NMR Restraints Grid |
Result table
image | mrblock_id | pdb_id | bmrb_id | cing | stage | position | program | type | subtype | subsubtype |
9246 | 1nku | 5668 | cing | 1-original | 1 | XPLOR/CNS | distance | NOE | ambi |
! !######################################################################## !NOE all for free TAG at 20C and pH6.6(ice cold), 10 mM NaH2PO4, 0.1M NaCl !A = ambiguous !R = redundant !U = useless restraint !E2 !INTRA assign (residue 2 and name hn) (residue 2 and name ha) 1.8 0.0 1.7 ! !SEQ assign (residue 2 and name hn) (residue 1 and name ha) 1.8 0.0 1.1 ! assign (residue 2 and name hn) (residue 1 and name hg#) 1.8 0.0 1.7 ! !R assign (residue 2 and name hn) (residue 3 and name hn) 1.8 0.0 3.2 ! !MED !LONG !R3 !INTRA !SEQ assign (residue 3 and name hn) (residue 2 and name hn) 1.8 0.0 3.2 ! assign (residue 3 and name hn) (residue 2 and name ha) 1.8 0.0 0.9 ! 4.8e7 very strong to E2ha also assign (residue 3 and name hn) (residue 2 and name hb#) 1.8 0.0 1.7 ! !R assign (residue 3 and name hn) (residue 4 and name hn) 1.8 0.0 3.2 ! !MED assign (residue 3 and name he) ((residue 7 and name hg1#) or (residue 7 and name hg2#)) 1.8 0.0 3.2 ! !LONG assign (residue 3 and name he) (residue 14 and name hg2#) 1.8 0.0 3.2 ! !C4 !INTRA !SEQ assign (residue 4 and name hn) (residue 3 and name hn) 1.8 0.0 3.2 ! assign (residue 4 and name hn) (residue 3 and name ha) 1.8 0.0 1.1 ! 1e7 !R assign (residue 4 and name hn) (residue 5 and name hn) 1.8 0.0 1.7 ! !MED assign (residue 4 and name hn) (residue 7 and name hg#) 1.8 0.0 3.2 ! !LONG !R assign (residue 176 and name hg#) (residue 4 and name ha) 1.8 0 1.5 ! 4d med for c4ha to 176hg'' assign (residue 4 and name hn) (residue 179 and name hb#) 1.8 0.0 3.2 !3.29ppm !G5 !INTRA !SEQ assign (residue 5 and name hn) (residue 4 and name hn) 1.8 0.0 3.2 ! assign (residue 5 and name hn) (residue 4 and name ha) 1.8 0.0 1.1 ! 2e7 !R assign (residue 5 and name hn) (residue 6 and name hn) 1.8 0.0 1.7 ! !MED !LONG assign (residue 5 and name hn) (residue 132 and name hd#) 1.8 0.0 1.7 !1.2e7, 132 hd' and hd'' see 8.89ppm (off for G5 initially but G5 has moved to 8.90) !W6 !INTRA assign (residue 6 and name hn) (residue 6 and name ha) 1.8 0.0 1.1 ! assign (residue 6 and name hn) (residue 6 and name hb#) 1.8 0.0 1.7 ! assign (residue 6 and name hn) (residue 6 and name hd1) 1.8 0.0 1.7 ! assign (residue 6 and name hn) (residue 6 and name he1) 1.8 0.0 3.2 ! assign (residue 6 and name he1) (residue 6 and name hb#) 1.8 0.0 3.2 ! !SEQ assign (residue 6 and name hn) (residue 5 and name hn) 1.8 0.0 1.7 ! !R assign (residue 6 and name hn) (residue 7 and name hn) 1.8 0.0 1.1 ! assign (residue 6 and name hn) (residue 7 and (name hg1# or name hg2#)) 1.8 0.0 3.2 ! 5e6 !MED assign (residue 6 and name hn) (residue 4 and name ha) 1.8 0.0 2.2 !amb, ovlps 5ha# assign (residue 6 and name he1) (residue 4 and name hb#) 1.8 0.0 2.2 !2.47ppm !LONG assign (residue 6 and name hn) (residue 132 and name hd#) 1.8 0.0 1.7 ! 1.8e7, 132hd' and 132 hd'' see 6.45ppm assign (residue 6 and name he1) (residue 132 and name hd#) 1.8 0 1.7 ! 3d15n assign (residue 6 and name hd1) (residue 132 and name hd#) 1.8 0 1.7 ! 13C aro and 13C to both 132 hds !V7 !INTRA assign (residue 7 and name hn) (residue 7 and name ha) 1.8 0.0 1.7 ! assign (residue 7 and name hn) (residue 7 and name hb) 1.8 0.0 1.7 ! assign (residue 7 and name hn) (residue 7 and (name hg1# or name hg2#)) 1.8 0.0 1.1 ! 1.7e7 !SEQ assign (residue 7 and name hn) (residue 6 and name hn) 1.8 0.0 1.1 ! assign (residue 7 and name hn) (residue 6 and name ha) 1.8 0.0 1.7 ! !A assign (residue 7 and name hn) (residue 6 and name hb#) 1.8 0.0 1.7 !not in both N15-NOESYS !MED !LONG assign ((residue 7 and name hg1#) or (residue 7 and name hg2#)) (residue 14 and name ha) 1.8 0.0 1.5 ! 3D assign ((residue 7 and name hg1#) or (residue 7 and name hg2#)) ((residue 14 and name hg11) or (residue 14 and name hg12)) 1.8 0.0 3.2 ! 4d assign ((residue 7 and name hg1#) or (residue 7 and name hg2#)) (residue 14 and name hg2#) 1.8 0.0 3.2 ! 4D !R assign ((residue 7 and name hg1#) or (residue 7 and name hg2#)) ! (residue 14 and name hd#) 1.8 0.0 3.2 ! wk to hg'(-0.39ppm) assign ((residue 7 and name hg1#) or (residue 7 and name hg2#)) (residue 14 and name hd#) 1.8 0.0 1.5 ! 4D assign (residue 14 and name hn) ((residue 7 and name hg1#) or (residue 7 and name hg2#)) 1.8 0.0 3.2 ! !R assign (residue 17 and name hn) !R ((residue 7 and name hg1#) or (residue 7 and name hg2#)) 1.8 0.0 3.2 ! 7hg' sees 17hn assign (residue 7 and name hn) ((residue 132 and name hd1#) or (residue 132 and name hd2#)) 1.8 0.0 3.2 ! weak assign ((residue 7 and name hg1#) or (residue 7 and name hg2#)) ((residue 132 and name hd1#) or (residue 132 and name hd2#)) 1.8 0.0 3.2 ! weak in 3D 13c !S8 unassigned !peaks to S8 ha and hb in 4d 14hd?? !INTRA !SEQ !MED !LONG !Q9 unassigned !INTRA !SEQ !MED !LONG !D10 unassigned !INTRA !SEQ !MED !LONG !P11 !INTRA !SEQ !MED assign (residue 11 and name ha) (residue 14 and name hn) 1.8 0.0 3.2 ! 3d 13c to p11ha assign (residue 11 and name ha) (residue 14 and name hb) 1.8 0.0 3.2 ! c13noesy, 4.3e5 assign (residue 11 and name ha) (residue 14 and name hd#) 1.8 0.0 1.5 ! c13noesy, 7.8e5, 4d to 14hd !LONG !L12 !INTRA assign (residue 12 and name hn) (residue 12 and name ha) 1.8 0.0 1.7 ! assign (residue 12 and name hn) ((residue 12 and name hb1) or (residue 12 and name hb2)) 1.8 0.0 3.2 ! !SEQ assign (residue 12 and name hn) ((residue 11 and name hb1) or (residue 11 and name hb2)) 1.8 0.0 3.2 ! !MED assign ((residue 12 and name hd1#) or (residue 12 and name hd2#)) (residue 15 and name hb#) 1.8 0.0 3.2 ! 3d !LONG assign (residue 12 and name hd1#) (residue 47 and name hd#) 1.8 0.0 3.2 ! 4D, to both L12 hd#s assign (residue 12 and name hd2#) (residue 47 and name hd#) 1.8 0.0 3.2 ! 4D, to both L12 hd#s assign ((residue 12 and name hd1#) or (residue 12 and name hd2#)) (residue 50 and name hn) 1.8 0.0 3.2 ! 3d to hd', 51hn sees it also assign ((residue 12 and name hd1#) or (residue 12 and name hd2#)) ((residue 50 and name hb1) or (residue 50 and name hb2)) 1.8 0.0 3.2 ! 3d assign ((residue 12 and name hd1#) or (residue 12 and name hd2#)) (residue 50 and name hg) 1.8 0.0 3.2 ! 4d !R assign ((residue 12 and name hd1#) or (residue 12 and name hd2#)) !R ((residue 50 and name hd1#) or (residue 50 and name hd2#)) 1.8 0.0 3.2 ! 4d to 12 hd'' !R assign ((residue 12 and name hd1#) or (residue 12 and name hd2#)) !R (residue 51 and name ha) 1.8 0.0 1.5 ! 3.80/59.0 in 4D, 1e6 in 3d so med, sees 12hd'' also, wk assign ((residue 12 and name hd1#) or (residue 12 and name hd2#)) ((residue 51 and name hg1) or (residue 51 and name hg2)) 1.8 0.0 3.2 ! 3d assign ((residue 12 and name hd1#) or (residue 12 and name hd2#)) (residue 51 and name hd#) 1.8 0.0 3.2 ! 4d to 12 hd'' assign ((residue 12 and name hd1#) or (residue 12 and name hd2#)) (residue 51 and name he#) 1.8 0.0 3.2 ! 4D !Y13 ! hn unassigned ! no noes to ha in c13noesy !INTRA !SEQ !MED assign (residue 13 and name hd#) (residue 16 and name hd#) 1.8 0.0 3.2 ! 2d noesy !LONG !A assign (residue 13 and name hd#) (residue 7 and name hg#) 1.8 0.0 3.2 ! 2D NOESY, AMB, V7hg' not see 7.57 assign (residue 13 and name hd#) (residue 46 and name hd1) 1.8 0.0 1.5 ! 2D NOESY assign (residue 13 and name hd#) (residue 47 and name hg2#) 1.8 0.0 3.2 ! 2D NOESY, AMB, 47hg2 not see 7.57 in 3d noesy assign (residue 13 and name hd#) (residue 47 and name hd#) 1.8 0.0 3.2 ! 47 hd sees 7.57 assign (residue 13 and name he#) (residue 47 and name hd#) 1.8 0.0 3.2 ! 47 hd sees 7.10 assign (residue 13 and name hd#) (residue 50 and name hd#) 1.8 0.0 3.2 ! 50 hd' sees 7.59 assign (residue 13 and name he#) (residue 50 and name hd#) 1.8 0.0 3.2 ! 50 hd' sees 7.10 !I14 ! HN SIGNALS WEAK AND OVERLAPPED !INTRA assign (residue 14 and name hn) (residue 14 and (name hg2# or name hd#)) 1.8 0.0 1.7 ! 1.7e7 !SEQ !A assign (residue 14 and name hn) (residue 13 and name hn) 1.8 0.0 ! 13hn unassigned !A assign (residue 14 and name hn) (residue 15 and name hn) 1.8 0.0 ! 15hn ovlps 14hn assign (residue 14 and name hg2#) (residue 15 and name hb#) 1.8 0.0 3.2 ! 4D !MED !(a->b,i-i+3) dont see any hb to 14ha, and 17hbs unassigned assign (residue 14 and name hg2#) ((residue 11 and name hb1) or (residue 11 and name hb2)) 1.8 0.0 3.2 ! 3d, dont see in 4D assign (residue 14 and name hd#) ((residue 11 and name hb1) or (residue 11 and name hb2)) 1.8 0.0 3.2 ! 3d assign (residue 14 and name hn) (residue 16 and name hn) 1.8 0.0 3.2 ! 4D !LONG assign (residue 14 and name hg2#) ((residue 7 and name hg1#) or (residue 7 and name hg2#)) 1.8 0.0 3.2 ! 4D assign (residue 14 and name hd#) ((residue 7 and name hg1#) or (residue 7 and name hg2#)) 1.8 0.0 3.2 ! 4D, wk in 3d assign (residue 14 and name ha) ((residue 7 and name hg1#) or (residue 7 and name hg2#) or (residue 149 and name hd1#) or (residue 149 and name hd2#)) 1.8 0.0 3.2 ! ?? !A assign (residue 14 and name hg2#) !A ((residue 132 and name hd1#) or (residue 132 and name hd2#)) 1.8 0.0 3.2 ! 4D, dont see 132hd'' to 14hg2 !A assign (residue 14 and name hg2#) !A ((residue xx and name he1) or (residue and name he2)) 1.8 0.0 3.2 ! 3D13c, R888 he1 sees med pk to 14hg2# !A15 ! hn peaks weak and overlapped !INTRA !SEQ !A assign (residue 15 and name hn) (residue 14 and name hn) 1.8 0.0 ! 14hn ovlps 15hn assign (residue 15 and name hn) (residue 14 and name ha) 1.8 0.0 3.2 ! 14hn ovlps 15hn assign (residue 15 and name hn) (residue 14 and name hg2#) 1.8 0.0 1.7 ! 3d assign (residue 15 and name ha) (residue 14 and name hg2#) 1.8 0.0 3.2 ! 3d !R assign (residue 15 and name hn) (residue 16 and name hn) 1.8 0.0 1.7 ! !R assign (residue 15 and name hb#) (residue 16 and name hn) 1.8 0.0 1.7 ! 3d !MED !(a->b,i-i+3) dont see 18 hb assign (residue 15 and name hb#) (residue 12 and name ha) 1.8 0.0 1.5 ! 4d, 6e5 in 3d assign (residue 15 and name hn) (residue 12 and name ha) 1.8 0.0 3.2 assign (residue 15 and name hb#) ((residue 12 and name hd1#) or (residue 12 and name hd2#)) 1.8 0.0 3.2 ! 4d !A assign (residue 15 and name hb#) (residue 16 and name he#) 1.8 0.0 1.5 ! 3d !R assign (residue 19 and name hn) (residue 15 and name hb#) 1.8 0.0 3.2 ! !LONG !Y16 ! hn peaks weak and overlapped !INTRA !SEQ assign (residue 16 and name hn) (residue 15 and name hn) 1.8 0.0 1.7 ! amb ovlpd assign (residue 16 and name hn) (residue 15 and name hb#) 1.8 0.0 1.7 ! 9e6 !R assign (residue 16 and name hn) (residue 17 and name hn) 1.8 0.0 3.2 ! !MED !nada to 16ha in c13noe !dont see 12ha, 13ha to 16hn assign (residue 16 and name hd#) (residue 13 and name ha) 1.8 0.0 3.2 ! !LONG assign (residue 16 and name hd#) (residue 46 and name hd1) 1.8 0.0 3.2 !3d aro !A assign (residue 16 and name hn) (residue 50 and name hd#) 1.8 0.0 3.2 ! assign (residue 16 and name hd#) (residue 50 and name hd#) 1.8 0.0 3.2 ! 50 hd' sees pks at 16hd and 16he !H17 !INTRA assign (residue 17 and name hn) (residue 17 and name ha) 1.8 0.0 1.7 ! !SEQ assign (residue 17 and name hn) (residue 16 and name hn) 1.8 0.0 1.7 ! assign (residue 17 and name hn) (residue 16 and name ha) 1.8 0.0 1.7 ! !R assign (residue 17 and name hn) (residue 18 and name hn) 1.8 0.0 1.7 ! !MED assign (residue 17 and name hn) (residue 14 and name ha) 1.8 0.0 3.2 ! pk at 3.35 rather than 3.32, could be H17 hb assign (residue 17 and name hn) (residue 14 and (name hg2# or name hd#)) 1.8 0.0 3.2 ! assign (residue 17 and name hn) (residue 15 and name hn) 1.8 0.0 3.2 ! !nada to 17ha in c13noe !LONG assign (residue 17 and name hn) (residue 7 and name hg#) 1.8 0.0 3.2 ! 7hg' sees 17hn !D18 !INTRA assign (residue 18 and name hn) (residue 18 and name ha) 1.8 0.0 1.7 ! amb ovlpd !SEQ assign (residue 18 and name hn) (residue 17 and name hn) 1.8 0.0 1.7 ! !R assign (residue 18 and name hn) (residue 19 and name hn) 1.8 0.0 1.7 ! !MED assign (residue 18 and name hn) (residue 14 and name hg2#) 1.8 0.0 3.2 ! 14hg2 sees wk pk at 8.77 assign (residue 18 and name hn) (residue 15 and name ha) 1.8 0.0 3.2 ! assign (residue 18 and name hn) (residue 16 and name hn) 1.8 0.0 3.2 ! !LONG !nada to 18ha in c13noe !N19 !INTRA assign (residue 19 and name hn) (residue 19 and name ha) 1.8 0.0 0.9 ! !SEQ assign (residue 19 and name hn) (residue 18 and name hn) 1.8 0.0 1.7 ! assign (residue 19 and name hn) (residue 18 and name ha) 1.8 0.0 3.2 ! !R assign (residue 19 and name hn) (residue 20 and name hn) 1.8 0.0 1.1 ! !MED assign (residue 19 and name hn) (residue 15 and name ha) 1.8 0.0 3.2 ! assign (residue 19 and name hn) (residue 15 and name hb*) 1.8 0.0 3.2 ! assign (residue 19 and name hn) (residue 16 and name ha) 1.8 0.0 3.2 ! assign ((residue 19 and name hb1) or (residue 19 and name hb2)) (residue 16 and name ha) 1.8 0.0 3.2 ! !LONG !19ha sees only 19hbs in c13noe !E20 !INTRA assign (residue 20 and name hn) (residue 20 and name ha) 1.8 0.0 1.1 ! assign (residue 20 and name hn) (residue 20 and name hg#) 1.8 0.0 1.5 ! !SEQ assign (residue 20 and name hn) (residue 19 and name hn) 1.8 0.0 1.1 ! !RA assign (residue 20 and name hn) (residue 19 and name ha) 1.8 0.0 1.7 ! assign (residue 20 and name hn) ((residue 19 and name hb1) or (residue 19 and name hb2)) 1.8 0.0 1.7 ! !MED assign (residue 20 and name hn) (residue 16 and name hd#) 1.8 0.0 3.2 ! assign (residue 20 and name hn) ((residue 23 and name hg1#) or (residue 23 and name hg2#)) 1.8 0.0 3.2 ! !R assign ((residue 23 and name hg1#) or (residue 23 and name hg2#)) !R (residue 20 and name ha) 1.8 0.0 1.5 ! 4d, 3d 7e5 !LONG !nada to 20ha in c13noe !W21 !hn overlapped !INTRA !SEQ !A assign (residue 21 and name hn) (residue 20 and name hn) 1.8 0.0 ! hn ovlp !R assign (residue 21 and name hn) (residue 22 and name hn) 1.8 0.0 3.2 ! !MED !nada to 21ha in c13noe assign (residue 21 and name hd1) (residue 17 and name ha) 1.8 0 3.2 ! 2d noesy !A assign (residue 21 and name hn) (residue 19 and name hn) 1.8 0.0 3.2 ! assign (residue 21 and name ha) (residue 23 and name hg#) 1.8 0.0 3.2 ! !LONG assign (residue 21 and name he1) (residue 16 and name he#) 1.8 0 3.2 ! 3d15n !W21 based on NOEs from hd1 to 21ha and 21 hb, and its not W117 or W6, ! !A assign (residue 21 and name he1) (residue 31 and (name hd1# or name hd2#)) 1.8 0 3.2 !A 31hds dont see it, 15n noesy assign (residue 21 and name he1) (residue 167 and name ha) 1.8 0 3.2 ! 3d15n, 67ha sees verywk to 21he1 assign (residue 21 and name he1) (residue 167 and name hb#) 1.8 0 3.2 ! 3d15n, peaks to 167hbs very wk assign (residue 21 and name he1) (residue 168 and name ha) 1.8 0 3.2 ! 3d15n, 68ha sees 10.44 assign (residue 21 and name he1) (residue 168 and name hb#) 1.8 0 3.2 !3d15n, 68ha sees 10.44 assign (residue 21 and name hd1) (residue 168 and name hb#) 1.8 0 3.2 !2dnoesy assign (residue 21 and name hd1) (residue 168 and name ha) 1.8 0 3.2 !2dnoesy !G22 !INTRA !SEQ !A assign (residue 22 and name hn) (residue 21 and name hn) 1.8 0.0 ! 21hn ovlps 22hn assign (residue 22 and name hn) (residue 21 and name ha) 1.8 0.0 1.1 ! 22hn to 21ha strong also !A assign (residue 22 and name hn) (residue 23 and name hn) 1.8 0.0 !23hn ovlps 22hn assign (residue 22 and name hn) (residue 23 and (name hg1# or name hg2#)) 1.8 0.0 4.2 !MED !LONG assign (residue 22 and name hn) (residue 168 and name hb#) 1.8 0.0 3.2 ! 168hb may see it as shoulder !A assign (residue 22 and name hn) (residue 168 and name ha) 1.8 0.0 3.2 ! !A assign (residue 22 and (name ha1 or name ha2)) (residue 168 and name ha) 1.8 0.0 3.2 ! 168ha not see 22has assign (residue 22 and name hn) (residue 170 and name hn) 1.8 0.0 3.2 ! not sure if 170 sees it bc 171hn ovlps 22hn !V23 !INTRA assign (residue 23 and name hn) (residue 23 and name ha) 1.8 0.0 1.7 ! assign (residue 23 and name hn) (residue 23 and name hb) 1.8 0.0 1.7 ! assign ((residue 23 and name hg1#) or (residue 23 and name hg2#)) (residue 23 and name hn) 1.8 0.0 1.7 !SEQ !A assign (residue 23 and name hn) (residue 22 and name hn) 1.8 0.0 ! 22hn ovlps 23hn assign (residue 23 and name hn) (residue 22 and name ha#) 1.8 0.0 3.2 ! assign (residue 23 and name hg#) (residue 24 and name ha) 1.8 0.0 3.2 ! assign (residue 23 and name hg#) (residue 24 and name hd#) 1.8 0.0 1.5 ! !MED assign (residue 23 and name hn) (residue 20 and name ha) 1.8 0.0 3.2 ! assign (residue 23 and name hg#) (residue 20 and name ha) 1.8 0.0 3.2 !4d, 3d 7e5 !LONG !P24 !INTRA !SEQ assign (residue 23 and name ha) (residue 24 and name hd#) 1.8 0.0 0.9 ! 3d 1e6 assign ((residue 23 and name hg1#) or (residue 23 and name hg2#)) (residue 24 and name hd#) 1.8 0.0 3.2 ! !MED !LONG !nada to ha or hbs in c13noe !E25 !nada to ha in c13noe !INTRA !SEQ assign (residue 25 and name hn) (residue 24 and name ha) 1.8 0.0 1.1 ! !R assign (residue 25 and name hn) (residue 26 and name hn) 1.8 0.0 ! dont see it !MED !LONG assign (residue 25 and name hn) ((residue 31 and name hd1#) or (residue 31 and name hd2#)) 1.8 0.0 3.2 ! 31hd' sees 8.57 also assign (residue 25 and name ha) ((residue 31 and name hd1#) or (residue 31 and name hd2#)) 1.8 0.0 3.2 ! 31hd' sees ? assign (residue 25 and name hn) ((residue 26 and name hb) or (residue 169 and name ha)) 1.8 0.0 3.2 ! assign (residue 25 and name hn) ((residue 170 and name ha1) or (residue 170 and name ha2)) 1.8 0.0 3.2 ! assign ((residue 171 and name hd1#) or (residue 171 and name hd2#)) (residue 25 and name hn) 1.8 0.0 3.2 ! assign (residue 25 and name hn) ((residue 26 and name hg2#) or (residue 171 and name hb1) or (residue 171 and name hb2)) 1.8 0.0 3.2 ! assign (residue 25 and name hn) (residue 170 and name hn) 1.8 0.0 3.2 ! 170hn sees it also !T26 !INTRA assign (residue 26 and name hn) (residue 26 and name hg2#) 1.8 0.0 1.7 ! 1.3e7 !SEQ assign (residue 26 and name hn) (residue 25 and name hn) 1.8 0.0 3.2 ! 2e6 assign (residue 26 and name hn) (residue 25 and name ha) 1.8 0.0 1.1 ! 2.5e7 amb - could be to 124ha assign (residue 26 and name hn) (residue 25 and name hb#) 1.8 0.0 1.7 ! assign (residue 26 and name hn) (residue 25 and name hg#) 1.8 0.0 3.2 ! !R assign (residue 26 and name hn) (residue 27 and name hn) 1.8 0.0 1.1 ! 1.3e7 assign (residue 26 and name hn) (residue 27 and name hb#) 1.8 0.0 3.2 !26hn sees both 27 hbs !MED assign (residue 26 and name hn) ((residue 30 and name hd#) or (residue 31 and name hb#)) 1.8 0.0 3.2 ! pk at 1.834, 30 hd closer 18dec01 !LONG assign (residue 26 and name hn) ((residue 31 and name hd1#) or (residue 31 and name hd2#)) 1.8 0.0 3.2 ! AMB, 31 hd' sees very wk from pk at 8.17 assign (residue 26 and name hg2#) (residue 31 and name hd#) 1.8 0.0 3.2 ! assign (residue 26 and name hg2#) (residue 113 and name hb#) 1.8 0.0 3.2 ! 4D assign (residue 26 and name hg2#) (residue 117 and name hd1) 1.8 0.0 3.2 ! AMB 117hd1 sees 0.47 with 0.53 on shoulder assign (residue 26 and name hb) (residue 117 and name he1) 1.8 0.0 3.2 ! !R assign (residue 26 and name hg2#) (residue 117 and name he1) 1.8 0.0 1.7 ! !D27 !INTRA assign (residue 27 and name hn) (residue 27 and name ha) 1.8 0.0 1.7 ! assign (residue 27 and name hn) ((residue 27 and name hb1) or (residue 27 and name hb2)) 1.8 0.0 1.1 ! !SEQ assign (residue 27 and name hn) (residue 26 and name hn) 1.8 0.0 1.1 ! strong? 1e7 assign (residue 27 and name hn) (residue 26 and name ha) 1.8 0.0 3.2 ! med? 5.6e6 assign (residue 27 and name hn) (residue 26 and name hg2#) 1.8 0.0 3.2 ! !R assign (residue 27 and name hn) (residue 28 and name hn) 1.8 0.0 3.2 ! 4.6e6 !MED assign (residue 27 and name hn) (residue 25 and name ha) 1.8 0.0 1.7 ! 9.3e6 assign (residue 27 and name hn) (residue 25 and name hb#) 1.8 0.0 1.7 ! !A assign (residue 27 and name hn) (residue 25 and name hg#) 1.8 0.0 3.2 ! not sure of 25hg assignment !R assign (residue 27 and name hn) (residue 30 and name hn) 1.8 0.0 3.2 ! assign (residue 27 and name hn) ((residue 30 and name hg#) or (residue 113 and name hb#)) 1.8 0.0 3.2 ! assign (residue 27 and name hn) ((residue 31 and name hb#) or (residue 30 and name hd#)) 1.8 0.0 3.2 assign (residue 27 and name hn) (residue 31 and name hd#) 1.8 0.0 3.2 ! !R assign (residue 27 and name hn) (residue 31 and name hn) 1.8 0.0 3.2 ! !LONG !nada to ha or to hbs in c13noe !S28 !INTRA assign (residue 28 and name hn) (residue 28 and name ha) 1.8 0.0 1.7 ! ! assign (residue 28 and name hn) (residue 28 and name hb#) 1.8 0.0 3.2 ! !SEQ assign (residue 28 and name hn) (residue 27 and name hn) 1.8 0.0 3.2 ! 3.8e6 assign (residue 28 and name hn) (residue 27 and name ha) 1.8 0.0 1.1 ! 2.6e7 assign (residue 28 and name hn) ((residue 27 and name hb1) or (residue 27 and name hb2)) 1.8 0.0 1.7 ! could be wk 3-5e6 !R assign (residue 28 and name hn) (residue 29 and name hn) 1.8 0.0 1.7 ! assign (residue 28 and name hn) ((residue 29 and name hd#) or (residue 29 and name hg#)) 1.8 0.0 3.2 ! !MED !LONG assign (residue 28 and name hn) (residue 113 and name hb#) 1.8 0.0 1.7 ! med, 6.7e6, 113 hb# sees it also !nada to ha in c13noe !K29 !INTRA assign (residue 29 and name hn) (residue 29 and name ha) 1.8 0.0 1.1 ! assign (residue 29 and name hn) ((residue 29 and name hb1) or (residue 29 and name hb2)) 1.8 0.0 1.1 ! !SEQ assign (residue 29 and name hn) (residue 28 and name hn) 1.8 0.0 1.7 ! assign (residue 29 and name hn) (residue 28 and name hb#) 1.8 0.0 1.7 ! !A assign (residue 29 and name hn) (residue 30 and name hn) 1.8 0.0 ? ! 30hn ovlps 29hn !MED assign (residue 29 and name hn) (residue 27 and name hb#) 1.8 0.0 3.2 ! !R assign (residue 29 and name hn) (residue 31 and name hn) 1.8 0.0 3.2 ! assign (residue 29 and name ha) (residue 32 and name hb#) 1.8 0.0 3.2 ! !LONG !nada to ha in c13noe !K30 !INTRA assign (residue 30 and name hn) (residue 30 and name ha) 1.8 0.0 1.7 ! 7.4e7 !SEQ !A assign (residue 30 and name hn) (residue 29 and name hn) 1.8 0.0 ! 29hn ovlps 30hn !R assign (residue 30 and name hn) (residue 31 and name hn) 1.8 0.0 1.1 ! !MED assign (residue 30 and name hn) (residue 27 and name hn) 1.8 0.0 3.2 ! assign (residue 30 and name hn) ((residue 27 and name hb1) or (residue 27 and name hb2)) 1.8 0.0 1.7 ! assign (residue 30 and name hn) (residue 28 and name hn) 1.8 0.0 3.2 ! assign (residue 30 and name ha) (residue 33 and name hb#) 1.8 0.0 3.2 ! amb !LONG !nada to ha in 4dc13noe !L31 !INTRA assign ((residue 31 and name hd1#) or (residue 31 and name hd2#)) (residue 31 and name hn) 1.8 0.0 1.7 !SEQ assign (residue 31 and name hn) (residue 30 and name hn) 1.8 0.0 1.1 ! !A assign (residue 31 and name hn) (residue 30 and name ha) 1.8 0.0 ! 128hn ovlps 31hn !AR assign (residue 31 and name hn) (residue and name h) 1.8 0.0 ! 32hn ovlps 31hn !MED !nada to ha in 3d or 4d c13noe assign ((residue 31 and name hd1#) or (residue 31 and name hd2#)) ((residue 27 and name hb1) or (residue 27 and name hb2)) 1.8 0.0 3.2 !29hn ovlps 30hn !S28ha ovlps 31ha and others !dont see 34hbs to 31 ha assign (residue 31 and name hn) (residue 33 and name hn) 1.8 0.0 3.2 ! !LONG !R assign (residue 25 and name hn) !R ((residue 31 and name hd1#) or (residue 31 and name hd2#)) 1.8 0.0 3.2 ! 31hd' sees 8.57 also assign (residue 31 and name hd#) (residue 25 and name ha) 1.8 0.0 3.2 ! 4d to 31 hd' assign (residue 31 and name hd#) (residue 25 and name hb#) 1.8 0.0 1.5 ! 4d to 31 hd' assign (residue 31 and name hd#) (residue 25 and name hg#) 1.8 0.0 3.2 ! 4d to 31 hd' assign (residue 31 and name hd#) (residue 113 and name hb#) 1.8 0.0 1.5 ! 4d to 31 hd'' and to hd'' !R assign ((residue 31 and name hd1#) or (residue 31 and name hd2#)) !R (residue 113 and name ha) 1.8 0.0 3.2 ! 4d to 31 hd'' assign ((residue 31 and name hd1#) or (residue 31 and name hd2#)) ((residue 116 and name hg1#) or (residue 116 and name hg2#)) 1.8 0.0 3.2 ! 4d to 31 hd' !A assign (residue 31 and name hd#) (residue 117 and name he3) 1.8 0.0 3.2 ! 7.00ppm, 3d to 31 hd', could be to 165ring assign ((residue 31 and name hd1#) or (residue 31 and name hd2#)) ((residue 171 and name hd1#) or (residue 171 and name hd2#)) 1.8 0.0 1.5 ! 4d to 31 hd', and L171 sees 1.15ppm !R assign (residue 169 and name hb#) !R (residue 31 and (name hd1# or name hd2#)) 1.8 0.0 3.2 ! assign (residue 31 and name hd#) ((residue 25 and name ha) or (residue 124 and name ha)) 1.8 0.0 3.2 ! peak at 4.70 ppm !F32 !INTRA assign (residue 32 and name hn) (residue 32 and name ha) 1.8 0.0 1.7 ! !he and hz unassigned !SEQ !A assign (residue 32 and name hn) (residue 31 and name hn) 1.8 0.0 1.1 ! 31hn ovlps 32hn assign (residue 32 and name hn) (residue 31 and name ha) 1.8 0.0 1.7 ! assign (residue 32 and name hn) (residue 31 and name hd#) 1.8 0.0 2.2 ! !R assign (residue 32 and name hn) (residue 33 and name hn) 1.8 0.0 1.7 ! !MED assign (residue 32 and name hn) (residue 29 and name ha) 1.8 0.0 3.2 ! assign (residue 32 and name hn) (residue 30 and name hn) 1.8 0.0 3.2 ! assign (residue 32 and name ha) (residue 35 and (name hb or name hg2#)) 1.8 0.0 1.5 ! 35hb ovlps 35hg2 !LONG !A assign (residue 32 and name hn) (residue 27 and name hb#) 1.8 0.0 3.2 ! assign (residue 32 and name hn) ((residue 112 and name hd#) or (residue 117 and name hd1) or (residue 32 and name he#)) 1.8 0.0 3.2 ! 3d15n noesy assign (residue 32 and name hn) (residue 102 and name he#) 1.8 0.0 3.2 ! 3d15n noesy !R assign (residue 32 and name hb#) (residue 102 and name he#) 1.8 0.0 3.2 ! 3d 13c noesy !E33 !INTRA assign (residue 33 and name hn) (residue 33 and name ha) 1.8 0.0 1.1 ! !SEQ assign (residue 33 and name hn) (residue 32 and name hn) 1.8 0.0 1.1 ! 7e6 !32ha ovlpd !R assign (residue 33 and name hn) (residue 34 and name hn) 1.8 0.0 1.1 ! !MED assign (residue 33 and name hn) (residue 30 and name ha) 1.8 0.0 3.2 ! amb !R assign (residue 31 and name hn) (residue 33 and name hn) 1.8 0.0 3.2 ! !31hn ovlps 32hn !36hb ovlps 33ha !LONG !M34 !INTRA assign (residue 34 and name hn) (residue 34 and name ha) 1.8 0.0 1.5 ! assign (residue 34 and name hg#) (residue 34 and name hn) 1.8 0.0 3.2 ! !hb's, hg's, and he unassigned !SEQ assign (residue 34 and name hn) (residue 33 and name hn) 1.8 0.0 1.1 ! assign (residue 34 and name hn) (residue 33 and name ha) 1.8 0.0 1.5 ! strong peak but ovlps side chain NH2 strip !R assign (residue 34 and name hn) (residue 35 and name hn) 1.8 0.0 1.1 ! !MED assign (residue 34 and name hn) ((residue 31 and name hd1#) or (residue 31 and name hd2#)) 1.8 0.0 3.2 ! assign (residue 34 and name hn) (residue 32 and name hn) 1.8 0.0 3.2 ! assign (residue 34 and name he#) ((residue 37 and name hd1#) or (residue 37 and name hd2#)) 1.8 0.0 3.2 ! 4d, not sure of 34 assignment !LONG assign (residue 34 and name he#) (residue 168 and name hb#) 1.8 0.0 1.5 ! !R assign (residue 34 and name he#) (residue 46 and name hz2) 1.8 0.0 3.2 ! 3d c13aro noesy ! !INTRA assign (residue 35 and name hn) (residue 35 and name hg2#) 1.8 0.0 3.2 ! 6e6 assign (residue 35 and name hn) (residue 35 and (name hd# or name hb)) 1.8 0.0 1.1 ! 2.4e7 assign (residue 35 and name hn) (residue 35 and name ha) 1.8 0.0 1.7 ! !SEQ assign (residue 35 and name hn) (residue 34 and name hn) 1.8 0.0 1.7 ! assign (residue 35 and name hn) ((residue 34 and name hb1) or (residue 34 and name hb2)) 1.8 0.0 1.7 ! !R assign (residue 35 and name hn) (residue 36 and name hn) 1.8 0.0 1.1 ! !MED !dont see 38hbs to 35 ha assign (residue 35 and name hg2#) (residue 32 and name ha) 1.8 0.0 3.2 ! 4d assign (residue 35 and name hn) (residue 32 and name ha) 1.8 0.0 3.2 ! assign (residue 35 and name hn) (residue 33 and name ha) 1.8 0.0 3.2 ! STRONG? assign (residue 35 and name hn) (residue 33 and name hn) 1.8 0.0 3.2 ! assign (residue 35 and name hn) (residue 37 and name hn) 1.8 0.0 3.2 ! !LONG !R assign (residue 35 and name hg2#) (residue 102 and name he#) 1.8 0.0 3.2 ! 3d noesy, 3d aro for 102 HE sees 1.15ppm assign (residue 35 and name hg2#) ((residue 165 and name hd#) or (residue 112 and name hz)) 1.8 0.0 3.2 ! 3d aro noe to 35 hg2, it sees 6.75ppm assign (residue 35 and name hg2#) ((residue 112 and name he#) or (residue 32 and name hd#)) 1.8 0.0 3.2 ! 3d aro noe to 35 hg2, it sees 7.05ppm assign (residue 35 and name hd#) ((residue 165 and name hd#) or (residue 112 and name hz)) 1.8 0.0 3.2 ! assign (residue 35 and name hd#) ((residue 112 and name he#) or (residue 32 and name hd#)) 1.8 0.0 3.2 ! 3d aro noe to 35 hg2, it sees 7.05ppm assign (residue 35 and name hd#) (residue 145 and name hd#) 1.8 0.0 3.2 ! 4d !R assign (residue 148 and name hn) (residue 35 and name hd#) 1.8 0.0 3.2 !R 35 hd# sees it also assign (residue 35 and name hd#) (residue 149 and name hd#) 1.8 0.0 1.5 ! 4d assign (residue 35 and name hd#) (residue 157 and name hg#) 1.8 0.0 1.5 ! 4d, sees both 157 ch3s assign (residue 35 and name hd#) (residue 157 and name hb) 1.8 0.0 3.2 ! assign (residue 35 and name hd#) (residue 161 and name hg2#) 1.8 0.0 1.5 ! 4d !C36 !INTRA assign (residue 36 and name hn) (residue 36 and name ha) 1.8 0.0 1.7 ! !SEQ assign (residue 36 and name hn) (residue 35 and name hn) 1.8 0.0 1.1 ! assign (residue 36 and name hn) ((residue 35 and name hb) or (residue 35 and name hg2#)) 1.8 0.0 1.7 ! 1.2e7, 35hb ovlps 35hg2 assign (residue 36 and name hn) (residue 35 and name hd#) 1.8 0.0 3.2 ! !R assign (residue 36 and name hn) (residue 37 and name hn) 1.8 0.0 1.1 ! !MED !cant see hbs in 3d 13c noesy assign (residue 36 and name hn) (residue 33 and name ha) 1.8 0.0 3.2 ! ovlps 36hb# assign (residue 36 and name hn) (residue 34 and name hn) 1.8 0.0 3.2 ! ! 38hn ovlps 37hn !LONG !L37 !INTRA assign (residue 37 and name hn) (residue 37 and name ha) 1.8 0.0 1.7 ! !SEQ assign (residue 37 and name hn) (residue 36 and name ha) 1.8 0.0 1.7 ! assign (residue 37 and name hn) (residue 36 and name hb#) 1.8 0.0 1.7 ! !AR assign (residue 37 and name hn) (residue 38 and name hn) 1.8 0.0 ! 38hn ovlps 37hn !MED !dont see 43ha to 37hb assign (residue 37 and name hn) (residue 35 and name hn) 1.8 0.0 3.2 ! assign (residue 37 and name hn) (residue 35 and name hg2#) 1.8 0.0 3.2 ! assign (residue 37 and name hn) (residue 34 and name ha) 1.8 0.0 3.2 ! assign (residue 37 and name hn) (residue 39 and name hn) 1.8 0.0 3.2 ! assign (residue 37 and name hd#) ((residue 34 and name hg#) or (residue 36 and name hb#)) 1.8 0.0 3.2 !3d to 37 hd' at 2.73ppm, 37hd'' sees it also !LONG !A assign (residue 37 and name hn) (residue 46 and (name hz2 or name hd1)) 1.8 0.0 3.2 ! 6.82 ppm to 15n noesy !A assign ((residue 37 and name hd1#) or (residue 37 and name hd2#)) !A ((residue 46 and name hz2) or (residue 46 and name hd1)) 1.8 0.0 3.2 ! 3d to 37 hd' at 6.821ppm !SD? assign (residue 37 and name hn) (residue 49 and name hg#) 1.8 0.0 3.2 ! no pk for 37hn-49hg' assign (residue 37 and name hd#) ((residue 49 and name hg1#) or (residue 49 and name hg2#)) 1.8 0.0 3.2 ! 4d to 37 hd'' at 0.71/26.8, and to 37hd' assign ((residue 37 and name hd1#) or (residue 37 and name hd2#)) (residue 53 and name ha) 1.8 0.0 3.2 ! 4d to 37 hd' !A assign (residue 37 and name hn) !A ((residue 161 and name hg11) or (residue 161 and name hg12)) 1.8 0.0 3.2 !A pk at 1.27 ppm, 161 only close choice bue 161 hg1' not see 37hn !E38 !INTRA assign (residue 38 and name hn) (residue 38 and name ha) 1.8 0.0 0.9 ! !SEQ !A assign (residue 38 and name hn) (residue 37 and name hn) 1.8 0.0 ! 37hn ovlps 38hn !R assign (residue 38 and name hn) (residue 39 and name hn) 1.8 0.0 ! !MED assign (residue 38 and name hn) (residue 35 and name ha) 1.8 0.0 3.2 ! assign (residue 38 and name hn) ( (residue 35 and name hg1#) or (residue 161 and (name hg2# or name hd#)) ) 1.8 0.0 3.2 ! amb, 35 hg1s done see 8.77, but dont see 35hn either !LONG assign (residue 38 and name hn) ((residue 49 and name hg1#) or (residue 49 and name hg2#)) 1.8 0.0 3.2 ! amb, 49 hg' does not see 8.77 !G39 !INTRA assign (residue 39 and name hn) ((residue 39 and name ha1) or (residue 39 and name ha2)) 1.8 0.0 0.9 ! !SEQ assign (residue 39 and name hn) (residue 38 and name hn) 1.8 0.0 1.1 ! !A assign (residue 39 and name hn) (residue 40 and name hn) 1.8 0.0 ! 40hn ovlps 39hn !MED !AR assign (residue 39 and name hn) (residue 37 and name hn) 1.8 0.0 3.2 ! 37hn ovlps 38hn !LONG assign (residue 39 and name hn) (residue 156 and (name hb1 or name hb2)) 1.8 0.0 3.2 ! looks close as of 12/20/01 but AMB assign (residue 39 and name hn) (residue 161 and (name hg2# or name hd#)) 1.8 0.0 3.2 !9.9e6, 161hg2 and 161hd see 39hn, 161hd ovlps hg2 assign (residue 39 and name hn) (residue 161 and name hg1#) 1.8 0.0 3.2 ! 161hd much stronger assign (residue 39 and name ha#) (residue 161 and name hg2#) 1.8 0.0 3.2 ! 161hg2 sees 39ha' also !Q40 !40hn ovlps 66hn !INTRA !ha ovlps 66ha !SEQ !A assign (residue 40 and name hn) (residue 39 and name hn) 1.8 0.0 ! 39hn ovlps 40hn assign (residue 40 and name hn) (residue 41 and name hn) 1.8 0.0 3.2 ! !MED !LONG assign (residue 40 and name hn) ((residue 49 and name hg1#) or (residue 49 and name hg2#)) 1.8 0.0 3.2 ! 0.66 ppm, 49hg'' sees 40hn but very wk !Q41 !INTRA assign (residue 41 and name hn) (residue 41 and name ha) 1.8 0.0 1.7 ! assign (residue 41 and name hn) (residue 41 and name hb#) 1.8 0.0 1.1 ! !SEQ assign (residue 41 and name hn) (residue 40 and name hn) 1.8 0.0 3.2 ! assign (residue 41 and name hn) (residue 40 and name ha) 1.8 0.0 3.2 ! !R assign (residue 41 and name hn) (residue 42 and name hn) 1.8 0.0 1.1 ! 7e6 assign (residue 41 and name hn) (residue 42 and name hb#) 1.8 0.0 3.2 ! 1.55ppm, 42b# sees 7.42 !MED !A assign (residue 41 and name hg#) (residue 45 and name hn) 1.8 0.0 3.2 ! AMB, 45 hn sees no pk at 2.75 !LONG assign (residue 41 and name hn) (residue 49 and name hg#) 1.8 0.0 1.7 ! 0.399ppm, 49 hg' sees it !R assign (residue 41 and name hn) !R ((residue 49 and name hg1#) or (residue 49 and name hg2#)) 1.8 0.0 3.2 ! 0.666ppm, 49hg'' sees it !A assign (residue 41 and name hn) (residue 49 and name hb) 1.8 0.0 3.2 ! Amb, 1.39ppm, spin diffusion? assign (residue 41 and name ha) (residue 49 and name hg#) 1.8 0.0 1.5 ! 5.3e6 3dnoesy to 49hg'', 3.94/55.3 to 49hg'' in 4d, 1.5e6 assign (residue 41 and name hb#) (residue 49 and name hg#) 1.8 0.0 3.2 ! both hbs see 49hg'', 4d at 2.3/28.9 and 2.0/29.0 assign (residue 41 and name ha) ((residue 161 and name hd#) or (residue 44 and name hd#)) 1.8 0.0 3.2 ! 161hd sees it also {A*** assign (residue 41 and name hn) ((residue 161 and name hd#) or (residue 44 and name hd1#) or (residue 44 and name hd2#) or (residue 47 and name hg11) or (residue 47 and name hg12)) 1.8 0.0 3.2 ! Amb, none of these see pk at 7.42ppm ***} !A42 #2 of typeII turn ? !INTRA assign (residue 42 and name hn) (residue 42 and name ha) 1.8 0.0 0.9 !1.1e7 !SEQ assign (residue 42 and name hn) (residue 41 and name hn) 1.8 0.0 1.1 !8e6 assign (residue 42 and name hn) (residue 41 and name ha) 1.8 0.0 3.2 ! assign (residue 42 and name hn) ((residue 41 and name hb1) or (residue 41 and name hb2)) 1.8 0.0 1.7 ! !R assign (residue 42 and name hn) (residue 43 and name hn) 1.8 0.0 3.2 ! assign (residue 42 and name hb#) ((residue 43 and name ha1) or (residue 43 and name ha2)) 1.8 0.0 3.2 ! !MED !LONG assign (residue 42 and name hn) (residue 49 and name hg#) 1.8 0.0 3.2 ! 49hg' sees very wk 7.18ppm assign (residue 42 and name hb#) (residue 156 and name hd#) 1.8 0.0 3.2 !3d and 2d noesy !A assign (residue 42 and name hb#) (residue 156 and name he#) 1.8 0.0 3.2 !3d and 2d noesy assign (residue 42 and name hn) (residue 161 and (name hd# or name hg2#)) 1.8 0.0 1.7 !9e6, 161hd sees 7.2 assign (residue 42 and name hb#) (residue 161 and name hd#) 1.8 0.0 1.5 !4d !G43 #3 of typeII turn ? !INTRA !SEQ !dont see 42hn assign (residue 43 and name hn) (residue 42 and name ha) 1.8 0.0 0.9 ! stronger than either 43 ha1 or ha2 assign (residue 43 and name hn) (residue 42 and name hb#) 1.8 0.0 1.7 ! !R assign (residue 43 and name hn) (residue 44 and name hn) 1.8 0.0 1.7 ! !MED !LONG !L44 #4 of typeII turn ? !dont see 44ha in 3dnoesy, only intras and 45hn to 44hbs !nada to 44hg !44 INTRA assign (residue 44 and name hn) (residue 44 and name ha) 1.8 0.0 1.1 !2e7 assign (residue 44 and name hn) (residue 44 and name hb#) 1.8 0.0 1.7 !1.7e7 assign (residue 44 and name hn) (residue 44 and name hg) 1.8 0.0 1.7 !1.7e7 assign (residue 44 and name hn) (residue 44 and name hd#) 1.8 0.0 1.1 !3e7 !SEQ assign (residue 44 and name hn) (residue 43 and name hn) 1.8 0.0 1.1 ! 1.1e7 assign (residue 44 and name hn) ((residue 43 and name ha1) or (residue 43 and name ha2)) 1.8 0.0 1.7 ! !R assign (residue 44 and name hn) (residue 45 and name hn) 1.8 0.0 1.7 ! !MED assign (residue 44 and name hn) (residue 41 and name ha) 1.8 0.0 3.2 ! amb assign (residue 44 and name hn) ((residue 41 and name hb1) or (residue 41 and name hb2)) 1.8 0.0 3.2 ! amb assign (residue 44 and name hn) (residue 41 and name hg#) 1.8 0.0 3.2 ! amb !A assign (residue 44 and name hn) (residue 42 and name ha) 1.8 0.0 2.2 ! 1.1e7 amb, 42ha not see 44hn assign ((residue 44 and name hd1#) or (residue 44 and name hd2#)) (residue 48 and name hg2#) 1.8 0.0 3.2 ! 4d, pk at 1.18/21.6 to 44hd' !LONG assign ((residue 44 and name hd1#) or (residue 44 and name hd2#)) ((residue 49 and name hg1#) or (residue 49 and name hg2#)) 1.8 0.0 3.2 ! 44hd' pk at 0.65ppm, 49hg'' sees 0.92 assign ((residue 44 and name hd1#) or (residue 44 and name hd2#)) (residue 86 and name hd#) 1.8 0.0 3.2 ! 4d, pk at 0.74/12.8 to 44hd' assign ((residue 44 and name hd1#) or (residue 44 and name hd2#)) ((residue 86 and name hg11) or (residue 86 and name hg12)) 1.8 0.0 3.2 ! 4d, pk at 0.74/12.8 to 44hd', L44hd'' ovlps L103hd'' !R assign (residue 86 and name hg2#) !R ((residue 44 and name hd1#) or (residue 44 and name hd2#)) 1.8 0.0 1.5 ! 4D, sees both 44hds !S45 !no pks to ha in 3dnoesy !INTRA assign (residue 45 and name hn) (residue 45 and name hb#) 1.8 0.0 1.7 ! !SEQ assign (residue 45 and name hn) (residue 44 and name hn) 1.8 0.0 3.2 ! 8.6e6, 45hn to 44hn 7.44e7, wk relative to 44ha-45hn 2e7 !A assign (residue 45 and name hn) (residue 44 and name ha) 1.8 0.0 1.1 ! AMB, ovlps 45ha somewhat and water assign (residue 45 and name hn) (residue 44 and name hb#) 1.8 0.0 1.1 ! 2e7 assign (residue 45 and name hn) (residue 44 and name hg) 1.8 0.0 3.2 ! 9e6, vios as med, all pks stronger to 45hn assign (residue 45 and name hn) (residue 44 and name hd#) 1.8 0.0 1.7 ! !R assign (residue 45 and name hn) (residue 46 and name hn) 1.8 0.0 1.7 ! !MED assign (residue 45 and name hn) ((residue 40 and name hb#) or (residue 41 and name hb#)) 1.8 0.0 3.2 ! !R assign (residue 45 and name hb#) (residue 46 and name hn) 1.8 0.0 1.7 ! assign (residue 45 and name hb#) (residue 47 and name hg2#) 1.8 0.0 3.2 ! assign (residue 45 and name hb#) (residue 47 and name hn) 1.8 0.0 3.2 ! assign (residue 45 and name hn) (residue 48 and name hg2#) 1.8 0.0 3.2 ! 5e4, 48hg sees it also !LONG !W46 !INTRA assign (residue 46 and name hn) (residue 46 and name ha) 1.8 0.0 1.7 ! !SEQ assign (residue 46 and name hn) (residue 45 and name ha) 1.8 0.0 3.2 ! assign (residue 46 and name hn) (residue 45 and name hb#) 1.8 0.0 1.7 ! assign (residue 46 and name hn) (residue 45 and name ha) 1.8 0.0 1.1 ! !R assign (residue 46 and name hn) (residue 47 and name hn) 1.8 0.0 1.7 ! assign (residue 46 and name hn) (residue 47 and name hg2#) 1.8 0.0 3.2 ! amb, 47hg2 doesnt see it !MED !LONG !A? assign (residue 46 and name hd1) (residue 16 and name hd#) 1.8 0.0 3.2 ! 2d noesy !A? assign (residue 46 and name hz2) (residue 34 and name he#) 1.8 0.0 3.2 ! 3d c13aro noesy assign (residue 46 and name hn) ((residue 41 and name hb1) or (residue 41 and name hb2)) 1.8 0.0 3.2 ! amb, wk !A? assign (residue 46 and name hz2) !A ((residue 50 and name hd1#) or (residue 50 and name hd2#)) 1.8 0.0 3.2 ! 3d c13aro noesy !I47 !INTRA assign (residue 47 and name hn) (residue 47 and name hb) 1.8 0.0 1.1 ! 1e7 assign (residue 47 and name hn) (residue 47 and name hg2#) 1.8 0.0 1.1 ! 1.8e7 assign (residue 47 and name hn) (residue 47 and name hg2#) 1.8 0.0 3.2 ! 5e6 !SEQ assign (residue 47 and name hn) (residue 46 and name hn) 1.8 0.0 1.7 ! assign (residue 47 and name hn) ((residue 46 and name hb1) or (residue 46 and name hb2)) 1.8 0.0 1.7 ! !R assign (residue 47 and name hn) (residue 48 and name hn) 1.8 0.0 1.7 ! assign (residue 47 and name hg2#) (residue 48 and name ha) 1.8 0.0 3.2 ! !MED !R assign (residue 47 and name hn) (residue 45 and name hb#) 1.8 0.0 3.2 ! !R assign (residue 47 and name hg2#) (residue 45 and name hb#) 1.8 0.0 1.5 ! !R assign (residue 47 and name hd#) (residue 50 and name hn) 1.8 0.0 3.2 ! 3d assign (residue 47 and name ha) ((residue 50 and name hb1) or (residue 50 and name hb2)) 1.8 0.0 3.2 ! !R assign (residue 47 and name hd#) (residue 51 and name hn) 1.8 0.0 3.2 ! 3d assign (residue 47 and name hd#) (residue 51 and name he#) 1.8 0.0 3.2 ! 4d assign (residue 47 and name hg2#) (residue 51 and name he#) 1.8 0.0 3.2 ! 4d !LONG assign (residue 47 and name hd#) ((residue 12 and name hb1) or (residue 12 and name hb2)) 1.8 0.0 3.2 ! !R assign (residue 12 and name hd1#) (residue 47 and name hd#) 1.8 0.0 3.2 ! 4D, to both L12 hd#s !R assign (residue 12 and name hd2#) (residue 47 and name hd#) 1.8 0.0 3.2 ! 4D, to both L12 hd#s !R assign (residue 47 and name hd#) !R ((residue 13 and name ha) or (residue 45 and name ha)) 1.8 0.0 3.2 ! pk at 4.87ppm !R assign (residue 13 and name hd#) (residue 47 and name hd#) 1.8 0.0 3.2 ! !R assign (residue 13 and name he#) (residue 47 and name hd#) 1.8 0.0 3.2 ! !T48 !INTRA assign (residue 48 and name hn) (residue 48 and name ha) 1.8 0.0 1.7 ! 1e7 assign (residue 48 and name hn) (residue 48 and name hb) 1.8 0.0 1.1 ! 1.6e7 assign (residue 48 and name hn) (residue 48 and name hg2#) 1.8 0.0 1.7 ! 1e7 !SEQ assign (residue 48 and name hn) (residue 47 and name hn) 1.8 0.0 1.1 ! 6.5e6 assign (residue 48 and name hn) (residue 47 and name hb) 1.8 0.0 3.2 ! 4e6 assign (residue 48 and name hn) (residue 47 and name hg2#) 1.8 0.0 1.1 ! 2e7 assign (residue 48 and name hg2#) (residue 47 and name hg2#) 1.8 0.0 3.2 ! 2e7 !R assign (residue 48 and name hn) (residue 49 and name hn) 1.8 0.0 1.1 ! 6e6 assign (residue 48 and name hn) ((residue 49 and name hg1#) or (residue 49 and name hg2#)) 1.8 0.0 3.2 !MED assign (residue 48 and name hn) ((residue 44 and name hd1#) or (residue 44 and name hd2#)) 1.8 0.0 3.2 assign (residue 48 and name hb) ((residue 44 and name hd1#) or (residue 44 and name hd2#)) 1.8 0.0 3.2 !R assign (residue 48 and name hg2#) !R ((residue 44 and name hd1#) or (residue 44 and name hd2#)) 1.8 0.0 3.2 ! pk at 0.93/22.6, sees both 44 hds assign (residue 48 and name hn) (residue 45 and name hn) 1.8 0.0 3.2 ! !R assign (residue 48 and name hn) (residue 50 and name hn) 1.8 0.0 3.2 ! assign (residue 48 and name ha) (residue 51 and name hd#) 1.8 0.0 3.2 ! !LONG assign (residue 48 and name hg2#) (residue 86 and name hd#) 1.8 0.0 1.5 ! 4d pk at 0.75/12.85, and 86hd sees 1.17, but could be 14hd# !V49 !INTRA assign (residue 49 and name hn) (residue 49 and name ha) 1.8 0.0 1.7 ! 5e6 assign (residue 49 and name hn) (residue 49 and name hb) 1.8 0.0 1.1 ! 1.1e7 assign (residue 49 and name hn) (residue 49 and (name hg1# or name hg2#)) 1.8 0.0 1.7 ! 1.1e7 0.64ppm !SEQ assign (residue 49 and name hn) (residue 48 and name hn) 1.8 0.0 1.1 ! 7e6 assign (residue 49 and name hn) (residue 48 and name ha) 1.8 0.0 3.2 ! 2.8e6 assign (residue 49 and name hn) (residue 48 and name hb) 1.8 0.0 1.1 ! 8e6 assign (residue 49 and name hn) (residue 48 and name hg2#) 1.8 0.0 1.7 ! 7e6 assign (residue 49 and name hn) (residue 50 and name hn) 1.8 0.0 1.1 ! 9e6 !MED assign (residue 49 and name hn) (residue 47 and name hg2#) 1.8 0.0 3.2 ! !LONG assign ((residue 49 and name hg1#) or (residue 49 and name hg2#)) (residue 37 and name ha) 1.8 0.0 3.2 ! 3d at 3.49ppm, 37ha sees it assign ((residue 49 and name hg1#) or (residue 49 and name hg2#)) (residue 37 and name hd1#) 1.8 0.0 3.2 !!4d at 0.065/21.5 assign ((residue 49 and name hg1#) or (residue 49 and name hg2#)) (residue 37 and name hd2#) 1.8 0.0 3.2 !4d at 0.72/26.8, 49 hg' sees both 37 hds so use both (see above) !R assign ((residue 49 and name hg1#) or (residue 49 and name hg2#)) !R (residue 41 and name ha) 1.8 0.0 3.2 ! 4d at 3.94/55.3 to 49hg'', 1.5e6 !R assign ((residue 49 and name hg1#) or (residue 49 and name hg2#)) !R ((residue 41 and name hb1) or (residue 41 and name hb2)) 1.8 0.0 3.2 ! 4d at 2.3/28.9 and 2.0/29.0 !R assign ((residue 49 and name hg1#) or (residue 49 and name hg2#)) !R ((residue 44 and name hd1#) or (residue 44 and name hd2#)) 1.8 0.0 3.2 ! 4d 0.93/26.4 !R assign ((residue 49 and name hg1#) or (residue 49 and name hg2#)) !R (residue 86 and name hd#) 1.8 0.0 1.5 ! 4d 0.77/12.8 !L50 !INTRA assign (residue 50 and name hn) (residue 50 and name ha) 1.8 0.0 1.1 ! assign (residue 50 and name hn) (residue 50 and name hg) 1.8 0.0 1.7 ! !SEQ !R assign (residue 50 and name hn) (residue 49 and name hn) 1.8 0.0 1.7 ! 5.6e6 assign (residue 50 and name hn) (residue 49 and name hb) 1.8 0.0 1.1 ! !MED !A assign (residue 50 and name hd#) (residue 46 and name hz2) 1.8 0.0 3.2 ! assign (residue 50 and name hn) (residue 47 and name ha) 1.8 0.0 3.2 ! assign (residue 50 and name hn) (residue 47 and name hd#) 1.8 0.0 3.2 !3d assign (residue 50 and name hb#) (residue 47 and name hd#) 1.8 0.0 3.2 !3d to 50 hb'' assign (residue 50 and name hd#) (residue 47 and name hd#) 1.8 0.0 3.2 !4d at 0.4/13.8 assign (residue 50 and name hn) (residue 48 and name hn) 1.8 0.0 3.2 ! assign (residue 50 and name hn) (residue 52 and name hn) 1.8 0.0 3.2 ! !dont see 50ha to 53 hb assign (residue 50 and name hd#) (residue 53 and name hb#) 1.8 0.0 3.2 ! 3d to 50 hd'' !LONG assign (residue 50 and name hd1#) (residue 12 and name hd#) 1.8 0.0 3.2 ! 4d at 0.81/24.9 to 50 hd'', dont see 50 to 12hd ?? assign (residue 50 and name hd2#) (residue 12 and name hd#) 1.8 0.0 3.2 !4d at 0.96/24.1 to 50 hd', assign (residue 50 and name hd#) (residue 12 and name hg) 1.8 0.0 3.2 !3d at 1.644, 12hg sees 50hd' also !R assign (residue 50 and name hd#) (residue 13 and name he#) 1.8 0.0 3.2 assign (residue 50 and name hd#) (residue 16 and name hb#) 1.8 0.0 3.2 ! !R assign (residue 50 and name hd#) (residue 16 and name hd#) 1.8 0.0 3.2 ! assign (residue 50 and name hd#) (residue 21 and name hd1) 1.8 0.0 3.2 ! !K51 !INTRA assign (residue 51 and name hn) (residue 51 and name ha) 1.8 0.0 1.7 ! 1.2e7 assign (residue 51 and name hn) (residue 51 and name hb#) 1.8 0.0 1.1 ! 1.25e7 !SEQ assign (residue 51 and name hn) (residue 50 and name ha) 1.8 0.0 3.2 ! assign (residue 51 and name hn) ((residue 50 and name hb1) or (residue 50 and name hb2)) 1.8 0.0 1.7 ! !R assign (residue 51 and name hn) (residue 52 and name hn) 1.8 0.0 1.7 ! !MED assign (residue 51 and name hn) (residue 47 and name hd#) 1.8 0.0 3.2 ! 3d assign (residue 51 and name hn) (residue 49 and name hn) 1.8 0.0 3.2 ! !dont see 51ha to 54hb !dont see 47ha to 51hb !LONG assign (residue 51 and name hn) ((residue 12 and name hd1#) or (residue 12 and name hd2#)) 1.8 0.0 3.2 ! both 12hds see 51hn assign (residue 51 and name ha) ((residue 12 and name hd1#) or (residue 12 and name hd2#)) 1.8 0.0 1.5 ! assign (residue 51 and name hg#) (residue 12 and name hd#) 1.8 0.0 3.2 ! 3d to 51hg' assign (residue 51 and name hd#) ((residue 12 and name hd1#) or (residue 12 and name hd2#)) 1.8 0.0 3.2 ! assign (residue 51 and name he#) ((residue 12 and name hd1#) or (residue 12 and name hd2#)) 1.8 0.0 3.2 ! !A assign (residue 51 and name hn) (residue 16 and name he#) 1.8 0.0 3.2 ! !A assign (residue 51 and name hn) !A ((residue 46 and name hz2) or (residue 46 and name hd1)) 1.8 0.0 3.2 ! !K52 !not sure of any side chain assignments !INTRA assign (residue 52 and name hn) (residue 52 and name ha) 1.8 0.0 1.7 ! !assign (residue 52 and name hn) (residue and name h) 1.8 0.0 ! !SEQ assign (residue 52 and name hn) (residue 51 and name hn) 1.8 0.0 1.1 assign (residue 52 and name hn) (residue 51 and name ha) 1.8 0.0 3.2 !R assign (residue 52 and name hn) (residue 53 and name hn) 1.8 0.0 1.1 ! !MED !dont see any peaks to ha, or hb assign (residue 52 and name hn) (residue 49 and name ha) 1.8 0.0 3.2 ! assign (residue 52 and name hn) ((residue 49 and name hg1#) or (residue 49 and name hg2#)) 1.8 0.0 3.2 ! !R assign (residue 52 and name hn) (residue 50 and name hn) 1.8 0.0 3.2 ! !R assign (residue 52 and name hn) (residue 54 and name hn) 1.8 0.0 3.2 ! !LONG !R53 !INTRA assign (residue 53 and name hn) (residue 53 and name ha) 1.8 0.0 1.7 ! 4.4e6 assign (residue 53 and name hn) (residue 53 and name hb#) 1.8 0.0 1.1 ! 1.2e7 !SEQ assign (residue 53 and name hn) (residue 52 and name hn) 1.8 0.0 1.1 ! assign (residue 53 and name hn) (residue 54 and name hn) 1.8 0.0 1.7 ! !MED !dont see 56hb to 53 ha assign (residue 53 and name hn) (residue 49 and name ha) 1.8 0.0 3.2 ! assign (residue 53 and name hn) ((residue 49 and name hg1#) or (residue 49 and name hg2#)) 1.8 0.0 3.2 ! assign (residue 53 and name hn) (residue 50 and name ha) 1.8 0.0 1.7 assign (residue 53 and name hn) ((residue 50 and name hd1#) or (residue 50 and name hd2#)) 1.8 0.0 3.2 ! assign (residue 53 and name hn) (residue 51 and name ha) 1.8 0.0 3.2 assign (residue 53 and name hn) (residue 51 and name hn) 1.8 0.0 3.2 ! !LONG assign (residue 53 and name hn) ((residue 37 and name hd1#) or (residue 37 and name hd2#) or (residue 86 and name hd#)) 1.8 0.0 3.2 ! pk at 0.73ppm assign (residue 53 and name he) ((residue 37 and name hd1#) or (residue 37 and name hd2#)) 1.8 0.0 3.2 ! pk at 0.705ppm assign (residue 53 and name hn) ((residue 37 and name hd1#) or (residue 37 and name hd2#) or (residue 85 and name hg2#)) 1.8 0.0 3.2 ! pk at 0.05ppm assign (residue 53 and name he) ((residue 50 and name hd1#) or (residue 50 and name hd2#)) 1.8 0.0 3.2 ! pk at 0.57ppm !E54 !INTRA assign (residue 54 and name hn) (residue 54 and name ha) 1.8 0.0 1.1 ! assign (residue 54 and name hn) ((residue 54 and name hb1) or (residue 54 and name hb2)) 1.8 0.0 1.1 ! !SEQ !A assign (residue 54 and name hn) (residue 53 and name hn) 1.8 0.0 1.1 ! 53hn ovlps 55hn assign (residue 54 and name hn) (residue 53 and name ha) 1.8 0.0 3.2 ! assign (residue 54 and name hn) (residue 53 and name hb#) 1.8 0.0 1.7 ! !A assign (residue 54 and name hn) (residue 55 and name hn) 1.8 0.0 1.1 ! 53hn ovlps 55hn !MED !not sure about 54ha to 57hb b/c dont have R57 hbs assigned !dont see 51ha to 54hbs assign (residue 54 and name hn) (residue 52 and name hn) 1.8 0.0 3.2 ! assign (residue 54 and name hn) (residue 56 and name hn) 1.8 0.0 3.2 ! !LONG assign (residue 54 and name hn) ((residue 37 and name hd1#) or (residue 37 and name hd2#) or (residue 85 and name hg2#)) 1.8 0.0 3.2 ! pk at 0.05ppm !N55 !INTRA assign (residue 55 and name hn) (residue 55 and name ha) 1.8 0.0 1.1 ! assign (residue 55 and name hn) ((residue 55 and name hb1) or (residue 55 and name hb2)) 1.8 0.0 1.1 ! !SEQ assign (residue 55 and name hn) (residue 54 and name hn) 1.8 0.0 1.1 ! assign (residue 55 and name hn) ((residue 54 and name hb1) or (residue 54 and name hb2)) 1.8 0.0 1.7 ! !R assign (residue 55 and name hn) (residue 56 and name hn) 1.8 0.0 1.7 ! !MED assign (residue 55 and name hn) (residue 52 and name ha) 1.8 0.0 3.2 ! assign (residue 55 and name hn) (residue 53 and name ha) 1.8 0.0 3.2 ! !53hn ovlps 55hn !57hn ovlps 56hn assign (residue 55 and name ha) (residue 58 and name hb#) 1.8 0.0 1.5 ! 3d and 4d to 58hb# !LONG assign (residue 55 and name hn) ((residue 37 and name hd1#) or (residue 37 and name hd2#) or (residue 85 and name hg2#)) 1.8 0.0 3.2 ! pk at 0.05ppm assign ((residue 55 and name hb1) or (residue 55 and name hb2)) (residue 85 and name hg2#) 1.8 0.0 3.2 ! pk at 0.03ppm, 85hg2 sees both 55hbs !Y56 !INTRA assign (residue 56 and name hn) (residue 56 and name ha) 1.8 0.0 1.1 assign (residue 56 and name hn) (residue 56 and name hd#) 1.8 0.0 2.2 ! 7.6e6, vios as med !Y56 SEQ assign (residue 56 and name hn) (residue 55 and name hn) 1.8 0 1.1 assign (residue 56 and name hn) (residue 55 and name ha) 1.8 0 3.2 assign (residue 56 and name hn) (residue 55 and name hb#) 1.8 0.0 1.7 !A assign (residue 56 and name hn) (residue 57 and name hn) 1.8 0 1.1 !Y56 MED !53ha ovlps 56ha !53ha to 56hbs not seen assign (residue 56 and name hn) (residue 54 and name hn) 1.8 0 3.2 !54ha to 56hn not seen assign (residue 56 and name ha) ((residue 59 and name hb1) or (residue 59 and name hb2)) 1.8 0 3.2 !58hn ovlps 55hn assign (residue 60 and name hd#) (residue 56 and name he#) 1.8 0.0 3.2 ! 2d noesy assign (residue 60 and name he#) (residue 56 and name he#) 1.8 0.0 3.2 ! 2d noesy !LONG assign (residue 56 and name hn) ((residue 85 and name hg2#) or (residue 37 and name hd1#) or (residue 37 and name hd2#) ) 1.8 0 1.7 ! 0.05ppm, 85hg2 sees 8.62, ovlps 37 hn at 8.71 assign (residue 56 and name ha) (residue 85 and name hg2#) 1.8 0.0 3.2 ! 4D to 56ha and 4d to 85hg2 assign (residue 56 and (name hb1 or name hb2)) (residue 85 and name hg2#) 1.8 0.0 3.2 !85hg2# sees wk pk to hb'' assign (residue 56 and name hd#) (residue 37 and (name hd1# or name hd2#)) 1.8 0 3.2 ! in 2d and 3d aro at 0.05ppm, 37hd' sees 7.15ppm assign (residue 56 and name he#) ((residue 37 and name hd1#) or (residue 37 and name hd2#)) 1.8 0 3.2 ! in 2d and 3d aro at 0.05ppm, 37hd' sees 6.67ppm assign (residue 56 and name hd#) (residue 95 and name hd#) 1.8 0 3.2 ! in 2d and 3d aro at 0.21ppm, 95hd sees 7.15ppm also assign (residue 56 and name he#) (residue 95 and name hd#) 1.8 0 3.2 ! in 2d and 3d aro at 0.21ppm, 95hd sees 6.67ppm also assign (residue 56 and name hd#) ((residue 95 and name hg11) or (residue 95 and name hg12)) 1.8 0 3.2 ! in 2d and 3d aro at 0.4ppm, 95hg1' sees 7.15ppm??? assign (residue 56 and name he#) ((residue 95 and name hg11) or (residue 95 and name hg12)) 1.8 0 3.2 ! in 2d and 3d aro at 0.4ppm, 95hg1' sees 6.67ppm !R57 !dont see ha in 3dnoesy !INTRA assign (residue 57 and name hn) (residue 57 and name ha) 1.8 0.0 1.7 ! assign (residue 57 and name hn) (residue 57 and name he) 1.8 0.0 3.2 ! !SEQ !56hn ovlps 57hn assign (residue 57 and name hn) (residue 56 and name ha) 1.8 0.0 3.2 ! assign (residue 57 and name hn) ((residue 56 and name hb1) or (residue 56 and name hb2)) 1.8 0.0 1.7 ! assign (residue 57 and name hn) (residue 56 and name hd#) 1.8 0.0 3.2 ! !R assign (residue 57 and name hn) (residue 58 and name hn) 1.8 0.0 1.1 ! !MED !55hn ovlps 58hn assign (residue 57 and name hn) (residue 54 and name ha) 1.8 0.0 1.7 ! !LONG assign (residue 57 and name hn) ((residue 37 and (name hd1# or name hd2#)) or (residue 85 and name hg2#)) 1.8 0.0 3.2 ! pk at 0.05ppm, neither 37hd' or 85hd see it !A58 !INTRA assign (residue 58 and name hn) (residue 58 and name ha) 1.8 0.0 1.1 ! assign (residue 58 and name hn) (residue 58 and name hb#) 1.8 0.0 1.7 ! !SEQ assign (residue 58 and name hn) (residue 57 and name hn) 1.8 0.0 1.1 ! assign (residue 58 and name hn) (residue 57 and name ha) 1.8 0.0 3.2 ! !R assign (residue 58 and name hn) (residue 59 and name hn) 1.8 0.0 1.1 ! !MED !54ha ovlps 58ha !dont see 56ha !56hn ovlps 57hn assign (residue 58 and name hn) (residue 55 and name ha) 1.8 0.0 1.7 ! assign (residue 58 and name hn) (residue 60 and name hn) 1.8 0.0 3.2 ! assign (residue 58 and name hb#) (residue 60 and name hn) 1.8 0.0 3.2 ! !LONG assign (residue 58 and name hn) (residue 85 and name hg2#) 1.8 0.0 3.2 ! !no long range to ha or hb* in 3dnoesy !C59 !dont see ha or hbs in 3d noesy !INTRA assign (residue 59 and name hn) (residue 59 and name ha) 1.8 0.0 1.1 ! assign (residue 59 and name hn) ((residue 59 and name hb1) or (residue 59 and name hb2)) 1.8 0.0 1.1 ! !SEQ assign (residue 59 and name hn) (residue 58 and name hn) 1.8 0.0 1.1 ! assign (residue 59 and name hn) (residue 58 and name ha) 1.8 0.0 1.7 ! assign (residue 59 and name hn) (residue 58 and name hb#) 1.8 0.0 1.1 ! 2e7 !R assign (residue 59 and name hn) (residue 60 and name h) 1.8 0.0 1.1 ! !MED assign (residue 59 and name hn) (residue 57 and name hn) 1.8 0.0 3.2 ! !LONG assign (residue 59 and name hn) (residue 85 and name hg2#) 1.8 0.0 3.2 ! pk at 0.05ppm, 85hg2 sees wk pk to 59hn assign (residue 59 and name hn) ((residue 79 and name hd1#) or (residue 79 and name hd2#)) 1.8 0.0 3.2 ! pks at 0.36 and 0.57ppm, 79hd''(0.57) sees wk pk to 59hn assign (residue 59 and name hb1) ((residue 79 and name hd1#) or (residue 79 and name hd2#)) 1.8 0.0 3.2 ! pks at 0.57ppm, 79hd''(0.57) sees both 59hbs assign (residue 59 and name hb2) ((residue 79 and name hd1#) or (residue 79 and name hd2#)) 1.8 0.0 3.2 ! pks at 0.57ppm, 79hd''(0.57) sees both 59hbs !F60 !INTRA assign (residue 60 and name hn) (residue 60 and name ha) 1.8 0.0 1.1 ! !SEQ assign (residue 60 and name hn) (residue 59 and name hn) 1.8 0.0 1.1 ! assign (residue 60 and name hn) (residue 59 and name ha) 1.8 0.0 1.7 ! !R assign (residue 60 and name hn) (residue 61 and name hn) 1.8 0.0 1.1 ! !MED assign (residue 60 and name hd#) (residue 56 and name ha) 1.8 0.0 3.2 ! 2d noesy !R assign (residue 60 and name hd#) (residue 56 and name he#) 1.8 0.0 3.2 ! 2d noesy !R assign (residue 60 and name he#) (residue 56 and name he#) 1.8 0.0 3.2 ! 2d noesy assign (residue 60 and name hn) (residue 57 and name ha) 1.8 0.0 3.2 ! !R assign (residue 60 and name hn) (residue 58 and name hn) 1.8 0.0 3.2 ! assign (residue 60 and name hn) (residue 58 and name ha) 1.8 0.0 3.2 ! !F60 LONG !A assign (residue 60 and name hn) (residue 68 and name hg#) 1.8 0.0 3.2 ! 1.107ppm, 68hg' sees 7.59, vios 3apr02 assign (residue 60 and name ha) (residue 68 and name hg#) 1.8 0.0 3.2 ! pk at 1.126, 68hg' sees 4.32 assign (residue 60 and name hd#) (residue 68 and name hg#) 1.8 0.0 3.2 ! 2d noesy, 68hg'' sees 7.40 !R assign (residue 60 and name hn) (residue 71 and name he#) 1.8 0.0 3.2 ! 71he sees 7.57 !R assign (residue 60 and name ha) (residue 71 and name he#) 1.8 0.0 3.2 ! 71he sees 4.32 assign (residue 60 and name hd#) (residue 71 and name he#) 1.8 0.0 3.2 !2d noesy, 71he sees 7.40 assign (residue 60 and name hd#) (residue 85 and name hg2#) 1.8 0.0 3.2 !2d noesy, 85hg2 sees 7.40 assign (residue 60 and name hd#) (residue 85 and name hd#) 1.8 0.0 3.2 !2d noesy, 85hd sees 7.40 !SD? assign (residue 60 and name hd#) (residue 85 and name hg1#) 1.8 0.0 3.2 !2d noesy assign (residue 60 and name hd#) (residue 95 and name hg2#) 1.8 0.0 3.2 !2d noesy, 95hg2 sees 7.40 assign (residue 60 and name hd#) (residue 95 and name hd#) 1.8 0.0 3.2 !2d noesy, 95hd sees 7.40 assign (residue 60 and name he#) (residue 95 and name hd#) 1.8 0.0 3.2 !2d noesy, 95hd sees 7.10 !A assign (residue 60 and name hd#) (residue 95 and name hg1#) 1.8 0.0 3.2 !2d noesy !??? pk at 1.69 ppm sees hn, ha, hbs, and hd ?? !H61 !INTRA assign (residue 61 and name hn) (residue 61 and name ha) 1.8 0.0 1.1 ! !SEQ assign (residue 61 and name hn) (residue 60 and name hn) 1.8 0.0 1.1 ! assign (residue 61 and name hn) (residue 60 and name ha) 1.8 0.0 1.7 ! !R assign (residue 61 and name hn) (residue 62 and name hn) 1.8 0.0 1.1 ! !MED assign (residue 61 and name hn) (residue 59 and name hn) 1.8 0.0 3.2 ! vios, 59hn sees 61hn also assign (residue 61 and name hn) (residue 63 and name hn) 1.8 0.0 3.2 ! assign (residue 61 and name ha) (residue 63 and name hn) 1.8 0.0 3.2 ! 63hn sees 61ha !LONG !A assign (residue 61 and name hn) (residue 68 and (name hg1# or name hg2#)) 1.8 0.0 3.2 ! pk at 1.104, neither 68hg' or 68 hg'' sees 7.42, could ovlp F60hd !Q62 !INTRA assign (residue 62 and name hn) (residue 62 and name ha) 1.8 0.0 1.1 ! !SEQ assign (residue 62 and name hn) (residue 61 and name hn) 1.8 0.0 1.7 ! assign (residue 62 and name hn) (residue 61 and name ha) 1.8 0.0 1.7 ! !R assign (residue 62 and name hn) (residue 63 and name hn) 1.8 0.0 1.1 ! !MED assign (residue 62 and name hn) (residue 60 and name hn) 1.8 0.0 3.2 ! assign (residue 62 and name hn) (residue 64 and name hn) 1.8 0.0 3.2 ! !LONG assign (residue 62 and name hn) (residue 57 and name ha) 1.8 0.0 3.2 !R57ha sees v wk pk to 62hn, vios 3apr02 but ave dist. = 4.7A for 20 strucs !F63 !INTRA assign (residue 63 and name hn) (residue 63 and name ha) 1.8 0.0 1.1 ! assign (residue 63 and name hn) (residue 63 and name hd#) 1.8 0.0 3.2 !7e6, 60he ovlps 63hd !SEQ assign (residue 63 and name hn) (residue 62 and name hn) 1.8 0.0 1.7 ! assign (residue 63 and name hn) (residue 62 and name hb#) 1.8 0.0 2.2 !4.6e6 !R assign (residue 63 and name hn) (residue 64 and name hn) 1.8 0.0 1.1 ! !MED assign (residue 63 and name hn) (residue 61 and name hn) 1.8 0.0 3.2 ! !R assign (residue 61 and name ha) (residue 63 and name hn) 1.8 0.0 3.2 ! 63hn sees 61ha assign (residue 63 and name hn) ((residue 61 and name hb1) or (residue 61 and name hb2)) 1.8 0.0 3.2 ! !LONG assign (residue 63 and name hn) ((residue 68 and name hg1#) or (residue 68 and name hg2#)) 1.8 0.0 3.2 ! pk at 1.106, 68hg' sees own hn at 8.41, could be 63hn also assign (residue 63 and name ha) ((residue 68 and name hg1#) or (residue 68 and name hg2#)) 1.8 0.0 3.2 ! pk at 1.106, 68hg' sees pk at 3.53 !D64 !dont see ha or hbs in 3d noesy !INTRA assign (residue 64 and name hn) (residue 64 and name ha) 1.8 0.0 1.7 ! assign (residue 64 and name hn) (residue 64 and name hb#) 1.8 0.0 1.1 ! !SEQ assign (residue 64 and name hn) (residue 63 and name hn) 1.8 0.0 1.7 ! assign (residue 64 and name hn) (residue 63 and name ha) 1.8 0.0 1.7 ! assign (residue 64 and name hn) (residue 63 and name hd#) 1.8 0.0 3.2 ! !A assign (residue 64 and name hn) (residue 65 and (name hb1 or name hb2)) 1.8 0.0 3.2 ! 1.45ppm !MED !A assign (residue 64 and name hn) (residue 61 and (name hb1 or name hb2)) 1.8 0.0 3.2 ! AMB !R assign (residue 64 and name hn) (residue 62 and name hn) 1.8 0.0 1.7 ! assign (residue 64 and name hn) (residue 62 and name hb#) 1.8 0.0 3.2 ! assign (residue 64 and name hn) (residue 67 and name hb#) 1.8 0.0 3.2 !AMB assign (residue 64 and name hn) (residue 67 and name hd#) 1.8 0.0 3.2 !AMB !LONG assign (residue 64 and name hn) ((residue 68 and name hg1#) or (residue 68 and name hg2#)) 1.8 0.0 3.2 ! pk at 1.11, 68hg' sees pk at 7.24 !P65 !SEQ assign ((residue 65 and name hd1) or (residue 65 and name hd2)) (residue 64 and name ha) 1.8 0.0 1.5 ! stronger to 65hd' assign ((residue 65 and name hb1) or (residue 65 and name hb2)) (residue 66 and name hn) 1.8 0.0 3.2 ! stronger to 65hb'' !MED assign (residue 65 and name ha) (residue 68 and name hn) 1.8 0.0 3.2 ! assign (residue 65 and name ha) (residue 69 and name hn) 1.8 0.0 3.2 ! !V66 !INTRA assign (residue 66 and name hn) (residue 66 and name ha) 1.8 0.0 1.1 ! assign (residue 66 and name hn) (residue 66 and name hb) 1.8 0.0 1.1 ! !SEQ assign (residue 66 and name hn) (residue 65 and name hb#) 1.8 0.0 1.7 ! assign (residue 66 and name ha) (residue 65 and name hb#) 1.8 0.0 3.2 assign (residue 66 and name hn) ((residue 65 and name hg#) or (residue 67 and name hg#)) 1.8 0.0 2.2 ! !A assign (residue 66 and name ha) (residue 65 and name hg#) 1.8 0.0 3.2 !65hgs dont see it assign (residue 66 and name hn) (residue 65 and name hd#) 1.8 0.0 3.2 ! assign (residue 66 and name hg#) (residue 65 and name hd#) 1.8 0.0 3.2 ! to both 66hgs in 3d !R assign (residue 66 and name hn) (residue 67 and name hn) 1.8 0.0 1.1 ! assign ((residue 66 and name hg1#) or (residue 66 and name hg2#)) (residue 67 and name hg#) 1.8 0.0 3.2 ! 4d to 66hd' assign ((residue 66 and name hg1#) or (residue 66 and name hg2#)) (residue 67 and name hd#) 1.8 0.0 3.2 ! 3d to 66hd' !MED !R assign (residue 66 and name hn) (residue 68 and name hn) 1.8 0.0 3.2 ! assign (residue 66 and name ha) (residue 69 and name hb#) 1.8 0.0 3.2 ! assign ((residue 66 and name hg1#) or (residue 66 and name hg2#)) (residue 70 and name hb#) 1.8 0.0 3.2 ! 4d to 66hd' !LONG assign (residue 66 and name ha) (residue 103 and name hd#) 1.8 0.0 1.5 assign ((residue 103 and name hd1#) or (residue 103 and name hd2#)) (residue 66 and name hn) 1.8 0.0 3.2 ! 3d to hd'' assign ((residue 66 and name hg1#) or (residue 66 and name hg2#)) ((residue 103 and name hd1#) or (residue 103 and name hd2#)) 1.8 0.0 1.5 ! 4d to 66hg'' !R assign ((residue 66 and name hg1#) or (residue 66 and name hg2#)) !R ((residue 103 and name hd1#) or (residue 103 and name hd2#)) 1.8 0.0 1.5 ! 66hg' 4d assign ((residue 66 and name hg1#) or (residue 66 and name hg2#)) ((residue 103 and name hb1) or (residue 103 and name hb2)) 1.8 0.0 3.2 ! 3d to 66hg' !K67 !INTRA assign (residue 67 and name hn) (residue 67 and name ha) 1.8 0.0 1.1 ! assign (residue 67 and name hn) ((residue 64 and name hb#) or (residue 67 and name he#)) 1.8 0.0 1.7 !8.2e6 assign (residue 67 and name hn) (residue 67 and name hg#) 1.8 0.0 2.2 ! assign (residue 67 and name ha) (residue 67 and name hd#) 1.8 0.0 3.2 ! !SEQ assign (residue 67 and name hn) (residue 66 and name hn) 1.8 0.0 1.1 ! assign (residue 67 and name hn) (residue 66 and name ha) 1.8 0.0 1.7 ! assign (residue 67 and name hn) (residue 66 and name hb) 1.8 0.0 1.7 ! 67hn to 66hb med at most (ovlps 81hn-80hb) !R assign (residue 67 and name hn) (residue 68 and name hn) 1.8 0.0 1.1 ! !MED assign (residue 67 and name hn) (residue 69 and name hn) 1.8 0.0 3.2 ! assign (residue 67 and name ha) (residue 70 and name hb#) 1.8 0.0 1.5 ! assign (residue 67 and name hg#) (residue 70 and name hb#) 1.8 0.0 3.2 !med to 67hg, wk to 70hb# !LONG !V68 !INTRA assign (residue 68 and name hn) (residue 68 and name ha) 1.8 0.0 1.1 ! !SEQ assign (residue 68 and name hn) (residue 67 and name hn) 1.8 0.0 1.1 ! assign (residue 68 and name hn) (residue 67 and name ha) 1.8 0.0 3.2 ! assign (residue 68 and name hn) (residue 67 and name hb#) 1.8 0.0 1.7 ! assign (residue 68 and name hn) ((residue 67 and name he#) or (residue 64 and name hb#)) 1.8 0.0 3.2 ! !R assign (residue 68 and name hn) (residue 69 and name hn) 1.8 0.0 1.1 ! !MED !R assign ((residue 68 and name hg1#) or (residue 68 and name hg2#)) !R (residue 64 and name hn) 1.8 0.0 3.2 ! 3d to 66hd' assign (residue 68 and name hn) (residue 66 and name hn) 1.8 0.0 3.2 ! assign ((residue 68 and name hg1#) or (residue 68 and name hg2#)) (residue 65 and name ha) 1.8 0.0 3.2 ! !R assign (residue 68 and name hn) (residue 70 and name hn) 1.8 0.0 3.2 ! !LONG !R assign (residue 60 and name ha) !R ((residue 68 and name hg1#) or (residue 68 and name hg2#)) 1.8 0.0 3.2 ! pk at 1.126, 68hg' sees 4.32 !R assign (residue 60 and name hn) !R ((residue 68 and name hg1#) or (residue 68 and name hg2#)) 1.8 0.0 3.2 ! pk at 1.107, 68hg' sees 7.59 !R assign (residue 60 and name hd#) !R ((residue 68 and name hg1#) or (residue 68 and name hg2#)) 1.8 0.0 3.2 ! 2d noesy, 68hg'' sees 7.40 !R assign ((residue 68 and name hg1#) or (residue 68 and name hg2#)) !R (residue 63 and name ha) 1.8 0.0 3.2 ! 4d to 66hd' assign ((residue 68 and name hg1#) or (residue 68 and name hg2#)) ((residue 63 and name hd#) or (residue 60 and name he#) or (residue 67 and name hn)) 1.8 0.0 3.2 ! 3d to 66hd' 7.08ppm, and 7.074ppm to 68hd'' !R assign ((residue 68 and name hg1#) or (residue 68 and name hg2#)) !R (residue 95 and name hg2#) 1.8 0.0 1.5 ! 4d to 66hd' and to 66hg''(stronger) assign ((residue 68 and name hg1#) or (residue 68 and name hg2#)) (residue 96 and name hn) 1.8 0.0 3.2 ! 4d to 66hd' and 66hd''(stronger) assign (residue 68 and name hn) (residue 99 and name hb#) 1.8 0.0 3.2 ! 99hb sees v wk pk at 8.40ppm assign ((residue 68 and name hg1#) or (residue 68 and name hg2#)) (residue 99 and name hb#) 1.8 0.0 1.5 ! 4d to 66hd' and 66hd''(stronger) !A69 !INTRA !SEQ assign (residue 69 and name hn) (residue 68 and name hn) 1.8 0.0 1.1 ! assign (residue 69 and name hn) ((residue 68 and name ha) or (residue 65 and name ha)) 1.8 0.0 1.7 ! assign (residue 69 and name hn) (residue 68 and name hb) 1.8 0.0 1.7 ! assign (residue 69 and name hn) ((residue 68 and name hg1#) or (residue 68 and name hg2#)) 1.8 0.0 1.7 ! !R assign (residue 69 and name hn) (residue 70 and name hn) 1.8 0.0 1.1 ! !MED !R assign (residue 69 and name hb#) (residue 66 and name ha) 1.8 0.0 1.5 !4d assign (residue 69 and name hb#) ((residue 66 and name hg1#) or (residue 66 and name hg2#)) 1.8 0.0 3.2 !4d !R assign (residue 69 and name hn) (residue 71 and name hn) 1.8 0.0 3.2 ! !LONG assign (residue 69 and name hn) ((residue 60 and name ha) or (residue 70 and name ha)) 1.8 0.0 3.2 ! assign (residue 69 and name ha) (residue 96 and name hg2#) 1.8 0.0 3.2 ! 4d to 96hg2 assign (residue 69 and name hn) (residue 99 and name hb#) 1.8 0.0 1.7 ! 99hb# sees 8.23 med, but 99hn at 8.25ppm assign (residue 69 and name hb#) (residue 99 and name hb#) 1.8 0.0 1.5 !4d assign (residue 69 and name hb#) (residue 100 and name ha) 1.8 0.0 3.2 !4d assign (residue 69 and name hb#) (residue 100 and name hn) 1.8 0.0 3.2 !3d assign (residue 69 and name hb#) (residue 100 and name hb#) 1.8 0.0 3.2 !4d assign (residue 69 and name hn) ((residue 103 and name hd1#) or (residue 103 and name hd2#)) 1.8 0.0 3.2 ! sees both 102 hd' and hd'' assign (residue 69 and name hb#) ((residue 103 and name hd1#) or (residue 103 and name hd2#)) 1.8 0.0 1.5 !4d !END HELIX 4 !A70 !INTRA assign (residue 70 and name hn) (residue 70 and name ha) 1.8 0.0 1.1 ! assign (residue 70 and name hn) (residue 70 and name hb#) 1.8 0.0 1.1 ! !SEQ assign (residue 70 and name hn) (residue 69 and name hn) 1.8 0.0 1.1 ! assign (residue 70 and name hn) (residue 69 and name ha) 1.8 0.0 3.2 ! !R assign (residue 70 and name hn) (residue 71 and name h) 1.8 0.0 1.1 ! !MED !R 66hg' to 70hb# assign (residue 70 and name hn) (residue 67 and name ha) 1.8 0.0 3.2 ! assign (residue 70 and name hb#) (residue 67 and name ha) 1.8 0.0 1.5 ! assign (residue 70 and name hn) (residue 68 and name hn) 1.8 0.0 3.2 ! assign (residue 70 and name hn) (residue 68 and name ha) 1.8 0.0 3.2 ! !LONG !AMB assign (residue 70 and name hn) (residue 60 and name hd#) 1.8 0.0 3.2 ! assign (residue 70 and name hn) (residue 99 and name hb#) 1.8 0.0 3.2 ! 99hb sees 70hn !M71 !INTRA assign (residue 71 and name hn) (residue 71 and name ha) 1.8 0.0 1.1 ! assign (residue 71 and name hn) (residue 71 and name he#) 1.8 0.0 3.2 ! assign (residue 71 and name he#) (residue 71 and name ha) 1.8 0.0 3.2 ! 4d !SEQ assign (residue 71 and name hn) (residue 70 and name hn) 1.8 0.0 1.1 ! assign (residue 71 and name hn) (residue 70 and name ha) 1.8 0.0 1.7 ! assign (residue 71 and name hn) (residue 70 and name hb#) 1.8 0.0 1.7 ! 1.3e7 !R assign (residue 71 and name hn) (residue 72 and name hn) 1.8 0.0 1.7 ! 5e6 !MED assign (residue 71 and name hn) ((residue 68 and name ha) or (residue 96 and name ha) or (residue 99 and name ha)) 1.8 0.0 1.7 ! assign (residue 71 and name he#) (residue 68 and name ha) 1.8 0.0 3.2 ! 4d assign (residue 71 and name hn) ((residue 68 and name hg1#) or (residue 68 and name hg2#)) 1.8 0.0 3.2 !AMB 68hg'' sees v wk to 71hn, at 7.69ppm assign (residue 71 and name hn) (residue 69 and name hn) 1.8 0.0 3.2 ! assign (residue 71 and name he#) (residue 75 and name ha) 1.8 0.0 3.2 ! 4D !R assign (residue 71 and name he#) (residue 75 and name hb#) 1.8 0.0 3.2 ! 4d !LONG assign (residue 71 and name he#) ((residue 60 and name hn) or (residue 76 and name hn)) 1.8 0.0 3.2 ! 60hn and 76hn see 1.94ppm assign (residue 71 and name he#) (residue 60 and name ha) 1.8 0.0 3.2 ! 4d !R assign (residue 71 and name he#) (residue 60 and name hd#) 1.8 0.0 3.2 ! 4d assign (residue 71 and name he#) (residue 63 and name hd#) 1.8 0.0 3.2 ! AMB 3d assign (residue 71 and name he#) (residue 76 and name hg#) 1.8 0.0 3.2 ! 4d !A assign (residue 71 and name hn) !A ((residue 78 and name hd1) or (residue 78 and name hd2)) 1.8 0.0 3.2 !AMB 78hd'' does not see 71hn !Aassign (residue 71 and name he#) (residue 78 and name hd#) 1.8 0.0 3.2 ! 78hds not see it assign (residue 71 and name he#) (residue 79 and name hd#) 1.8 0.0 1.5 !4d, vios but looks like a med assign (residue 71 and name hn) (residue 96 and name hd#) 1.8 0.0 3.2 ! 96hd sees v wk to 71hn assign (residue 71 and name hn) (residue 96 and name hg2#) 1.8 0.0 3.2 ! 96g2 sees v wk to 71hn ? but 71hn ovlps 100hn assign (residue 71 and name he#) (residue 96 and name hd#) 1.8 0.0 3.2 ! 4d, wk to 96hd assign (residue 71 and name he#) (residue 96 and name hn) 1.8 0.0 3.2 ! 3d !Q72 !no peaks to ha in 3d noesy !INTRA assign (residue 72 and name hn) (residue 72 and name ha) 1.8 0.0 3.2 ! assign (residue 72 and name hn) (residue 72 and name hb#) 1.8 0.0 1.1 ! !SEQ assign (residue 72 and name hn) (residue 71 and name hn) 1.8 0.0 3.2 ! 4.6e5, vios for med, go to w assign (residue 72 and name hn) (residue 71 and name ha) 1.8 0.0 1.1 ! 1.2e7, looks strong assign (residue 72 and name hn) (residue 71 and name he#) 1.8 0.0 3.2 !9.6e6 assign (residue 72 and name hn) (residue 71 and name hg#) 1.8 0.0 1.7 ! !R assign (residue 72 and name hn) (residue 73 and name hn) 1.8 0.0 1.7 ! !MED !R assign (residue 72 and name hn) (residue 75 and name hn) 1.8 0.0 1.7 ! !LONG !E73 !nada to hbs in 3d noesy !INTRA assign (residue 73 and name hn) (residue 73 and name ha) 1.8 0.0 1.1 ! assign (residue 73 and name hn) (residue 73 and name hb#) 1.8 0.0 1.1 ! !SEQ assign (residue 73 and name hn) (residue 72 and name hn) 1.8 0.0 3.2 ! assign (residue 73 and name hn) (residue 72 and name ha) 1.8 0.0 1.1 ! assign (residue 73 and name hn) (residue 72 and name hb#) 1.8 0.0 1.1 ! !MED assign (residue 73 and name hn) (residue 75 and name hn) 1.8 0.0 3.2 ! assign (residue 73 and name hn) ((residue 76 and name hg1#) or (residue 76 and name hg2#)) 1.8 0.0 3.2 assign (residue 73 and name ha) ((residue 76 and name hg1#) or (residue 76 and name hg2#)) 1.8 0.0 1.5 assign (residue 73 and name hg#) ((residue 76 and name hg1#) or (residue 76 and name hg2#)) 1.8 0.0 3.2 !LONG assign (residue 73 and name hg#) (residue 96 and name hg2#) 1.8 0.0 3.2 ! 96hg2 sees 2.39 !E74 !INTRA assign (residue 74 and name hn) (residue 74 and name ha) 1.8 0.0 1.1 ! ovlps 73ha !SEQ !R assign (residue 74 and name hn) (residue 75 and name hn) 1.8 0.0 1.1 ! !MED assign (residue 74 and name hn) (residue 72 and name hn) 1.8 0.0 3.2 ! assign (residue 74 and name hn) (residue 72 and name ha) 1.8 0.0 3.2 ! assign (residue 74 and name hn) (residue 72 and name hb#) 1.8 0.0 3.2 ! !R assign (residue 74 and name ha) (residue 77 and name hn) 1.8 0.0 1.7 ! assign (residue 74 and name ha) (residue 77 and name hb#) 1.8 0.0 3.2 ! AMB ovlps 74hb'' assign (residue 74 and name ha) (residue 77 and name hg#) 1.8 0.0 3.2 ! !LONG !D75 !INTRA assign (residue 75 and name hn) (residue 75 and name ha) 1.8 0.0 1.7 ! assign (residue 75 and name hn) (residue 75 and name hb#) 1.8 0.0 1.1 ! !SEQ assign (residue 75 and name hn) (residue 74 and name hn) 1.8 0.0 1.1 ! assign (residue 75 and name hn) (residue 74 and name ha) 1.8 0.0 1.7 ! !A assign (residue 75 and name hn) (residue 76 and name hn) 1.8 0.0 1.1 !76hn ovlps 75hn assign ((residue 76 and name hg1#) or (residue 76 and name hg2#)) (residue 75 and name hn) 1.8 0.0 3.2 !MED assign (residue 75 and name hb#) (residue 71 and name he#) 1.8 0.0 3.2 ! 4d to 71he assign (residue 75 and name hn) (residue 72 and name hn) 1.8 0.0 1.7 ! !A assign (residue 75 and name hn) (residue 73 and name hn) 1.8 0.0 1.7 ! 73hn oclps 74hn assign (residue 75 and name hn) (residue 77 and name hn) 1.8 0.0 3.2 ! !LONG !A assign (residue 75 and name hn) (residue 96 and name hd#) 1.8 0.0 3.2 ! AMB 96hd sees 7.59 ppm not 7.55 ppm !V76 !INTRA assign (residue 76 and name hn) (residue 76 and name ha) 1.8 0.0 1.7 ! assign (residue 76 and name hn) (residue 76 and name hb) 1.8 0.0 1.7 ! ovlps 75hb# !SEQ !A assign (residue 75 and name hn) (residue 76 and name hn) 1.8 0.0 1.1 !76hn ovlps 75hn assign (residue 76 and name hn) (residue 75 and name ha) 1.8 0.0 3.2 ! assign (residue 76 and name hn) (residue 75 and name hb#) 1.8 0.0 1.7 ! !R assign (residue 76 and name hn) (residue 77 and name hn) 1.8 0.0 1.1 ! !MED assign (residue 76 and name hn) (residue 73 and name ha) 1.8 0.0 1.7 ! assign (residue 76 and name hb) (residue 73 and name ha) 1.8 0.0 3.2 ! !R assign ((residue 76 and name hg1#) or (residue 76 and name hg2#)) !R (residue 73 and name ha) 1.8 0.0 1.5 ! 4d, to both 76hgs !R assign (residue 73 and name hn) !R ((residue 76 and name hg1#) or (residue 76 and name hg2#)) 1.8 0.0 3.2 !R assign (residue 73 and name hg#) !R ((residue 76 and name hg1#) or (residue 76 and name hg2#)) 1.8 0.0 3.2 ! 4d to 76hg' and 76 hg'' assign (residue 76 and name hn) (residue 74 and name hn) 1.8 0.0 3.2 ! !A assign (residue 76 and name hn) (residue 78 and name hn) 1.8 0.0 3.2 ! pk off by .04 ppm assign (residue 76 and name ha) ((residue 79 and name hd1#) or (residue 79 and name hd2#)) 1.8 0.0 3.2 assign (residue 76 and name ha) (residue 80 and name hg#) 1.8 0.0 3.2 !4d to 80hg'' !LONG assign (residue 76 and name hg#) (residue 89 and name ha) 1.8 0.0 3.2 !4d assign (residue 76 and name hg#) (residue 89 and name hg#) 1.8 0.0 3.2 !4d, sees both 89 hgs assign (residue 76 and name hg#) (residue 89 and name hd#) 1.8 0.0 3.2 ! 3d, sees both 89 hds assign (residue 76 and name hn) (residue 92 and name hg2#) 1.8 0.0 3.2 ! 92HG2 SEES 7.60 assign ((residue 76 and name hg1#) or (residue 76 and name hg2#)) (residue 92 and name hb) 1.8 0.0 3.2 ! 3d !R assign (residue 76 and name ha) (residue 92 and name hg2#) 1.8 0.0 1.5 ! 4D !R assign ((residue 76 and name hg1#) or (residue 76 and name hg2#)) !R (residue 92 and name hg2#) 1.8 0.0 3.2 ! 4d, sees both 76 hgs !A assign (residue 76 and name hn) (residue 93 and name ha) 1.8 0.0 3.2 !A !R assign ((residue 76 and name hg1#) or (residue 76 and name hg2#)) !R (residue 93 and name ha) 1.8 0.0 3.2 !4d to 76hg'' assign ((residue 76 and name hg1#) or (residue 76 and name hg2#)) (residue 93 and name hb#) 1.8 0.0 3.2 ! 4d to 76hg'' assign (residue 76 and name hg1#) ((residue 93 and name hg1) or (residue 93 and name hg2)) 1.8 0.0 3.2 assign (residue 76 and name hg2#) ((residue 93 and name hg1) or (residue 93 and name hg2)) 1.8 0.0 3.2 ! 4Ds, 76hg' and hg'' see both 93 hgs assign (residue 76 and name hn) (residue 96 and name hd#) 1.8 0.0 3.2 ! 96hd# sees 7.59ppm assign ((residue 76 and name hg1#) or (residue 76 and name hg2#)) (residue 96 and name hd#) 1.8 0.0 1.5 ! 4d to hg'' assign ((residue 76 and name hg1#) or (residue 76 and name hg2#)) (residue 93 and name ha) 1.8 0.0 3.2 !4d !E77 !INTRA assign (residue 77 and name hn) (residue 77 and name ha) 1.8 0.0 1.1 ! assign (residue 77 and name hn) (residue 77 and name hb#) 1.8 0.0 1.1 ! assign (residue 77 and name hn) (residue 77 and name hg#) 1.8 0.0 2.2 ! !SEQ assign (residue 77 and name hn) (residue 76 and name hn) 1.8 0.0 1.1 ! assign (residue 77 and name hn) (residue 76 and name ha) 1.8 0.0 3.2 ! assign (residue 77 and name hn) (residue 76 and name hb) 1.8 0.0 1.7 ! assign (residue 77 and name hn) (residue 76 and name hg#) 1.8 0.0 1.7 ! 1.3e7 !R assign (residue 77 and name hn) (residue 78 and name hn) 1.8 0.0 1.1 ! !MED assign (residue 77 and name hn) (residue 74 and name ha) 1.8 0.0 1.7 ! !AR assign (residue 77 and name hb#) (residue 74 and name ha) 1.8 0.0 3.2 ! assign (residue 77 and name hg#) (residue 74 and name ha) 1.8 0.0 3.2 ! !R assign (residue 75 and name hn) (residue 77 and name hn) 1.8 0.0 3.2 ! 75hn ovlps 76hn assign (residue 77 and name ha) (residue 80 and name hn) 1.8 0.0 3.2 ! assign (residue 77 and name ha) ((residue 80 and name hg1#) or (residue 80 and name hg2#)) 1.8 0.0 3.2 !4d to 80hg'', stronger 3d to 80 hg' assign (residue 77 and name hb#) ((residue 80 and name hg1#) or (residue 80 and name hg2#)) 1.8 0.0 3.2 ! assign (residue 77 and name hg#) ((residue 80 and name hg1#) or (residue 80 and name hg2#)) 1.8 0.0 3.2 ! !LONG !R78 !only intras to ha, hbs, hgs, and hds !INTRA assign (residue 78 and name hn) (residue 78 and name ha) 1.8 0.0 1.1 ! assign (residue 78 and name hn) (residue 78 and name hb#) 1.8 0.0 1.1 ! assign (residue 78 and name hn) (residue 78 and name hg#) 1.8 0.0 2.2 ! assign (residue 78 and name hn) (residue 78 and name hd#) 1.8 0.0 3.2 ! !SEQ assign (residue 78 and name hn) (residue 77 and name hn) 1.8 0.0 1.1 ! assign (residue 78 and name hn) (residue 77 and name ha) 1.8 0.0 1.7 ! assign (residue 78 and name hn) (residue 77 and name hg#) 1.8 0.0 3.2 ! !R assign (residue 78 and name hn) (residue 79 and name hn) 1.8 0.0 1.1 ! assign (residue 78 and name he) (residue 79 and name hd#) 1.8 0.0 3.2 ! 15n noesy sees both 79 hds !MED assign (residue 78 and name hn) (residue 75 and name ha) 1.8 0.0 1.7 ! !A assign (residue 78 and name he) (residue 75 and name ha) 1.8 0.0 3.2 ! assign (residue 78 and name hn) (residue 76 and name hn) 1.8 0.0 3.2 ! ovlped by 7.52 ppm !R assign (residue 78 and name hn) (residue 80 and name hn) 1.8 0.0 3.2 ! !LONG !L79 !INTRA assign (residue 79 and name hn) (residue 79 and name ha) 1.8 0.0 1.7 ! assign (residue 79 and name hn) (residue 79 and name hb#) 1.8 0.0 1.1 ! 1.1e7 assign (residue 79 and name hn) (residue 79 and name hg) 1.8 0.0 1.1 ! 1e7 !SEQ assign (residue 79 and name hn) (residue 78 and name hn) 1.8 0.0 1.1 ! assign (residue 79 and name hn) (residue 78 and name ha) 1.8 0.0 1.7 ! assign (residue 79 and name hn) (residue 78 and name hb#) 1.8 0.0 1.7 ! !R assign (residue 79 and name hn) (residue 80 and name hn) 1.8 0.0 1.7 ! !MED assign (residue 79 and name hd#) (residue 75 and name ha) 1.8 0.0 3.2 !AMB 3d assign (residue 79 and name hd#) (residue 75 and name hb#) 1.8 0.0 3.2 ! AMB 3d assign (residue 79 and name hn) (residue 76 and name ha) 1.8 0.0 3.2 ! assign ((residue 79 and name hd1#) or (residue 79 and name hd2#)) ((residue 76 and name hg1#) or (residue 76 and name hg2#)) 1.8 0.0 3.2 ! 4d assign ((residue 79 and name hd1#) or (residue 79 and name hd2#)) (residue 76 and name ha) 1.8 0.0 3.2 !AMB 3d assign (residue 79 and name hn) (residue 77 and name hn) 1.8 0.0 3.2 ! !SD? assign (residue 79 and name hd#) (residue 82 and name ha) 1.8 0.0 3.2 ! 3d 79hd'' assign (residue 79 and name ha) (residue 82 and name hb#) 1.8 0.0 3.2 ! assign (residue 82 and name hb#) (residue 79 and name hd#) 1.8 0.0 3.2 !79hd'' sees both 82hbs, 82hb'' in 4D !R assign ((residue 79 and name hd1#) or (residue 79 and name hd2#)) !R (residue 83 and name hb#) 1.8 0.0 3.2 !4d to 79 hd'' at 1.40/18.65 !LONG !R assign ((residue 79 and name hd1#) or (residue 79 and name hd2#)) !R (residue 59 and name hn) 1.8 0.0 3.2 !R assign ((residue 59 and name hb1) or (residue 59 and name hb2)) !R ((residue 79 and name hd1#) or (residue 79 and name hd2#)) 1.8 0.0 3.2 ! 59hbs see 0.57ppm, 79hd'' sees both 59hbs in 4D assign (residue 79 and name hd#) ((residue 63 and name hd#) or (residue 60 and name he#)) 1.8 0.0 3.2 !AMB 3d to 79hd'' pk 7.086ppm !A assign (residue 79 and name hd#) (residue 63 and name he#) 1.8 0.0 3.2 !AMB v wk 6.86ppm, to 79hd'' !R assign ((residue 79 and name hd1#) or (residue 79 and name hd2#)) !R (residue 71 and name he#) 1.8 0.0 1.5 !R assign ((residue 79 and name hd1#) or (residue 79 and name hd2#)) !R (residue 85 and name hd#) 1.8 0.0 3.2 ! 4d to 79hd'' and hd' assign ((residue 79 and name hd1#) or (residue 79 and name hd2#)) ((residue 85 and name hg11) or (residue 85 and name hg12)) 1.8 0.0 3.2 !4d to 79hd'' assign ((residue 79 and name hd1#) or (residue 79 and name hd2#)) (residue 92 and name hg2#) 1.8 0.0 3.2 !4d to 79hd' and wk to hd'' assign ((residue 79 and name hd1#) or (residue 79 and name hd2#)) (residue 92 and name hd#) 1.8 0.0 3.2 !4d to 79hd' and wk to hd'' assign (residue 79 and name hn) ((residue 92 and name hg2#) or (residue 92 and name hg11) or (residue 92 and name hg12) or (residue 68 and name hg1#) or (residue 68 and name hg2#)) 1.8 0.0 3.2 ! 1.165ppm !SD assign (residue 79 and name hn) ((residue 85 and name hd#) or !SD (residue 96 and name hd#) or (residue 86 and name hg2#)) 1.8 0.0 3.2 ! 0.82ppm, 85hd closest, prob spinb diffusion !V80 !intras only to ha, and hb !INTRA assign (residue 80 and name hn) (residue 80 and name ha) 1.8 0.0 1.7 !1.5e7 assign (residue 80 and name hn) (residue 80 and name hb) 1.8 0.0 1.1 !2.2e7 assign (residue 80 and name hn) (residue 80 and name hg#) 1.8 0.0 1.1 !4e7 !SEQ assign (residue 80 and name hn) (residue 79 and name hn) 1.8 0.0 1.7 !8.5e7 assign (residue 80 and name hn) (residue 79 and name ha) 1.8 0.0 1.7 !9.4e6 assign (residue 80 and name hn) (residue 79 and name hb#) 1.8 0.0 2.2 ! assign (residue 80 and name hn) (residue 79 and name hg) 1.8 0.0 3.2 ! assign (residue 80 and name hn) (residue 79 and name hd#) 1.8 0.0 3.2 ! !R assign (residue 80 and name hn) (residue 81 and name hn) 1.8 0.0 1.1 ! assign ((residue 80 and name hg1#) or (residue 80 and name hg2#)) (residue 81 and name ha) 1.8 0.0 3.2 !4d to 80hg' !R assign ((residue 80 and name hg1#) or (residue 80 and name hg2#)) !R ((residue 81 and name hg1) or (residue 81 and name hg2)) 1.8 0.0 3.2 !4d both 81hgs to 80hg' !MED !R assign ((residue 80 and name hg1#) or (residue 80 and name hg2#)) !R (residue 76 and name ha) 1.8 0.0 3.2 ! 4d to 80hg'' !A assign (residue 80 and name hn) (residue 77 and name ha) 1.8 0.0 1.7 ! AMB ovlps79, 77ha sees 80 hn weak !R assign ((residue 80 and name hg1#) or (residue 80 and name hg2#)) !R (residue 77 and name ha) 1.8 0.0 3.2 !4d to 80hg'', stronger 3d to 80 hg' assign (residue 80 and name hn) (residue 78 and name hn) 1.8 0.0 3.2 ! assign (residue 80 and name hn) (residue 82 and name hn) 1.8 0.0 3.2 ! !R assign ((residue 80 and name hg1#) or (residue 80 and name hg2#)) !R (residue 82 and name hn) 1.8 0.0 3.2 !3d to 80hg' !LONG assign ((residue 80 and name hg1#) or (residue 80 and name hg2#)) (residue 88 and name ha) 1.8 0.0 3.2 !3d to 80hg' assign ((residue 80 and name hg1#) or (residue 80 and name hg2#)) (residue 89 and name ha) 1.8 0.0 3.2 !4d to 80hg' and hg'' assign ((residue 80 and name hg1#) or (residue 80 and name hg2#)) ((residue 89 and name hb1) or (residue 89 and name hb2)) 1.8 0.0 3.2 !4d to 80hg'' !R assign ((residue 80 and name hg1#) or (residue 80 and name hg2#)) !R ((residue 89 and name hg1) or (residue 89 and name hg2)) 1.8 0.0 3.2 !4d to 80hg' assign ((residue 80 and name hg1#) or (residue 80 and name hg2#)) ((residue 89 and name hd1) or (residue 89 and name hd2)) 1.8 0.0 3.2 !4d to 80hg' !Q81 !INTRA assign (residue 81 and name hn) (residue 81 and name ha) 1.8 0.0 1.1 ! assign (residue 81 and name hn) (residue 81 and name hb#) 1.8 0.0 1.7 assign (residue 81 and name hn) (residue 81 and name hg#) 1.8 0.0 2.2 ! !SEQ assign (residue 81 and name hn) (residue 80 and name hn) 1.8 0.0 1.1 !9.6e6, 81hn to 80hn 1.2e7 assign (residue 81 and name ha) (residue 80 and name ha) 1.8 0.0 3.2 ! assign (residue 81 and name hn) (residue 80 and name hb) 1.8 0.0 1.7 ! assign (residue 81 and name hn) (residue 80 and name hg#) 1.8 0.0 1.7 assign (residue 80 and name hg#) (residue 81 and name hg#) 1.8 0.0 3.2 !4d both 81hgs to 80hg'Hi Pam, !R assign (residue 81 and name hn) (residue 82 and name hn) 1.8 0.0 1.1 ! assign (residue 81 and name hn) ((residue 82 and name hb1) or (residue 82 and name hb2)) 1.8 0.0 3.2 ! 3.08ppm wk pk !MED assign (residue 81 and name hn) (residue 79 and name hn) 1.8 0.0 3.2 ! assign (residue 81 and name hn) (residue 79 and name ha) 1.8 0.0 3.2 ! assign (residue 81 and name hn) (residue 79 and name hd#) 1.8 0.0 3.2 !A assign (residue 81 and name ha) !A ((residue 79 and name hd1#) or (residue 79 and name hd2#)) 1.8 0.0 3.2 ! 79hd'' not see 81ha !D82 !INTRA assign (residue 82 and name hn) (residue 82 and name ha) 1.8 0.0 1.7 !amb, ovlps 81ha assign (residue 82 and name hn) ((residue 82 and name hb1) or (residue 82 and name hb2)) 1.8 0.0 1.1 !one strong, one med !SEQ assign (residue 82 and name hn) (residue 81 and name hn) 1.8 0.0 1.1 !1.7e7 !A assign (residue 82 and name hn) (residue 81 and name ha) 1.8 0.0 1.7 !ovlps 82ha !R assign (residue 82 and name hn) (residue 83 and name hn) 1.8 0.0 1.1 !9.9e6 !A assign (residue 82 and name hn) (residue 83 and name hb#) 1.8 0.0 3.2 !83hb sees 7.74 as shoulder of larger pk assign (residue 82 and name ha) (residue 83 and name hb#) 1.8 0.0 3.2 !83hb sees it !MED assign (residue 82 and name hn) (residue 79 and name ha) 1.8 0.0 1.7 ! 7.9e6 assign (residue 82 and name hn) (residue 79 and name hb#) 1.8 0.0 3.2 ! 5e6 assign (residue 82 and name hn) (residue 79 and name hd#) 1.8 0.0 3.2 !hd' see 82hn !RA assign (residue 82 and name hn) (residue 80 and name hn) 1.8 0.0 3.2 !80hn sees 82hn, 83hn ovlps 80hn assign ((residue 80 and name hg1#) or (residue 80 and name hg2#)) (residue 82 and name hn) 1.8 0.0 3.2 !3d to 80hg' !A assign (residue 82 and name hn) (residue 85 and name hd#) 1.8 0.0 3.2 ! 85hd not see 82hn !LONG !A83 #? in typeII turn ? !INTRA assign (residue 83 and name hn) (residue 83 and name ha) 1.8 0.0 1.1 ! 5e7 assign (residue 83 and name hn) (residue 83 and name hb#) 1.8 0.0 1.1 ! 1.8e7 !SEQ assign (residue 83 and name hn) (residue 82 and name hn) 1.8 0.0 3.2 !7e6, wk b/c all pks stronger to 83hn assign (residue 83 and name hn) (residue 82 and name ha) 1.8 0.0 0.9 ! very strong! 5e7 assign (residue 83 and name hn) (residue 82 and name hb#) 1.8 0.0 2.2 ! 8e6 for hb', med?, back off b/c of vios, all pks stronger to 83hn !R assign (residue 82 and name ha) (residue 83 and name hb#) 1.8 0.0 3.2 ! !R assign (residue 83 and name hn) (residue 84 and name hn) 1.8 0.0 1.1 !1.3e7 assign (residue 83 and name ha) (residue 84 and name hn) 1.8 0.0 1.7 !83ha-84hn as strong as 83ha-83hn, which is strong in 15n noesy !R assign (residue 83 and name hb#) (residue 84 and name hn) 1.8 0.0 3.2 ! !MED assign (residue 83 and name hb#) (residue 79 and name hd#) 1.8 0.0 3.2 !4d !LONG !A assign (residue 83 and name ha) !A ((residue 88 and name hb#) or (residue 87 and name hb#)) 1.8 0.0 3.2 ! looks like 88hb !G84 #? in typeII turn ? !INTRA assign (residue 84 and name hn) ((residue 84 and name ha1) or (residue 84 and name ha2)) 1.8 0.0 0.9 ! ha' 2e7, ha'' 3e7 !SEQ assign (residue 84 and name hn) (residue 83 and name hn) 1.8 0.0 1.1 ! 1.1e7 !A assign (residue 84 and name hn) (residue 83 and name ha) 1.8 0.0 1.1 ! ovlps 84ha assign (residue 84 and name hn) (residue 83 and name hb#) 1.8 0.0 1.7 ! 1.8e7 !R assign (residue 84 and name hn) (residue 85 and name hn) 1.8 0.0 1.1 ! very strong! 1.9e7 !SD? assign (residue 84 and name hn) (residue 85 and name hg2#) 1.8 0.0 3.2 ! assign (residue 84 and name hn) (residue 85 and name hd#) 1.8 0.0 4.2 ! assign (residue 84 and name hn) (residue 85 and (name hg11 or name hg12)) 1.8 0.0 4.2 ! !MED assign (residue 84 and name hn) (residue 82 and name ha) 1.8 0.0 3.2 ! 9.7e6, but wk for 84hn to 82ha !LONG !I85 !INTRA assign (residue 85 and name hn) (residue 85 and name ha) 1.8 0.0 1.7 !7.3e6 !A assign (residue 85 and name hn) ((residue 85 and name hb) 1.8 0.0 1.1 ! 1.38ppm, 83hb* closer in shift assign (residue 85 and name hn) (residue 85 and name hg2#) 1.8 0.0 1.7 ! 1.3e7 assign (residue 85 and name hn) (residue 85 and name hd#) 1.8 0.0 3.2 ! 1.1e7 !SEQ assign (residue 85 and name hn) (residue 84 and name hn) 1.8 0.0 1.1 ! 1.6e7 assign (residue 85 and name hn) (residue 84 and name ha#) 1.8 0.0 1.7 ! ha'' 1.2e7 !R assign (residue 85 and name hn) (residue 86 and name hn) 1.8 0.0 3.2 ! 7.3e6 !MED !A assign (residue 85 and name hn) (residue 82 and name hn) 1.8 0.0 3.2 ! 4.5e6, dont see 85hn to 82hn assign (residue 85 and name hn) (residue 83 and name hn) 1.8 0.0 3.2 ! 4.5e6 !A assign (residue 85 and name hn) (residue 83 and name hb#) 1.8 0.0 1.7 ! 1.2e7, vio, dont see 85hn to 83hb, !A assign (residue 85 and name hd#) (residue 87 and name ha) 1.8 0.0 3.2 ! 4D !LONG !R assign (residue 55 and name hb#) (residue 85 and name hg2#) 1.8 0.0 3.2 !pk at 0.03ppm, 85hg2 sees both 55hbs !R assign (residue 85 and name hg2#) (residue 56 and name ha) 1.8 0.0 3.2 !4D !R assign (residue 85 and name hg2#) (residue 56 and name hn) 1.8 0 1.7 !0.05ppm, 85hg2 sees 8.62, could also be 37hd' to 56hn assign (residue 85 and name hg2#) (residue 56 and name hb#) 1.8 0.0 3.2 !85hg2# sees wk pk to hb'' !A assign (residue 85 and name ha) (residue 58 and name hb#) 1.8 0.0 3.2 !vio, not clear that 58b sees it assign (residue 85 and name hg2#) (residue 58 and name hb#) 1.8 0.0 3.2 ! 58hb# not see 85gh2#, but 58hb only one makes sense !R assign (residue 85 and name hg2#) (residue 58 and name hn) 1.8 0.0 3.2 !58hn sees 85gh2# !R assign (residue 60 and name hd#) (residue 85 and name hg2#) 1.8 0.0 3.2 !2d noesy, 85hg2 sees 7.40 assign (residue 85 and name hg2#) (residue 60 and name he#) 1.8 0.0 3.2 !3d noesy, ovlpd in 2d noesy !R assign (residue 85 and name hd#) (residue 60 and name hd#) 1.8 0.0 3.2 !2d noesy, 85hd sees 7.40 !R assign (residue 60 and name hd#) (residue 85 and name hg1#) 1.8 0.0 3.2 !2d noesy assign (residue 85 and name hg2#) ((residue 79 and name hd1#) or (residue 79 and name hd2#)) 1.8 0.0 3.2 ! 4D to 79hd'' assign (residue 85 and name hd#) (residue 79 and name hd1#) 1.8 0.0 3.2 ! 4d, 0.37/25.8, 79hd' sees 85hd also assign (residue 85 and name hd#) (residue 79 and name hd2#) 1.8 0.0 3.2 ! 4d, 0.57/23.4 assign (residue 85 and name hd#) (residue 92 and name hg1#) 1.8 0.0 3.2 ! 4d assign (residue 85 and name hd#) (residue 92 and name hg2#) 1.8 0.0 3.2 ! 4d !A assign (residue 85 and name hg2#) (residue 92 and name hg2#) 1.8 0.0 3.2 ! v wk at 1.16ppm !A assign (residue 85 and name hg2#) (residue 92 and name hd#) 1.8 0.0 3.2 ! 92hd# not see 85gh2# !I86 HN signals all very weak !INTRA !A assign (residue 86 and name hn) (residue 86 and name hg2#) 1.8 0.0 1.7 ! !SEQ assign (residue 86 and name hn) (residue 85 and name ha) 1.8 0.0 1.7 ! assign (residue 86 and name hn) (residue 85 and name hg2#) 1.8 0.0 3.2 ! !MED !R assign (residue 86 and name hg2#) (residue 88 and name hn) 1.8 0.0 3.2 ! 3D !R assign (residue 86 and name hg2#) (residue 88 and name hb#) 1.8 0.0 3.2 ! 3D, H88hb sees it also !LONG assign (residue 86 and name hd#) (residue 40 and name ha) 1.8 0.0 3.2 ! 3D assign (residue 86 and name hd#) (residue 41 and name ha) 1.8 0.0 3.2 ! 4D !R assign (residue 86 and name hd#) !R ((residue 44 and name hd1#) or (residue 44 and name hd2#)) 1.8 0.0 1.5 ! 4D, sees both 44hds assign (residue 86 and name hg2#) (residue 44 and name hd#) 1.8 0.0 3.2 ! 4D sees both 44hd' !R assign (residue 86 and name hd#) (residue 48 and name hg2#) 1.8 0.0 1.5 ! 4D, 0.39/21.8 assign (residue 86 and name hd#) (residue 49 and name hg1#) 1.8 0.0 3.2 ! 4D, sees both 49 hgs assign (residue 86 and name hd#) (residue 49 and name hg1#) 1.8 0.0 3.2 ! 4D, sees both 49 hgs !R87 HN signals all very weak' !INTRA !SEQ assign (residue 87 and name hn) (residue 86 and name hn) 1.8 0.0 3.2 ! assign (residue 87 and name hn) (residue 86 and name ha) 1.8 0.0 1.1 ! assign (residue 87 and name hn) (residue 86 and name hd#) 1.8 0.0 3.2 ! assign (residue 87 and name hn) (residue 86 and name hg2#) 1.8 0.0 3.2 ! !MED !LONG !H88 ! dont see ha in 3d noesy !INTRA assign (residue 88 and name hn) (residue 88 and name ha) 1.8 0.0 1.7 ! assign (residue 88 and name hn) (residue 88 and name hb#) 1.8 0.0 1.7 ! !SEQ assign (residue 88 and name hn) (residue 87 and name hn) 1.8 0.0 3.2 ! assign (residue 88 and name hn) (residue 87 and name ha) 1.8 0.0 1.1 ! !R assign (residue 88 and name hn) (residue 89 and name hn) 1.8 0.0 3.2 ! !MED assign (residue 88 and name hb#) (residue 86 and name hg2#) 1.8 0.0 3.2 ! 3D to 86hg2, H88hb sees it also assign (residue 88 and name hn) (residue 86 and name hg2#) 1.8 0.0 3.2 assign (residue 88 and name hn) (residue 92 and name hd#) 1.8 0.0 3.2 ! 0.90ppm, 1.5e7, 86hg2 and 92hd both see it as wk assign (residue 88 and name hn) (residue 92 and (name hg2# or name hg1#)) 1.8 0.0 3.2 ! 3D, 92hg2 sees it as wk, could be 92hg1# also !R assign (residue 88 and name hn) (residue 91 and name hn) 1.8 0.0 3.2 ! !R89 !INTRA assign (residue 89 and name hn) (residue 89 and name ha) 1.8 0.0 1.7 ! assign (residue 89 and name hn) (residue 89 and name hb#) 1.8 0.0 1.1 ! !SEQ assign (residue 89 and name hn) (residue 88 and name hn) 1.8 0.0 3.2 ! assign (residue 89 and name hn) (residue 88 and name ha) 1.8 0.0 1.1 ! 1.9e7, vios 3apr02, 184hn to 183ha stronger than 183ha-hbs !R assign (residue 89 and name hn) (residue 90 and name hn) 1.8 0.0 3.2 ! assign (residue 89 and name hn) (residue 88 and name hb#) 1.8 0.0 3.2 ! 4.5e6 !MED !LONG !R assign ((residue 76 and name hg1#) or (residue 76 and name hg2#)) !R (residue 89 and name ha) 1.8 0.0 3.2 !4d to 76hg? !R assign ((residue 76 and name hg1#) or (residue 76 and name hg2#)) !R ((residue 89 and name hg1) or (residue 89 and name hg2)) 1.8 0.0 3.2 ! 4d, sees both 76 hgs !R assign ((residue 76 and name hg1#) or (residue 76 and name hg2#)) !R ((residue 89 and name hd1) or (residue 89 and name hd2)) 1.8 0.0 3.2 ! 3d, sees both 76 hds assign (residue 89 and name hn) (residue 80 and name hg#) 1.8 0.0 1.7 ! 1.1e7 to 89hn, 80 hg'' sees 8.98 as wk !R assign ((residue 80 and name hg1#) or (residue 80 and name hg2#)) !R (residue 89 and name ha) 1.8 0.0 3.2 !4d to 80hg' and hg'', 76hg' also contributes !R assign ((residue 80 and name hg1#) or (residue 80 and name hg2#)) !R ((residue 89 and name hb1) or (residue 89 and name hb2)) 1.8 0.0 3.2 !4d to 80hg' assign ((residue 80 and name hg1#) or (residue 80 and name hg2#)) ((residue 89 and name hg1) or (residue 89 and name hg2)) 1.8 0.0 3.2 !4d to 80hg' !R assign ((residue 80 and name hg1#) or (residue 80 and name hg2#)) !R ((residue 89 and name hd1) or (residue 89 and name hd2)) 1.8 0.0 3.2 !4d to 80hg' !########## stop here 1/14/02 #################### !G90 !INTRA assign (residue 90 and name hn) (residue 90 and (name ha1 or name ha2)) 1.8 0.0 1.1 ! !SEQ assign (residue 90 and name hn) (residue 89 and name hn) 1.8 0.0 2.2 ! 3.3e6, mw assign (residue 90 and name hn) (residue 89 and name ha) 1.8 0.0 3.2 ! assign (residue 90 and name hn) ((residue 89 and name hd1) or (residue 89 and name hd2)) 1.8 0.0 3.2 ! !R assign (residue 90 and name hn) (residue 91 and name hn) 1.8 0.0 1.1 ! !MED assign (residue 90 and name hn) (residue 88 and name ha) 1.8 0.0 3.2 ! assign (residue 90 and name hn) (residue 88 and name hn) 1.8 0.0 3.2 ! !R assign (residue 90 and name hn) (residue 92 and name hn) 1.8 0.0 3.2 ! !LONG assign (residue 90 and name hn) ((residue 80 and name hg1#) or (residue 80 and name hg2#)) 1.8 0.0 3.2 ! 80 hg'' sees wk pk to 90 hn !K91 HN signals very weak !INTRA !SEQ assign (residue 91 and name hn) (residue 90 and name hn) 1.8 0.0 1.1 ! !R assign (residue 91 and name hn) (residue 92 and name hn) 1.8 0.0 1.1 ! !MED assign (residue 91 and name hn) (residue 88 and name hn) 1.8 0.0 3.2 ! assign (residue 91 and name ha) (residue 94 and name hb#) 1.8 0.0 1.5 ! !LONG !I92 !INTRA assign (residue 92 and name hn) (residue 92 and name ha) 1.8 0.0 1.7 ! assign (residue 92 and name hn) (residue 92 and name hb) 1.8 0.0 1.7 ! assign (residue 92 and name hn) (residue 92 and name hd#) 1.8 0.0 1.7 ! assign (residue 92 and name hn) (residue 92 and name hg2#) 1.8 0.0 3.2 ! assign (residue 92 and name ha) (residue 92 and name hg2#) 1.8 0.0 1.5 ! !SEQ assign (residue 92 and name hn) (residue 91 and name hn) 1.8 0.0 1.1 ! rel. weak 3.7e6 assign (residue 92 and name hn) (residue 91 and name ha) 1.8 0.0 3.2 ! assign (residue 92 and name hn) (residue 93 and name hn) 1.8 0.0 1.1 ! 5e6 !MED assign (residue 92 and name hn) (residue 88 and name hn) 1.8 0.0 3.2 ! assign (residue 92 and name hn) (residue 89 and name ha) 1.8 0.0 3.2 ! assign (residue 92 and name hg2#) (residue 89 and name ha) 1.8 0.0 3.2 ! 4d assign (residue 92 and name hd#) (residue 89 and name ha) 1.8 0.0 3.2 ! 4d assign (residue 92 and name hn) (residue 90 and name hn) 1.8 0.0 3.2 ! !LONG assign (residue 92 and name hg2#) ((residue 60 and name he#) or (residue 63 and name hd#)) 1.8 0.0 3.2 ! think its 60he assign (residue 92 and name hg2#) (residue 60 and name hz) 1.8 0.0 3.2 ! 3D 7.18ppm assign (residue 92 and name hg2#) (residue 76 and name ha) 1.8 0.0 1.5 ! 4D assign (residue 92 and name hg2#) (residue 76 and name hg1#) 1.8 0.0 3.2 assign (residue 92 and name hg2#) (residue 76 and name hg2#) 1.8 0.0 3.2 ! 4D sees both 76hgs !SD? assign (residue 92 and name hd#) (residue 79 and name ha) 1.8 0.0 3.2 ! vio, dont see 92hd to 79ha assign (residue 92 and name hd#) (residue 79 and name hb#) 1.8 0.0 3.2 ! 4d !R assign (residue 92 and name hg2#) !R ((residue 79 and name hd1#) or (residue 79 and name hd2#)) 1.8 0.0 3.2 ! sees both 79 hds assign (residue 92 and name hd#) (residue 79 and name hd1#) 1.8 0.0 3.2 assign (residue 92 and name hd#) (residue 79 and name hd2#) 1.8 0.0 3.2 ! 4d, 92hd sees both 79 hds assign (residue 92 and name hd#) (residue 80 and name ha) 1.8 0.0 1.5 ! 4d assign (residue 92 and name hd#) (residue 80 and name hb) 1.8 0.0 3.2 ! 4d assign (residue 92 and name hd#) ((residue 80 and name hg1#) or (residue 80 and name hg2#)) 1.8 0.0 1.5 ! 4d sees both 80hgs !Q93 !INTRA assign (residue 93 and name hn) (residue 93 and name ha) 1.8 0.0 1.1 ! assign (residue 93 and name hn) (residue 93 and name hb#) 1.8 0.0 1.7 ! assign (residue 93 and name hn) (residue 93 and name hg#) 1.8 0.0 3.2 ! !SEQ assign (residue 93 and name hn) (residue 92 and name hn) 1.8 0.0 1.1 ! rel weak and ovlps 94hn 6e6 helix based on chem shift assign (residue 93 and name hn) (residue 92 and name ha) 1.8 0.0 3.2 ! assign (residue 93 and name hn) (residue 92 and name hb) 1.8 0.0 1.7 ! assign (residue 93 and name hn) (residue 92 and name hg2#) 1.8 0.0 3.2 ! 4d !R assign (residue 93 and name hn) (residue 94 and name hn) 1.8 0.0 1.1 ! rel weak and ovlps 92hn 6e6 helix based on chem shift !MED assign (residue 93 and name hn) (residue 89 and name ha) 1.8 0.0 3.2 ! assign (residue 93 and name hn) (residue 90 and name hn) 1.8 0.0 3.2 ! assign (residue 93 and name hn) (residue 91 and name hn) 1.8 0.0 3.2 ! assign (residue 93 and name hn) (residue 95 and name hn) 1.8 0.0 3.2 ! assign (residue 93 and name ha) (residue 96 and name hd#) 1.8 0.0 3.2 ! assign (residue 93 and name ha) (residue 96 and name hb) 1.8 0.0 3.2 ! !LONG assign (residue 93 and name hn) ((residue 76 and name hg1#) or (residue 76 and name hg2#)) 1.8 0.0 1.7 ! 3d assign (residue 93 and name ha) ((residue 76 and name hg1#) or (residue 76 and name hg2#)) 1.8 0.0 3.2 ! 4d to 76hg'' {R assign (residue 76 and name hg1#) ((residue 93 and name hg1) or (residue 93 and name hg2)) 1.8 0.0 3.2 assign (residue 76 and name hg2#) ((residue 93 and name hg1) or (residue 93 and name hg2)) 1.8 0.0 3.2 ! 4Ds, 76hg' and hg'' see both 93 hgs R} !A94 !INTRA assign (residue 94 and name hn) (residue 94 and name ha) 1.8 0.0 1.1 ! assign (residue 94 and name hn) (residue 94 and name hb#) 1.8 0.0 1.1 ! 3.3e7 !SEQ assign (residue 94 and name hn) (residue 93 and name hn) 1.8 0.0 1.1 ! 1e7 assign (residue 94 and name hn) (residue 93 and name ha) 1.8 0.0 1.7 ! assign (residue 94 and name hn) ((residue 93 and name hg1) or (residue 93 and name hg2)) 1.8 0.0 3.2 ! !R assign (residue 94 and name hn) (residue 95 and name hn) 1.8 0.0 1.1 ! !MED assign (residue 94 and name hn) ((residue 90 and name ha1) or (residue 90 and name ha2)) 1.8 0.0 3.2 assign (residue 94 and name hn) (residue 91 and name ha) 1.8 0.0 1.7 ! !R assign (residue 94 and name hb#) (residue 91 and name ha) 1.8 0.0 1.5 ! assign (residue 94 and name hn) (residue 92 and name hn) 1.8 0.0 3.2 ! assign (residue 94 and name hn) (residue 96 and name hn) 1.8 0.0 3.2 ! assign (residue 94 and name ha) (residue 97 and name hn) 1.8 0.0 3.2 ! !LONG assign (residue 94 and name hb#) ((residue 155 and name hb1) or (residue 155 and name hb2)) 1.8 0.0 3.2 ! 4D assign (residue 94 and name hb#) (residue 155 and name hg#) 1.8 0.0 3.2 ! 4D assign (residue 94 and name hb#) (residue 156 and name hd#) 1.8 0.0 1.5 ! 3D, 156hd sees it assign (residue 94 and name hb#) (residue 156 and name he#) 1.8 0.0 3.2 ! 3D, 156 he# sees it !I95 !not much to hb, !INTRA assign (residue 95 and name hn) (residue 95 and name ha) 1.8 0.0 1.1 ! 5.8e6 assign (residue 95 and name hn) (residue 95 and name hb) 1.8 0.0 1.1 ! 1e7 assign (residue 95 and name hn) (residue 95 and name hd#) 1.8 0.0 1.7 ! 7e6 assign (residue 95 and name hn) (residue 95 and name hg2#) 1.8 0.0 3.2 ! 5e6 !SEQ assign (residue 95 and name hn) (residue 94 and name hn) 1.8 0.0 1.1 !rel. weak 4e6 assign (residue 95 and name hn) (residue 94 and name ha) 1.8 0.0 1.7 !rel. weak 4e6 assign (residue 95 and name hn) (residue 96 and name hn) 1.8 0.0 1.1 !rel weak 4e6 assign (residue 95 and name hg2#) (residue 96 and name ha) 1.8 0.0 3.2 ! !MED assign (residue 95 and name hn) (residue 92 and name ha) 1.8 0.0 3.2 ! assign (residue 95 and name hd#) (residue 92 and name hg2#) 1.8 0.0 3.2 ! !R assign (residue 93 and name hn) (residue 95 and name hn) 1.8 0.0 3.2 ! !R assign (residue 95 and name hn) (residue 97 and name hn) 1.8 0.0 3.2 ! !R assign (residue 95 and name ha) (residue 98 and name hn) 1.8 0.0 3.2 ! assign (residue 95 and name ha) (residue 98 and name hb#) 1.8 0.0 3.2 ! !LONG !A assign (residue 95 and name hg2#) (residue 37 and name hd#) 1.8 0.0 3.2 !37hd' not see it !A assign (residue 95 and name hd#) !A ((residue 37 and name hd#) or (residue 149 and name hd#)) 1.8 0.0 3.2 ! 4D, 37hds closer as of 1-16-02 !R assign (residue 56 and name hd#) (residue 95 and name hd#) 1.8 0 3.2 ! in 2d and 3d aro at 0.21ppm, 95hd sees 7.15ppm also !R assign (residue 56 and name he#) (residue 95 and name hd#) 1.8 0 3.2 ! in 2d and 3d aro at 0.21ppm, 95hd sees 6.67ppm also !R assign (residue 56 and name hd#) !R ((residue 95 and name hg11) or (residue 95 and name hg12)) 1.8 0 3.2 ! in 2d and 3d aro at 0.4ppm, 95hg1' sees 7.15ppm??? !R assign (residue 56 and name he#) (residue 95 and name hg1#) 1.8 0 3.2 !2d and 3d aro at 0.4ppm, 95hg1' sees 6.67ppm !R assign (residue 60 and name hd#) (residue 95 and name hg2#) 1.8 0.0 3.2 !2d noesy, 95hg2 sees 7.40 !R assign (residue 60 and name hd#) (residue 95 and name hd#) 1.8 0.0 3.2 !2d noesy, 95hd sees 7.40 !R assign (residue 60 and name he#) (residue 95 and name hd#) 1.8 0.0 3.2 !2d noesy, 95hd sees 7.10 !R assign (residue 60 and name hd#) !R ((residue 95 and name hg11) or (residue 95 and name hg12)) 1.8 0.0 3.2 !2d noesy assign (residue 95 and name hg2#) ((residue 63 and name hd#) or (residue 60 and name he#) or (residue 156 and name he#)) 1.8 0.0 3.2 ! 7.08ppm !A assign (residue 95 and name hg2#) ((residue 63 and name he#) or !6.87ppm assign (residue 95 and name hg2#) (residue 68 and name hg#) 1.8 0.0 1.5 !4d sees hg'' !I96 !INTRA assign (residue 96 and name hn) (residue 96 and name ha) 1.8 0.0 1.7 ! assign (residue 96 and name hn) (residue 96 and name hb) 1.8 0.0 1.1 ! 1.3e7 assign (residue 96 and name hn) (residue 96 and name hg2#) 1.8 0.0 2.2 ! 8.5e6 assign (residue 96 and name hn) (residue 96 and name hd#) 1.8 0.0 1.7 ! 7e6 !SEQ assign (residue 96 and name hn) (residue 95 and name hn) 1.8 0.0 1.1 ! weak 2.3e6 assign (residue 96 and name hn) (residue 95 and name hg2#) 1.8 0.0 3.2 ! 2.9e6 assign (residue 96 and name hn) (residue 95 and name hd#) 1.8 0.0 3.2 ! 2.9e6 !R assign (residue 96 and name hn) (residue 97 and name hn) 1.8 0.0 1.1 ! med 5e6 !MED assign (residue 96 and name hd#) (residue 92 and name hg2#) 1.8 0.0 3.2 ! 4d assign (residue 96 and name hn) (residue 93 and name ha) 1.8 0.0 3.2 ! assign (residue 96 and name hn) (residue 94 and name hn) 1.8 0.0 3.2 ! assign (residue 96 and name hn) (residue 98 and name hn) 1.8 0.0 3.2 ! assign (residue 96 and name ha) (residue 99 and name hb#) 1.8 0.0 1.5 ! assign (residue 96 and name hg2#) ((residue 99 and name hb#) or (residue 94 and name hb#)) 1.8 0.0 3.2 ! !LONG !R assign ((residue 68 and name hg1#) or (residue 68 and name hg2#)) !R (residue 96 and name hn) 1.8 0.0 3.2 !4d to 66hd' and 66hd''(stronger) assign (residue 96 and name ha) ((residue 68 and name hg1#) or (residue 68 and name hg2#)) 1.8 0.0 3.2 ! 3d, 68 hg'' assign (residue 96 and name hd#) ((residue 68 and name hg1#) or (residue 68 and name hg2#)) 1.8 0.0 3.2 ! 4d, 68 hg'' assign (residue 96 and name hg2#) ((residue 68 and name hg1#) or (residue 68 and name hg2#)) 1.8 0.0 3.2 ! 4d, 68 hg'' !R assign (residue 96 and name hg2#) (residue 69 and name ha) 1.8 0.0 3.2 ! 4d assign (residue 96 and name hg2#) (residue 69 and name hb#) 1.8 0.0 3.2 ! 4d !R assign (residue 96 and name hd#) !R ((residue 76 and name hg1#) or (residue 76 and name hg2#)) 1.8 0.0 1.5 ! 4d, 76hg'' assign (residue 96 and name hd#) ((residue 79 and name hd1#) or (residue 79 and name hd2#)) 1.8 0.0 3.2 ! 4d, think its 79hd'', but 149hd'' close in 1h and 13c shift !L79hd'' sees 95hd !G97 !INTRA !SEQ assign (residue 97 and name hn) (residue 96 and name hn) 1.8 0.0 1.1 ! rel weak 6e6 assign (residue 97 and name hn) (residue 96 and name hb) 1.8 0.0 1.1 ! assign (residue 97 and name hn) (residue 96 and name hg2#) 1.8 0.0 1.7 ! 8.6e6 assign (residue 97 and name hn) (residue 96 and name hd#) 1.8 0.0 3.2 ! 6e6 assign (residue 97 and name hn) (residue 98 and name hn) 1.8 0.0 1.1 ! 1e7 !MED !prev 3 ha resonances ovlped with own !R assign (residue 94 and name ha) (residue 97 and name hn) 1.8 0.0 3.2 ! assign (residue 97 and name hn) (residue 95 and name hn) 1.8 0.0 3.2 ! !R assign (residue 97 and name hn) (residue 99 and name hn) 1.8 0.0 3.2 ! !LONG !A assign (residue 97 and name hn) !A ((residue 155 and name hb1) or (residue 155 and name hb2)) 1.8 0.0 3.2 ! !N98 !pks to 98hbs very wk !INTRA assign (residue 98 and name hn) (residue 98 and name ha) 1.8 0.0 1.1 ! assign (residue 98 and name hn) ((residue 98 and name hb1) or (residue 98 and name hb2)) 1.8 0.0 1.7 !SEQ assign (residue 98 and name hn) (residue 97 and name hn) 1.8 0.0 1.1 ! assign (residue 98 and name hn) ((residue 97 and name ha1) or (residue 97 and name ha2)) 1.8 0.0 1.1 ! assign (residue 98 and name hn) (residue 99 and name hn) 1.8 0.0 1.1 ! !MED assign (residue 98 and name hn) (residue 95 and name ha) 1.8 0.0 1.7 ! ovlps 98hb'' assign (residue 98 and name hn) (residue 96 and name hn) 1.8 0.0 3.2 ! assign (residue 98 and name hn) (residue 100 and name hn) 1.8 0.0 3.2 ! assign (residue 98 and name hn) (residue 101 and name hn) 1.8 0.0 3.2 ! assign (residue 98 and name ha) (residue 101 and name hb#) 1.8 0.0 1.5 ! !LONG assign (residue 98 and name hn) (residue 68 and name hg#) 1.8 0.0 3.2 !A V68hg'' not see 9.15 assign (residue 98 and name hn) (residue 154 and name he#) 1.8 0.0 3.2 ! 4.6e6 assign (residue 98 and name hn) ((residue 154 and name hz) or (residue 156 and name he#)) 1.8 0.0 3.2 !7.10ppm !A assign (residue 98 and name hn) (residue 155 and name hn) 1.8 0.0 3.2 ! very wk, in 750 data only, 155hn sees 98hn also !A assign (residue 98 and name hn) (residue 155 and name hb#) 1.8 0.0 3.2 !A pk at 1.64 dont see 155hb' to 98 hn but all pks wk to 155hbs !A assign (residue 98 and name hn) !A ((residue 155 and name hg1) or (residue 155 and name hg2)) 1.8 0.0 3.2 !A pk at 1.47 dont see 155hb' to 98 hn but all pks wk to 155hbs !A99 !INTRA assign (residue 99 and name hn) (residue 99 and name hb#) 1.8 0.0 1.7 ! !SEQ assign (residue 99 and name hn) (residue 98 and name hn) 1.8 0.0 1.1 ! assign (residue 99 and name hn) ((residue 98 and name hb1) or (residue 98 and name hb2)) 1.8 0.0 3.2 ! !R assign (residue 99 and name hn) (residue 100 and name hn) 1.8 0.0 1.1 ! !MED assign (residue 99 and name hb#) (residue 95 and name hg2#) 1.8 0.0 3.2 ! 4d assign (residue 99 and name hb#) ((residue 96 and name ha) or (residue 65 and name ha)) 1.8 0.0 1.5 ! 4d assign (residue 99 and name hb#) (residue 96 and name hg2#) 1.8 0.0 3.2 ! 4d !A assign (residue 99 and name hb#) (residue 96 and name hd#) 1.8 0.0 3.2 ! 96cd not see it assign (residue 99 and name hn) (residue 97 and name ha#) 1.8 0.0 3.2 ! assign (residue 99 and name hn) (residue 97 and name hn) 1.8 0.0 3.2 ! !R assign (residue 99 and name hn) (residue 101 and name hn) 1.8 0.0 3.2 ! assign (residue 99 and name ha) ((residue 102 and name hb1) or (residue 102 and name hb2)) 1.8 0.0 3.2 ! assign (residue 99 and name hb#) ((residue 103 and name hd1#) or (residue 103 and name hd2#) or (residue 65 and name hg1) or (residue 65 and name hg2)) 1.8 0.0 3.2 ! 4d 0.77/26.5 !LONG !A assign (residue 99 and name hn) (residue 63 and name he#) 1.8 0.0 1.7 ! 63hz may be 6.79??, F32 rind ?? !Aassign (residue 99 and name hn) !A ((residue 63 and name hd#) or (residue 154 and name hz) !A or (residue 60 and name he#) or (residue 156 and name he#)) 1.8 0.0 1.7 ! !Aassign (residue 99 and name hb#) !A ((residue 63 and name hd#) or (residue 154 and name hz) !A or (residue 60 and name he#) or (residue 156 and name he#)) 1.8 0.0 3.2 ! 7.087ppm assign (residue 99 and name hb#) ((residue 65 and name hb1) or (residue 65 and name hb2)) 1.8 0.0 3.2 ! 4d assign (residue 99 and name hb#) (residue 66 and name ha) 1.8 0.0 3.2 ! 4D !A assign (residue 99 and name hn) (residue 68 and name hb) 1.8 0.0 3.2 ! assign (residue 99 and name hb#) (residue 68 and name hb) 1.8 0.0 3.2 ! assign (residue 99 and name hn) (residue 68 and (name hg1# or name hg2#)) 1.8 0.0 1.7 ! 5.8e6 !R assign (residue 99 and name hb#) !R ((residue 68 and name hg1#) or (residue 68 and name hg2#)) 1.8 0.0 1.5 ! 4d assign (residue 99 and name hn) (residue 69 and name hb#) 1.8 0.0 3.2 ! assign (residue 99 and name hb#) (residue 69 and name hb#) 1.8 0.0 1.5 ! 4d assign (residue 99 and name hn) (residue 69 and name ha) 1.8 0.0 3.2 ! assign (residue 99 and name hb#) (residue 69 and name ha) 1.8 0.0 3.2 ! 4d !R assign (residue 99 and name hb#) (residue 70 and name hn) 1.8 0.0 3.2 ! 99hb sees 70hn !R100 !INTRA assign (residue 100 and name hn) (residue 100 and name ha) 1.8 0.0 1.1 ! assign (residue 100 and name hn) ((residue 100 and name hd1) or (residue 100 and name hd2)) 1.8 0.0 3.2 ! !SEQ assign (residue 100 and name hn) (residue 99 and name hn) 1.8 0.0 1.1 ! assign (residue 100 and name hn) (residue 99 and name ha) 1.8 0.0 1.7 ! assign (residue 100 and name hn) (residue 99 and name hb#) 1.8 0.0 1.7 ! !R|A assign (residue 100 and name hn) (residue 101 and name hn) 1.8 0.0 1.1 ! assign (residue 100 and name ha) ((residue 103 and name hb1) or (residue 103 and name hb2)) 1.8 0.0 1.5 ! !MED assign (residue 100 and name he) (residue 96 and name hg2#) 1.8 0.0 3.2 ! assign (residue 100 and name hn) ((residue 97 and name ha1) or (residue 97 and name ha2)) 1.8 0.0 1.7 ! assign (residue 100 and name hn) (residue 98 and name hn) 1.8 0.0 3.2 ! assign (residue 100 and name hn) (residue 102 and name hn) 1.8 0.0 3.2 ! assign (residue 100 and name ha) ((residue 103 and name hd1#) or (residue 103 and name hd2#)) 1.8 0.0 3.2 ! assign (residue 100 and name ha) (residue 103 and name hn) 1.8 0.0 3.2 ! !LONG assign (residue 100 and name he) (residue 69 and name hb#) 1.8 0.0 3.2 ! 69hb# sees 100he and 100ha, hb#, and hg# assign (residue 100 and name he) (residue 69 and name ha) 1.8 0.0 3.2 ! AMB !A101 !INTRA assign (residue 101 and name hn) (residue 101 and name ha) 1.8 0.0 0.9 ! !SEQ assign (residue 101 and name hn) (residue 100 and name hn) 1.8 0.0 1.1 ! assign (residue 101 and name hn) (residue 100 and name ha) 1.8 0.0 1.7 ! assign (residue 101 and name hn) (residue 100 and name hb#) 1.8 0.0 1.7 ! assign (residue 101 and name hn) ((residue 100 and name hd1) or (residue 100 and name hd2)) 1.8 0.0 3.2 ! !R assign (residue 101 and name hn) (residue 102 and name hn) 1.8 0.0 1.1 ! !MED assign (residue 101 and name hn) (residue 98 and name ha) 1.8 0.0 1.7 ! assign (residue 101 and name hb#) (residue 98 and name ha) 1.8 0.0 1.5 ! assign (residue 101 and name hn) (residue 99 and name hn) 1.8 0.0 3.2 ! assign (residue 101 and name ha) (residue 104 and name hb#) 1.8 0.0 1.5 ! assign (residue 101 and name ha) (residue 104 and name hg#) 1.8 0.0 3.2 ! !LONG assign (residue 101 and name hn) (residue 69 and name hb#) 1.8 0.0 3.2 ! A69hb sees very wk A101hn assign (residue 101 and name hn) (residue 154 and name he#) 1.8 0.0 3.2 ! assign (residue 101 and name hb#) (residue 154 and name hd#) 1.8 0.0 3.2 ! assign (residue 101 and name hb#) ((residue 154 and name hz) or (residue 156 and name he#)) 1.8 0.0 3.2 ! think its 154 !Y102 !****** lots more peaks to hd and he in 2d noesy !INTRA assign (residue 102 and name hn) (residue 102 and name ha) 1.8 0.0 1.1 ! assign (residue 102 and name hn) ((residue 102 and name hb1) or (residue 102 and name hb2)) 1.8 0.0 1.7 ! assign (residue 102 and name hn) (residue 102 and name hd#) 1.8 0.0 2.2 ! 6.6e6, vios as med, mw? !SEQ assign (residue 102 and name hn) (residue 101 and name hn) 1.8 0.0 1.1 ! assign (residue 102 and name hn) (residue 101 and name ha) 1.8 0.0 1.7 ! AMB, ovlps 102ha assign (residue 102 and name hn) (residue 101 and name hb#) 1.8 0.0 1.7 ! 1.4e7 !R assign (residue 102 and name hn) (residue 103 and name hn) 1.8 0.0 1.1 ! assign (residue 102 and name hd#) ((residue 103 and name hd1#) or (residue 103 and name hd2#)) 1.8 0 1.5 !MED assign (residue 102 and name hn) (residue 99 and name ha) 1.8 0.0 3.2 ! !R assign (residue 102 and name hn) (residue 100 and name hn) 1.8 0.0 3.2 ! assign (residue 102 and name ha) (residue 105 and name hn) 1.8 0.0 3.2 ! !LONG assign (residue 102 and name he#) (residue 28 and name hb#) 1.8 0.0 3.2 ! 2d noesy, 4.75ppm, 28hb not seen in 3d - too close to water assign (residue 102 and name he#) ((residue 28 and name ha) or (residue 31 and name ha) or (residue 65 and name hd1) or (residue 65 and name hd2) or (residue 26 and name ha)) 1.8 0.0 3.2 !2d noesy 4.45ppm, 28ha closest 26jan02 assign (residue 102 and name he#) (residue 29 and name ha) 1.8 0.0 3.2 !2d noesy 4.22ppm, 29ha sees 6.64ppm assign (residue 102 and name he#) ((residue 29 and name hb1) or (residue 29 and name hb2) or (residue 104 and name hb#) or (residue 106 and name hg#)) 1.8 0.0 3.2 !AMB 2d noesy 2.18ppm assign (residue 102 and name he#) ((residue 29 and name hg#) or (residue 29 and name hd#) or (residue 103 and name hg) or (residue 22 and name hg#) or (residue 30 and name hb#)) 1.8 0.0 3.2 !2d noesy 1.91ppm, 103hg sees 102hd assign (residue 102 and name he#) ((residue 32 and name hb1) or (residue 32 and name hb2)) 1.8 0.0 3.2 ! 3d 13c noesy, 32hbs see 6.64ppm !A assign (residue 102 and name he#) (residue 35 and name hg2#) 1.8 0.0 3.2 ! !A assign (residue 102 and name hd#) !A ((residue 65 and name hb1) or (residue 65 and name hb2)) 1.8 0.0 3.2 ! assign (residue 102 and name hn) (residue 154 and name he#) 1.8 0.0 3.2 ! assign (residue 102 and name ha) (residue 154 and name he#) 1.8 0.0 3.2 ! !R assign (residue 102 and name hd#) (residue 154 and name he#) 1.8 0.0 3.2 ! assign (residue 102 and name hn) (residue 154 and name hz) 1.8 0.0 3.2 ! 5.6e6 assign (residue 102 and name ha) (residue 154 and name hz) 1.8 0.0 3.2 ! !A assign (residue 102 and name hd#) (residue 154 and name hz) 1.8 0.0 3.2 ! !AMB assign (residue 102 and name he#) ((residue 32 and name hd#) or (residue 112 and name he#)) 1.8 0.0 3.2 ! 2D NOESY to 7.06 !L103 !INTRA assign (residue 103 and name hn) (residue 103 and name hd#) 1.8 0.0 1.7 ! !SEQ assign (residue 103 and name hn) (residue 102 and name hn) 1.8 0.0 1.1 ! assign (residue 103 and name hn) ((residue 102 and name hb1) or (residue 102 and name hb2)) 1.8 0.0 3.2 ! assign (residue 103 and name hn) (residue 102 and name hd#) 1.8 0.0 3.2 ! !R assign (residue 103 and name hn) (residue 104 and name hn) 1.8 0.0 1.1 ! !MED assign (residue 103 and name hn) (residue 99 and name ha) 1.8 0.0 3.2 ! !R assign ((residue 103 and name hd1#) or (residue 103 and name hd2#)) !R (residue 99 and name hb#) 1.8 0.0 3.2 ! 4d assign (residue 103 and name hn) (residue 101 and name hn) 1.8 0.0 3.2 ! !R assign (residue 100 and name ha) (residue 103 and name hn) 1.8 0.0 3.2 ! !R assign ((residue 103 and name hd1#) or (residue 103 and name hd2#)) !R (residue 100 and name ha) 1.8 0.0 3.2 ! 4d assign (residue 103 and name hn) (residue 105 and name hn) 1.8 0.0 3.2 ! assign ((residue 103 and name hd1#) or (residue 103 and name hd2#)) (residue 107 and name hn) 1.8 0.0 3.2 ! 3d assign ((residue 103 and name hd1#) or (residue 103 and name hd2#)) (residue 107 and name hg#) 1.8 0.0 3.2 ! 3d !LONG assign ((residue 103 and name hd1#) or (residue 103 and name hd2#)) ((residue 65 and name hb1) or (residue 65 and name hb2)) 1.8 0.0 3.2 ! 4d assign ((residue 103 and name hd1#) or (residue 103 and name hd2#)) ((residue 65 and name hg1) or (residue 65 and name hg2)) 1.8 0.0 3.2 ! 4d to 103hd'' !R assign ((residue 103 and name hd1#) or (residue 103 and name hd2#)) !R (residue 66 and name ha) 1.8 0.0 1.5 ! 4d to both hds assign ((residue 103 and name hd1#) or (residue 103 and name hd2#)) (residue 66 and name hg1#) 1.8 0.0 3.2 assign ((residue 103 and name hd1#) or (residue 103 and name hd2#)) (residue 66 and name hg2#) 1.8 0.0 3.2 !L103 hd' sees both 66hgs !R assign ((residue 103 and name hd1#) or (residue 103 and name hd2#)) !R (residue 69 and name hb#) 1.8 0.0 3.2 ! 4d !Q104 !INTRA assign (residue 104 and name hn) (residue 104 and name hb#) 1.8 0.0 1.1 ! !SEQ assign (residue 104 and name hn) (residue 103 and name hn) 1.8 0.0 1.1 ! assign (residue 104 and name hn) ((residue 103 and name hb1) or (residue 103 and name hb2)) 1.8 0.0 1.7 ! assign (residue 104 and name hn) ((residue 103 and name hd1#) or (residue 103 and name hd2#)) 1.8 0.0 3.2 ! !R assign (residue 104 and name hn) (residue 105 and name hn) 1.8 0.0 1.1 ! !R assign (residue 104 and name hg#) (residue 105 and name hn) 1.8 0.0 3.2 ! !MED !101ha ovlps 104ha !R assign (residue 101 and name ha) (residue 104 and name hb#) 1.8 0.0 1.5 ! assign (residue 104 and name hn) (residue 102 and name hn) 1.8 0.0 3.2 ! assign (residue 104 and name hn) (residue 106 and name hn) 1.8 0.0 3.2 ! assign (residue 104 and name ha) (residue 107 and name hb#) 1.8 0.0 1.5 ! !LONG !M105 !INTRA assign (residue 105 and name hn) (residue 105 and name ha) 1.8 0.0 1.1 ! assign (residue 105 and name hn) ((residue 105 and name hb1) or (residue 105 and name hb2)) 1.8 0.0 1.1 ! assign (residue 105 and name ha) ((residue 105 and name hg1) or (residue 105 and name hg2)) 1.8 0.0 0.9 ! assign (residue 105 and name he#) ((residue 105 and name hb1) or (residue 105 and name hb2)) 1.8 0.0 3.2 ! !SEQ assign (residue 105 and name hn) (residue 104 and name hn) 1.8 0.0 1.1 ! !R assign (residue 105 and name hn) (residue 106 and name hn) 1.8 0.0 1.1 ! !MED !R assign ((residue 105 and name hn) residue 102 and name ha) 1.8 0.0 3.2 ! !R assign (residue 105 and name hn) (residue 103 and name hn) 1.8 0.0 3.2 ! assign (residue 105 and name ha) (residue 108 and name hn) 1.8 0.0 3.2 ! !LONG assign (residue 105 and name he#) (residue 112 and name ha) 1.8 0.0 3.2 ! 4d assign (residue 105 and name he#) (residue 112 and name hn) 1.8 0.0 3.2 ! 3d, 112hn sees 1.38 assign (residue 105 and name he#) ((residue 112 and name hd#) or (residue 32 and name he#)) 1.8 0.0 3.2 ! 7.58ppm to 3d, 112 assignment not sure assign (residue 105 and name he#) (residue 114 and name hn) 1.8 0.0 4.2 ! 3d, 114hn sees 1.37ppm very wk assign (residue 105 and name he#) (residue 115 and name hn) 1.8 0.0 3.2 ! 3d, 115hn sees 1.37ppm assign (residue 105 and name he#) (residue 115 and name hb#) 1.8 0.0 3.2 ! 4d assign (residue 105 and name he#) (residue 115 and name hd#) 1.8 0.0 3.2 ! 6.93ppm in 3d, AMB 115 assignment not sure assign (residue 105 and name he#) ((residue 115 and name he#) or (residue 112 and name he#) or (residue 32 and name hd#)) 1.8 0.0 3.2 ! 7.05ppm in 3d, 112 assignment not sure, could be 32hd assign (residue 105 and name he#) (residue 116 and name hn) 1.8 0.0 3.2 ! 3d, 116hn sees 1.37ppm assign (residue 105 and name he#) ((residue 116 and name hg1#) or (residue 116 and name hg2#)) 1.8 0.0 4.2 assign (residue 105 and name he#) ((residue 149 and name hd1#) or (residue 149 and name hd2#)) 1.8 0.0 3.2 ! sees both 149hds, hd' stronger !A assign (residue 105 and name ha) (residue 152 and name hd#) 1.8 0.0 3.2 ! assign (residue 105 and name he#) ((residue 152 and name hd1) or (residue 152 and name hd2)) 1.8 0.0 3.2 ! assign (residue 105 and name he#) (residue 152 and name he) 1.8 0.0 3.2 ! 3d, 152he sees 1.38ppm !E106 !INTRA assign (residue 106 and name hn) (residue 106 and name ha) 1.8 0.0 1.1 ! assign (residue 106 and name hn) ((residue 106 and name hb1) or (residue 106 and name hb2)) 1.8 0.0 1.1 ! !SEQ assign (residue 106 and name hn) (residue 105 and name hn) 1.8 0.0 1.1 ! ovlps 107hn assign (residue 106 and name hn) (residue 105 and name ha) 1.8 0.0 1.7 ! ovlps 103ha assign (residue 106 and name hn) ((residue 105 and name hb1) or (residue 105 and name hb2)) 1.8 0.0 1.7 ! assign (residue 106 and name hn) (residue 105 and name he#) 1.8 0.0 4.2 ! v wk to 105he# !R assign (residue 106 and name hn) (residue 107 and name hn) 1.8 0.0 1.1 ! ovlps 105hn !R assign (residue 106 and name ha) (residue 107 and name hn) 1.8 0.0 1.7 ! !MED assign (residue 106 and name hn) (residue 104 and name hn) 1.8 0.0 3.2 ! assign (residue 106 and name hn) (residue 103 and name ha) 1.8 0.0 1.7 ! ovlps 103ha assign (residue 106 and name hn) ((residue 103 and name hd1#) or (residue 103 and name hd2#)) 1.8 0.0 3.2 ! assign (residue 106 and name hn) (residue 108 and name hn) 1.8 0.0 3.2 ! !A assign (residue 106 and name ha) !R ((residue 108 and name hn) (residue 109 and name hn)) 1.8 0.0 3.2 ! !A assign (residue 106 and name hn) (residue 110 and name hn) 1.8 0.0 3.2 ! 110hn sees it also !R assign (residue 106 and name ha) (residue 110 and name hn) 1.8 0.0 3.2 ! 110hn sees it as med !LONG !Q107 !INTRA assign (residue 107 and name hn) (residue 107 and name ha) 1.8 0.0 1.1 ! assign (residue 107 and name hn) (residue 107 and name hb#) 1.8 0.0 1.1 ! !SEQ assign (residue 107 and name hn) (residue 106 and name hn) 1.8 0.0 1.1 ! assign (residue 107 and name hn) (residue 106 and name ha) 1.8 0.0 1.7 ! assign (residue 107 and name hn) (residue 108 and name hn) 1.8 0.0 1.1 ! !R assign (residue 107 and name hg#) (residue 108 and name hn) 1.8 0.0 1.1 ! !MED assign (residue 107 and name hn) (residue 104 and name ha) 1.8 0.0 1.7 ! ovlps 107ha !R assign (residue 104 and name ha) (residue 107 and name hb#) 1.8 0.0 1.5 ! assign (residue 104 and name ha) (residue 107 and name hg#) 1.8 0.0 3.2 ! !LONG !N108 !INTRA assign (residue 108 and name hn) (residue 108 and name ha) 1.8 0.0 1.1 ! assign (residue 108 and name hn) (residue 108 and (name hb1 or name hb2)) 1.8 0.0 1.1 ! !SEQ !RA assign (residue 108 and name hn) (residue 107 and name hn) 1.8 0.0 1.1 ! ovlped assign (residue 108 and name hn) (residue 107 and name ha) 1.8 0.0 1.7 !** vios, looks strong 2.3e7, but 108hn ovlps 100hn assign (residue 108 and name hn) (residue 107 and name hb#) 1.8 0.0 1.7 ! assign (residue 108 and name hn) (residue 107 and name hg#) 1.8 0.0 3.2 ! !R assign (residue 108 and name hn) (residue 109 and name hn) 1.8 0.0 1.1 ! ovlps 107hn !MED !R assign (residue 108 and name hb#) (residue 105 and name ha) 1.8 0.0 1.5 ! !R assign (residue 108 and name hn) (residue 106 and name hn) 1.8 0.0 1.7 ! !LONG !G109 !INTRA assign (residue 109 and name hn) ((residue 109 and name ha1) or (residue 109 and name ha2)) 1.8 0.0 0.9 ! !SEQ !A assign (residue 109 and name hn) (residue 108 and name hn) 1.8 0.0 ! assign (residue 109 and name hn) (residue 108 and name ha) 1.8 0.0 1.7 ! assign (residue 109 and name hn) ((residue 108 and name hb1) or (residue 108 and name hb2)) 1.8 0.0 3.2 ! !R assign (residue 109 and name hn) (residue 110 and name hn) 1.8 0.0 1.1 ! 1.9e7 !MED assign (residue 109 and name hn) (residue 106 and name ha) 1.8 0.0 1.7 ! assign (residue 109 and name hn) ((residue 106 and name hg1) or (residue 106 and name hg2)) 1.8 0.0 1.7 ! assign (residue 109 and name hn) (residue 107 and name hn) 1.8 0.0 3.2 ! !LONG !E110 !dont see ha in 3d noesy !dont see hb in noesy !INTRA assign (residue 110 and name hn) (residue 110 and name hb#) 1.8 0.0 1.1 ! 2.8e7 !SEQ assign (residue 110 and name hn) (residue 109 and name hn) 1.8 0.0 1.1 ! 2.8e7 assign (residue 110 and name hn) ((residue 109 and name ha1) or (residue 109 and name ha2)) 1.8 0.0 1.1 ! 1.9e7 !MED assign (residue 110 and name hn) (residue 106 and name ha) 1.8 0.0 1.7 ! !R assign (residue 110 and name hn) (residue 106 and name hn) 1.8 0.0 3.2 ! assign (residue 110 and name hn) ((residue 108 and name hb1) or (residue 108 and name hb2)) 1.8 0.0 3.2 ! 1.9e7 !LONG !P111 !INTRA !SEQ assign (residue 111 and name hd#) (residue 110 and name ha) 1.8 0.0 1.5 ! 4.5e5 assign (residue 111 and name hb#) (residue 112 and name hn) 1.8 0.0 3.2 ! !MED assign (residue 111 and name hb#) (residue 113 and name hn) 1.8 0.0 3.2 ! assign (residue 111 and name hb#) (residue 114 and name hn) 1.8 0.0 3.2 ! assign (residue 111 and name hg#) (residue 114 and name hb#) 1.8 0.0 1.5 ! 8e5 to D114HB# assign (residue 111 and name hd#) (residue 114 and name hb#) 1.8 0.0 3.2 ! 4.5e5, 114hb sees both 111hds ! !LONG !F112 !INTRA assign (residue 112 and name hn) (residue 112 and name ha) 1.8 0.0 1.7 ! assign (residue 112 and name hn) (residue 112 and (name hb1 or name hb2)) 1.8 0.0 1.7 ! assign (residue 112 and name hn) (residue 112 and name hd#) 1.8 0.0 3.2 ! !SEQ !i-1 is P111 assign (residue 112 and name hn) (residue 111 and name ha) 1.8 0.0 0.9 ! 1.3e7 assign (residue 112 and name hn) (residue 111 and (name hb1 or name hb2)) 1.8 0.0 3.2 ! assign (residue 112 and name hn) (residue 111 and (name hg1 or name hg2)) 1.8 0.0 3.2 ! med? but ovlps 126hbs to hn assign (residue 112 and name hn) (residue 111 and (name hd1 or name hd2)) 1.8 0.0 3.2 ! !A assign (residue 112 and name hn) (residue 113 and name hn) 1.8 0.0 3.2 ! 113hn ovlps 112hn !MED assign (residue 112 and name ha) (residue 115 and name hb#) 1.8 0.0 3.2 ! assign (residue 112 and name ha) (residue 115 and name hn) 1.8 0.0 3.2 ! assign (residue 112 and name ha) (residue 116 and name hn) 1.8 0.0 3.2 ! !LONG assign (residue 112 and name hd#) ((residue 31 and name hd1#) or (residue 31 and name hd2#)) 1.8 0.0 3.2 ! 3d aro noesy to 31 hd'', it sees 7.59ppm, also to W117 hd1 !R assign (residue 112 and name hz) (residue 35 and name hg2#) 1.8 0.0 3.2 ! 3d aro noe to 35 hg2, it sees 6.75ppm !R assign (residue 112 and name he#) (residue 35 and name hg2#) 1.8 0.0 3.2 ! 3d aro noe to 35 hg2, it sees 7.05ppm !R assign (residue 112 and name hz) (residue 35 and name hd#) 1.8 0.0 3.2 ! 3d aro noe to 35 hd, it sees 6.75ppm !R assign (residue 112 and name he#) (residue 35 and name hd#) 1.8 0.0 3.2 ! 3d aro noe to 35 hd, it sees 7.05ppm assign (residue 112 and name hn) (residue 102 and name he#) 1.8 0.0 3.2 ! 3d 6.65ppm assign (residue 112 and name hz) (residue 102 and name hd#) 1.8 0.0 3.2 ! 2d assign (residue 112 and name hd#) (residue 105 and name he#) 1.8 0.0 3.2 ! 1.38 in 2dnoesy, and in 3d 13c aro, 105he sees it assign (residue 112 and name he#) ((residue 105 and name hg1) or (residue 105 and name hg2) or (residue 105 and name hb1) or (residue 105 and name hb2)) 1.8 0.0 3.2 ! 2.68 3daro assign (residue 112 and name hz) (residue 154 and name he#) 1.8 0.0 3.2 ! 2dnoesy assign (residue 112 and name hz) (residue 154 and name hz) 1.8 0.0 3.2 ! 2dnoesy !A113 !INTRA !SEQ !A assign (residue 113 and name hn) (residue 112 and name hn) 1.8 0.0 1.1 ! 112hn ovlps 112hn assign (residue 113 and name hn) (residue 112 and name ha) 1.8 0.0 1.7 ! assign (residue 113 and name hn) ((residue 112 and name hb1) or (residue 112 and name hb2)) 1.8 0.0 1.7 ! assign (residue 113 and name hn) (residue 112 and name hd#) 1.8 0.0 1.7 ! !R assign (residue 113 and name hn) (residue 114 and name hn) 1.8 0.0 1.1 ! !MED assign (residue 113 and name hn) (residue 111 and name ha) 1.8 0.0 3.2 ! !R assign (residue 113 and name hn) (residue 115 and name hn) 1.8 0.0 3.2 ! assign (residue 113 and name ha) (residue 116 and name hg#) 1.8 0.0 3.2 ! 3d to 116 hg'' assign (residue 113 and name hb#) (residue 116 and name hg#) 1.8 0.0 3.2 ! 4d to 116 hg'' !LONG assign (residue 113 and name hb#) (residue 26 and name ha) 1.8 0.0 3.2 !4D assign (residue 113 and name hb#) (residue 27 and name ha) 1.8 0.0 3.2 !3D, v wk in 4d assign (residue 113 and name hb#) (residue 27 and name hb#) 1.8 0.0 3.2 !3D 27hb' !R assign (residue 113 and name hb#) (residue 28 and name hg#) 1.8 0.0 3.2 !4D assign (residue 113 and name hn) (residue 28 and name hn) 1.8 0.0 4.2 !28hn sees 113hn !R assign (residue 113 and name hb#) (residue 28 and name hn) 1.8 0.0 3.2 !113 hb# sees it also assign (residue 113 and name hb#) (residue 28 and name ha) 1.8 0.0 1.5 ! 4D assign (residue 113 and name hn) (residue 31 and name hd#) 1.8 0.0 3.2 ! assign (residue 113 and name ha) (residue 31 and name hd#) 1.8 0.0 1.5 ! 4d to 31 hd'' assign (residue 113 and name hb#) (residue 31 and name hd#) 1.8 0.0 0.9 ! 4d to 31 hd'', med for 113hb to 31hd'' assign (residue 113 and name hb#) (residue 32 and name hn) 1.8 0.0 3.2 ! !AMB assign (residue 113 and name hb#) ((residue 112 and name hd#) or (residue 117 and name hd1)) 1.8 0.0 3.2 ! !D114 !INTRA assign (residue 114 and name hn) (residue 114 and name ha) 1.8 0.0 1.1 ! !SEQ assign (residue 114 and name hn) (residue 113 and name hn) 1.8 0.0 1.1 ! assign (residue 114 and name hn) (residue 113 and name ha) 1.8 0.0 1.7 ! assign (residue 114 and name hn) (residue 113 and name hb#) 1.8 0.0 1.1 ! 2.5e7 !R assign (residue 114 and name hn) (residue 115 and name hn) 1.8 0.0 1.1 ! !MED !R assign (residue 114 and name hn) (residue 111 and name hb#) 1.8 0.0 3.2 !2.435ppm assign (residue 114 and name hn) (residue 111 and name hg#) 1.8 0.0 2.2 !2.14ppm !R assign ((residue 111 and name hg1) or (residue 111 and name hg2)) !R (residue 114 and name hb#) 1.8 0.0 1.5 !8e5 to D114HB# !R assign ((residue 111 and name hd1) or (residue 111 and name hd2)) !R (residue 114 and name hb#) 1.8 0.0 1.5 !4.5e5, 114hb sees both 111hds !112hn ovlps 114hn !R assign (residue 114 and name hn) (residue 116 and name hn) 1.8 0.0 3.2 ! assign (residue 114 and name ha) (residue 117 and name hb#) 1.8 0.0 3.2 ! assign (residue 114 and name ha) (residue 117 and name hn) 1.8 0.0 3.2 ! !LONG !F115 !INTRA assign (residue 115 and name hn) (residue 115 and name ha) 1.8 0.0 1.1 ! assign (residue 115 and name hn) (residue 115 and name hb#) 1.8 0.0 1.1 ! assign (residue 115 and name hn) (residue 115 and name hd#) 1.8 0.0 3.2 ! assign (residue 115 and name hd#) (residue 115 and name ha) 1.8 0.0 1.7 ! 4.13 in 2dnoesy !SEQ assign (residue 115 and name hn) (residue 114 and name hn) 1.8 0.0 1.1 ! assign (residue 115 and name hn) (residue 114 and name ha) 1.8 0.0 1.7 ! assign (residue 115 and name hn) (residue 114 and name hb#) 1.8 0.0 1.1 ! !R assign (residue 115 and name hn) (residue 116 and name hn) 1.8 0.0 1.1 ! assign (residue 115 and name hd#) (residue 116 and (name hg1# or name hg2#)) 1.8 0.0 3.2 ! 2dnoesy, V116 sees 6.94 !MED !R assign (residue 112 and name ha) (residue 115 and name hb#) 1.8 0.0 3.2 ! assign (residue 115 and name hd#) (residue 112 and name hd#) 1.8 0.0 3.2 ! assign (residue 115 and name ha) (residue 118 and name hb#) 1.8 0.0 3.2 ! assign (residue 115 and name hd#) (residue 119 and name hd#) 1.8 0.0 3.2 ! 2dnoesy assign (residue 115 and name hd#) (residue 119 and name he#) 1.8 0.0 3.2 ! 2dnoesy assign (residue 115 and name he#) (residue 119 and name he#) 1.8 0.0 3.2 ! 2dnoesy !LONG assign (residue 115 and name hn) (residue 105 and name he#) 1.8 0.0 3.2 ! 1.38 in 3d N15noesy, 105he# sees it also assign (residue 115 and name hd#) (residue 145 and (name hd1# or name hd2#)) 1.8 0.0 3.2 ! 0.26 in 2dnoesy, 145hd' sees 6.94 assign (residue 115 and name hd#) (residue 148 and name hb#) 1.8 0.0 3.2 ! 1.83 in 2dnoesy, 148hb# sees 6.94 assign (residue 115 and name hd#) (residue 149 and (name hd1# or name hd2#)) 1.8 0.0 3.2 ! 0.07 in 2dnoesy, 149hd' sees 6.94 !V116 !INTRA assign (residue 116 and name hn) (residue 116 and name ha) 1.8 0.0 1.7 ! assign (residue 116 and name hn) (residue 116 and name hb) 1.8 0.0 1.7 ! assign (residue 116 and name hn) (residue 116 and name hg1#) 1.8 0.0 1.7 assign (residue 116 and name hn) (residue 116 and name hg2#) 1.8 0.0 1.7 ! both are med !SEQ assign (residue 116 and name hn) (residue 115 and name hn) 1.8 0.0 1.1 ! assign (residue 116 and name hn) (residue 115 and name ha) 1.8 0.0 1.7 ! assign (residue 116 and name hn) (residue 115 and name hb#) 1.8 0.0 1.7 ! assign (residue 116 and name hn) (residue 115 and name hd#) 1.8 0.0 1.7 ! !R assign (residue 116 and name hn) (residue 117 and name hn) 1.8 0.0 1.1 ! assign (residue 116 and (name hg1# or name hg2#)) (residue 117 and name ha) 1.8 0.0 3.2 !3d to 116hg' assign (residue 116 and (name hg1# or name hg2#)) (residue 117 and name he1) 1.8 0.0 3.2 ! 3d to 116hg'', 117he1 sees it also !MED assign (residue 116 and name hn) (residue 113 and name hb#) 1.8 0.0 4.2 ! assign (residue 116 and name hn) (residue 114 and name hn) 1.8 0.0 3.2 ! assign (residue 116 and (name hg1# or name hg2#)) (residue 113 and name ha) 1.8 0.0 3.2 ! 4d !R assign ((residue 116 and name hg1#) or (residue 116 and name hg2#)) !R (residue 113 and name hb#) 1.8 0.0 3.2 ! 4d assign (residue 116 and name ha) (residue 119 and name hd#) 1.8 0.0 3.2 ! assign (residue 117 and name he3) (residue 120 and (name hg1# or name hg2#)) 1.8 0.0 3.2 ! both 120hgs in 2d noesy !LONG assign (residue 116 and name hn) (residue 31 and (name hd1# or name hd2#)) 1.8 0.0 3.2 ! assign ((residue 116 and name hg1#) or (residue 116 and name hg2#)) ((residue 31 and name hd1#) or (residue 31 and name hd2#)) 1.8 0.0 3.2 ! 4d, to 116hg'' !R assign (residue 116 and name hn) (residue 105 and name he#) 1.8 0.0 3.2 ! assign (residue 116 and name hn) (residue 145 and (name hd1# or name hd2#)) 1.8 0.0 3.2 ! assign ((residue 116 and name hg1#) or (residue 116 and name hg2#)) ((residue 145 and name hd1#) or (residue 145 and name hd2#)) 1.8 0.0 3.2 ! 4d, to 116hg' assign ((residue 116 and name hg1#) or (residue 116 and name hg2#)) ((residue 149 and name hd1#) or (residue 149 and name hd2#)) 1.8 0.0 3.2 ! 4d, 116hg' assign (residue 116 and (name hg1# or name hg2#)) ((residue 165 and name hd#) or (residue 112 and name hz) or (residue 119 and name hz)) 1.8 0.0 3.2 ! 3d to 116hg' and to hg'' !R assign (residue 116 and name hg1#) (residue 171 and name hd1#) 1.8 0.0 3.2 !R assign (residue 116 and name hg2#) (residue 171 and name hd2#) 1.8 0.0 3.2 !R assign (residue 116 and name hg2#) (residue 171 and name hd1#) 1.8 0.0 3.2 !R assign (residue 116 and name hg2#) (residue 171 and name hd2#) 1.8 0.0 3.2 ! 4d, both hgs see pks to both 171hds !W117 !INTRA assign (residue 117 and name hn) (residue 117 and name hb#) 1.8 0.0 1.7 ! assign (residue 117 and name he3) (residue 117 and name hb#) 1.8 0.0 1.5 ! 3.266 2d noesy assign (residue 117 and name hn) (residue 117 and name hd1) 1.8 0.0 1.7 ! assign (residue 117 and name hn) (residue 117 and name he1) 1.8 0.0 4.2 !v wk assign (residue 117 and name hn) (residue 117 and name he3) 1.8 0.0 3.2 ! assign (residue 117 and name ha) (residue 117 and name he3) 1.8 0.0 3.2 ! !A assign (residue 117 and name hz3) (residue 117 and name ha) 1.8 0.0 3.2 !2d noesy, assignment hz3 based on NOEs !SEQ assign (residue 117 and name hn) (residue 116 and name hn) 1.8 0.0 1.7 ! assign (residue 117 and name hn) (residue 116 and name ha) 1.8 0.0 3.2 ! assign (residue 117 and name hn) (residue 116 and name hg#) 1.8 0 1.7 ! 1e7 assign (residue 117 and name hd1) (residue 116 and name hg#) 1.8 0 3.2 ! !A assign (residue 117 and name he3) (residue 116 and name hg#) 1.8 0 3.2 ! 0.95ppm 2d noesy, 116hg'' sees 7.01ppm !R assign (residue 117 and name hn) (residue 118 and name hn) 1.8 0.0 1.7 ! !MED assign (residue 117 and name hn) (residue 113 and name hb#) 1.8 0 3.2 ! assign (residue 117 and name he1) (residue 113 and name hb#) 1.8 0 3.2 ! assign (residue 117 and name hn) (residue 114 and name ha) 1.8 0.0 3.2 ! !R assign (residue 117 and name hb#) (residue 114 and name ha) 1.8 0.0 3.2 ! assign (residue 117 and name hn) (residue 115 and name hn) 1.8 0.0 3.2 ! !R assign (residue 117 and name ha) (residue 120 and name hg#) 1.8 0.0 3.2 ! !A assign (residue 117 and name hd1) (residue 120 and name hg#) 1.8 0 3.2 ! 2d noesy, 120hg' sees 7.58 could be F112hd# assign (residue 117 and name hh2) (residue 120 and name hg#) 1.8 0 3.2 ! 2d noesy, 120hg'' sees 6.90 assign (residue 117 and name hz3) (residue 120 and name hg#) 1.8 0 3.2 ! 2d noesy, 120hg'' sees 6.47 !A assign (residue 117 and name he3) (residue 121 and name hb1) 1.8 0 3.2 !A assign (residue 117 and name he3) (residue 121 and name hb2) 1.8 0 3.2 ! 2d noesy to 2.737 and 3.076, 121hbs see 7.01ppm !LONG assign (residue 117 and name he1) (residue 26 and name ha) 1.8 0 1.7 !1.6e7, 26ha sees it as strong, D114ha at 4.41, does not see 117he1 assign (residue 117 and name he1) (residue 26 and name hg2#) 1.8 0 1.7 !1.7e7 assign (residue 117 and name hn) (residue 31 and name hd#) 1.8 0 3.2 ! assign (residue 117 and name he1) (residue 31 and name hd#) 1.8 0 3.2 !1.7e7 assign (residue 117 and name hd1) (residue 31 and name hd#) 1.8 0 3.2 ! 3d 13c aro !A assign (residue 117 and name he3) !A ((residue 121 and name ha) or (residue 172 and name ha)) 1.8 0.0 3.2 ! 4.28ppm 2d noesy, 121ha sees 7.02 assign (residue 117 and name he3) (residue 122 and name ha) 1.8 0.0 3.2 ! 3.93ppm 2d noesy, 9.7e4, 122ha sees 7.02 as v wk assign (residue 117 and name he3) ((residue 122 and name hb#) or (residue 171 and name ha)) 1.8 0.0 3.2 ! 3.32ppm 2d noesy, 122hbs see wk 7.02 assign (residue 117 and name hz3) (residue 123 and name ha) 1.8 0.0 3.2 ! hz3 at 6.47 in 2d noesy, 123ha sees 6.47 assign (residue 117 and name hz3) (residue 123 and name ha) 1.8 0.0 4.2 ! hz3 at 6.47 in 2d noesy, 123ha sees 6.47 assign (residue 117 and name he3) ((residue 124 and name hb#) or (residue 123 and name hg#) or (residue 125 and name hg#)) 1.8 0.0 3.2 ! 2.39ppm 2d noesy assign (residue 117 and name hz3) ((residue 124 and name ha) or (residue 25 and name ha)) 1.8 0.0 3.2 !AMB hz3 at 6.47 in 2d noesy !A assign (residue 117 and name hh2) !A ((residue 124 and name ha) or (residue 25 and name ha)) 1.8 0.0 3.2 !AMB pk at 4.71, hz3 at 6.47 in 2d noesy assign (residue 117 and name hn) (residue 171 and name hd#) 1.8 0.0 3.2 ! !R assign (residue 171 and name hd#) (residue 117 and name ha) 1.8 0.0 3.2 ! assign (residue 117 and name he1) (residue 171 and name hd#) 1.8 0 3.2 ! 3d15n, sees 171hd' assign (residue 117 and name hz3) ((residue 171 and name ha) or (residue 122 and name hb#)) 1.8 0.0 3.2 !2d noesy, 171ha sees wk pk 6.47 !S118 !INTRA assign (residue 118 and name hn) (residue 118 and name ha) 1.8 0.0 1.7 ! assign (residue 118 and name hn) (residue 118 and (name hb1 or name hb2)) 1.8 0.0 1.1 ! !SEQ assign (residue 118 and name hn) (residue 117 and name hn) 1.8 0.0 1.7 ! assign (residue 118 and name hn) (residue 117 and name ha) 1.8 0.0 3.2 ! !R assign (residue 118 and name hn) (residue 119 and name hn) 1.8 0.0 1.7 ! !MED assign (residue 118 and name hn) (residue 116 and name ha) 1.8 0.0 3.2 ! 9.7e6 seems too strong for 116ha-118hn assign (residue 118 and name hn) (residue 116 and name hn) 1.8 0.0 3.2 ! !LONG !A assign (residue 118 and name hn) !A (residue 171 and (name hd1# or name hd2#)) 1.8 0.0 3.2 ! L171hd'' not see 118hn !##### stop here 1-29-02 need to finish the ring !F119 !INTRA assign (residue 119 and name hn) (residue 119 and name ha) 1.8 0.0 1.1 ! assign (residue 119 and name hn) (residue 119 and (name hb1 or name hb2)) 1.8 0.0 1.7 ! assign (residue 119 and name hn) (residue 119 and name he#) 1.8 0.0 3.2 ! !SEQ assign (residue 119 and name hn) (residue 118 and name hn) 1.8 0.0 1.1 ! assign (residue 119 and name hn) (residue 118 and (name hb1 or name hb2)) 1.8 0.0 1.7 ! assign (residue 119 and name hn) (residue 120 and name hn) 1.8 0.0 1.1 ! !MED !dont see 116ha-119hn !dont see 117hn-119hn !R assign (residue 119 and name hn) (residue 121 and name hn) 1.8 0.0 3.2 ! assign (residue 119 and name hd#) (residue 115 and name hd#) 1.8 0.0 3.2 !AMB, 2d noesy assign (residue 119 and name he#) (residue 115 and name hd#) 1.8 0.0 3.2 !AMB, 2d noesy assign (residue 119 and name he#) ((residue 115 and name hd#) or (residue 165 and name he#)) 1.8 0.0 3.2 !AMB, 2d noesy !LONG assign (residue 119 and name hn) (residue 141 and name hb#) 1.8 0.0 4.2 !SD? v wk, 141hb* sees v wk also !A assign (residue 119 and name he#) (residue 141 and name ha) 1.8 0.0 3.2 ! assign (residue 119 and name hd#) ((residue 144 and name ha) or (residue 115 and name ha)) 1.8 0.0 3.2 !4.13ppm in 2d noesy, 144ha sees very wk pk assign (residue 119 and name he#) ((residue 144 and name ha) or (residue 115 and name ha)) 1.8 0.0 3.2 !4.12ppm in 2d noesy !R assign (residue 119 and name hd#) (residue 144 and name hb#) 1.8 0.0 1.5 ! 2d noesy, 144hb sees both hd and he !R assign (residue 119 and name he#) (residue 144 and name hb#) 1.8 0.0 1.5 ! 2d noesy, 144hb sees both hd and he !A assign (residue 119 and name hz) (residue 144 and name hb#) 1.8 0.0 3.2 ! 2d noesy, 144hb not see it assign (residue 119 and name hn) (residue 145 and (name hd1# or name hd2#)) 1.8 0.0 3.2 ! 0.26 !R assign (residue 119 and name hd#) (residue 145 and (name hd1# or name hd2#)) 1.8 0.0 3.2 ! 0.26 in 2dnoesy and 13caro, 145hd' sees wk 7.34 assign (residue 119 and name he#) ((residue 145 and name hd1#) or (residue 145 and name hd2#)) 1.8 0.0 3.2 ! 0.26 in 2dnoesy and 13caro, 145hd' sees wk 6.30 assign (residue 119 and name hd#) (residue 148 and name hb#) 1.8 0.0 3.2 ! 2d noesy, 148hb sees it as v wk assign (residue 119 and name he#) (residue 148 and name hb#) 1.8 0.0 1.5 ! 2d noesy, 148hb sees it !R assign (residue 119 and name hz) (residue 148 and name hb#) 1.8 0.0 3.2 ! 2d noesy, 148hb sees it !V120 !INTRA assign (residue 120 and name hn) (residue 120 and (name hg1# or name hg2#)) 1.8 0.0 1.7 ! assign (residue 120 and name hn) (residue 120 and name ha) 1.8 0.0 1.7 ! !SEQ assign (residue 120 and name hn) (residue 119 and name hn) 1.8 0.0 1.7 ! assign (residue 120 and name hn) (residue 119 and name ha) 1.8 0.0 1.7 ! !A assign (residue 120 and name hn) (residue 121 and name ha) 1.8 0.0 1.7 ! 121ha sees wk 7.02 !R assign (residue 120 and name hn) (residue 121 and name hn) 1.8 0.0 1.1 ! !MED assign (residue 120 and (name hg1# or name hg2#)) (residue 117 and name ha) 1.8 0.0 3.2 ! 4d to 120hg'' !R assign (residue 117 and name hd1) (residue 120 and (name hg1# or name hg2#)) 1.8 0 3.2 ! 2d noesy, 120hg' sees 7.58 but could be F112hd# !R assign (residue 117 and name hh2) (residue 120 and (name hg1# or name hg2#)) 1.8 0 3.2 ! 2d noesy, 120hg'' sees 6.90 !R assign (residue 117 and name hz3) (residue 120 and (name hg1# or name hg2#)) 1.8 0 3.2 ! 2d noesy, 120hg'' sees 6.47 assign (residue 120 and name hn) (residue 122 and name hn) 1.8 0.0 2.2 ! 5.4e7 !R assign (residue 123 and name hn) (residue 120 and (name hg1# or name hg2#)) 1.8 0.0 3.2 ! 3d to 120hg'' !LONG !R assign (residue 120 and (name hg1# or name hg2#)) (residue 125 and name hn) 1.8 0.0 3.2 ! 120hg'' 3d !R assign (residue 120 and (name hg1# or name hg2#)) (residue 125 and name hg1) 1.8 0.0 3.2 !R assign (residue 120 and (name hg1# or name hg2#)) (residue 125 and name hg2) 1.8 0.0 3.2 ! 120hg' sees both, 3d and 4d assign (residue 120 and (name hg1# or name hg2#)) (residue 141 and name hb#) 1.8 0.0 3.2 ! 4d assign (residue 120 and (name hg1# or name hg2#)) (residue 166 and name he#) 1.8 0.0 1.5 !4d to hg', 1.62/16.6, 2.9e6 assign (residue 120 and name hn) ((residue 171 and name hd1#) or (residue 171 and name hd2#)) 1.8 0.0 3.2 ! !R assign (residue 120 and name hg1#) (residue 171 and (name hd1# or name hd2#)) 1.8 0.0 3.2 !R assign (residue 120 and name hg2#) (residue 171 and (name hd1# or name hd2#)) 1.8 0.0 3.2 ! 4D assign (residue 120 and (name hg1# or name hg2#)) (residue 171 and name hg) 1.8 0.0 3.2 ! 4d to 120hg'' assign (residue 120 and (name hg1# or name hg2#)) (residue 171 and name ha) 1.8 0.0 3.2 ! 4d to 120hg'' !A assign ((residue 120 and name hg1#) or (residue 120 and name hg2#)) ! ((residue 172 and name hg1#) or (residue 172 and name hg2#) ! or (residue 95 and name hd#)) 1.8 0.0 3.2 ! 0.198 ppm !N121 !INTRA assign (residue 121 and name hn) (residue 121 and name ha) 1.8 0.0 1.1 ! assign (residue 121 and name hn) (residue 121 and (name hb1 or name hb2)) 1.8 0.0 1.7 ! !SEQ assign (residue 121 and name hn) (residue 120 and name hn) 1.8 0.0 1.1 ! assign (residue 121 and name hn) (residue 120 and name ha) 1.8 0.0 1.7 ! assign (residue 121 and name hn) (residue 120 and (name hg1# or name hg2#)) 1.8 0.0 1.7 !R assign (residue 121 and name hn) (residue 122 and name hn) 1.8 0.0 1.7 ! !MED !R assign (residue 121 and name ha) (residue 117 and name he3) 1.8 0.0 3.2 ! assign (residue 121 and name hn) (residue 118 and name ha) 1.8 0.0 3.2 ! assign (residue 121 and name hn) (residue 119 and name hn) 1.8 0.0 3.2 ! assign (residue 121 and name hn) ((residue 119 and name ha) or (residue 122 and name ha)) 1.8 0.0 1.7 ! 5.2e6 !R assign (residue 121 and name hn) (residue 123 and name hn) 1.8 0.0 3.2 ! !R assign (residue 121 and (name hb1 or name hb2)) (residue 123 and name hn) 1.8 0.0 3.2 ! !LONG !H122 !INTRA assign (residue 122 and name hn) (residue 122 and name ha) 1.8 0.0 1.1 ! !SEQ assign (residue 122 and name hn) (residue 121 and name hn) 1.8 0.0 1.7 ! assign (residue 122 and name hn) (residue 121 and name ha) 1.8 0.0 1.7 ! assign (residue 122 and name hn) ((residue 121 and name hb1) or (residue 121 and name hb2)) 1.8 0.0 1.7 ! !R assign (residue 122 and name hn) (residue 123 and name hn) 1.8 0.0 1.7 ! !MED assign (residue 122 and name hn) (residue 120 and (name hg1# or name hg2#)) 1.8 0.0 3.2 ! !R assign (residue 122 and name hn) (residue 120 and name hn) 1.8 0.0 1.7 ! !LONG !R assign (residue 122 and name ha) (residue 117 and name he3) 1.8 0.0 3.2 ! !R assign (residue 122 and name hb#) (residue 117 and name he3) 1.8 0.0 3.2 ! !Q123 !INTRA assign (residue 123 and name hn) (residue 123 and name ha) 1.8 0.0 1.1 ! assign (residue 123 and name hn) (residue 123 and name hb#) 1.8 0.0 1.1 ! assign (residue 123 and name hn) (residue 123 and name hg#) 1.8 0.0 2.2 ! !SEQ assign (residue 123 and name hn) (residue 122 and name hn) 1.8 0.0 1.1 ! assign (residue 123 and name hn) (residue 122 and name ha) 1.8 0.0 1.7 ! assign (residue 123 and name hn) (residue 122 and name hb#) 1.8 0.0 3.2 ! 5.4e6 !R assign (residue 123 and name ha) (residue 124 and (name hd1 or name hd2)) 1.8 0.0 1.5 assign (residue 123 and name hg#) (residue 124 and (name hd1 or name hd2)) 1.8 0.0 1.5 !MED assign (residue 123 and name hn) (residue 120 and name hg#) 1.8 0.0 1.7 ! 1.7e7, 120hg'' sees it med !A assign (residue 123 and name hn) (residue 120 and name hb) 1.8 0.0 3.2 !ovlped assign (residue 123 and name hn) (residue 121 and name hn) 1.8 0.0 3.2 ! assign (residue 123 and name hn) (residue 121 and name ha) 1.8 0.0 3.2 ! assign (residue 123 and name hn) (residue 121 and (name hb1 or name hb1)) 1.8 0.0 3.2 ! assign (residue 123 and name hg#) (residue 121 and (name hb1 or name hb1)) 1.8 0.0 3.2 !LONG !AMB assign (residue 123 and name hn) ((residue 117 and name ha) or (residue 124 and (name hd1 or name hd2))) 1.8 0.0 3.2 !3.81ppm !P124 ! nada to ha, hbs, hgs, hds !INTRA !SEQ assign (residue 124 and (name hd1 or name hd2)) (residue 123 and name ha) 1.8 0.0 1.5 !MED !LONG !Q125 !INTRA assign (residue 125 and name hn) (residue 125 and name ha) 1.8 0.0 1.7 ! assign (residue 125 and name hn) (residue 125 and name hb#) 1.8 0.0 1.7 ! assign (residue 125 and name hn) (residue 125 and (name hg1 or name hg2)) 1.8 0.0 3.2 ! !SEQ assign (residue 125 and name hn) (residue 124 and name ha) 1.8 0.0 0.7 ! very strong assign (residue 125 and name hn) (residue 124 and (name hb1 or name hb2)) 1.8 0.0 1.7 ! !R assign (residue 125 and name hn) (residue 126 and name hn) 1.8 0.0 3.2 ! !MED !A assign (residue 125 and name hn) (residue 123 and name hn) 1.8 0.0 3.2 ! !LONG assign (residue 125 and name hn) (residue 120 and (name hg1# or name hg2#)) 1.8 0.0 3.2 ! assign (residue 125 and name hg1) (residue 120 and name hb) 1.8 0.0 3.2 assign (residue 125 and name hg2) (residue 120 and name hb) 1.8 0.0 3.2 ! 120hb sees both 125hgs assign (residue 125 and name hg1) (residue 120 and (name hg1# or name hg2#)) 1.8 0.0 3.2 assign (residue 125 and name hg2) (residue 120 and (name hg1# or name hg2#)) 1.8 0.0 3.2 ! assign (residue 125 and name hn) (residue 172 and name ha) 1.8 0.0 1.7 ! 172ha sees it med assign (residue 125 and name hn) (residue 172 and name hg#) 1.8 0.0 3.2 ! 5e6, 125hn sees both, both 172hgs see 125hn assign (residue 125 and name ha) (residue 172 and (name hg1# or name hg2#)) 1.8 0.0 3.2 assign (residue 125 and name hb#) (residue 172 and (name hg1# or name hg2#)) 1.8 0.0 3.2 assign (residue 125 and name hn) (residue 173 and name hn) 1.8 0.0 3.2 ! !M126 !INTRA assign (residue 126 and name hn) (residue 126 and name ha) 1.8 0.0 1.7 !8e6 assign (residue 126 and name hn) (residue 126 and name hb#) 1.8 0.0 1.1 !2.2e7 assign (residue 126 and name hn) (residue 126 and name hg#) 1.8 0.0 2.2 !1.2e7 !SEQ assign (residue 126 and name hn) (residue 125 and name hn) 1.8 0.0 3.2 ! ovlps 127hn assign (residue 126 and name hn) (residue 125 and name ha) 1.8 0.0 1.1 ! 3.4e7, v strong assign (residue 126 and name hn) (residue 125 and name ha) 1.8 0.0 3.2 ! !R assign (residue 126 and name hn) (residue 127 and name hn) 1.8 0.0 3.2 !ovlps 125hn !MED !LONG ! No long range pks to 126HE !T127 !INTRA assign (residue 127 and name hn) (residue 127 and name ha) 1.8 0.0 1.1 ! assign (residue 127 and name hn) (residue 127 and name hg2#) 1.8 0.0 1.7 ! 1.6e7 !SEQ assign (residue 127 and name hn) (residue 126 and name hn) 1.8 0.0 3.2 ! 4e6 assign (residue 127 and name hn) (residue 126 and name ha) 1.8 0.0 0.9 ! 2.2e7 assign (residue 127 and name hg2#) (residue 126 and name ha) 1.8 0.0 3.2 ! 2.2e7 !R assign (residue 127 and name hn) (residue 128 and name hn) 1.8 0.0 3.2 ! 4e6 !R assign (residue 127 and name ha) (residue 128 and name hn) 1.8 0.0 0.7 ! 4e6 !MED assign (residue 127 and name hg2#) (residue 129 and name hb#) 1.8 0.0 3.2 ! 4d !LONG assign (residue 127 and name hg2#) (residue 135 and name hd#) 1.8 0.0 3.2 ! 4d assign (residue 127 and name hn) (residue 173 and name hn) 1.8 0.0 3.2 ! assign (residue 127 and name hg2#) (residue 173 and name ha) 1.8 0.0 3.2 ! assign (residue 127 and name hn) (residue 174 and name ha) 1.8 0.0 3.2 ! assign (residue 127 and name hg2#) (residue 174 and name ha) 1.8 0.0 1.1 ! 4d, 5.34 ppm, 2d noesy also assign (residue 127 and name hg2#) (residue 176 and (name hg1# or name hg2#)) 1.8 0.0 3.2 ! 3d, 176cg' ovlps 127cg, thus peak obscured in 4d, 176hg' see it !R assign (residue 182 and name hd#) (residue 127 and name hg2#) 1.8 0.0 3.2 ! 3d aro, 127 sees 6.87 and 7.07 !R assign (residue 182 and name he#) (residue 127 and name hg2#) 1.8 0.0 3.2 ! 3d aro, 127 sees 6.87 and 7.07 {***AMB dont see it id 3d aroNOE data assign (residue 127 and name hg2#) ((residue 6 and name hz2) or (residue 21 and name hz2) or (residue 46 and name hz2) or (residue 117 and name hz2)) 1.8 0.0 3.2 ! 4d, 7.08/111, think its Trp hz2 based on C shift ****AMB} !Q128 !INTRA assign (residue 128 and name hn) (residue 128 and name ha) 1.8 0.0 1.1 ! ovlps 127ha assign (residue 128 and name hn) (residue 128 and (name hb1 or name hb2)) 1.8 0.0 1.7 ! !SEQ assign (residue 128 and name hn) (residue 127 and name hn) 1.8 0.0 3.2 ! assign (residue 128 and name hn) (residue 127 and name ha) 1.8 0.0 0.7 ! !R assign (residue 128 and name hn) (residue 129 and name hn) 1.8 0.0 1.1 ! !MED !LONG assign (residue 128 and name ha) (residue 177 and (name hg1# or name hg2#)) 1.8 0.0 3.2 ! assign (residue 128 and name hg#) (residue 177 and (name hg1# or name hg2#)) 1.8 0.0 3.2 ! !A129 !INTRA assign (residue 129 and name hn) (residue 129 and name ha) 1.8 0.0 1.7 ! assign (residue 129 and name hn) (residue 129 and name hb#) 1.8 0.0 1.7 ! !SEQ assign (residue 129 and name hn) (residue 128 and name hn) 1.8 0.0 1.1 ! 1e7 assign (residue 129 and name hn) (residue 128 and name ha) 1.8 0.0 0.9 ! 1.4e7 assign (residue 129 and name hn) ( (residue 128 and (name hb1 or name hb2)) or (residue 134 and name hg#) ) 1.8 0.0 3.2 ! !R assign (residue 129 and name hn) (residue 130 and name h) 1.8 0.0 1.1 ! ovlps 129hn !MED !R assign (residue 129 and name hb#) (residue 127 and name hg2#) 1.8 0.0 3.2 ! 4d assign (residue 129 and name hn) (residue 127 and name hg2#) 1.8 0.0 3.2 ! assign (residue 129 and name ha) (residue 131 and name hn) 1.8 0.0 3.2 ! assign (residue 129 and name hb#) (residue 131 and name hn) 1.8 0.0 3.2 ! !LONG !R assign (residue 129 and name hb#) (residue 134 and name hn) 1.8 0.0 3.2 ! 3d assign (residue 129 and name hb#) (residue 134 and name hb#) 1.8 0.0 3.2 ! 4d assign (residue 129 and name hb#) (residue 134 and name hg#) 1.8 0.0 3.2 ! 4d assign (residue 129 and name hb#) (residue 135 and name hg11) 1.8 0.0 3.2 assign (residue 129 and name hb#) (residue 135 and name hg12) 1.8 0.0 3.2 ! 4d assign (residue 129 and name hb#) ((residue 135 and name hg2#) or (residue 137 and name hg2#)) 1.8 0.0 3.2 ! 4d assign (residue 129 and name hb#) (residue 135 and name hd#) 1.8 0.0 1.5 ! 4d assign (residue 129 and name hn) (residue 135 and name hd#) 1.8 0.0 3.2 ! 4d assign (residue 129 and name hb#) ((residue 176 and name hg1#) or (residue 176 and name hg2#)) 1.8 0.0 3.2 ! 4d to 176 hg' assign (residue 129 and name hn) ((residue 177 and name hg1#) or (residue 177 and name hg2#)) 1.8 0.0 3.2 ! 177 hg'' sees wk 8.908ppm !AMB !*********** stop here 2-1-02 ******************* !T130 !INTRA assign (residue 130 and name hn) (residue 130 and name ha) 1.8 0.0 1.7 ! assign (residue 130 and name hn) (residue 130 and name hg2#) 1.8 0.0 3.2 ! 1.4e7, vios for med after conf. database, SD via hb? !SEQ !A assign (residue 130 and name hn) (residue 129 and name hn) 1.8 0.0 ! 129hn ovlps 130hn assign (residue 130 and name hn) ((residue 129 and name ha) or (residue 130 and name hb)) 1.8 0.0 1.1 !AMB 129ha ovlps 130ha, but 129ha sees strong to 8.81ppm, not 8.88 ppm assign (residue 130 and name hn) (residue 129 and name hb#) 1.8 0.0 1.7 ! 1.2e7 assign (residue 130 and name hg2#) (residue 129 and name hb#) 1.8 0.0 4.2 !vios 3apr02, w to vw !R assign (residue 130 and name hn) (residue 131 and name hn) 1.8 0.0 1.1 ! !R assign (residue 130 and name hn) (residue 131 and name hb) 1.8 0.0 3.2 ! !R assign (residue 130 and name ha) (residue 131 and name hn) 1.8 0.0 1.1 ! !MED assign (residue 130 and name hn) (residue 134 and name hn) 1.8 0.0 3.2 ! v wk, 134hn sees it also assign (residue 130 and name hn) (residue 134 and name hb#) 1.8 0.0 3.2 ! 2.19ppm, 4e6 !A assign (residue 130 and name hn) (residue 134 and name hg#) 1.8 0.0 3.2 ! it doesnt see 8.94ppm !LONG !R assign (residue 176 and name hg#) (residue 130 and name ha) 1.8 0.0 3.2 ! 4d to hg' assign (residue 130 and name ha) (residue 177 and name hb) 1.8 0.0 3.2 ! assign (residue 130 and name hn) (residue 177 and name hg#) 1.8 0.0 3.2 ! 0.633 ppm !R assign (residue 177 and name hg#) (residue 130 and name ha) 1.8 0.0 1.5 !4d to hg'' !R assign (residue 177 and name hg#) (residue 130 and name hb) 1.8 0.0 3.2 !4d to hg'' !R assign (residue 130 and name hg2#) (residue 177 and name hg#) 1.8 0.0 1.5 !4d, 0.62/20.8 177hg'' and 0.58/20.4(ovlped) assign (residue 130 and name hg2#) (residue 177 and name hb) 1.8 0.0 3.2 !4d !T131 !INTRA assign (residue 131 and name hn) (residue 131 and name ha) 1.8 0.0 1.7 ! 1.3e7, ovlps water assign (residue 131 and name hn) ((residue 131 and name hb) or (residue 130 and name ha)) 1.8 0.0 1.7 !1.6e7 !SEQ assign (residue 131 and name hn) (residue 130 and name hn) 1.8 0.0 1.1 !2.2e7 !A assign (residue 131 and name hn) (residue 130 and name ha) 1.8 0.0 !ovlps 131hb assign (residue 131 and name hn) (residue 130 and name hb) 1.8 0.0 1.1 !129ha also close, both see 131hn !R assign (residue 131 and name hn) (residue 132 and name hn) 1.8 0.0 3.2 ! 4.6e6 !MED assign (residue 131 and name hn) (residue 129 and name hb#) 1.8 0.0 1.7 ! 1.6e7 assign (residue 131 and name hn) (residue 133 and name hn) 1.8 0.0 3.2 ! assign (residue 131 and name hn) (residue 134 and name hn) 1.8 0.0 3.2 ! assign (residue 131 and name hn) ((residue 134 and name hb#) or (residue 135 and name hb) or (residue 176 and name hb)) 1.8 0.0 1.7 ! assign (residue 131 and name hn) (residue 134 and name hg#) 1.8 0.0 1.7 ! assign (residue 131 and name hg2#) (residue 134 and name hg#) 1.8 0.0 3.2 ! 4d assign (residue 131 and name hg2#) (residue 133 and name hn) 1.8 0.0 3.2 ! 1.6e7 !LONG assign (residue 131 and name hn) (residue 176 and (name hg1# or name hg2#)) 1.8 0.0 3.2 ! sees both 176hgs !SD? assign (residue 131 and name hn) (residue 177 and name hg#) 1.8 0.0 3.2 ! 0.586 ppm !L132 !INTRA assign (residue 132 and name hn) (residue 132 and name ha) 1.8 0.0 1.7 ! assign (residue 132 and name hn) (residue 132 and name hg) 1.8 0.0 1.1 !2.1e7 !SEQ assign (residue 132 and name hn) (residue 131 and name hn) 1.8 0.0 3.2 ! assign (residue 132 and name hn) (residue 131 and name ha) 1.8 0.0 1.1 !2.8e7 assign (residue 132 and name hn) (residue 131 and name hb) 1.8 0.0 1.7 !2e7, 132hn to 131hb med assign (residue 132 and name hn) (residue 131 and name hg2#) 1.8 0.0 3.2 ! !R assign (residue 132 and name hn) (residue 133 and name hn) 1.8 0.0 2.2 ! !MED !LONG assign (residue 132 and name hd#) (residue 4 and name ha) 1.8 0.0 3.2 ! to 132hg' and 132hg'' assign (residue 132 and name hd#) (residue 4 and name hb#) 1.8 0.0 3.2 ! to 132hg' assign (residue 132 and name hd#) (residue 5 and name ha#) 1.8 0.0 3.2 ! to 132hg' and hg'' 4d !R assign (residue 132 and (name hd1# or name hd2#)) (residue 5 and name hn) 1.8 0.0 3.2 ! to 132hg' assign (residue 132 and name hd#) (residue 6 and name ha) 1.8 0.0 3.2 ! to 132hg' and hg'' !R assign (residue 132 and (name hd1# or name hd2#)) (residue 6 and name hn) 1.8 0.0 3.2 ! to 132hg' assign (residue 132 and (name hd1# or name hd2#)) (residue 6 and (name hb1 or name hb2)) 1.8 0.0 3.2 ! to 132hg' !R assign (residue 132 and (name hd1# or name hd2#)) (residue 6 and name he1) 1.8 0.0 3.2 ! to 132hg' !R assign (residue 132 and (name hd1# or name hd2#)) (residue 7 and name hn) 1.8 0.0 3.2 ! to 132hg' assign (residue 132 and name hn) (residue 176 and (name hg1# or name hg2#)) 1.8 0.0 3.2 ! 176hg' sees it assign (residue 132 and name ha) (residue 176 and (name hg1# or name hg2#)) 1.8 0.0 3.2 ! 176hg' sees it assign (residue 132 and (name hd1# or name hd2#)) (residue 176 and (name hg1# or name hg2#)) 1.8 0.0 3.2 ! 4d, to 132hd' !S133 !INTRA assign (residue 133 and name hn) (residue 133 and name ha) 1.8 0.0 1.1 ! assign (residue 133 and name hn) (residue 133 and name hb#) 1.8 0.0 1.1 ! !SEQ assign (residue 133 and name hn) (residue 132 and name hn) 1.8 0.0 1.7 ! !A assign (residue 133 and name hn) (residue 132 and name ha) 1.8 0.0 !ovlps 133ha assign (residue 133 and name hn) (residue 132 and name hb#) 1.8 0.0 1.7 ! !R assign (residue 133 and name hn) (residue 134 and name hn) 1.8 0.0 1.1 ! assign (residue 133 and name hn) (residue 134 and name hb#) 1.8 0.0 3.2 ! assign (residue 133 and name hn) (residue 134 and name hb#) 1.8 0.0 3.2 ! !MED !A assign (residue 133 and name hn) ((residue 131 and name hb) or !A (residue 130 and name ha)) 1.8 0.0 1.1 ! 1.9e7, neither one see pk at 8.29 ?? assign (residue 133 and name hn) (residue 131 and name hg2#) 1.8 0.0 1.1 ! 1.8e7 !R assign (residue 133 and name hn) (residue 135 and name hn) 1.8 0.0 3.2 ! !LONG !E134 !INTRA !R assign (residue 134 and name hn) ((residue 133 and name ha) or !R (residue 134 and name ha)) 1.8 0.0 0.9 ! 134ha ovlps 134ha assign (residue 134 and name hn) (residue 134 and name hg#) 1.8 0.0 1.1 ! !SEQ assign (residue 134 and name hn) (residue 133 and name hn) 1.8 0.0 1.1 ! assign (residue 134 and name hn) ((residue 133 and name ha) or (residue 134 and name ha)) 1.8 0.0 0.9 ! 134ha ovlps 134ha !R assign (residue 134 and name hn) (residue 135 and name hn) 1.8 0.0 1.1 ! !MED !R assign (residue 130 and name hn) (residue 134 and name hn) 1.8 0.0 3.2 ! v wk, 134hn sees it also !R assign (residue 131 and name hn) (residue 134 and name hn) 1.8 0.0 3.2 ! assign (residue 134 and name hn) ((residue 130 and name hg2#) or (residue 131 and name hg2#)) 1.8 0.0 3.2 ! 131hg sees 7.44, 130hg sees 7.48 (134hn 7.45) !LONG assign (residue 134 and name hn) (residue 129 and name hb#) 1.8 0.0 3.2 ! 3d !I135 !INTRA assign (residue 135 and name hn) (residue 134 and name ha) 1.8 0.0 1.7 ! !A assign (residue 135 and name hn) (residue 135 and name hb) 1.8 0.0 2.2 !ovlps 134hb# assign (residue 135 and name hn) (residue 135 and name hg2#) 1.8 0.0 1.7 !1.9e7, wk to hg2 assign (residue 135 and name hn) (residue 135 and name hd#) 1.8 0.0 1.7 !1.2e7 !SEQ assign (residue 135 and name hn) (residue 134 and name hn) 1.8 0.0 1.1 ! assign (residue 135 and name hn) (residue 134 and name ha) 1.8 0.0 1.7 ! assign (residue 135 and name ha) (residue 136 and (name hd1 or name hd2)) 1.8 0.0 1.5 ! assign (residue 135 and name hg2#) (residue 136 and (name hd1 or name hd2)) 1.8 0.0 1.5 ! !MED assign (residue 135 and name hn) (residue 131 and name hn) 1.8 0.0 3.2 ! assign (residue 135 and name hn) ( (residue 136 and (name hd1 or name hd2)) or (residue 133 and name hb#) ) 1.8 0.0 3.2 ! !SD? assign (residue 135 and name hg2#) (residue 132 and name ha) 1.8 0.0 3.2 ! 3d, v. wk assign (residue 135 and name hd#) (residue 132 and name ha) 1.8 0.0 3.2 ! 4d !A assign (residue 135 and name hg2#) (residue 132 and (name hb1 or name hb2)) 1.8 0.0 3.2 ! 3d, v. wk assign (residue 135 and name hd#) (residue 132 and (name hd1# or name hd2#)) 1.8 0.0 3.2 ! 4d !LONG !R assign (residue 127 and name hg2#) (residue 135 and name hd#) 1.8 0.0 3.2 ! 4d assign (residue 135 and name hn) (residue 129 and name hb#) 1.8 0.0 3.2 ! 3d, 129hb sees v wk 135hn assign (residue 135 and name hg2#) (residue 129 and name hb#) 1.8 0.0 3.2 ! 4d !R assign (residue 129 and name hb#) (residue 135 and name hd#) 1.8 0.0 1.5 ! 4d !R assign (residue 135 and name hd#) (residue 127 and name hg2#) 1.8 0.0 3.2 ! 4d !R assign (residue 135 and name hd#) (residue 129 and name hb#) 1.8 0.0 1.5 ! 4d assign (residue 135 and name hg2#) (residue 163 and name hd#) 1.8 0.0 3.2 ! 3d, wk assign (residue 135 and name hg2#) (residue 163 and name he#) 1.8 0.0 1.5 ! 3d, 6e5, assignment amb for 163he, very close in structure !A assign (residue 135 and name hd#) (residue 167 and name ha) 1.8 0.0 3.2 ! 4d !R assign (residue 135 and name hg2#) (residue 174 and name ha) 1.8 0.0 3.2 ! !R assign (residue 135 and name hd#) (residue 174 and name ha) 1.8 0.0 3.2 ! assign (residue 135 and name hd#) (residue 174 and name hb#) 1.8 0.0 3.2 ! 3d assign (residue 135 and name hd#) (residue 176 and (name hg1# or name hg2#)) 1.8 0.0 2.2 ! 4d !P136 !INTRA !SEQ !R assign (residue 136 and name ha) (residue 137 and name hn) 1.8 0.0 1.7? ! !MED assign (residue 136 and (name hb1 or name hb2)) (residue 138 and name hn) 1.8 0.0 3.2 ! assign (residue 136 and (name hb1 or name hb2)) (residue 139 and name hg2#) 1.8 0.0 3.2 ! assign (residue 136 and (name hg1 or name hg2)) (residue 139 and name hg2#) 1.8 0.0 1.5 ! med, as strong as 136hbs to 136 hgs !LONG !T137 !INTRA assign (residue 137 and name hn) (residue 137 and name ha) 1.8 0.0 1.1 !1.7e7 assign (residue 137 and name hn) (residue 137 and name hg2#) 1.8 0.0 1.7 !2e7 !SEQ assign (residue 137 and name hn) (residue 136 and name ha) 1.8 0.0 1.1 !very strong 3.7e7, 137hn to 136ha strong assign (residue 137 and name hn) (residue 136 and name hb#) 1.8 0.0 1.7 ! 1.6e7 and 1.1 e7 assign (residue 137 and name hn) (residue 136 and (name hd1 or name hd2)) 1.8 0.0 3.2 ! !R assign (residue 137 and name hn) (residue 138 and name hn) 1.8 0.0 1.1 ! 2.2e7 !MED assign (residue 137 and name hn) (residue 139 and name hg2#) 1.8 0.0 3.2 ! !LONG assign (residue 137 and name ha) (residue 163 and name hd#) 1.8 0.0 3.2 ! !***** stop here 5feb02 !S138 !INTRA assign (residue 138 and name hn) (residue 138 and name ha) 1.8 0.0 1.7 ! 8e6 assign (residue 138 and name hn) (residue 138 and name hb#) 1.8 0.0 3.2 ! 8e6 !SEQ assign (residue 138 and name hn) (residue 137 and name hn) 1.8 0.0 1.1 ! 2.7e7 v. strong assign (residue 138 and name hn) (residue 137 and (name ha or name hb)) 1.8 0.0 1.7 ! 1.5e7, vios, s-m, 137 ha ovlps hb assign (residue 138 and name hn) (residue 137 and name hg2#) 1.8 0.0 2.2 ! 1.2e7 assign (residue 138 and name ha) (residue 137 and name hg2#) 1.8 0.0 3.2 ! wk !R assign (residue 138 and name hn) (residue 139 and name hn) 1.8 0.0 3.2 ! assign (residue 138 and name hn) (residue 137 and name hg2#) 1.8 0.0 3.2 ! 5e6 !MED assign (residue 138 and name hn) (residue 136 and name ha) 1.8 0.0 1.7 ! 2.2e7, AMB: 138hn to 136ha wk but so is 136hb' to 136ha (all wk to 136ha) assign (residue 138 and name hn) (residue 136 and (name hb1 or name hb2)) 1.8 0.0 1.1 ! 2e7 and 1.2e7, med? for 138hn to 136hbs assign (residue 138 and name hn) (residue 136 and (name hg1 or name hg2)) 1.8 0.0 3.2 ! 8e6 ovlps 136hb' !LONG !T139 !INTRA assign (residue 139 and name hn) (residue 139 and name hg2#) 1.8 0.0 3.2 ! !SEQ assign (residue 139 and name hn) (residue 138 and name hn) 1.8 0.0 3.2 ! assign (residue 139 and name hn) (residue 138 and name ha) 1.8 0.0 1.1 ! assign (residue 139 and name hn) (residue 138 and name hb#) 1.8 0.0 2.2 !6.6e6 assign (residue 139 and name hg2#) (residue 138 and name ha) 1.8 0.0 3.2 ! assign (residue 139 and name hg2#) (residue 140 and name hd#) 1.8 0.0 3.2 ! !MED !R assign (residue 136 and (name hb1 or name hb2)) (residue 139 and name hg2#) 1.8 0.0 3.2 ! !R assign (residue 136 and (name hg1 or name hg2)) (residue 139 and name hg2#) 1.8 0.0 1.5 ! med, as strong as 136hbs to 136 hgs assign (residue 139 and name hn) ((residue 159 and name hg2#) or (residue 127 and name hg2#) or (residue 141 and name hb#)) 1.8 0.0 3.2 ! assign (residue 139 and name hn) (residue 141 and name hn) 1.8 0.0 3.2 ! assign (residue 139 and name hg2#) (residue 141 and name hb#) 1.8 0.0 3.2 ! 4d assign (residue 139 and name hn) (residue 142 and name hn) 1.8 0.0 3.2 ! !R assign (residue 139 and name hn) (residue 143 and name hn) 1.8 0.0 3.2 ! !LONG assign (residue 139 and name hn) (residue 137 and name ha) 1.8 0.0 3.2 !4.8e5, 137ha not see it !A assign (residue 139 and name hn) (residue 163 and name hb#) 1.8 0.0 3.2 ! 3.27ppm, wk and in only one of 15n noesy expts assign (residue 139 and name hn) (residue 163 and name hd#) 1.8 0.0 3.2 ! 6.716ppm !R assign (residue 139 and name hg2#) (residue 163 and name hd#) 1.8 0.0 3.2 ! 6.716ppm !SD assign (residue 139 and name hn) (residue 163 and name he#) 1.8 0.0 3.2 ! !SD assign (residue 139 and name hg2#) (residue 163 and name he#) 1.8 0.0 3.2 ! !P140 !INTRA !SEQ !MED assign (residue 140 and name ha) (residue 143 and (name hb1 or name hb2)) 1.8 0.0 1.5 ! !LONG !A141 !INTRA assign (residue 141 and name hn) (residue 141 and name ha) 1.8 0.0 1.1 ! assign (residue 141 and name hn) (residue 141 and name hb#) 1.8 0.0 0.7 ! 3.5e7 !SEQ assign (residue 141 and name hn) (residue 140 and name ha) 1.8 0.0 1.7 ! assign (residue 141 and name hn) (residue 140 and name hb#) 1.8 0.0 1.7 ! !AR assign (residue 141 and name hn) (residue 142 and name hn) 1.8 0.0 ! ovlps 141hn !MED !R assign (residue 139 and name hn) (residue 141 and name hn) 1.8 0.0 3.2 ! assign (residue 141 and name hn) (residue 139 and name hb) 1.8 0.0 2.2 ! 8e6 assign (residue 141 and name hn) (residue 139 and name hg2#) 1.8 0.0 3.2 ! 8e6 assign (residue 141 and name hb#) (residue 139 and name hb) 1.8 0.0 3.2 ! 4d !R assign (residue 141 and name hb#) (residue 139 and name hg2#) 1.8 0.0 3.2 ! 4d !R assign (residue 141 and name hb#) (residue 144 and name hb#) 1.8 0.0 3.2 ! 4d assign (residue 141 and name hn) (residue 143 and name hn) 1.8 0.0 3.2 ! !LONG assign (residue 141 and name hb#) (residue 119 and name hb1) 1.8 0.0 3.2 assign (residue 141 and name hb#) (residue 119 and name hb2) 1.8 0.0 3.2 ! !R assign (residue 141 and name hb#) (residue 119 and name hd#) 1.8 0.0 3.2 assign (residue 141 and name hn) (residue 120 and name hg#) 1.8 0 3.2 ! assign (residue 141 and name hb#) (residue 120 and (name hg1# or name hg2#)) 1.8 0 3.2 ! 4d assign (residue 141 and name hn) (residue 166 and name he#) 1.8 0.0 3.2 ! assign (residue 141 and name hb#) (residue 166 and name he#) 1.8 0.0 1.5 ! 4d at 1.62/16.6 !! ****** stop here 6feb02 !S142 !dont see 142ha or hb in 3d noesy !INTRA !SEQ assign (residue 142 and name hn) (residue 141 and name hn) 1.8 0.0 1.1 ! assign (residue 142 and name hn) (residue 141 and name ha) 1.8 0.0 1.7 ! assign (residue 142 and name hn) (residue 141 and name hb#) 1.8 0.0 1.1 ! !R assign (residue 142 and name hn) (residue 143 and name hn) 1.8 0.0 1.1 ! !MED assign (residue 142 and name hn) (residue 139 and name hn) 1.8 0.0 3.2 ! assign (residue 142 and name hn) (residue 139 and name hb) 1.8 0.0 3.2 ! assign (residue 142 and name hn) (residue 139 and name hg2#) 1.8 0.0 3.2 ! 139hg sees it assign (residue 142 and name hn) (residue 140 and (name hd1 or name hd2)) 1.8 0.0 3.2 ! !LONG assign (residue 142 and name hn) (residue 166 and name he#) 1.8 0.0 3.2 ! 166he sees it !D143 !INTRA assign (residue 143 and name hn) (residue 143 and name ha) 1.8 0.0 0.9 ! !SEQ assign (residue 143 and name hn) (residue 142 and name hn) 1.8 0.0 1.1 ! assign (residue 143 and name hn) (residue 142 and name ha) 1.8 0.0 1.7 ! assign (residue 143 and name hn) (residue 142 and name hb#) 1.8 0.0 1.7 ! !R assign (residue 143 and name hn) (residue 144 and name hn) 1.8 0.0 1.1 ! !MED assign (residue 143 and name hn) ((residue 140 and name ha) or (residue 142 and name hb#)) 1.8 0.0 1.7 ! assign (residue 143 and (name hb1 or name hb2)) (residue 140 and name ha) 1.8 0.0 1.5 ! assign (residue 139 and name hn) (residue 143 and name hn) 1.8 0.0 3.2 ! !R assign (residue 143 and name hn) (residue 145 and name hn) 1.8 0.0 3.2 ! !LONG !AMB assign (residue 143 and name hn) ((residue 141 and name hb#) or (residue 159 and name hg2#)) 1.8 0.0 3.2 ! 1.34ppm !A144 !INTRA assign (residue 144 and name hn) (residue 144 and name hb#) 1.8 0.0 1.1 ! !SEQ assign (residue 144 and name hn) (residue 143 and name hn) 1.8 0.0 1.1 ! assign (residue 144 and name hn) (residue 143 and (name hb1 or name hb2)) 1.8 0.0 1.7 ! !R assign (residue 144 and name hn) (residue 145 and name hn) 1.8 0.0 1.1 ! !MED assign (residue 144 and name hn) (residue 140 and name ha) 1.8 0.0 3.2 ! assign (residue 144 and name hn) (residue 141 and name ha) 1.8 0.0 1.7 ! assign (residue 144 and name hb#) (residue 141 and name ha) 1.8 0.0 1.5 ! 4d assign (residue 144 and name hb#) (residue 141 and name hb#) 1.8 0.0 3.2 ! 4d assign (residue 144 and name hn) (residue 142 and name ha) 1.8 0.0 4.2 ! ! 142hn ovlps 144hn ! 146hn ovlps 145hn !R assign (residue 144 and name ha) (residue 147 and name hb#) 1.8 0.0 1.5 ! assign (residue 144 and name ha) ( (residue 147 and name he#) or (residue 143 and (name hb1 or name hb2)) ) 1.8 0.0 3.2 ! !LONG assign (residue 144 and name hb#) (residue 119 and (name hb1 or name hb2)) 1.8 0.0 3.2 ! amb 3d assign (residue 144 and name hb#) (residue 119 and name hd#) 1.8 0.0 1.5 ! 7.34ppm assign (residue 144 and name hb#) (residue 119 and name he#) 1.8 0.0 1.5 ! 6.28ppm !AMB !#### stop 7feb02 !L145 !INTRA assign (residue 145 and name hn) (residue 145 and name ha) 1.8 0.0 1.1 ! assign (residue 145 and name hn) (residue 145 and name hb#) 1.8 0.0 1.7 ! assign (residue 145 and name hn) (residue 145 and (name hd1# or name hd2#)) 1.8 0.0 1.7 ! !SEQ assign (residue 145 and name hn) (residue 144 and name hn) 1.8 0.0 1.1 ! assign (residue 145 and name hn) (residue 144 and name ha) 1.8 0.0 1.7 ! assign (residue 145 and name hn) (residue 144 and name hb#) 1.8 0.0 1.1 ! 1.7e7 !MED assign (residue 145 and name hn) (residue 141 and name ha) 1.8 0.0 3.2 ! assign (residue 145 and name hn) (residue 142 and name ha) 1.8 0.0 1.7 ! assign (residue 145 and name hn) (residue 143 and name hn) 1.8 0.0 3.2 ! !R assign (residue 145 and (name hd1# or name hd2#)) (residue 148 and name hb#) 1.8 0.0 3.2 ! 4d to 145hd' !R assign (residue 148 and name hb#) (residue 145 and name ha) 1.8 0.0 1.5 ! 4d, wk assign (residue 145 and (name hd1# or name hd2#)) (residue 149 and name ha) 1.8 0.0 3.2 ! 4d to 145hd' !R assign ((residue 145 and name hd1#) or (residue 145 and name hd2#)) !R ((residue 149 and name hd1#) or (residue 149 and name hd2#)) 1.8 0.0 3.2 ! 4d, to 145hd', sees both 149hds !LONG !R assign (residue 145 and name hd#) (residue 115 and name hd#) 1.8 0.0 3.2 ! 0.26 in 2dnoesy, 145hd' sees wk 7.34 assign (residue 145 and name hd#) ((residue 115 and name he#) or (residue 115 and name hz) or (residue 165 and name he#)) 1.8 0.0 1.5 ! 7.05ppm to 145hd' 3d assign (residue 145 and name hd#) (residue 116 and name ha) 1.8 0.0 3.2 !4d to 145hd' assign (residue 145 and name hd#) (residue 116 and name hg#) 1.8 0.0 3.2 !4d, 116hg' and 116hg'' to 145hd' assign (residue 145 and name hn) (residue 119 and name hd#) 1.8 0.0 3.2 ! assign (residue 145 and name hd#) (residue 119 and name hd#) 1.8 0.0 3.2 ! 0.26 in 2dnoesy and 13caro, 145hd' sees wk 7.34 !R assign (residue 145 and name hd#) (residue 119 and name he#) 1.8 0.0 3.2 ! 0.26 in 2dnoesy and 13caro, 145hd' sees wk 6.30 assign (residue 145 and name hd#) (residue 161 and name hg2#) 1.8 0.0 3.2 ! 3d to 145hd'' assign (residue 145 and name hd#) (residue 162 and name ha) 1.8 0.0 3.2 ! 3d to 145hd'' assign (residue 145 and name hd#) (residue 162 and name hb#) 1.8 0.0 1.5 ! 3d to 145hd'' assign (residue 145 and name hd#) (residue 165 and name hd#) 1.8 0.0 3.2 ! 3d to 145hd'' assign (residue 145 and (name hd1# or name hd2#)) (residue 166 and name he#) 1.8 0.0 1.5 !4d to 145hg'', 5e5 !S146 ! dont see ha or hbs in 3d noesy !INTRA assign (residue 146 and name hn) (residue 146 and name ha) 1.8 0.0 1.1 ! !SEQ assign (residue 146 and name hn) (residue 145 and name hn) 1.8 0.0 1.1 ! amb - ovlps 146hn assign (residue 146 and name hn) (residue 145 and name hb#) 1.8 0.0 3.2 ! assign (residue 146 and name hn) (residue 145 and (name hd1# or name hd2#)) 1.8 0.0 1.7 ! 145hd'' stronger assign (residue 146 and name hn) (residue 145 and name hg) 1.8 0.0 3.2 ! !R assign (residue 146 and name hn) (residue 147 and name hn) 1.8 0.0 1.1 ! !MED ! 143 ha ovlps 146hbs !A assign (residue 146 and name hn) (residue 144 and name hn) 1.8 0.0 3.2 ! ovlps 147hn !R assign (residue 148 and name hn) (residue 146 and name hn) 1.8 0.0 3.2 ! !LONG !A assign (residue 146 and name hn) (residue 162 and name ha) 1.8 0.0 3.2 ! shoulder of 146ha !A assign (residue 146 and name hn) (residue 159 and name hn) 1.8 0.0 3.2 ! 146hn to 159hn amb, but only assignment makes sense !K147 !INTRA assign (residue 147 and name hn) (residue 147 and name ha) 1.8 0.0 1.1 ! 1.3e7 assign (residue 147 and name hn) (residue 147 and name hb#) 1.8 0.0 1.1 ! assign (residue 147 and name ha) (residue 147 and name hd#) 1.8 0.0 3.2 ! !SEQ assign (residue 147 and name hn) (residue 146 and name hn) 1.8 0.0 1.1 ! assign (residue 147 and name hn) (residue 146 and name ha) 1.8 0.0 1.7 ! 1.2e7 assign (residue 147 and name hn) (residue 146 and name hb#) 1.8 0.0 1.7 ! 1.2e7 !A assign (residue 147 and name hn) (residue 148 and name hn) 1.8 0.0 ! ovlps 147hn !MED assign (residue 147 and name hb#) (residue 144 and name ha) 1.8 0.0 1.5 ! ! 145hn ovlps 146hn assign (residue 147 and name hn) (residue 149 and name hn) 1.8 0.0 3.2 ! !R assign (residue 150 and name hb#) (residue 147 and name ha) 1.8 0.0 1.5 ! !LONG !A148 !INTRA assign (residue 148 and name hn) (residue 148 and name ha) 1.8 0.0 1.1 ! strong 1.5e7 assign (residue 148 and name hn) (residue 148 and name ha) 1.8 0.0 1.1 ! strong 3e7 !SEQ assign (residue 148 and name hn) (residue 147 and name ha) 1.8 0.0 1.7 ! assign (residue 148 and name hn) (residue 147 and (name hg1 or name hg2)) 1.8 0.0 3.2 ! !R assign (residue 148 and name hn) (residue 149 and name hn) 1.8 0.0 1.1 ! assign (residue 148 and name hb#) (residue 149 and name hd#) 1.8 0.0 3.2 ! 4d !MED assign (residue 148 and name hn) (residue 144 and name ha) 1.8 0.0 3.2 ! assign (residue 148 and name hb#) (residue 144 and name ha) 1.8 0.0 3.2 ! assign (residue 148 and name hn) (residue 145 and name ha) 1.8 0.0 1.7 ! assign (residue 148 and name hb#) (residue 145 and name ha) 1.8 0.0 1.5 ! 4d assign (residue 148 and name hn) (residue 145 and (name hd1# or name hd2#)) 1.8 0.0 3.2 ! 145hd#' assign (residue 148 and name hb#) (residue 145 and (name hd1# or name hd2#)) 1.8 0.0 3.2 !4d, 0.245 ppm assign (residue 148 and name hn) (residue 146 and name hn) 1.8 0.0 3.2 ! assign (residue 148 and name hn) (residue 146 and name ha) 1.8 0.0 3.2 ! !R assign (residue 148 and name hn) (residue 150 and name hn) 1.8 0.0 3.2 ! assign (residue 148 and name ha) (residue 151 and name hb#) 1.8 0.0 1.5 ! !LONG !A assign (residue 148 and name hb#) (residue 112 and name he#) 1.8 0.0 3.2 ! !R assign (residue 148 and name hb#) (residue 115 and name hd#) 1.8 0.0 3.2 ! !AMB assign (residue 148 and name hb#) (residue 115 and name he#) 1.8 0.0 3.2 ! not sure if its 115he or 165he assign (residue 148 and name hb#) (residue 115 and name hz) 1.8 0.0 1.5 ! 13c aro noesy !R assign (residue 148 and name hb#) (residue 119 and name hd#) 1.8 0.0 3.2 ! 2d noesy, 148hb sees it as v wk !R assign (residue 148 and name hb#) (residue 119 and name he#) 1.8 0.0 1.5 ! 2d noesy, 148hb sees it assign (residue 148 and name hn) (residue 119 and name he#) 1.8 0.0 3.2 assign (residue 148 and name hb#) (residue 119 and name hz) 1.8 0.0 1.5 ! 8e5, !A assign (residue 148 and name hb#) (residue 154 and name hd#) 1.8 0.0 3.2 ! 7.19ppm 3d noesy to 148hb !L149 !INTRA assign (residue 149 and name hn) (residue 149 and name ha) 1.8 0.0 1.7 ! assign (residue 149 and name hn) (residue 149 and name hb#) 1.8 0.0 1.7 ! assign (residue 149 and name hn) (residue 149 and name hg) 1.8 0.0 1.7 ! assign (residue 149 and name hn) (residue 149 and (name hd1# or name hd2#)) 1.8 0.0 1.7 ! !SEQ assign (residue 149 and name hn) (residue 148 and name hn) 1.8 0.0 1.1 ! assign (residue 149 and name hn) (residue 148 and name ha) 1.8 0.0 1.7 ! assign (residue 149 and name hn) (residue 148 and name hb#) 1.8 0.0 1.1 ! !R assign (residue 149 and name hn) (residue 150 and name hn) 1.8 0.0 1.1 ! !MED assign (residue 149 and name hn) (residue 145 and name ha) 1.8 0.0 3.2 ! assign (residue 149 and name hn) (residue 145 and (name hd1# or name hd2#)) 1.8 0.0 3.2 ! assign (residue 145 and name hd#) (residue 149 and name hd#) 1.8 0.0 1.5 ! 4d, to 145hd', sees both 149hds assign (residue 149 and name hn) (residue 146 and name ha) 1.8 0.0 3.2 ! ! 147hn ovlps 148hn assign (residue 149 and name hn) (residue 146 and name ha) 1.8 0.0 1.7 ! !A assign (residue 149 and name hn) (residue 147 and name hn) 1.8 0.0 3.2 ! ovlps 148hn ! 151hn ovlps 148hn !LONG assign (residue 149 and (name hd1# or name hd2#)) (residue 35 and name hg2#) 1.8 0.0 3.2 ! 4d !A assign (residue 149 and name hn) (residue 154 and name hd#) 1.8 0.0 3.2 ! 7.195ppm assign (residue 149 and name hd#) (residue 154 and name hb#) 1.8 0.0 3.2 ! 4d assign (residue 149 and name hn) (residue 157 and name hg#) 1.8 0.0 3.2 ! sees both 157hgs, 157hg'' sees it assign (residue 149 and name hd#) (residue 157 and name hg#) 1.8 0.0 3.2 ! 4d assign (residue 149 and name hn) ((residue 112 and name he#) or (residue 165 and name he#) or (residue 115 and name he#) or (residue 115 and name hz) or (residue 32 and name hd#)) 1.8 0.0 3.2 ! 7.06ppm assign (residue 149 and name hd#) ((residue 112 and name he#) or (residue 165 and name he#) or (residue 115 and name he#) or (residue 115 and name hz) or (residue 32 and name hd#)) 1.8 0.0 3.2 ! 7.07ppm !A assign (residue 149 and name hn) (residue 161 and name hg2#) 1.8 0.0 3.2 ! 0.88ppm !K150 !INTRA assign (residue 150 and name hn) (residue 150 and name ha) 1.8 0.0 1.1 ! assign (residue 150 and name hn) (residue 150 and name hb#) 1.8 0.0 1.1 ! assign (residue 150 and name hn) (residue 150 and name hg#) 1.8 0.0 2.2 ! !SEQ assign (residue 150 and name hn) (residue 149 and name hn) 1.8 0.0 1.1 ! ovlps 150hn assign (residue 150 and name hn) (residue 145 and name hd#) 1.8 0.0 3.2 ! !R assign (residue 150 and name hn) (residue 151 and name hn) 1.8 0.0 1.1 ! !MED assign (residue 150 and name hn) (residue 146 and name ha) 1.8 0.0 3.2 ! assign (residue 150 and name hn) (residue 147 and name ha) 1.8 0.0 1.7 ! assign (residue 150 and name hb#) (residue 147 and name ha) 1.8 0.0 1.5 ! !A assign (residue 150 and name hn) (residue 148 and name h) 1.8 0.0 !ovlps 151hn !R assign (residue 150 and name hn) (residue 152 and name hn) 1.8 0.0 3.2 ! assign (residue 150 and name ha) (residue 153 and name hn) 1.8 0.0 1.7 ! 154hn sees it assign (residue 150 and name ha) (residue 154 and name hn) 1.8 0.0 1.7 ! 154hn sees it !LONG !R assign (residue 150 and name ha) ((residue 157 and (name hg1# or name hg2#)) 1.8 0.0 3.2 ! 4d to 157hg' !R assign (residue 150 and name hn) ((residue 157 and (name hg1# or name hg2#)) 1.8 0.0 3.2 ! assign (residue 150 and name hb#) (residue 157 and (name hg1# or name hg2#)) 1.8 0.0 3.2 ! 4d to 157hg' assign (residue 150 and name hg1) (residue 157 and (name hg1# or name hg2#)) 1.8 0.0 3.2 assign (residue 150 and name hg2) (residue 157 and (name hg1# or name hg2#)) 1.8 0.0 3.2 ! 4d to 157hg' !A assign (residue 150 and name hn) (residue 161 and (name hg2# or name hd#)) 1.8 0.0 4.2 ! 0.89ppm, very wk to 161hg2 !K151 !INTRA assign (residue 151 and name hn) (residue 151 and name ha) 1.8 0.0 1.1 ! assign (residue 151 and name hn) (residue 151 and name hb#) 1.8 0.0 1.1 ! !SEQ assign (residue 151 and name hn) (residue 150 and name hn) 1.8 0.0 1.1 ! assign (residue 151 and name hn) (residue 150 and name hb#) 1.8 0.0 1.7 ! 1.7e7 but ovlps 151hd# !R assign (residue 151 and name hn) (residue 152 and name hn) 1.8 0.0 1.1 ! !MED assign (residue 151 and name hn) (residue 147 and name ha) 1.8 0.0 3.2 assign (residue 151 and name hn) (residue 148 and name ha) 1.8 0.0 1.7 ! amb - ovlps 151ha !A assign (residue 151 and name hn) (residue 149 and name hn) 1.8 0.0 ! ovlps 150hn !R assign (residue 153 and name hn) (residue 151 and name hn) 1.8 0.0 2.2 ! 4.6e6 !LONG !R152 !INTRA assign (residue 152 and name hn) (residue 152 and name ha) 1.8 0.0 1. ! assign (residue 152 and name hn) (residue 152 and name he) 1.8 0.0 3.2 ! !SEQ assign (residue 152 and name hn) (residue 151 and name hn) 1.8 0.0 1.1 ! 6.3e6 assign (residue 152 and name hn) (residue 151 and name ha) 1.8 0.0 1.7 ! assign (residue 152 and name hn) (residue 151 and name hb#) 1.8 0.0 1.7 ! assign (residue 152 and name hn) (residue 151 and name hg#) 1.8 0.0 3.2 ! 1.63ppm !R assign (residue 152 and name hn) (residue 153 and name hn) 1.8 0.0 1.1 ! 8.2e6 !MED assign (residue 152 and name hn) (residue 149 and name ha) 1.8 0.0 3.2 ! amb - ovlps 151ha assign (residue 152 and name hn) (residue 149 and (name hd1# or name hd2#)) 1.8 0.0 3.2 ! assign (residue 152 and name hn) (residue 150 and name hn) 1.8 0.0 3.2 ! assign (residue 152 and name hn) (residue 154 and name hn) 1.8 0.0 3.2 ! !LONG assign (residue 152 and name hn) (residue 101 and name hb#) 1.8 0.0 4.2 ! v wk !G153 !INTRA assign (residue 153 and name hn) (residue 153 and (name ha1 or name ha2)) 1.8 0.0 0.9 ! 2.9e7 !SEQ assign (residue 153 and name hn) (residue 152 and name hn) 1.8 0.0 1.1 ! 1.2e7 assign (residue 153 and name hn) (residue 152 and (name hb1 or name hb2)) 1.8 0.0 1.7 ! 1.2e7 !R assign (residue 153 and name hn) (residue 154 and name hn) 1.8 0.0 1.1 ! 1.3e7 !MED assign (residue 153 and name hn) (residue 151 and name hn) 1.8 0.0 2.2 ! 4.6e6 assign (residue 153 and name hn) (residue 150 and name ha) 1.8 0.0 3.2 assign (residue 153 and name hn) (residue 151 and name ha) 1.8 0.0 3.2 ! 4.146ppm, both 150 and 151 see wk pks to 153hn !LONG assign (residue 153 and name hn) (residue 101 and name hb#) 1.8 0.0 3.2 ! 101hb sees 7.70ppm assign (residue 153 and (name ha1 or name ha2)) (residue 101 and name hb#) 1.8 0.0 3.2 !F154 !INTRA assign (residue 154 and name hn) (residue 154 and name ha) 1.8 0.0 1.7 ! assign (residue 154 and name hn) (residue 154 and name hd#) 1.8 0.0 1.1 ! !SEQ assign (residue 154 and name hn) (residue 153 and name hn) 1.8 0.0 1.1 ! 9e6 assign (residue 154 and name hn) (residue 153 and (name ha1 or name ha2)) 1.8 0.0 1.7 ! !R assign (residue 154 and name hn) (residue 155 and name hn) 1.8 0.0 3.2 ! !MED assign (residue 154 and name hn) (residue 150 and name hn) 1.8 0.0 3.2 ! !R assign (residue 154 and name hn) (residue 150 and name ha) 1.8 0.0 3.2 ! assign (residue 154 and name hn) (residue 157 and (name hg1# or name hg2#)) 1.8 0.0 3.2 ! !LONG !A assign (residue 154 and name he#) !A ((residue 112 and name he#) or (residue 32 and name hd#)) 1.8 0.0 3.2 ! 2D NOESY, 7.06 ppm, lots choices for 7.06 assign (residue 154 and name hn) (residue 101 and name hb#) 1.8 0.0 3.2 ! assign (residue 154 and name he#) (residue 102 and name hd#) 1.8 0.0 3.2 ! 2dnoesy !K155 !INTRA assign (residue 155 and name hn) (residue 155 and (name hb1 or name hb2)) 1.8 0.0 1.1 !SEQ assign (residue 155 and name hn) (residue 154 and name hn) 1.8 0.0 3.2 ! assign (residue 155 and name hn) (residue 154 and name ha) 1.8 0.0 0.9 ! 1.8e7 assign (residue 155 and name hn) (residue 154 and name hd#) 1.8 0.0 2.2 ! 5.5e6 !R assign (residue 155 and name hn) (residue 156 and name hn) 1.8 0.0 3.2 ! 2e6 !MED assign (residue 155 and name hn) (residue 157 and name hg#) 1.8 0.0 3.2 ! sees both 157hgs, hg' 3.7e6 !LONG assign (residue 155 and name hn) ((residue 153 and name ha#) or (residue 98 and name ha)) 1.8 0.0 3.2 ! !R assign (residue 94 and name hb#) (residue 155 and name hb#) 1.8 0.0 3.2 ! 4D to 94hb !R assign (residue 94 and name hb#) (residue 155 and name hg#) 1.8 0.0 3.2 ! 4D to 94 hb !F156 !INTRA !assign (residue 156 and name hn) (residue 156 and name ha) 1.8 0.0 1.1 ! 1.3e7 !SEQ assign (residue 156 and name hn) (residue 155 and name hn) 1.8 0.0 3.2 ! assign (residue 156 and name hn) (residue 155 and name ha) 1.8 0.0 1.1 ! 1.2e7 assign (residue 156 and name hn) (residue 155 and (name hb1 or name hb2)) 1.8 0.0 1.7 ! !R assign (residue 156 and name hn) (residue 157 and name hn) 1.8 0.0 1.1 ! assign (residue 156 and name hn) (residue 157 and name hg#) 1.8 0.0 3.2 ! 157hgs see it !MED !LONG !R assign (residue 156 and name hd#) (residue 94 and name hb#) 1.8 0.0 1.5 ! 3D, 156hd sees it !R assign (residue 156 and name he#) (residue 94 and name hb#) 1.8 0.0 3.2 ! 3D, 156 he# sees it !SD? assign (residue 156 and name hn) (residue 161 and name hd#) 1.8 0.0 3.2 ! !V157 !INTRA assign (residue 157 and name hn) (residue 157 and name ha) 1.8 0.0 1.7 ! 6.6e6 assign (residue 157 and name hn) (residue 157 and (name hg1# or name hg2#)) 1.8 0.0 1.1 ! 1.5e7 for hg' !SEQ assign (residue 157 and name hn) (residue 156 and name hn) 1.8 0.0 1.1 ! assign (residue 157 and name hn) (residue 156 and name ha) 1.8 0.0 0.9 ! assign (residue 157 and name hn) (residue 156 and name hd#) 1.8 0.0 3.2 ! !A assign (residue 157 and name hn) (residue 158 and name hn) 1.8 0.0 ! ovlps 157hn !MED assign (residue 157 and name hg#) (residue 154 and name ha) 1.8 0.0 3.2 !4d assign (residue 157 and name hg#) (residue 154 and name hb#) 1.8 0.0 1.5 !4d assign (residue 157 and name hn) (residue 155 and name ha) 1.8 0.0 3.2 ! 5.8e6 assign (residue 157 and name hg#) (residue 155 and name ha) 1.8 0.0 3.2 !4d assign (residue 157 and name hn) (residue 155 and name hb#) 1.8 0.0 3.2 ! 1.63 and 1.86ppm assign (residue 157 and name hn) (residue 161 and (name hg2# or name hd#)) 1.8 0.0 3.2 ! 7.9e6, 0.905ppm, only assignemnt that looks close assign (residue 157 and name ha) (residue 161 and (name hg2# or name hd#)) 1.8 0.0 3.2 ! 0.88ppm, only assignemnt that looks close assign ((residue 157 and name hg1#) or (residue 157 and name hg2#)) (residue 161 and name hg2#) 1.8 0.0 3.2 !4d !LONG !R assign (residue 35 and name hd#) !R ((residue 157 and name hg1#) or (residue 157 and name hg2#)) 1.8 0.0 1.5 ! 4d, sees both 157 ch3s assign (residue 157 and name hg#) (residue 35 and name hg1#) 1.8 0.0 3.2 ! 4d to 157hg'' assign (residue 157 and name hg#) (residue 35 and name hg2#) 1.8 0.0 3.2 ! 4d to 157hg'' assign (residue 157 and name hn) ((residue 39 and name ha#) or (residue 158 and name ha#)) 1.8 0.0 3.2 !ha' sees it also assign (residue 157 and (name hg1# or name hg2#)) (residue 149 and name ha) 1.8 0.0 3.2 ! 4d to 157hg' !R assign ((residue 157 and name hg1#) or (residue 157 and name hg2#)) !R ((residue 149 and name hd1#) or (residue 149 and name hd2#)) 1.8 0.0 3.2 ! 4d assign (residue 157 and (name hg1# or name hg2#)) (residue 150 and name hn) 1.8 0.0 3.2 ! 4d to 157hg' assign (residue 157 and (name hg1# or name hg2#)) (residue 150 and name ha) 1.8 0.0 3.2 ! 4d to 157hg' !R assign (residue 150 and name hb#) (residue 157 and (name hg1# or name hg2#)) 1.8 0.0 3.2 ! 4d to 157hg' !R assign (residue 150 and name hg1) (residue 157 and (name hg1# or name hg2#)) 1.8 0.0 3.2 !R assign (residue 150 and name hg2) (residue 157 and (name hg1# or name hg2#)) 1.8 0.0 3.2 ! 4d to 157hg' assign (residue 157 and (name hg1# or name hg2#)) (residue 150 and name he#) 1.8 0.0 3.2 ! 4d to 157hg' !aros in 4d !G158 !INTRA assign (residue 158 and name hn) ((residue 158 and name ha1) or (residue 158 and name ha2)) 1.8 0.0 0.9 ! !SEQ !A assign (residue 158 and name hn) (residue 157 and name hn) 1.8 0.0 ! 157hn ovlps 158hn assign (residue 158 and name hn) (residue 157 and name ha) 1.8 0.0 1.7 ! assign (residue 158 and name hn) (residue 157 and (name hg1# or name hg2#)) 1.8 0.0 3.2 ! 4d to 157hg' !R assign (residue 158 and name hn) (residue 159 and name hn) 1.8 0.0 3.2 ! !MED assign (residue 158 and name hn) (residue 156 and name ha) 1.8 0.0 1.7 ! assign (residue 158 and name hn) (residue 156 and name hn) 1.8 0.0 3.2 ! assign (residue 158 and name hn) (residue 160 and name hn) 1.8 0.0 3.2 ! 160hn sees it also assign (residue 158 and name hn) (residue 161 and name hd#) 1.8 0.0 1.7 ! 1.4e7, 3d to 161hd# assign (residue 158 and name hn) (residue 161 and name hn) 1.8 0.0 3.2 ! 161hn sees it also assign (residue 158 and name hn) (residue 161 and name hg1#) 1.8 0.0 3.2 ! sees both 161hg11 and hg12 !LONG !T159 ! hn signals very weak and ovlp 113hn ! ha or hb wk in 3d c13 noesy !INTRA !SEQ assign (residue 159 and name hg2#) (residue 160 and name ha) 1.8 0.0 3.2 ! !MED !LONG assign (residue 159 and name hg2#) (residue 138 and name ha) 1.8 0.0 3.2 ! 4d assign (residue 159 and name hg2#) (residue 138 and name hb#) 1.8 0.0 3.2 ! 4d !T160 !INTRA assign (residue 160 and name hn) (residue 160 and name ha) 1.8 0.0 1.1 ! assign (residue 160 and name hn) ((residue 160 and name hb) or (residue 159 and name hb)) 1.8 0.0 1.7 ! !SEQ assign (residue 160 and name hn) (residue 159 and name hn) 1.8 0.0 1.7 ! assign (residue 160 and name hn) (residue 159 and name ha) 1.8 0.0 1.7 ! assign (residue 160 and name hn) (residue 161 and name hb) 1.8 0.0 3.2 ! assign (residue 160 and name hn) (residue 161 and name hd#) 1.8 0.0 3.2 ! !MED !R assign (residue 160 and name hn) (residue 158 and name hn) 1.8 0.0 3.2 ! !R assign (residue 160 and name hn) (residue 162 and name hn) 1.8 0.0 3.2 ! !LONG !I161 !INTRA assign (residue 161 and name hn) (residue 161 and name ha) 1.8 0.0 1.7 ! 6e6 assign (residue 161 and name hn) (residue 161 and name hb) 1.8 0.0 1.1 ! 9e6 !SEQ assign (residue 161 and name hn) (residue 160 and name hn) 1.8 0.0 1.7 ! 7.6e6 assign (residue 161 and name hn) (residue 160 and name ha) 1.8 0.0 2.2 ! assign (residue 161 and name hn) (residue 160 and name hb) 1.8 0.0 2.2 ! !R assign (residue 161 and name hn) (residue 162 and name hn) 1.8 0.0 1.7 ! 5.5e6 !MED assign (residue 161 and name hg2#) (residue 157 and name ha) 1.8 0.0 3.2 ! 4d assign (residue 161 and name hd#) (residue 157 and name ha) 1.8 0.0 3.2 ! 4d assign (residue 161 and name hd#) (residue 157 and name hg#) 1.8 0.0 3.2 ! 3d !R assign (residue 161 and name hn) (residue 158 and name hn) 1.8 0.0 3.2 ! !R assign (residue 161 and name hd#) (residue 158 and name hn) 1.8 0.0 1.7 ! 3d assign (residue 161 and name hn) (residue 159 and name ha) 1.8 0.0 3.2 ! !R assign (residue 163 and name hn) (residue 161 and name hn) 1.8 0.0 3.2 ! !LONG assign (residue 161 and name hg2#) (residue 35 and name hd#) 1.8 0.0 3.2 ! 4D assign ((residue 161 and name hg11) or (residue 161 and name hg12)) ((residue 35 and name hd#) or (residue 35 and name hb)) 1.8 0.0 3.2 ! assign (residue 161 and name hd#) ( (residue 41 and (name hb1 or name hb2)) or (residue 162 and name hb#) ) 1.8 0.0 3.2 ! 2.31 ppm, 3D assign (residue 161 and name hd#) (residue 39 and name ha#) 1.8 0.0 3.2 ! 3d for ha'' and 4d for ha' ! 4d assign (residue 161 and name hd#) (residue 41 and name hg#) 1.8 0.0 3.2 ! 4d assign (residue 161 and name hd#) (residue 42 and name ha) 1.8 0.0 3.2 ! 4d, 2.7e6 !R assign (residue 161 and name hd#) (residue 42 and name hb#) 1.8 0.0 1.1 ! 4d, 2.7e6 assign (residue 161 and name hd#) (residue 156 and name ha) 1.8 0.0 3.2 ! assign (residue 161 and name hd#) (residue 156 and name hd#) 1.8 0.0 3.2 ! !A assign (residue 161 and name hd#) (residue 156 and name he#) 1.8 0.0 3.2 ! !C162 !INTRA assign (residue 162 and name hn) (residue 162 and name ha) 1.8 0.0 1.1 ! !SEQ assign (residue 162 and name hn) (residue 161 and name hn) 1.8 0.0 1.1 ! 7.2e6 assign (residue 162 and name hn) (residue 161 and name ha) 1.8 0.0 1.7 ! assign (residue 162 and name hn) (residue 161 and name hb) 1.8 0.0 1.7 ! 7e7 assign (residue 162 and name hn) (residue 161 and (name hg11 or name hg12)) 1.8 0.0 3.2 ! hg1' 6e6 but AMB, hg1'' wkdrohat assign (residue 162 and name hn) (residue 161 and (name hd# or name hg2#)) 1.8 0.0 1.7 ! 1e7 !R assign (residue 162 and name hn) (residue 163 and name hn) 1.8 0.0 1.1 ! 6e6 !MED !R assign (residue 158 and name hn) (residue 162 and name hn) 1.8 0.0 3.2 ! assign (residue 162 and name hn) (residue 159 and name ha) 1.8 0.0 1.7 ! assign (residue 162 and name hn) (residue 160 and name hn) 1.8 0.0 3.2 ! !LONG assign (residue 162 and name hn) (residue 145 and name hd#) 1.8 0.0 3.2 ! assign (residue 162 and name ha) ( (residue 145 and (name hd1# or name hd2#)) or (residue 35 and name hd#) ) 1.8 0.0 3.2 ! !Y163 !dont see hbs in 13c noesy !INTRA assign (residue 163 and name hn) (residue 163 and name ha) 1.8 0.0 0.9 ! 8.6e6 !SEQ assign (residue 163 and name hn) (residue 162 and name hn) 1.8 0.0 1.1 ! med ? 4.8e6 assign (residue 163 and name hn) (residue 162 and name ha) 1.8 0.0 1.7 ! !R assign (residue 163 and name hn) (residue 164 and name hn) 1.8 0.0 ! 6e6 !MED assign (residue 163 and name hn) (residue 160 and name ha) 1.8 0.0 1.7 assign (residue 163 and name hd#) (residue 160 and name ha) 1.8 0.0 3.2 assign (residue 163 and name hn) (residue 161 and name hn) 1.8 0.0 3.2 ! !R assign (residue 163 and name hn) (residue 165 and name hn) 1.8 0.0 3.2 ! !LONG !R assign (residue 163 and name hd#) (residue 135 and name hg2#) 1.8 0.0 3.2 ! !A assign (residue 163 and name hd#) (residue 135 and name hd#) 1.8 0.0 3.2 ! assign (residue 163 and name hd#) ((residue 136 and name ha) or (residue 160 and name ha)) 1.8 0.0 3.2 ! 3.95ppm 2d assign (residue 163 and name hd#) ((residue 136 and (name hd1 or name hd2)) or (residue 138 and name ha)) 1.8 0.0 3.2 ! 3.89ppm 2d assign (residue 163 and name hd#) ((residue 136 and (name hd1 or name hd2)) or (residue 133 and name hb#) or (residue 142 and name ha)) 1.8 0.0 3.2 ! 3.95ppm 2d !R assign (residue 163 and name hd#) (residue 137 and name ha) 1.8 0.0 3.2 ! assign (residue 163 and name he#) (residue 137 and name hb) 1.8 0.0 3.2 ! 2d noesy assign (residue 163 and name hd#) (residue 139 and name hg2#) 1.8 0.0 1.5 ! assign (residue 163 and name hd#) (residue 166 and name he#) 1.8 0.0 3.2 ! assign (residue 163 and name hd#) (residue 172 and (name hg1# or name hg2#)) 1.8 0.0 3.2 ! assign (residue 163 and name he#) (residue 172 and (name hg1# or name hg2#)) 1.8 0.0 3.2 ! !S164 !INTRA assign (residue 164 and name hn) (residue 164 and name ha) 1.8 0.0 0.9 ! assign (residue 164 and name hn) (residue 164 and name hb#) 1.8 0.0 1.7 ! !SEQ assign (residue 164 and name hn) (residue 163 and name hn) 1.8 0.0 1.1 ! assign (residue 164 and name hn) (residue 163 and name ha) 1.8 0.0 3.2 ! assign (residue 164 and name hn) (residue 163 and name hb#) 1.8 0.0 1.7 ! assign (residue 164 and name hn) (residue 165 and name hn) 1.8 0.0 1.1 ! !MED assign (residue 164 and name hn) (residue 160 and name ha) 1.8 0.0 3.2 ! assign (residue 164 and name hn) (residue 161 and name ha) 1.8 0.0 1.7 ! AMB ovlps 164hb' assign (residue 164 and name hn) (residue 161 and name hg2#) 1.8 0.0 3.2 ! assign (residue 164 and name hn) ( (residue 161 and (name hg11 or name hg12)) or (residue 160 and name hg2#) ) 1.8 0.0 3.2 ! assign (residue 164 and name hn) (residue 162 and name hn) 1.8 0.0 3.2 ! !LONG assign (residue 164 and name hn) ( (residue 35 and name hd#) or (residue 149 and (name hd1# or name hd2#)) ) 1.8 0.0 4.2 ! v wk !F165 !INTRA assign (residue 165 and name hn) (residue 165 and name ha) 1.8 0.0 1.7 ! ovlps 162ha assign (residue 165 and name hn) (residue 165 and name hb#) 1.8 0.0 1.7 ! assign (residue 165 and name hn) (residue 165 and name hd#) 1.8 0.0 3.2 ! !SEQ !A assign (residue 165 and name hn) (residue 164 and name hn) 1.8 0.0 1.1 ! assign (residue 165 and name hn) (residue 164 and name ha) 1.8 0.0 3.2 ! assign (residue 165 and name hn) (residue 164 and (name hb1 or name hb2)) 1.8 0.0 1.7 ! !A assign (residue 165 and name hn) (residue 166 and name h) 1.8 0.0 1.1 ! ovlps 165hn !MED assign (residue 165 and name hn) (residue 161 and name ha) 1.8 0.0 3.2 ! amb - ovlps 164hb assign (residue 165 and name hn) (residue 162 and name ha) 1.8 0.0 1.7 ! amb assign (residue 165 and name hn) (residue 163 and name hn) 1.8 0.0 3.2 ! assign (residue 165 and name hd#) (residue 162 and name ha) 1.8 0.0 3.2 ! 2dnoesy assign (residue 165 and name hd#) (residue 168 and name hb#) 1.8 0.0 3.2 ! 2dnoesy and 168 hb sees 6.777 assign (residue 165 and name hd#) ((residue 166 and name ha) or (residue 169 and name hb#)) 1.8 0.0 3.2 ! 2dnoesy and 168 hb sees 6.777 !LONG assign (residue 165 and name hn) (residue 34 and name hg#) 1.8 0.0 3.2 ! 2.73ppm, wk in 500data assign (residue 165 and name hd#) (residue 34 and name hg#) 1.8 0.0 1.7 ! 2.736ppm assign (residue 165 and name hn) (residue 34 and name hg#) 1.8 0.0 3.2 ! 2.08ppm assign (residue 165 and name hd#) (residue 149 and (name hd1# or name hd2#)) 1.8 0.0 3.2 ! 2d noesy assign (residue 165 and name hn) ( (residue 35 and name hd#) or (residue 149 and (name hd1# or name hd2#)) ) 1.8 0.0 3.2 ! assign (residue 165 and name hn) ( (residue 35 and (name hg11 or name hg12)) or (residue 161 and (name hd# or name hg2#)) ) 1.8 0.0 4.2 ! v wk assign (residue 165 and name hd#) (residue 35 and name hd#) 1.8 0.0 3.2 ! 3c13caro, and 35 hd sees it assign (residue 165 and name hd#) (residue 35 and name hg2#) 1.8 0.0 3.2 ! 3c13caro, and 35 hg2 sees it ! assign (residue 165 and name hd#) ! ((residue 172 and name hg1#) or (residue 172 and name hg2#)) 1.8 0.0 3.2 ! 2d noesy, 172 hg' sees 6.795 {****** need to confirm assignments to other 165 aros assign (residue 165 and name he#) (residue 35 and name hg2#) 1.8 0.0 3.2 ! 3c13caro, and 35 hg2 sees it assign (residue 165 and name he#) (residue 148 and name hb#) 1.8 0.0 1.5 ! 3c13caro, and 148 hb sees 7.07 as med assign (residue 165 and name he#) ((residue 149 and name hd1#) or (residue 149 and name hd2#)) 1.8 0.0 1.5 ! 3c13caro, and 149 hd'' sees it *******} !M166 !INTRA !SEQ !A assign (residue 166 and name hn) (residue 1 and name h) 1.8 0.0 1.1 ! ovlps 166 assign (residue 166 and name hn) (residue 166 and name he#) 1.8 0.0 3.2 ! assign (residue 166 and name hn) (residue 167 and name hn) 1.8 0.0 1.1 ! !MED assign (residue 166 and name hn) (residue 162 and name ha) 1.8 0.0 3.2 ! assign (residue 166 and name hn) (residue 163 and name ha) 1.8 0.0 3.2 ! assign (residue 166 and name he#) (residue 163 and name ha) 1.8 0.0 3.2 ! assign (residue 166 and name he#) (residue 163 and name hd#) 1.8 0.0 3.2 assign (residue 166 and name hn) (residue 164 and name hn) 1.8 0.0 3.2 ! !LONG !R assign (residue 120 and name hg#) (residue 166 and name he#) 1.8 0.0 1.5 !4d to hg', 1.62/16.6, 2.9e6 assign (residue 166 and name ha) (residue 171 and name hb#) 1.8 0.0 3.2 ! 0.52ppm, could be 120hg or 145 hds but 171hbs closest 5apr02 !A assign (residue 166 and name he#) (residue 133 and name hb#) 1.8 0.0 3.2 ! assign (residue 166 and name he#) (residue 141 and name ha) 1.8 0.0 3.2 ! !R assign (residue 141 and name hb#) (residue 166 and name he#) 1.8 0.0 1.5 !A assign (residue 166 and name he#) (residue 145 and name hn) 1.8 0.0 3.2 ! !A assign (residue 166 and name he#) (residue 145 and name hg) 1.8 0.0 3.2 ! assign (residue 166 and name he#) (residue 171 and name hb#) 1.8 0.0 3.2 ! assign (residue 166 and name he#) (residue 171 and name hg) 1.8 0.0 3.2 ! assign (residue 166 and name hn) (residue 171 and name hd#) 1.8 0.0 3.2 ! assign (residue 166 and name ha) (residue 171 and name hd#) 1.8 0.0 3.2 ! assign (residue 166 and name hn) (residue 172 and name hg#) 1.8 0.0 3.2 ! assign (residue 166 and name ha) (residue 172 and name hg#) 1.8 0.0 3.2 ! assign (residue 166 and name he#) (residue 172 and name hn) 1.8 0.0 3.2 ! !R assign (residue 166 and name he#) (residue 172 and name hg#) 1.8 0.0 1.5 ! hg' 0.20ppm !Q167 all peaks to HN rel. weak !INTRA assign (residue 167 and name hn) (residue 167 and name ha) 1.8 0.0 0.9 ! 5.4e7 !SEQ assign (residue 167 and name hn) (residue 166 and name hn) 1.8 0.0 1.7 ! 2.9e6 assign (residue 167 and name hn) (residue 166 and name ha) 1.8 0.0 1.7 ! 3e7 !A assign (residue 167 and name hn) (residue 168 and name hn) 1.8 0.0 ! ovlps 167ha !MED assign (residue 167 and name hn) (residue 163 and name hd#) 1.8 0.0 3.2 ! assign (residue 167 and name hn) (residue 164 and name ha) 1.8 0.0 1.7 ! !LONG assign (residue 167 and name hn) ((residue 172 and name hg1#) or (residue 172 and name hg2#)) 1.8 0.0 3.2 !A168 !INTRA assign (residue 168 and name hn) (residue 168 and name ha) 1.8 0.0 0.9 ! 6.7e6 !SEQ !A assign (residue 168 and name hn) (residue 167 and name hn) 1.8 0.0 ! ovlps 168hn assign (residue 168 and name hn) (residue 167 and name ha) 1.8 0.0 1.7 ! assign (residue 168 and name hn) (residue 167 and name hb#) 1.8 0.0 1.7 ! 6.7e6 assign (residue 168 and name hn) (residue 169 and name hn) 1.8 0.0 1.1 ! 6.4e6 !MED assign (residue 168 and name hn) (residue 165 and name ha) 1.8 0.0 3.2 ! assign (residue 168 and name hb#) (residue 165 and name ha) 1.8 0.0 1.5 ! assign (residue 168 and name hn) (residue 164 and name ha) 1.8 0.0 3.2 ! !LONG !A assign (residue 168 and name hn) (residue 31 and name hd#) 1.8 0.0 3.2 !A 31hd' or hd'' not see it !R assign (residue 168 and name hb#) (residue 34 and name he#) 1.8 0.0 1.5 ! 4d, 2.09/16.4 !A assign (residue 168 and name hn) (residue 172 and name hg#) 1.8 0.0 3.2 !C169 ! hn peaks obscured by side chain NH2 !INTRA !SEQ !MED assign (residue 169 and name hb#) (residue 171 and (name hd1# or name hd2#)) 1.8 0.0 3.2 ! 169 hbs see both 171hds !LONG assign (residue 169 and name hb#) (residue 31 and (name hd1# or name hd2#)) 1.8 0.0 1.5 ! 31 hd' sees med !G170 ! nada to the ha's in 13c noesy !INTRA !SEQ assign (residue 170 and name hn) (residue 169 and name hn) 1.8 0.0 1.1 ! !R assign (residue 170 and name hn) (residue 171 and name hn) 1.8 0.0 1.7 ! ovlps 169hn assign (residue 170 and name hn) (residue 171 and name hd#) 1.8 0.0 3.2 ! ovlps 169hn !MED assign (residue 170 and name hn) (residue 168 and name hn) 1.8 0.0 3.2 ! !LONG assign (residue 170 and name hn) (residue 22 and (name ha1 or name ha2)) 1.8 0.0 3.2 ! not sure if 170 sees it bc 171hn ovlps 22hn !R assign (residue 22 and name hn) (residue 170 and name hn) 1.8 0.0 3.2 ! not sure if 170 sees it bc 171hn ovlps 22hn !R assign (residue 25 and name hn) (residue 170 and name hn) 1.8 0.0 3.2 ! 25hn sees it also !L171 !INTRA assign (residue 171 and name hn) (residue 171 and name hg) 1.8 0.0 3.2 ! 3.3e6 assign (residue 171 and name hn) ((residue 171 and name hb1) or (residue 171 and name hb2)) 1.8 0.0 1.7 assign (residue 171 and name hn) (residue 171 and name hg) 1.8 0.0 3.2 ! assign (residue 171 and name hn) ((residue 171 and name hd1#) or (residue 171 and name hd2#)) 1.8 0.0 1.7 assign (residue 171 and name ha) (residue 171 and name hg) 1.8 0.0 1.5 ! !SEQ assign (residue 171 and name hn) (residue 170 and name hn) 1.8 0.0 1.7 ! !R assign (residue 171 and name hn) (residue 172 and name hn) 1.8 0.0 1.1 ! 8.8e6 !MED assign (residue 171 and name hn) ((residue 169 and name hb#) or (residue 166 and name ha)) 1.8 0.0 3.2 ! 2.92ppm assign (residue 171 and name hd#) (residue 169 and name hn) 1.8 0.0 3.2 ! 7.54 to 171hd' !LONG !R assign ((residue 31 and name hd1#) or (residue 31 and name hd2#)) !R ((residue 171 and name hd1#) or (residue 171 and name hd2#)) 1.8 0.0 1.5 ! 4d to 31 hd', and L171 sees 1.15ppm !A assign (residue 171 and name hd#) (residue 113 and name hb#) 1.8 0.0 3.2 ! to hd', 113CB not see it assign ((residue 171 and name hd1#) or (residue 171 and name hd2#)) ((residue 113 and name ha) or (residue 172 and name ha)) 1.8 0.0 3.2 ! to hd' !SD? assign ((residue 171 and (name hd1# or name hd2#)) !SD (residue 116 and name ha) 1.8 0.0 3.2 ! 3.66 171hd' !A assign (residue 171 and name hd#) (residue 116 and name hb) 1.8 0.0 3.2 ! 4d 171hd' assign (residue 171 and name hd#) (residue 116 and name hg#) 1.8 0.0 2.2 !4d to 171hd', med to 116hg' wk 116hg'' assign (residue 171 and name hd#) (residue 117 and name ha) 1.8 0.0 3.2 ! 4d to hd'' !SD? assign (residue 171 and name hn) (residue 120 and (name hg1# or name hg2#)) 1.8 0.0 3.2 ! 0.73ppm 120hg' assign (residue 171 and name ha) (residue 120 and (name hg1# or name hg2#)) 1.8 0.0 3.2 ! 120hg'' assign (residue 171 and (name hd1# or name hd2#)) (residue 169 and name ha) 1.8 0.0 3.2 ! 4.40 to 171hd' assign (residue 171 and (name hd1# or name hd2#)) (residue 120 and (name hg1# or name hg2#)) 1.8 0.0 1.5 ! 4D assign ((residue 171 and name hd1#) or (residue 171 and name hd2#)) (residue 124 and (name hb1 or name hb2)) 1.8 0.0 3.2 ! 1.76 ppm to hd'', 4d sees 1.79/31.7, 124hb' at 1.75/31.7 assign ((residue 171 and name hd1#) or (residue 171 and name hd2#)) ((residue 124 and (name hg1 or name hg2)) or (residue 125 and name hb#)) 1.8 0.0 3.2 ! 2.08ppm to hd' assign (residue 171 and name hd#) (residue 166 and name ha) 1.8 0.0 1.5 ! 4d to hd' assign ((residue 171 and name hd1#) or (residue 171 and name hd2#)) (residue 166 and name he#) 1.8 0.0 3.2 ! 4d to hd'' !V172 !INTRA assign (residue 172 and name hn) (residue 172 and name hb) 1.8 0.0 1.7 ! assign (residue 172 and name hn) (residue 172 and (name hg1# or name hg2#)) 1.8 0.0 1.7 ! assign ((residue 172 and name hg1#) or (residue 172 and name hg2#)) (residue 172 and name ha) 1.8 0.0 3.2 ! 4d to hg' !SEQ assign (residue 172 and name hn) (residue 171 and name hn) 1.8 0.0 1.1 ! assign (residue 172 and name hn) (residue 171 and name ha) 1.8 0.0 3.2 ! 3e6 assign (residue 172 and name hn) (residue 171 and (name hb1 or name hb2)) 1.8 0.0 1.7 ! assign (residue 172 and name hn) (residue 171 and (name hd1# or name hd2#)) 1.8 0.0 3.2 ! !R assign (residue 172 and name hn) (residue 173 and name hn) 1.8 0.0 ! dont see 173hn !MED assign (residue 172 and name hn) ((residue 169 and name hb#) or (residue 166 and name ha)) 1.8 0.0 3.2 ! 2.93ppm !LONG assign ((residue 172 and name hg1#) or (residue 172 and name hg2#)) ((residue 120 and name hg1#) or (residue 120 and name hg2#)) 1.8 0.0 3.2 ! 4d to hg' !R assign (residue 172 and name ha) (residue 125 and name hn) 1.8 0.0 1.7 ! 172ha sees it med assign (residue 172 and name hn) (residue 125 and name hb#) 1.8 0.0 3.2 ! 2.08ppm assign ((residue 172 and name hg1#) or (residue 172 and name hg2#)) (residue 125 and name hb#) 1.8 0.0 0.9 ! 4d to hg' and hg'' assign ((residue 172 and name hg1#) or (residue 172 and name hg2#)) (residue 125 and name hg#) 1.8 0.0 3.2 ! 4d to hg'', both 125hgs in 3d, hg' in 4d assign ((residue 172 and name hg1#) or (residue 172 and name hg2#)) (residue 166 and name he#) 1.8 0.0 1.5 !4d, wk to hg' med to hg'' assign ((residue 172 and name hg1#) or (residue 172 and name hg2#)) (residue 167 and name ha) 1.8 0.0 1.5 !N173 !nada to ha / hbs in 13c noesy !INTRA !ha to hn wk assign (residue 173 and name hn) (residue 173 and (name hb1 or name hb2)) 1.8 0.0 1.7 ! 3.10ppm !SEQ assign (residue 173 and name hn) (residue 172 and name ha) 1.8 0.0 0.7 ! stronger than own ha, 172ha-173hn vs also assign (residue 173 and name hn) (residue 172 and name hb) 1.8 0.0 3.2 ! wk for 173hn - 172hb assign (residue 173 and name hn) (residue 172 and name hg#) 1.8 0.0 1.7 ! !MED !LONG !R assign (residue 125 and name hn) (residue 173 and name hn) 1.8 0.0 3.2 ! assign (residue 173 and name hn) (residue 126 and name hn) 1.8 0.0 3.2 ! assign (residue 173 and name hn) (residue 126 and name ha) 1.8 0.0 1.7 ! 7.6e7 !D174 !INTRA assign (residue 174 and name hn) (residue 174 and name ha) 1.8 0.0 1.7 ! !SEQ ! dont see 173hn assign (residue 174 and name hn) (residue 173 and name ha) 1.8 0.0 0.7 ! 5.8e6, strongest to 174hn !R assign (residue 174 and name hn) (residue 175 and name hn) 1.8 0.0 3.2 ! !MED assign (residue 174 and name hn) ((residue 172 and name hg1#) or (residue 172 and name hg2#)) 1.8 0.0 3.2 ! 0.205 ppm !LONG !R assign (residue 174 and name hn) (residue 127 and name hg2#) 1.8 0.0 3.2 ! wk pk to 127hg# !R assign (residue 127 and name hg2#) (residue 174 and name ha) 1.8 0.0 1.1 ! 4d, 5.34 ppm, 2d noesy also assign (residue 174 and name ha) (residue 135 and name hg2#) 1.8 0.0 3.2 ! assign (residue 174 and name ha) (residue 135 and name hd#) 1.8 0.0 3.2 ! !A assign (residue 174 and name ha) (residue 182 and name hd#) 1.8 0.0 3.2 ! !H175 !nada to ha or hb in 13c noesy !INTRA assign (residue 175 and name hn) (residue 175 and (name hb1 or name hb2)) 1.8 0.0 3.2 ! !SEQ assign (residue 175 and name hn) (residue 174 and name hn) 1.8 0.0 3.2 ! assign (residue 175 and name hn) (residue 174 and name ha) 1.8 0.0 2.2 ! !R assign (residue 175 and name hn) (residue 176 and name hn) 1.8 0.0 3.2 ! assign (residue 175 and name hn) (residue 176 and (name hg1# or name hg2#)) 1.8 0.0 3.2 ! !MED !LONG assign (residue 175 and name hn) (residue 127 and name hg2#) 1.8 0.0 3.2 ! !A assign (residue 175 and name hn) (residue 180 and name ha) 1.8 0.0 3.2 ! assign (residue 175 and name hn) (residue 182 and name hd#) 1.8 0.0 3.2 ! !V176 !INTRA !SEQ !A assign (residue 176 and name hn) (residue 175 and name ha) 1.8 0.0 0.9 ! amb, ovlps h2o assign (residue 176 and name hn) (residue 175 and name hn) 1.8 0.0 3.2 ! !dont see 177hn assign ((residue 176 and name hg1#) or (residue 176 and name hg2#)) ((residue 177 and name hg1#) or (residue 177 and name hg2#)) 1.8 0.0 3.2 ! 3d to hg' !MED assign ((residue 176 and name hg1#) or (residue 176 and name hg2#)) (residue 179 and name hn) 1.8 0.0 1.7 ! 3d to hg'' assign ((residue 176 and name hg1#) or (residue 176 and name hg2#)) (residue 179 and name hb#) 1.8 0.0 3.2 ! !A assign (residue 176 and name hg#) (residue 180 and name hb#) 1.8 0.0 3.2 ! !LONG assign (residue 176 and name hg#) (residue 4 and name ha) 1.8 0.0 3.2 ! 4d to hg'', and C4 sees it assign ((residue 176 and name hg1#) or (residue 176 and name hg2#)) (residue 4 and name hn) 1.8 0 3.2 ! 3d to hg'', C4 may see it ovlped with R3 assign (residue 176 and name ha) (residue 129 and name hb#) 1.8 0.0 3.2 ! assign ((residue 176 and name hg1#) or (residue 176 and name hg2#)) (residue 129 and name hn) 1.8 0.0 3.2 ! 3d to hg'' assign ((residue 176 and name hg1#) or (residue 176 and name hg2#)) (residue 129 and name hb#) 1.8 0.0 3.2 ! 4d assign ((residue 176 and name hg1#) or (residue 176 and name hg2#)) (residue 130 and name ha) 1.8 0.0 3.2 ! 4d to hg' assign ((residue 176 and name hg1#) or (residue 176 and name hg2#)) (residue 130 and name hb) 1.8 0.0 3.2 ! 4d to hg' and hg'' !R assign ((residue 176 and name hg1#) or (residue 176 and name hg2#)) !R ((residue 132 and name hd1#) or (residue 132 and name hd2#)) 1.8 0.0 1.5 ! 4d to hg' !R assign ((residue 176 and name hg1#) or (residue 176 and name hg2#)) !R (residue 135 and name hd#) 1.8 0.0 1.5 ! 4d to hg' assign (residue 176 and name hn) (residue 182 and name hb#) 1.8 0.0 3.2 ! 4d to hg' !V177 unasigned !INTRA !SEQ assign ((residue 177 and name hg1#) or (residue 177 and name hg2#)) (residue 176 and name ha) 1.8 0.0 3.2 ! 4d to hg' !MED !LONG !R assign (residue 177 and name hb) (residue 130 and name ha) 1.8 0.0 3.2 ! !R assign (residue 177 and name hb) (residue 130 and name hg2#) 1.8 0.0 3.2 ! assign ((residue 177 and name hg1#) or (residue 177 and name hg2#)) (residue 128 and name ha) 1.8 0.0 3.2 ! 4d to hg' assign ((residue 177 and name hg1#) or (residue 177 and name hg2#)) (residue 128 and name hb#) 1.8 0.0 3.2 ! 3d to hg' assign ((residue 177 and name hg1#) or (residue 177 and name hg2#)) (residue 128 and name hg#) 1.8 0.0 3.2 ! 3d to hg' assign ((residue 177 and name hg1#) or (residue 177 and name hg2#)) (residue 130 and name ha) 1.8 0.0 1.5 ! 4d to hg'', wk to hg' assign ((residue 177 and name hg1#) or (residue 177 and name hg2#)) (residue 130 and name hb) 1.8 0.0 3.2 ! 4d to hg'' assign (residue 177 and name hg#) (residue 130 and name hg2#) 1.8 0.0 1.5 ! 4d to hg'' assign (residue 177 and (name hg1# or name hg2#)) (residue 182 and name hd#) 1.8 0.0 3.2 ! !R assign (residue 182 and name he#) (residue 177 and name hg1#) 1.8 0.0 3.2 !R assign (residue 182 and name he#) (residue 177 and name hg2#) 1.8 0.0 3.2 ! 3d aro, both V177 hgs see 6.89 assign ((residue 177 and name hg1#) or (residue 177 and name hg2#)) ((residue 183 and name ha) or (residue 132 and name hb)) 1.8 0.0 3.2 ! 4d to hg' !aros to 177hgs - 182he ?? !G178 hn unassigned !INTRA !SEQ !MED !LONG !C179 ! nothing to ha and hbs in 3d noesy !INTRA !SEQ !178hn unassigned !R assign (residue 179 and name hn) (residue 180 and name hn) 1.8 0.0 1.7 ! !MED assign (residue 179 and name hn) (residue 176 and (name hg1# or name hg2#)) 1.8 0.0 1.7 ! assign (residue 179 and name hn) (residue 177 and name ha) 1.8 0.0 3.2 ! assign (residue 179 and name hn) (residue 177 and (name hg1# or name hg2#)) 1.8 0.0 3.2 ! !LONG !C180 ! nothing to ha and hbs in 3d noesy !INTRA !assign (residue 180 and name hn) (residue 180 and name h) 1.8 0.0 1.1 ! !SEQ assign (residue 180 and name hn) (residue 179 and name hn) 1.8 0.0 3.2 ! assign (residue 180 and name hn) (residue 179 and name ha) 1.8 0.0 1.1 ! 1.7e7 !R assign (residue 180 and name hn) (residue 181 and name hn) 1.8 0.0 1.7 ! !MED assign (residue 180 and name hn) (residue 176 and (name hg1# or name hg2#)) 1.8 0.0 3.2 ! !LONG assign (residue 180 and name hn) (residue 1 and name hg#) 1.8 0.0 3.2 ! assign (residue 180 and name hn) (residue 2 and name hg#) 1.8 0.0 3.2 ! assign (residue 180 and name hn) (residue 3 and name ha) 1.8 0.0 3.2 ! !AMB !C181 !INTRA assign (residue 181 and name hn) (residue 181 and name ha) 1.8 0.0 0.9 ! assign (residue 181 and name hn) (residue 181 and name hb#) 1.8 0.0 1.7 !1e7 !SEQ assign (residue 181 and name hn) (residue 180 and name hn) 1.8 0.0 3.2 !4.8e6 assign (residue 181 and name hn) (residue 180 and name ha) 1.8 0.0 1.7 ! assign (residue 181 and name hn) (residue 180 and name hb#) 1.8 0.0 1.5 ! !R assign (residue 181 and name hn) (residue 182 and name hn) 1.8 0.0 1.1 ! !MED assign (residue 181 and name hn) ((residue 184 and name ha#) or (residue 179 and name ha) or (residue 178 and name ha#)) 1.8 0.0 3.2 ! 3.92ppm !LONG !Y182 !INTRA assign (residue 182 and name hn) (residue 182 and (name hb1 or name hb2)) 1.8 0.0 1.1 ! assign (residue 182 and name he#) ((residue 182 and name ha) or (residue 129 and name ha)) 1.8 0.0 3.2 ! 4.25ppm 2d noesy !SEQ assign (residue 182 and name hn) (residue 181 and name hn) 1.8 0.0 1.1 ! assign (residue 182 and name hn) (residue 181 and name ha) 1.8 0.0 1.7 ! !A assign (residue 182 and name he#) (residue 183 and name ha) 1.8 0.0 3.2 ! 4.17ppm 2d noesy !MED assign (residue 182 and name hn) (residue 179 and name hn) 1.8 0.0 3.2 ! assign (residue 182 and name hn) (residue 180 and name hn) 1.8 0.0 3.2 ! !LONG assign (residue 182 and name hd#) (residue 127 and name hg2#) 1.8 0.0 3.2 ! 3d aro, 127 sees 6.87 and 7.07 assign (residue 182 and name he#) (residue 127 and name hg2#) 1.8 0.0 3.2 ! 3d aro, 127 sees 6.87 and 7.07 assign (residue 182 and name he#) (residue 128 and name hg#) 1.8 0.0 3.2 ! 2d and 3d aro assign (residue 182 and name he#) ((residue 128 and name ha) or (residue 176 and name ha)) 1.8 0.0 3.2 ! 4.34ppm 2d noesy assign (residue 182 and name he#) (residue 177 and name ha) 1.8 0.0 2.2 ! vios for med, 2d and 3d aro assign (residue 182 and name he#) (residue 177 and name hb) 1.8 0.0 3.2 ! 2d and 3d aro assign (residue 182 and name he#) (residue 177 and name hg1#) 1.8 0.0 3.2 assign (residue 182 and name he#) (residue 177 and name hg2#) 1.8 0.0 3.2 ! 3d aro, both V177 hgs see 6.89 !P183 !INTRA !SEQ assign (residue 183 and (name hd1 or name hd2)) (residue 182 and name ha) 1.8 0.0 1.5 ! assign (residue 183 and (name hd1 or name hd2)) (residue 182 and name hd#) 1.8 0.0 3.2 ! assign (residue 183 and (name hd1 or name hd2)) (residue 182 and name he#) 1.8 0.0 3.2 ! !MED assign (residue 183 and name ha) (residue 186 and name hn) 1.8 0.0 3.2 ! 186hn sees wk 183ha !LONG !G184 !INTRA assign (residue 184 and name hn) (residue 184 and name ha#) 1.8 0.0 1.1 ! !SEQ assign (residue 184 and name hn) (residue 183 and name ha) 1.8 0.0 1.7 !184hn to 183ha strong also assign (residue 184 and name hn) (residue 183 and name hb#) 1.8 0.0 3.2 ! 5.6e5 to hb'' assign (residue 184 and name hn) (residue 183 and name hg#) 1.8 0.0 3.2 ! 3.4e5 to hg' !R assign (residue 184 and name hn) (residue 185 and name hn) 1.8 0.0 1.1 ! !MED assign (residue 184 and name hn) (residue 182 and name he#) 1.8 0.0 3.2 ! !LONG !N185 !INTRA assign (residue 185 and name hn) (residue 185 and name ha) 1.8 0.0 1.1 ! !SEQ assign (residue 185 and name hn) (residue 184 and name hn) 1.8 0.0 1.7 ! assign (residue 185 and name hn) (residue 184 and name ha#) 1.8 0.0 1.1 ! !A assign (residue 185 and name hn) (residue 186 and name hn) 1.8 0.0 1.7 ! ovlps 185hn !MED assign (residue 185 and name hn) (residue 183 and name ha) 1.8 0.0 3.2 ! !LONG !K186 !INTRA assign (residue 186 and name hn) (residue 186 and name ha) 1.8 0.0 1.1 ! !SEQ assign (residue 186 and name hn) (residue 185 and name ha) 1.8 0.0 1.1 ! assign (residue 186 and name hn) (residue 185 and name hb#) 1.8 0.0 2.2 ! !A assign (residue 186 and name hn) (residue 185 and name hn) 1.8 0.0 ! 185hn ovlps 186 !MED !R assign (residue 186 and name hn) (residue 183 and name ha) 1.8 0.0 3.2 ! assign (residue 186 and name hn) (residue 184 and name ha#) 1.8 0.0 3.2 ! !LONG !P187 !INTRA !SEQ !MED !LONG !AMB
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