.792 ppm2=0.653 assign ( resid 184 and name HD1# ) ( resid 184 and name HA ) 3.5 1.8 1.4 volume=0.579 peak=3490 ppm1=0.894 ppm2=3.631 assign ( resid 21 and name HG2# ) ( resid 20 and name HB2 ) 3.1 1.4 1.2 volume=1.187 peak=3554 ppm1=1.148 ppm2=2.715 assign ( resid 28 and name HN ) ( resid 28 and name HA ) 2.9 1.2 1.2 volume=1.795 peak=751 ppm1=7.807 ppm2=4.407 assign ( resid 14 and name HB ) ( resid 14 and name HG2# ) 3.0 1.3 1.2 volume=1.531 peak=3931 ppm1=1.713 ppm2=0.760 assign ( resid 187 and name HG2# ) ( resid 184 and name HA ) 3.2 1.5 1.3 volume=0.996 peak=3165 ppm1=1.055 ppm2=3.642 assign ( resid 167 and name HN ) ( resid 156 and name HB1 ) 4.2 2.5 1.7 volume=0.186 peak=875 ppm1=8.642 ppm2=3.366 assign ( resid 29 and name HB ) ( resid 33 and name HG12 ) 3.2 1.4 1.3 volume=1.071 peak=4624 ppm1=3.929 ppm2=1.941 assign ( resid 71 and name HB1 ) ( resid 78 and name HD1# ) 3.5 1.8 1.4 volume=0.537 peak=4441 ppm1=1.526 ppm2=0.512 assign ( resid 59 and name HN ) ( resid 58 and name HB2 ) 3.3 1.5 1.3 volume=0.885 peak=506 ppm1=8.092 ppm2=2.133 assign ( resid 71 and name HN ) ( resid 74 and name HD1 ) 3.5 1.8 1.4 volume=0.576 peak=1061 ppm1=7.219 ppm2=6.925 assign ( resid 72 and name HA ) ( resid 76 and name HN ) 4.1 2.4 1.6 volume=0.219 peak=4028 ppm1=3.637 ppm2=6.739 assign ( resid 156 and name HN ) ( resid 154 and name HG2# ) 3.1 1.4 1.2 volume=1.162 peak=2419 ppm1=8.550 ppm2=0.881 assign ( resid 18 and name HN ) ( resid 19 and name HN ) 2.9 1.1 1.1 volume=1.935 peak=1822 ppm1=7.765 ppm2=7.518 assign ( resid 184 and name HG2# ) ( resid 185 and name HG1 ) 3.8 2.0 1.5 volume=0.384 peak=2766 ppm1=1.095 ppm2=2.390 assign ( resid 54 and name HB ) ( resid 61 and name HG ) 3.2 1.5 1.3 volume=0.965 peak=3743 ppm1=1.778 ppm2=1.713 assign ( resid 166 and name HD2 ) ( resid 168 and name HG1# ) 3.0 1.3 1.2 volume=1.383 peak=3376 ppm1=1.427 ppm2=0.771 assign ( resid 94 and name HN ) ( resid 93 and name HB ) 4.0 2.2 1.6 volume=0.277 peak=1731 ppm1=9.601 ppm2=1.223 assign ( resid 83 and name HG2 ) ( resid 86 and name HG2 ) 2.3 0.6 0.9 volume=7.625 peak=4398 ppm1=1.722 ppm2=1.429 assign ( resid 68 and name HG2# ) ( resid 83 and name HG1 ) 2.9 1.2 1.2 volume=1.893 peak=3454 ppm1=0.751 ppm2=1.743 assign ( resid 165 and name HN ) ( resid 166 and name HN ) 3.5 1.8 1.4 volume=0.543 peak=354 ppm1=8.464 ppm2=9.041 assign ( resid 128 and name HN ) ( resid 11 and name HB# ) 3.9 2.2 1.6 volume=0.305 peak=2382 ppm1=9.932 ppm2=1.665 assign ( resid 24 and name HD1 ) ( resid 24 and name HE1 ) 3.1 1.4 1.2 volume=1.174 peak=74 ppm1=6.802 ppm2=10.150 assign ( resid 76 and name HN ) ( resid 76 and name HB1 ) 3.0 1.3 1.2 volume=1.367 peak=1058 ppm1=6.697 ppm2=1.931 assign ( resid 206 and name HN ) ( resid 203 and name HN ) 3.0 1.2 1.2 volume=1.618 peak=2326 ppm1=7.462 ppm2=7.668 assign ( resid 65 and name HN ) ( resid 64 and name HB2 or resid 64 and name HB1 ) 3.2 1.5 1.3 volume=0.919 peak=303 ppm1=7.740 ppm2=2.966 assign ( resid 132 and name HB ) ( resid 114 and name HB2 ) 3.8 2.0 1.5 volume=0.383 peak=4521 ppm1=2.283 ppm2=1.613 assign ( resid 49 and name HN ) ( resid 49 and name HA ) 3.6 1.9 1.4 volume=0.493 peak=1863 ppm1=8.910 ppm2=4.885 assign ( resid 186 and name HN ) ( resid 184 and name HG2# ) 3.2 1.5 1.3 volume=0.918 peak=1239 ppm1=7.370 ppm2=1.093 assign ( resid 200 and name HD1 ) ( resid 54 and name HN ) 3.9 2.1 1.5 volume=0.325 peak=3711 ppm1=1.549 ppm2=9.036 assign ( resid 160 and name HA ) ( resid 159 and name HB2 ) 4.1 2.4 1.6 volume=0.227 peak=4942 ppm1=4.010 ppm2=1.874 assign ( resid 8 and name HG1 or resid 8 and name HG2 ) ( resid 7 and name HB# ) 3.6 1.9 1.4 volume=0.513 peak=4156 ppm1=2.322 ppm2=0.770 assign ( resid 65 and name HD2# ) ( resid 65 and name HD1# ) 2.5 0.8 1.0 volume=4.329 peak=3973 ppm1=0.320 ppm2=0.175 assign ( resid 130 and name HB1 ) ( resid 10 and name HG2# ) 3.3 1.6 1.3 volume=0.864 peak=4538 ppm1=1.886 ppm2=1.090 assign ( resid 166 and name HN ) ( resid 165 and name HA ) 3.0 1.3 1.2 volume=1.536 peak=1798 ppm1=9.001 ppm2=5.181 assign ( resid 160 and name HA ) ( resid 163 and name HB# ) 3.8 2.0 1.5 volume=0.377 peak=4605 ppm1=4.011 ppm2=1.144 assign ( resid 5 and name HB# ) ( resid 4 and name HN ) 3.8 2.1 1.5 volume=0.330 peak=4750 ppm1=1.342 ppm2=8.191 assign ( resid 137 and name HB1 ) ( resid 136 and name HB1 ) 3.6 1.9 1.5 volume=0.462 peak=2584 ppm1=2.809 ppm2=1.747 assign ( resid 95 and name HN ) ( resid 82 and name HN ) 3.3 1.5 1.3 volume=0.882 peak=2126 ppm1=9.124 ppm2=8.569 assign ( resid 21 and name HG2# ) ( resid 24 and name HE1 ) 4.0 2.3 1.6 volume=0.251 peak=2833 ppm1=1.148 ppm2=10.147 assign ( resid 188 and name HB2 ) ( resid 191 and name HN ) 4.0 2.3 1.6 volume=0.257 peak=2767 ppm1=1.448 ppm2=7.660 assign ( resid 203 and name HD1# ) ( resid 56 and name HN ) 3.9 2.2 1.6 volume=0.287 peak=3174 ppm1=-0.010 ppm2=8.651 assign ( resid 22 and name HN ) ( resid 24 and name HN ) 3.2 1.5 1.3 volume=0.949 peak=1241 ppm1=8.193 ppm2=7.849 assign ( resid 42 and name HG2 ) ( resid 42 and name HB1 ) 3.8 2.1 1.5 volume=0.371 peak=2830 ppm1=1.288 ppm2=1.663 assign ( resid 153 and name HN ) ( resid 128 and name HA ) 3.7 1.9 1.5 volume=0.450 peak=2136 ppm1=9.328 ppm2=5.573 assign ( resid 207 and name HN ) ( resid 206 and name HA ) 3.0 1.3 1.2 volume=1.416 peak=1048 ppm1=7.834 ppm2=4.397 assign ( resid 194 and name HB2 ) ( resid 194 and name HN ) 4.0 2.2 1.6 volume=0.280 peak=4455 ppm1=2.825 ppm2=7.777 assign ( resid 202 and name HN ) ( resid 204 and name HN ) 3.9 2.2 1.6 volume=0.288 peak=2038 ppm1=8.576 ppm2=6.735 assign ( resid 40 and name HN ) ( resid 39 and name HB# ) 3.1 1.4 1.2 volume=1.236 peak=171 ppm1=8.508 ppm2=1.154 assign ( resid 102 and name HA ) ( resid 102 and name HN ) 3.4 1.7 1.4 volume=0.676 peak=4826 ppm1=4.116 ppm2=8.512 assign ( resid 6 and name HB ) ( resid 5 and name HB# ) 4.1 2.3 1.6 volume=0.241 peak=2911 ppm1=1.723 ppm2=1.322 assign ( resid 154 and name HN ) ( resid 153 and name HB1 ) 3.4 1.7 1.4 volume=0.654 peak=2251 ppm1=10.007 ppm2=2.831 assign ( resid 130 and name HB2 ) ( resid 130 and name HB1 ) 2.6 0.9 1.0 volume=3.467 peak=4174 ppm1=1.833 ppm2=1.888 assign ( resid 67 and name HB2 ) ( resid 67 and name HA ) 3.4 1.6 1.3 volume=0.753 peak=3962 ppm1=2.151 ppm2=3.957 assign ( resid 196 and name HD1# ) ( resid 197 and name HN ) 3.9 2.2 1.6 volume=0.292 peak=4648 ppm1=0.727 ppm2=8.002 assign ( resid 24 and name HZ2 ) ( resid 24 and name HH2 ) 3.2 1.4 1.3 volume=1.081 peak=104 ppm1=7.537 ppm2=6.803 assign ( resid 60 and name HN ) ( resid 61 and name HN ) 3.3 1.6 1.3 volume=0.829 peak=672 ppm1=7.266 ppm2=8.696 assign ( resid 177 and name HN ) ( resid 144 and name HG12 ) 3.5 1.7 1.4 volume=0.615 peak=220 ppm1=8.461 ppm2=1.275 assign ( resid 76 and name HB2 ) ( resid 76 and name HG1 ) 3.1 1.4 1.2 volume=1.217 peak=2757 ppm1=1.984 ppm2=1.376 assign ( resid 193 and name HN ) ( resid 193 and name HG1# ) 2.5 0.7 1.0 volume=4.788 peak=1457 ppm1=7.622 ppm2=0.755 assign ( resid 168 and name HG2# ) ( resid 166 and name HG2 ) 4.0 2.3 1.6 volume=0.257 peak=4055 ppm1=0.198 ppm2=1.284 assign ( resid 8 and name HA ) ( resid 11 and name HB# ) 2.9 1.2 1.2 volume=1.792 peak=2771 ppm1=3.838 ppm2=1.631 assign ( resid 63 and name HB2 ) ( resid 60 and name HA ) 3.9 2.1 1.5 volume=0.324 peak=4523 ppm1=2.687 ppm2=3.919 assign ( resid 56 and name HN ) ( resid 54 and name HG2# ) 3.1 1.4 1.2 volume=1.278 peak=1170 ppm1=8.638 ppm2=0.575 assign ( resid 112 and name HG2# ) ( resid 113 and name HN ) 3.3 1.6 1.3 volume=0.841 peak=3825 ppm1=0.679 ppm2=8.325 assign ( resid 36 and name HB1 ) ( resid 26 and name HG2# ) 3.9 2.1 1.5 volume=0.320 peak=5073 ppm1=3.861 ppm2=0.906 assign ( resid 114 and name HA ) ( resid 114 and name HD1# ) 4.4 2.7 1.6 volume=0.153 peak=3113 ppm1=4.461 ppm2=0.536 assign ( resid 164 and name HN ) ( resid 165 and name HN ) 3.9 2.2 1.6 volume=0.304 peak=1099 ppm1=7.977 ppm2=8.441 assign ( resid 5 and name HB# ) ( resid 9 and name HG2 or resid 9 and name HG1 ) 3.3 1.6 1.3 volume=0.875 peak=2502 ppm1=1.342 ppm2=2.401 assign ( resid 84 and name HN ) ( resid 84 and name HG1# ) 3.3 1.5 1.3 volume=0.884 peak=585 ppm1=8.505 ppm2=0.501 assign ( resid 3 and name HE1 or resid 3 and name HE2 ) ( resid 93 and name HG2# ) 3.7 2.0 1.5 volume=0.387 peak=1 ppm1=7.213 ppm2=0.007 assign ( resid 87 and name HD1# ) ( resid 87 and name HN ) 4.1 2.4 1.6 volume=0.225 peak=4830 ppm1=0.439 ppm2=8.063 assign ( resid 24 and name HZ2 ) ( resid 36 and name HB2 ) 3.9 2.2 1.6 volume=0.296 peak=87 ppm1=7.536 ppm2=3.461 assign ( resid 65 and name HD1# ) ( resid 65 and name HA ) 3.9 2.1 1.5 volume=0.327 peak=2652 ppm1=0.176 ppm2=3.889 assign ( resid 139 and name HB2 ) ( resid 139 and name HD2 ) 3.3 1.6 1.3 volume=0.867 peak=2865 ppm1=2.197 ppm2=3.618 assign ( resid 74 and name HZ1 ) ( resid 74 and name HH2 ) 3.9 2.2 1.6 volume=0.299 peak=94 ppm1=5.952 ppm2=6.509
Contact the webmaster for help, if required. Thursday, May 23, 2024 3:23:36 PM GMT (wattos1)