BMRB

NMR Restraints Grid

Result table
 (Save to zip file containing files for each block)

image mrblock_id pdb_id bmrb_id cing stage program type subtype subsubtype
441547 2kb2 RC 16037 cing 4-filtered-FRED Wattos check completeness distance


data_2kb2


save_NOE_Completeness
    _NOE_completeness_stats.Sf_category                      NOE_completeness_statistics
    _NOE_completeness_stats.Model_count                      20
    _NOE_completeness_stats.Residue_count                    149
    _NOE_completeness_stats.Total_atom_count                 2425
    _NOE_completeness_stats.Observable_atom_definition       ob_standard
    _NOE_completeness_stats.Observable_atom_count            830
    _NOE_completeness_stats.Use_intra_residue_restraints     no
    _NOE_completeness_stats.Redundancy_threshold_pct         5.0
    _NOE_completeness_stats.Distance_averaging_power         1.00
    _NOE_completeness_stats.Completeness_cutoff              4.00
    _NOE_completeness_stats.Completeness_cumulative_pct      56.7
    _NOE_completeness_stats.Constraint_unexpanded_count      3694
    _NOE_completeness_stats.Constraint_count                 5368
    _NOE_completeness_stats.Constraint_exp_unfiltered_count  3204
    _NOE_completeness_stats.Constraint_exceptional_count     0
    _NOE_completeness_stats.Constraint_nonobservable_count   112
    _NOE_completeness_stats.Constraint_intraresidue_count    1454
    _NOE_completeness_stats.Constraint_surplus_count         755
    _NOE_completeness_stats.Constraint_observed_count        3047
    _NOE_completeness_stats.Constraint_expected_count        2661
    _NOE_completeness_stats.Constraint_matched_count         1510
    _NOE_completeness_stats.Constraint_unmatched_count       1537
    _NOE_completeness_stats.Constraint_exp_nonobs_count      1151
    _NOE_completeness_stats.Details                          
;
A detailed methodology description is available at:
http://nmr.cmbi.ru.nl/~jd/wattos/doc/Wattos/Soup/Constraint/dc_completeness.html

Please note that the contributions in ambiguous restraints are considered
separate 'restraints' for the sets defined below.
The cut off for all statistics except those in the by-shell table is
given below by the above tag: _NOE_completeness_stats.Completeness_cutoff

Description of the tags in this list:
*  1 * Administrative tag
*  2 * Administrative tag
*  3 * Administrative tag
*  4 * Number of models
*  5 * Number of residues
*  6 * Number of atoms
*  7 * Standard set name of observable atom definitions
see: Doreleijers et al., J.Biomol.NMR 14, 123-132 (1999).
*  8 * Observable atom(group)s
*  9 * Include intra residue restraints
*  10 * Surplus threshold for determining redundant restraints
*  11 * Power for averaging the distance over models
*  12 * Up to what distance are NOEs expected
*  13 * Cumulative completeness percentage
*  14 * Number of unexpanded restraints in restraint list.
*  15 * Number of restraints in restraint list.           Set U
*  16 * Expected restraints based on criteria in list.    Set V
Set V differs from set B only if intra residue restraints are analyzed.
*  17 * Exceptional restraints, i.e. with an unknown atom.Set E
*  18 * Not observable NOEs with e.g. hydroxyl Ser HG.    Set O
Even though restraints with these atom types might have been observed they are
excluded from the analysis.
*  19 * Intra-residue restraints if not to be analyzed.   Set I
*  20 * Surplus like double restraints.                   Set S
*  21 * Observed restraints.                              Set A = U - (E u O u I u S)
*  22 * Expected restraints based on criteria as in A.    Set B = V - (I u S)
*  23 * Observed restraints matched to the expected.      Set M = A n B
*  24 * Observed restraints that were not expected.       Set C = A - M
*  25 * Expected restraints that were not observed.       Set D = B - M
*  26 * This tag

Description of the tags in the class table:
*  1 * Class of restraint. Note that 'medium-range' involves (2<=i<=4) contacts.
Possible values are: intraresidue,sequential,medium-range,long-range, and intermolecular.
*  2 * Observed restraints.                              Set A = U - (E u O u I u S)
*  3 * Expected restraints based on criteria as in A.    Set B = V - (I u S)
*  4 * Observed restraints matched to the expected.      Set M = A n B
*  5 * Completeness percentage
*  6 * Standard deviation from the average over the classes.
*  7 * Extra information
*  8 * Administrative tag
*  9 * Administrative tag

Description of the tags in the shell table.
The first row shows the lower limit of the shells requested and
The last row shows the total number of restraints over the shells.
*  1 * Description of the content of the row: edges, shell, or sums.
The value determines the meaning of the values to the nine 'Matched_shell_x' tags among others.
*  2 * Lower limit of shell of expected restraints.
*  3 * Upper limit of shell of expected restraints.
*  4 * Expected restraints based on criteria as in A.    Set B = V - (I u S)
*  5 * Observed restraints matched to the expected.      Set M = A n B
*  6 * Matched restraints with experimental distance in shell 1
*  7 * Matched restraints with experimental distance in shell 2
*  8 * Matched restraints with experimental distance in shell 3
*  9 * Matched restraints with experimental distance in shell 4
*  10 * Matched restraints with experimental distance in shell 5
*  11 * Matched restraints with experimental distance in shell 6
*  12 * Matched restraints with experimental distance in shell 7
*  13 * Matched restraints with experimental distance in shell 8
*  14 * Matched restraints with experimental distance in shell 9
*  15 * Matched restraints overflowing the last shell
*  16 * Completeness percentage for this shell
*  17 * Completeness percentage up to upper limit of this shell
*  18 * Administrative tag
*  19 * Administrative tag

Description of the tags in the residue table:
*  1 * Chain identifier
*  2 * Residue number
*  3 * Residue name
*  4 * Observable atom(group)s for this residue.
*  5 * Observed restraints.                              Set A = U - (E u O u I u S)
*  6 * Expected restraints based on criteria as in A.    Set B = V - (I u S)
*  7 * Observed restraints matched to the expected.      Set M = A n B
*  8 * Completeness percentage
*  9 * Standard deviation from the average over the residues.
*  10 * Extra information
*  11 * Administrative tag
*  12 * Administrative tag
;


    loop_
       _NOE_completeness_class.Type
       _NOE_completeness_class.Constraint_observed_count
       _NOE_completeness_class.Constraint_expected_count
       _NOE_completeness_class.Constraint_matched_count
       _NOE_completeness_class.Completeness_cumulative_pct
       _NOE_completeness_class.Std_dev
       _NOE_completeness_class.Details

       intraresidue      0    0   0    .    . "no intras"   
       sequential      874  739 531 71.9  1.0  >sigma       
       medium-range    708  558 294 52.7 -0.4  .            
       long-range     1465 1364 685 50.2 -0.6  .            
       intermolecular    0    0   0    .    . "no multimer" 
    stop_

    loop_
       _NOE_completeness_shell.Type
       _NOE_completeness_shell.Shell_start
       _NOE_completeness_shell.Shell_end
       _NOE_completeness_shell.Constraint_expected_count
       _NOE_completeness_shell.Constraint_matched_count
       _NOE_completeness_shell.Matched_shell_1
       _NOE_completeness_shell.Matched_shell_2
       _NOE_completeness_shell.Matched_shell_3
       _NOE_completeness_shell.Matched_shell_4
       _NOE_completeness_shell.Matched_shell_5
       _NOE_completeness_shell.Matched_shell_6
       _NOE_completeness_shell.Matched_shell_7
       _NOE_completeness_shell.Matched_shell_8
       _NOE_completeness_shell.Matched_shell_9
       _NOE_completeness_shell.Matched_shell_overflow
       _NOE_completeness_shell.Completeness_shell_pct
       _NOE_completeness_shell.Completeness_cumulative_pct

       edges    .    .     .    . 2.00 2.50 3.00 3.50 4.00 4.50 5.00 5.50 .  .    .    . 
       shell 0.00 2.00   101   80   11   33   25    8    1    2    0    0 .  0 79.2 79.2 
       shell 2.00 2.50   321  249   24   87   75   35   18    6    3    0 .  0 77.6 78.0 
       shell 2.50 3.00   475  326   13   75   96   73   41   22    5    1 .  0 68.6 73.0 
       shell 3.00 3.50   703  386    8   45  114   91   74   31   15    4 .  4 54.9 65.1 
       shell 3.50 4.00  1061  469    1   20   85  137  112   66   37   10 .  1 44.2 56.7 
       shell 4.00 4.50  1698  499    0   16   47  100  141  124   46   22 .  3 29.4 46.1 
       shell 4.50 5.00  2178  350    0    7   28   48   92  101   50   19 .  5 16.1 36.1 
       shell 5.00 5.50  2531  264    0    2   15   49   58   81   32   23 .  4 10.4 28.9 
       shell 5.50 6.00  3064  162    0    1    5   31   41   41   30    9 .  4  5.3 23.0 
       shell 6.00 6.50  3403  127    0    1    1   10   38   38   25   12 .  2  3.7 18.7 
       shell 6.50 7.00  3671   68    0    0    0    3   14   20   20    9 .  2  1.9 15.5 
       shell 7.00 7.50  4120   38    0    0    0    2    6   14   13    2 .  1  0.9 12.9 
       shell 7.50 8.00  4462   16    0    0    1    0    2    7    4    2 .  0  0.4 10.9 
       shell 8.00 8.50  4926    7    0    0    0    0    0    0    2    3 .  2  0.1  9.3 
       shell 8.50 9.00  5247    3    0    0    0    0    0    1    2    0 .  0  0.1  8.0 
       sums     .    . 37961 3044   57  287  492  587  638  554  284  116 . 28    .    . 
    stop_

    loop_
       _NOE_completeness_comp.Entity_assembly_ID
       _NOE_completeness_comp.Comp_index_ID
       _NOE_completeness_comp.Comp_ID
       _NOE_completeness_comp.Obs_atom_count
       _NOE_completeness_comp.Constraint_observed_count
       _NOE_completeness_comp.Constraint_expected_count
       _NOE_completeness_comp.Constraint_matched_count
       _NOE_completeness_comp.Completeness_cumulative_pct
       _NOE_completeness_comp.Std_dev
       _NOE_completeness_comp.Details

       1   1 GLY 3   0  2  0  0.0 -4.1 >sigma 
       1   2 GLU 5   6  6  3 50.0 -0.6 .      
       1   3 PHE 7  18 10  6 60.0  0.1 .      
       1   4 MET 6  26 15 11 73.3  1.0 >sigma 
       1   5 LEU 7  62 49 31 63.3  0.3 .      
       1   6 THR 4  50 46 30 65.2  0.5 .      
       1   7 THR 4  60 36 25 69.4  0.8 .      
       1   8 LEU 7  96 89 50 56.2 -0.2 .      
       1   9 ILE 6 113 87 52 59.8  0.1 .      
       1  10 TYR 6 102 72 38 52.8 -0.4 .      
       1  11 ARG 7  64 55 32 58.2 -0.0 .      
       1  12 SER 4  43 39 24 61.5  0.2 .      
       1  13 GLN 7  50 53 30 56.6 -0.1 .      
       1  14 VAL 5  57 53 28 52.8 -0.4 .      
       1  15 HIS 6  28 29 13 44.8 -1.0 .      
       1  16 PRO 5  25 23 13 56.5 -0.1 .      
       1  17 ASP 4  14 12  9 75.0  1.2 >sigma 
       1  18 ARG 7  16 23 11 47.8 -0.8 .      
       1  19 PRO 5   9 10  7 70.0  0.8 .      
       1  20 PRO 5  13  9  8 88.9  2.1 >sigma 
       1  21 VAL 5  60 57 33 57.9 -0.0 .      
       1  22 ASP 4  22 23 13 56.5 -0.1 .      
       1  23 LEU 7  73 67 39 58.2 -0.0 .      
       1  24 ASP 4  32 16 14 87.5  2.0 >sigma 
       1  25 ALA 3  33 25 20 80.0  1.5 >sigma 
       1  26 LEU 7  61 63 35 55.6 -0.2 .      
       1  27 VAL 5  57 57 29 50.9 -0.5 .      
       1  28 HIS 6  29 22 15 68.2  0.7 .      
       1  29 ARG 7  22 20  8 40.0 -1.3 >sigma 
       1  30 ALA 3  40 25 16 64.0  0.4 .      
       1  31 SER 4  37 30 21 70.0  0.8 .      
       1  32 SER 4  22 14  8 57.1 -0.1 .      
       1  33 LYS 7  24 37 16 43.2 -1.1 >sigma 
       1  34 ASN 6  66 48 36 75.0  1.2 >sigma 
       1  35 LEU 7  41 29 22 75.9  1.2 >sigma 
       1  36 PRO 5  28 23 15 65.2  0.5 .      
       1  37 LEU 7  42 45 20 44.4 -1.0 .      
       1  38 GLY 3  20 11 10 90.9  2.3 >sigma 
       1  39 ILE 6  62 62 34 54.8 -0.3 .      
       1  40 THR 4  38 36 21 58.3 -0.0 .      
       1  41 GLY 3  33 27 21 77.8  1.4 >sigma 
       1  42 ILE 6  61 67 30 44.8 -1.0 .      
       1  43 LEU 7  99 78 48 61.5  0.2 .      
       1  44 LEU 7 101 94 48 51.1 -0.5 .      
       1  45 PHE 7  92 72 42 58.3 -0.0 .      
       1  46 ASN 6  55 41 25 61.0  0.2 .      
       1  47 GLY 3  13 21  7 33.3 -1.8 >sigma 
       1  48 LEU 7  44 40 25 62.5  0.3 .      
       1  49 GLN 7  57 45 30 66.7  0.6 .      
       1  50 PHE 7  99 63 41 65.1  0.5 .      
       1  51 PHE 7 111 79 51 64.6  0.4 .      
       1  52 GLN 7  76 49 34 69.4  0.8 .      
       1  53 VAL 5  57 56 28 50.0 -0.6 .      
       1  54 LEU 7  81 68 38 55.9 -0.2 .      
       1  55 GLU 5  58 36 27 75.0  1.2 >sigma 
       1  56 GLY 3  36 25 16 64.0  0.4 .      
       1  57 THR 4  34 23 17 73.9  1.1 >sigma 
       1  58 GLU 5  39 30 20 66.7  0.6 .      
       1  59 GLU 5  28 19 14 73.7  1.1 >sigma 
       1  60 ALA 3  36 28 15 53.6 -0.3 .      
       1  61 LEU 7  73 77 37 48.1 -0.7 .      
       1  62 GLU 5  36 23 15 65.2  0.5 .      
       1  63 SER 4  22 17 13 76.5  1.3 >sigma 
       1  64 LEU 7  57 58 27 46.6 -0.8 .      
       1  65 PHE 7  96 74 46 62.2  0.3 .      
       1  66 SER 4  31 18 12 66.7  0.6 .      
       1  67 GLU 5  38 25 16 64.0  0.4 .      
       1  68 ILE 6  67 51 28 54.9 -0.3 .      
       1  69 GLN 7  54 34 22 64.7  0.4 .      
       1  70 SER 4  13 11  7 63.6  0.4 .      
       1  71 ASP 4  19 17  9 52.9 -0.4 .      
       1  72 PRO 5   7 10  4 40.0 -1.3 >sigma 
       1  73 ARG 7  28 43 18 41.9 -1.2 >sigma 
       1  74 HIS 6  46 43 21 48.8 -0.7 .      
       1  75 ARG 7  49 50 26 52.0 -0.5 .      
       1  76 ASP 4  25 20 12 60.0  0.1 .      
       1  77 VAL 5  78 54 36 66.7  0.6 .      
       1  78 VAL 5  28 19 11 57.9 -0.0 .      
       1  79 GLU 5  49 32 24 75.0  1.2 >sigma 
       1  80 LEU 7  58 67 29 43.3 -1.1 >sigma 
       1  81 MET 6  81 67 43 64.2  0.4 .      
       1  82 ARG 7  49 51 24 47.1 -0.8 .      
       1  83 ASP 4  44 19 17 89.5  2.2 >sigma 
       1  84 TYR 6  31 20 17 85.0  1.9 >sigma 
       1  85 SER 4  23 21 12 57.1 -0.1 .      
       1  86 ALA 3  19 15 12 80.0  1.5 >sigma 
       1  87 TYR 6  31 28 19 67.9  0.7 .      
       1  88 ARG 7  25 29 16 55.2 -0.2 .      
       1  89 ARG 7  31 25 15 60.0  0.1 .      
       1  90 PHE 7  51 62 29 46.8 -0.8 .      
       1  91 HIS 6  12 13  7 53.8 -0.3 .      
       1  92 GLY 3   7  7  3 42.9 -1.1 >sigma 
       1  93 THR 4  23 23 15 65.2  0.5 .      
       1  94 GLY 3  22 23 15 65.2  0.5 .      
       1  95 MET 6  53 55 28 50.9 -0.5 .      
       1  96 ARG 7  36 41 22 53.7 -0.3 .      
       1  97 ILE 6  74 83 43 51.8 -0.5 .      
       1  98 LEU 7  83 83 36 43.4 -1.1 >sigma 
       1  99 ASP 4  55 30 23 76.7  1.3 >sigma 
       1 100 LEU 7  89 67 33 49.3 -0.6 .      
       1 101 ARG 7  32 26 12 46.2 -0.9 .      
       1 102 LEU 7  43 25 21 84.0  1.8 >sigma 
       1 103 PHE 7  82 58 40 69.0  0.7 .      
       1 104 GLU 5  24 23 12 52.2 -0.4 .      
       1 105 THR 4  28 24 15 62.5  0.3 .      
       1 106 ASP 4  17 18 12 66.7  0.6 .      
       1 107 GLY 3  26 21 13 61.9  0.2 .      
       1 108 ALA 3  58 44 29 65.9  0.5 .      
       1 109 LEU 7  56 69 25 36.2 -1.6 >sigma 
       1 110 GLU 5  28 19 13 68.4  0.7 .      
       1 111 GLU 5  53 40 23 57.5 -0.1 .      
       1 112 ILE 6  46 74 25 33.8 -1.7 >sigma 
       1 113 LEU 7  34 42 21 50.0 -0.6 .      
       1 114 ARG 7  32 17 14 82.4  1.7 >sigma 
       1 115 PHE 7  41 43 20 46.5 -0.8 .      
       1 116 SER 4  25 23 14 60.9  0.2 .      
       1 117 THR 4  10 10  5 50.0 -0.6 .      
       1 118 PHE 7  32 39 18 46.2 -0.9 .      
       1 119 GLY 3  10  6  4 66.7  0.6 .      
       1 120 VAL 5  29 35 18 51.4 -0.5 .      
       1 121 THR 4  10 13  9 69.2  0.8 .      
       1 122 GLU 5  21 29 15 51.7 -0.5 .      
       1 123 PRO 5  18 26 13 50.0 -0.6 .      
       1 124 VAL 5  25 26 15 57.7 -0.1 .      
       1 125 ASN 6  16 18 13 72.2  1.0 .      
       1 126 ASP 4  22 17  9 52.9 -0.4 .      
       1 127 ARG 7  14 18  4 22.2 -2.6 >sigma 
       1 128 MET 6  52 58 25 43.1 -1.1 >sigma 
       1 129 PHE 7  54 50 25 50.0 -0.6 .      
       1 130 ARG 7  31 25 10 40.0 -1.3 >sigma 
       1 131 LEU 7  66 67 31 46.3 -0.9 .      
       1 132 LEU 7  82 91 43 47.3 -0.8 .      
       1 133 SER 4  45 33 18 54.5 -0.3 .      
       1 134 ALA 3  37 18 11 61.1  0.2 .      
       1 135 PHE 7  91 76 48 63.2  0.3 .      
       1 136 ILE 6  70 73 32 43.8 -1.0 >sigma 
       1 137 ALA 3  27 22 15 68.2  0.7 .      
       1 138 ASP 4  24 11  7 63.6  0.4 .      
       1 139 GLY 3  15 14  6 42.9 -1.1 >sigma 
       1 140 GLY 3  13  6  4 66.7  0.6 .      
       1 141 ARG 7  15  8  5 62.5  0.3 .      
       1 142 TYR 6  12 15  8 53.3 -0.4 .      
       1 143 CYS 4   6  8  6 75.0  1.2 >sigma 
       1 144 LEU 7  13 15 10 66.7  0.6 .      
       1 145 PRO 5  11 14 10 71.4  0.9 .      
       1 146 GLU 5  10  9  6 66.7  0.6 .      
       1 147 PRO 5   3  9  3 33.3 -1.8 >sigma 
       1 148 LEU 7   1  3  0  0.0 -4.1 >sigma 
    stop_

save_