*HEADER    DNA                                     05-SEP-03   1QXB              
*TITLE     NMR STRUCTURE DETERMINATION OF THE SELF COMPLEMENTARY DNA             
*TITLE    2 DODECAMER CGCGAATT*CGCG IN WHICH A RIBOSE IS INSERTED                
*TITLE    3 BETWEEN THE 3'-OH OF T8 AND THE 5'-PHOSPHATE GROUP OF C9             
*COMPND    MOL_ID: 1;                                                            
*COMPND   2 MOLECULE: 5'-D(CPGPCPGPAPAPTPTPCPGPCPG)-3';                          
*COMPND   3 CHAIN: A, B;                                                         
*COMPND   4 ENGINEERED: YES                                                      
*SOURCE    MOL_ID: 1;                                                            
*SOURCE   2 SYNTHETIC: YES                                                       
*KEYWDS    DISACCHARIDE NUCLEOTIDE, BACKBONE MODIFICATION, B-HELIX,              
*KEYWDS   2 RIBOSE                                                               
*EXPDTA    NMR, MINIMIZED AVERAGE STRUCTURE                                      
*AUTHOR    K.NAUWELAERTS, K.VASTMANS, M.FROEYEN, V.KEMPENEERS,                   
*AUTHOR   2 J.ROZENSKI, H.ROSEMEYER, A.VAN AERSCHOT, R.BUSSON,                   
*AUTHOR   3 E.EFIMTSEVA, S.MIKHAILOV, E.LESCRINIER, P.HERDEWIJN                  
*REVDAT   1   03-FEB-04 1QXB    0                                                

!H-bridges    distances as noe restraints			

assign (resi    1  and name   N3)    (resi   24  and name   N1)	2.95	0.1	0.1
assign (resi    1  and name   N4)    (resi   24  and name   O6)	2.91	0.1	0.1
assign (resi    1  and name   O2)    (resi   24  and name   N2)	2.86	0.1	0.1
assign (resi    2  and name   N1)    (resi   23  and name   N3)	2.95	0.1	0.1
assign (resi    2  and name   O6)    (resi   23  and name   N4)	2.91	0.1	0.1
assign (resi    2  and name   N2)    (resi   23  and name   O2)	2.86	0.1	0.1
assign (resi    3  and name   N3)    (resi   22  and name   N1)	2.95	0.1	0.1
assign (resi    3  and name   N4)    (resi   22  and name   O6)	2.91	0.1	0.1
assign (resi    3  and name   O2)    (resi   22  and name   N2)	2.86	0.1	0.1
assign (resi    4  and name   N1)    (resi   21  and name   N3)	2.95	0.1	0.1
assign (resi    4  and name   O6)    (resi   21  and name   N4)	2.91	0.1	0.1
assign (resi    4  and name   N2)    (resi   21  and name   O2)	2.86	0.1	0.1
assign (resi    5  and name   N1)    (resi   20  and name   N3)	2.82	0.1	0.1
assign (resi    5  and name   N6)    (resi   20  and name   O4)	2.95	0.1	0.1
assign (resi    6  and name   N1)    (resi   19  and name   N3)	2.82	0.1	0.1
assign (resi    6  and name   N6)    (resi   19  and name   O4)	2.95	0.1	0.1
assign (resi    7  and name   N3)    (resi   18  and name   N1)	2.82	0.1	0.1
assign (resi    7  and name   O4)    (resi   18  and name   N6)	2.95	0.1	0.1
assign (resi    8  and name   N3)    (resi   17  and name   N1)	2.82	0.1	0.1
assign (resi    8  and name   O4)    (resi   17  and name   N6)	2.95	0.1	0.1
assign (resi    9  and name   N3)    (resi   16  and name   N1)	2.95	0.1	0.1
assign (resi    9  and name   N4)    (resi   16  and name   O6)	2.91	0.1	0.1
assign (resi    9  and name   O2)    (resi   16  and name   N2)	2.86	0.1	0.1
assign (resi   10  and name   N1)    (resi   15  and name   N3)	2.95	0.1	0.1
assign (resi   10  and name   O6)    (resi   15  and name   N4)	2.91	0.1	0.1
assign (resi   10  and name   N2)    (resi   15  and name   O2)	2.86	0.1	0.1
assign (resi   11  and name   N3)    (resi   14  and name   N1)	2.95	0.1	0.1
assign (resi   11  and name   N4)    (resi   14  and name   O6)	2.91	0.1	0.1
assign (resi   11  and name   O2)    (resi   14  and name   N2)	2.86	0.1	0.1
assign (resi   12  and name   N1)    (resi   13  and name   N3)	2.95	0.1	0.1
assign (resi   12  and name   O6)    (resi   13  and name   N4)	2.91	0.1	0.1
assign (resi   12  and name   N2)    (resi   13  and name   O2)	2.86	0.1	0.1


!Interresidue restraints			

assign (resi    8  and name   H6)    (resi    7  and name H2'')	3.95	0.8	0.8
assign (resi   20  and name   H6)    (resi   19  and name H2'')	3.87	0.8	0.8
assign (resi    3  and name   H6)    (resi    2  and name H2'')	3.75	0.8	0.8
assign (resi   15  and name   H6)    (resi   14  and name H2'')	3.81	0.8	0.8
assign (resi    3  and name   H6)    (resi    2  and name  H2')	2.15	0.4	0.4
assign (resi    7  and name   H6)    (resi    6  and name  H2')	2.19	0.4	0.4
assign (resi    8  and name   H6)    (resi    7  and name  H2')	2.48	0.5	0.5
assign (resi   11  and name   H6)    (resi   10  and name  H2')	2.02	0.4	0.4
assign (resi   15  and name   H6)    (resi   14  and name  H2')	2.07	0.4	0.4
assign (resi   19  and name   H6)    (resi   18  and name  H2')	2.13	0.4	0.4
assign (resi   20  and name   H6)    (resi   19  and name  H2')	2.44	0.5	0.5
assign (resi   23  and name   H6)    (resi   22  and name  H2')	2.1	0.4	0.4
assign (resi    8  and name   H6)    (resi    7  and name  H3')	4.98	1	1
assign (resi    9  and name   H6)    (resi    8  and name  H3')	4.45	0.9	0.9
assign (resi   20  and name   H6)    (resi   19  and name  H3')	4.97	1	1
assign (resi   21  and name   H6)    (resi   20  and name  H3')	4.6	0.9	0.9
assign (resi    7  and name   H6)    (resi    8  and name  C5A)	4.01	0.8	0.8
assign (resi   19  and name   H6)    (resi   20  and name  C5A)	3.89	0.8	0.8
assign (resi    7  and name   H6)    (resi    6  and name H2'')	3.58	0.7	0.7
assign (resi   11  and name   H6)    (resi   10  and name H2'')	3.51	0.7	0.7
assign (resi   19  and name   H6)    (resi   18  and name H2'')	3.55	0.7	0.7
assign (resi   23  and name   H6)    (resi   22  and name H2'')	3.5	0.7	0.7
assign (resi    4  and name   H8)    (resi    3  and name  H2')	2.44	0.5	0.5
assign (resi    5  and name   H8)    (resi    4  and name  H2')	2.52	0.5	0.5
assign (resi   10  and name   H8)    (resi    9  and name  H2')	2.5	0.5	0.5
assign (resi   16  and name   H8)    (resi   15  and name  H2')	2.46	0.5	0.5
assign (resi   17  and name   H8)    (resi   16  and name  H2')	2.47	0.5	0.5
assign (resi   22  and name   H8)    (resi   21  and name  H2')	2.41	0.5	0.5
assign (resi   10  and name   H8)    (resi    9  and name  H3')	4.67	0.9	0.9
assign (resi   22  and name   H8)    (resi   21  and name  H3')	4.69	0.9	0.9
assign (resi    6  and name   H8)    (resi    7  and name  C5A)	3.93	0.8	0.8
assign (resi   18  and name   H8)    (resi   19  and name  C5A)	3.89	0.8	0.8
assign (resi    2  and name   H8)    (resi    1  and name H2'')	3.02	0.6	0.6
assign (resi    4  and name   H8)    (resi    3  and name H2'')	3.73	0.7	0.7
assign (resi   10  and name   H8)    (resi    9  and name H2'')	3.58	0.7	0.7
assign (resi   12  and name   H8)    (resi   11  and name H2'')	3.31	0.7	0.7
assign (resi   14  and name   H8)    (resi   13  and name H2'')	3.06	0.6	0.6
assign (resi   16  and name   H8)    (resi   15  and name H2'')	3.51	0.7	0.7
assign (resi   22  and name   H8)    (resi   21  and name H2'')	3.37	0.7	0.7
assign (resi   24  and name   H8)    (resi   23  and name H2'')	3.42	0.7	0.7
assign (resi    2  and name  H1')    (resi    3  and name   H6)	3.47	0.7	0.7
assign (resi   10  and name  H1')    (resi   11  and name   H6)	3.3	0.7	0.7
assign (resi   14  and name  H1')    (resi   15  and name   H6)	3.34	0.7	0.7
assign (resi   22  and name  H1')    (resi   23  and name   H6)	3.15	0.6	0.6
assign (resi    4  and name  H1')    (resi    5  and name   H8)	3.37	0.7	0.7
assign (resi   16  and name  H1')    (resi   17  and name   H8)	3.49	0.7	0.7
assign (resi    6  and name  H2')    (resi    7  and name  C5A)	2.99	0.6	0.6
assign (resi    7  and name  H2')    (resi    8  and name  C5A)	3.01	0.6	0.6
assign (resi   18  and name  H2')    (resi   19  and name  C5A)	3.14	0.6	0.6
assign (resi   19  and name  H2')    (resi   20  and name  C5A)	3.05	0.6	0.6
assign (resi    8  and name  C5A)    (resi    7  and name   H6)	3.97	0.8	0.8
assign (resi   20  and name  C5A)    (resi   19  and name   H6)	3.87	0.8	0.8
assign (resi    7  and name  C5A)    (resi    6  and name  H3')	4.83	1	1
assign (resi   19  and name  C5A)    (resi   18  and name  H3')	5.12	1	1
assign (resi    6  and name H2'')    (resi    7  and name  C5A)	3.14	0.6	0.6
assign (resi   18  and name H2'')    (resi   19  and name  C5A)	3.16	0.6	0.6
assign (resi    9  and name H5'')    (resi    8  and name  RH3)	2.73	0.5	0.5
assign (resi   21  and name H5'')    (resi   20  and name  RH3)	2.66	0.5	0.5
assign (resi    3  and name   H5)    (resi    2  and name  H3')	4.87	1	1
assign (resi    9  and name   H5)    (resi    8  and name  H3')	4.96	1	1
assign (resi   11  and name   H5)    (resi   10  and name  H3')	5.14	1	1
assign (resi   15  and name   H5)    (resi   14  and name  H3')	4.93	1	1
assign (resi   21  and name   H5)    (resi   20  and name  H3')	4.81	1	1
assign (resi   23  and name   H5)    (resi   22  and name  H3')	5.29	1.1	1.1
assign (resi    9  and name   H5)    (resi    8  and name  C5A)	3.35	0.7	0.7
assign (resi   21  and name   H5)    (resi   20  and name  C5A)	3.55	0.7	0.7
assign (resi    7  and name   H6)    (resi    8  and name   H6)	5.23	1	1
assign (resi    8  and name   H6)    (resi    9  and name   H6)	4.22	0.8	0.8
assign (resi   19  and name   H6)    (resi   20  and name   H6)	5.42	1.1	1.1
assign (resi   20  and name   H6)    (resi   21  and name   H6)	4.05	0.8	0.8
assign (resi    1  and name   H6)    (resi    2  and name   H8)	4.75	1	1
assign (resi   13  and name   H6)    (resi   14  and name   H8)	4.44	0.9	0.9
assign (resi    3  and name   H6)    (resi    2  and name  H3')	4.94	1	1
assign (resi    7  and name   H6)    (resi    6  and name  H3')	4.68	0.9	0.9
assign (resi   11  and name   H6)    (resi   10  and name  H3')	4.55	0.9	0.9
assign (resi   15  and name   H6)    (resi   14  and name  H3')	4.72	0.9	0.9
assign (resi   19  and name   H6)    (resi   18  and name  H3')	4.83	1	1
assign (resi   23  and name   H6)    (resi   22  and name  H3')	4.86	1	1
assign (resi   12  and name   H8)    (resi   11  and name   H6)	4.76	1	1
assign (resi    6  and name   H8)    (resi    7  and name   H6)	5.09	1	1
assign (resi   24  and name   H8)    (resi   23  and name   H6)	4.73	0.9	0.9
assign (resi   18  and name   H8)    (resi   19  and name   H6)	4.97	1	1
assign (resi    4  and name   H8)    (resi    5  and name   H8)	5.07	1	1
assign (resi   16  and name   H8)    (resi   17  and name   H8)	5.04	1	1
assign (resi    4  and name   H8)    (resi    3  and name  H3')	5.04	1	1
assign (resi    5  and name   H8)    (resi    4  and name  H3')	5.37	1.1	1.1
assign (resi    6  and name   H8)    (resi    5  and name  H4')	5.64	1.1	1.1
assign (resi   18  and name   H8)    (resi   17  and name  H4')	5.85	1.2	1.2
assign (resi    2  and name  H1')    (resi    3  and name   H5)	4.3	0.9	0.9
assign (resi    8  and name  H1')    (resi    9  and name   H5)	4.58	0.9	0.9
assign (resi   10  and name  H1')    (resi   11  and name   H5)	4.52	0.9	0.9
assign (resi   14  and name  H1')    (resi   15  and name   H5)	4.27	0.9	0.9
assign (resi   20  and name  H1')    (resi   21  and name   H5)	4.66	0.9	0.9
assign (resi   22  and name  H1')    (resi   23  and name   H5)	4.51	0.9	0.9
assign (resi    8  and name  H1')    (resi    9  and name   H6)	3.71	0.7	0.7
assign (resi   20  and name  H1')    (resi   21  and name   H6)	3.49	0.7	0.7
assign (resi    5  and name  H1')    (resi    6  and name   H8)	3.55	0.7	0.7
assign (resi   17  and name  H1')    (resi   18  and name   H8)	3.52	0.7	0.7
assign (resi    8  and name  H1')    (resi    9  and name  H1')	5.15	1	1
assign (resi   20  and name  H1')    (resi   21  and name  H1')	5.13	1	1
assign (resi    4  and name  H1')    (resi    5  and name  H4')	4.58	0.9	0.9
assign (resi    5  and name  H1')    (resi    6  and name  H4')	4.88	1	1
assign (resi   16  and name  H1')    (resi   17  and name  H4')	4.7	0.9	0.9
assign (resi   17  and name  H1')    (resi   18  and name  H4')	4.8	1	1
assign (resi    6  and name  H1')    (resi    7  and name  C5A)	4.77	1	1
assign (resi    7  and name  H1')    (resi    8  and name  C5A)	4.91	1	1
assign (resi   18  and name  H1')    (resi   19  and name  C5A)	4.68	0.9	0.9
assign (resi   19  and name  H1')    (resi   20  and name  C5A)	4.72	0.9	0.9
assign (resi    9  and name  H4')    (resi    8  and name  RH3)	4.06	0.8	0.8
assign (resi   21  and name  H4')    (resi   20  and name  RH3)	4.14	0.8	0.8
assign (resi    8  and name  C5A)    (resi    7  and name  H3')	4.93	1	1
assign (resi   20  and name  C5A)    (resi   19  and name  H3')	4.97	1	1



!interstrand noe distances			

assign (resi   19  and name  H1')    (resi    6  and name   H2)	4.96	1	1
assign (resi   20  and name  H1')    (resi    5  and name   H2)	4.69	0.9	0.9
assign (resi   20  and name  H1')    (resi    6  and name   H2)	4.23	0.8	0.8
assign (resi    7  and name  H1')    (resi   18  and name   H2)	4.87	1	1
assign (resi    8  and name  H1')    (resi   17  and name   H2)	4.88	1	1
assign (resi    8  and name  H1')    (resi   18  and name   H2)	4.17	0.8	0.8


  Entry H atom name         Submitted Coord H atom name
    1   1H5*    C   1          H5'         C   1 198.366  40.530 130.168
    2   2H5*    C   1          H5''        C   1 197.379  39.302 129.330
    3    H4*    C   1           H4'        C   1 200.417  39.617 129.307
    4    H3*    C   1           H3'        C   1 198.488  40.995 127.838
    5    H1*    C   1           H1'        C   1 200.359  37.859 126.465
    6   1H4     C   1          H41         C   1 195.292  33.634 125.703
    7   2H4     C   1          H42         C   1 196.612  33.051 124.713
    8    H5     C   1           H5         C   1 195.419  35.648 127.026
    9    H6     C   1           H6         C   1 196.852  37.519 127.705
   10    H5T    C   1           H5T        C   1 198.738  37.757 130.588
   11   2H2*    C   1          H2''        C   1 199.195  39.628 125.543
   12   1H2*    C   1          H2'         C   1 197.701  39.273 126.499
   13   1H5*    G   2          H5'         G   2 202.727  39.776 125.489
   14   2H5*    G   2          H5''        G   2 203.054  41.378 124.774
   15    H4*    G   2           H4'        G   2 203.837  39.560 123.327
   16    H3*    G   2           H3'        G   2 202.126  41.629 122.530
   17    H1*    G   2           H1'        G   2 201.821  37.967 121.338
   18    H8     G   2           H8         G   2 198.948  39.140 123.674
   19    H1     G   2           H1         G   2 198.016  33.546 120.776
   20   1H2     G   2          H21         G   2 201.195  34.080 119.457
   21   2H2     G   2          H22         G   2 199.794  33.034 119.551
   22   2H2*    G   2          H2''        G   2 201.010  40.010 120.589
   23   1H2*    G   2          H2'         G   2 200.198  40.375 122.167
   24   1H5*    C   3          H5'         C   3 203.709  38.213 119.574
   25   2H5*    C   3          H5''        C   3 204.349  39.150 118.198
   26    H4*    C   3           H4'        C   3 203.546  36.935 117.507
   27    H3*    C   3           H3'        C   3 202.763  39.376 116.370
   28    H1*    C   3           H1'        C   3 200.394  36.367 116.930
   29   1H4     C   3          H41         C   3 195.278  37.315 120.545
   30   2H4     C   3          H42         C   3 195.786  38.940 120.955
   31    H5     C   3           H5         C   3 197.850  39.912 120.168
   32    H6     C   3           H6         C   3 199.880  39.519 118.855
   33   2H2*    C   3          H2''        C   3 200.355  38.269 115.603
   34   1H2*    C   3          H2'         C   3 200.537  39.383 117.014
   35   1H5*    G   4          H5'         G   4 201.292  35.019 114.332
   36   2H5*    G   4          H5''        G   4 201.812  35.449 112.681
   37    H4*    G   4           H4'        G   4 199.933  33.915 112.600
   38    H3*    G   4           H3'        G   4 199.918  36.445 111.385
   39    H1*    G   4           H1'        G   4 196.884  34.785 113.058
   40    H8     G   4           H8         G   4 198.073  38.035 114.776
   41    H1     G   4           H1         G   4 192.726  35.537 117.155
   42   1H2     G   4          H21         G   4 192.299  33.596 116.174
   43   2H2     G   4          H22         G   4 193.338  32.926 114.935
   44   2H2*    G   4          H2''        G   4 197.174  36.578 111.594
   45   1H2*    G   4          H2'         G   4 198.294  37.441 112.725
   46   1H5*    A   5          H5'         A   5 196.710  32.835 111.111
   47   2H5*    A   5          H5''        A   5 196.701  32.734 109.330
   48    H4*    A   5           H4'        A   5 194.750  31.629 110.351
   49    H3*    A   5           H3'        A   5 194.672  33.465 108.280
   50    H1*    A   5           H1'        A   5 192.130  33.651 111.271
   51    H8     A   5           H8         A   5 194.781  36.440 110.900
   52   1H6     A   5          H61         A   5 191.889  39.211 115.562
   53   2H6     A   5          H62         A   5 193.166  39.351 114.372
   54    H2     A   5           H2         A   5 189.949  35.194 114.897
   55   2H2*    A   5          H2''        A   5 192.219  34.428 109.105
   56   1H2*    A   5          H2'         A   5 193.777  35.301 109.379
   57   1H5*    A   6          H5'         A   6 190.704  31.377 109.889
   58   2H5*    A   6          H5''        A   6 189.959  30.734 108.401
   59    H4*    A   6           H4'        A   6 188.263  31.166 110.096
   60    H3*    A   6           H3'        A   6 188.203  32.200 107.525
   61    H1*    A   6           H1'        A   6 187.293  34.401 110.645
   62    H8     A   6           H8         A   6 190.493  35.232 108.653
   63   1H6     A   6          H61         A   6 191.686  39.287 110.936
   64   2H6     A   6          H62         A   6 191.018  40.137 112.313
   65    H2     A   6           H2         A   6 187.487  37.715 113.725
   66   2H2*    A   6          H2''        A   6 186.884  34.472 108.374
   67   1H2*    A   6          H2'         A   6 188.646  34.429 107.962
   68   1H5*    T   7          H5'         T   7 184.517  32.816 110.281
   69   2H5*    T   7          H5''        T   7 182.991  32.575 109.387
   70    H4*    T   7           H4'        T   7 182.753  34.275 111.137
   71    H3*    T   7           H3'        T   7 182.182  34.666 108.398
   72   1H2*    T   7          H2'         T   7 183.681  36.343 107.925
   73   2H2*    T   7          H2''        T   7 182.508  37.395 108.811
   74    H1*    T   7           H1'        T   7 183.726  37.328 110.773
   75    H3     T   7           H3         T   7 187.587  39.545 110.412
   76   1H5M    T   7          H51         T   7 188.646  37.569 106.380
   77   2H5M    T   7          H52         T   7 187.012  37.201 105.782
   78   3H5M    T   7          H53         T   7 187.960  35.946 106.614
   79    H6     T   7           H6         T   7 185.537  36.102 107.765
   80   1H5*    T   8          H5'         T   8 180.435  37.609 111.650
   81   2H5*    T   8          H5''        T   8 178.789  38.092 111.162
   82    H4*    T   8           H4'        T   8 180.028  39.838 112.423
   83    H3*    T   8           H3'        T   8 178.621  40.178 109.999
   84   1H2*    T   8          H2'         T   8 180.359  40.708 108.599
   85   2H2*    T   8          H2''        T   8 180.258  42.329 109.393
   86    H1*    T   8           H1'        T   8 182.039  41.906 110.782
   87    H3     T   8           H3         T   8 185.956  41.437 108.684
   88   1H5M    T   8          H51         T   8 182.972  37.698 106.499
   89   2H5M    T   8          H52         T   8 184.242  38.511 105.553
   90   3H5M    T   8          H53         T   8 182.567  39.106 105.488
   91    H6     T   8           H6         T   8 181.646  39.412 108.047
   92   1H5*    C   9          H5'         C   9 179.546  43.854 110.787
   93   2H5*    C   9          H5''        C   9 178.246  44.974 110.304
   94    H4*    C   9           H4'        C   9 180.247  46.156 111.132
   95    H3*    C   9           H3'        C   9 178.892  46.734 108.811
   96    H1*    C   9           H1'        C   9 182.802  46.532 108.817
   97   1H4     C   9          H41         C   9 185.098  42.113 104.892
   98   2H4     C   9          H42         C   9 183.628  41.166 104.994
   99    H5     C   9           H5         C   9 181.734  41.817 106.342
  100    H6     C   9           H6         C   9 180.838  43.532 107.848
  101   2H2*    C   9          H2''        C   9 181.166  47.371 107.417
  102   1H2*    C   9          H2'         C   9 180.340  45.770 107.261
  103   1H5*    G  10          H5'         G  10 183.042  49.423 109.263
  104   2H5*    G  10          H5''        G  10 182.245  51.014 109.163
  105    H4*    G  10           H4'        G  10 184.461  51.063 108.135
  106    H3*    G  10           H3'        G  10 182.077  51.804 106.813
  107    H1*    G  10           H1'        G  10 185.130  50.105 105.228
  108    H8     G  10           H8         G  10 181.917  47.936 105.125
  109    H1     G  10           H1         G  10 186.866  45.599 101.864
  110   1H2     G  10          H21         G  10 188.592  48.335 103.145
  111   2H2     G  10          H22         G  10 188.634  46.900 102.146
  112   2H2*    G  10          H2''        G  10 183.292  51.277 104.387
  113   1H2*    G  10          H2'         G  10 182.103  50.157 105.170
  114   1H5*    C  11          H5'         C  11 186.708  52.730 105.506
  115   2H5*    C  11          H5''        C  11 186.523  54.450 105.067
  116    H4*    C  11           H4'        C  11 188.510  53.383 104.037
  117    H3*    C  11           H3'        C  11 186.650  54.963 102.741
  118    H1*    C  11           H1'        C  11 187.867  51.577 101.135
  119   1H4     C  11          H41         C  11 182.143  48.237 101.433
  120   2H4     C  11          H42         C  11 183.257  47.282 100.476
  121    H5     C  11           H5         C  11 182.735  50.347 102.428
  122    H6     C  11           H6         C  11 184.527  51.986 102.742
  123   2H2*    C  11          H2''        C  11 186.898  53.521 100.396
  124   1H2*    C  11          H2'         C  11 185.493  53.363 101.523
  125   1H5*    G  12          H5'         G  12 190.287  53.099  99.973
  126   2H5*    G  12          H5''        G  12 190.789  54.566  99.090
  127    H4*    G  12           H4'        G  12 191.014  52.527  97.722
  128    H3*    G  12           H3'        G  12 189.742  54.862  96.926
  129    H1*    G  12           H1'        G  12 188.413  51.373  96.108
  130    H8     G  12           H8         G  12 186.119  53.260  98.601
  131    H1     G  12           H1         G  12 183.942  47.585  96.674
  132   1H2     G  12          H21         G  12 185.448  46.612  95.373
  133   2H2     G  12          H22         G  12 186.984  47.360  94.998
  134   2H2*    G  12          H2''        G  12 187.882  53.549  95.420
  135   1H2*    G  12          H2'         G  12 187.528  54.093  97.116
  136   1H5*    C  13          H5'         C  13 179.913  40.541  92.597
  137   2H5*    C  13          H5''        C  13 179.778  41.549  94.063
  138    H4*    C  13           H4'        C  13 181.653  41.924  91.679
  139    H3*    C  13           H3'        C  13 181.893  40.219  93.876
  140    H1*    C  13           H1'        C  13 183.561  43.733  93.722
  141   1H4     C  13          H41         C  13 180.487  46.808  98.738
  142   2H4     C  13          H42         C  13 181.930  47.731  98.374
  143    H5     C  13           H5         C  13 179.881  44.785  97.586
  144    H6     C  13           H6         C  13 180.491  43.238  95.788
  145    H5T    C  13           H5T        C  13 179.306  43.308  92.507
  146   2H2*    C  13          H2''        C  13 183.888  41.802  94.946
  147   1H2*    C  13          H2'         C  13 182.187  41.785  95.562
  148   1H5*    G  14          H5'         G  14 186.125  42.356  92.164
  149   2H5*    G  14          H5''        G  14 187.098  40.859  92.160
  150    H4*    G  14           H4'        G  14 188.451  42.848  92.676
  151    H3*    G  14           H3'        G  14 188.348  40.500  94.192
  152    H1*    G  14           H1'        G  14 188.572  44.051  95.710
  153    H8     G  14           H8         G  14 185.227  42.196  96.358
  154    H1     G  14           H1         G  14 185.967  47.647  99.561
  155   1H2     G  14          H21         G  14 187.863  48.619  98.968
  156   2H2     G  14          H22         G  14 188.943  47.918  97.783
  157   2H2*    G  14          H2''        G  14 188.966  41.899  96.491
  158   1H2*    G  14          H2'         G  14 187.291  41.342  96.085
  159   1H5*    C  15          H5'         C  15 191.052  44.199  95.209
  160   2H5*    C  15          H5''        C  15 192.690  43.543  95.477
  161    H4*    C  15           H4'        C  15 192.282  45.610  96.755
  162    H3*    C  15           H3'        C  15 193.262  43.213  97.802
  163    H1*    C  15           H1'        C  15 190.770  45.506  99.642
  164   1H4     C  15          H41         C  15 185.142  43.126 101.297
  165   2H4     C  15          H42         C  15 185.450  41.628 100.447
  166    H5     C  15           H5         C  15 187.469  41.218  99.188
  167    H6     C  15           H6         C  15 189.606  42.167  98.463
  168   2H2*    C  15          H2''        C  15 192.161  43.750 100.265
  169   1H2*    C  15          H2'         C  15 191.412  42.606  99.079
  170   1H5*    G  16          H5'         G  16 192.962  47.411 100.819
  171   2H5*    G  16          H5''        G  16 194.650  47.180 101.347
  172    H4*    G  16           H4'        G  16 193.312  48.243 103.093
  173    H3*    G  16           H3'        G  16 194.801  45.895 103.459
  174    H1*    G  16           H1'        G  16 191.385  46.605 105.071
  175    H8     G  16           H8         G  16 191.390  43.629 102.605
  176    H1     G  16           H1         G  16 185.883  44.582 105.657
  177   1H2     G  16          H21         G  16 187.453  47.420 106.924
  178   2H2     G  16          H22         G  16 186.009  46.432 106.871
  179   2H2*    G  16          H2''        G  16 193.089  45.058 105.451
  180   1H2*    G  16          H2'         G  16 193.018  44.424 103.756
  181   1H5*    A  17          H5'         A  17 192.168  48.631 106.464
  182   2H5*    A  17          H5''        A  17 193.543  48.968 107.549
  183    H4*    A  17           H4'        A  17 191.382  49.502 108.594
  184    H3*    A  17           H3'        A  17 193.375  47.957 109.730
  185    H1*    A  17           H1'        A  17 189.603  46.853 109.912
  186    H8     A  17           H8         A  17 192.047  44.821 107.704
  187   1H6     A  17          H61         A  17 189.058  41.236 106.516
  188   2H6     A  17          H62         A  17 187.369  40.920 106.850
  189    H2     A  17           H2         A  17 185.874  44.376 109.323
  190   2H2*    A  17          H2''        A  17 191.537  46.397 111.075
  191   1H2*    A  17          H2'         A  17 192.414  45.853 109.591
  192   1H5*    A  18          H5'         A  18 189.358  48.942 112.150
  193   2H5*    A  18          H5''        A  18 189.978  49.550 113.709
  194    H4*    A  18           H4'        A  18 187.770  48.552 113.983
  195    H3*    A  18           H3'        A  18 190.015  47.827 115.441
  196    H1*    A  18           H1'        A  18 187.508  45.152 114.048
  197    H8     A  18           H8         A  18 191.080  45.274 112.588
  198   1H6     A  18          H61         A  18 190.811  41.388 109.779
  199   2H6     A  18          H62         A  18 189.525  40.264 109.396
  200    H2     A  18           H2         A  18 185.890  41.648 111.671
  201   2H2*    A  18          H2''        A  18 189.107  45.235 115.714
  202   1H2*    A  18          H2'         A  18 190.416  45.722 114.564
  203   1H5*    T  19          H5'         T  19 185.862  46.080 116.689
  204   2H5*    T  19          H5''        T  19 185.699  46.082 118.466
  205    H4*    T  19           H4'        T  19 184.524  44.184 117.447
  206    H3*    T  19           H3'        T  19 186.496  43.995 119.460
  207   1H2*    T  19          H2'         T  19 188.073  42.749 118.347
  208   2H2*    T  19          H2''        T  19 186.943  41.373 118.652
  209    H1*    T  19           H1'        T  19 186.036  41.475 116.532
  210    H3     T  19           H3         T  19 188.971  40.231 113.400
  211   1H5M    T  19          H51         T  19 191.855  42.916 116.789
  212   2H5M    T  19          H52         T  19 191.362  44.280 115.764
  213   3H5M    T  19          H53         T  19 192.305  42.947 115.069
  214    H6     T  19           H6         T  19 189.163  43.437 116.970
  215   1H5*    T  20          H5'         T  20 183.605  40.394 118.464
  216   2H5*    T  20          H5''        T  20 183.096  39.711 120.029
  217    H4*    T  20           H4'        T  20 183.111  38.048 118.206
  218    H3*    T  20           H3'        T  20 184.312  37.739 120.723
  219   1H2*    T  20          H2'         T  20 186.529  37.728 120.127
  220   2H2*    T  20          H2''        T  20 186.185  36.026 119.627
  221    H1*    T  20           H1'        T  20 186.042  36.568 117.405
  222    H3     T  20           H3         T  20 189.864  38.032 115.631
  223   1H5M    T  20          H51         T  20 190.622  40.372 119.748
  224   2H5M    T  20          H52         T  20 188.959  40.777 120.219
  225   3H5M    T  20          H53         T  20 189.739  41.640 118.880
  226    H6     T  20           H6         T  20 187.345  39.352 119.500
  227   1H5*    C  21          H5'         C  21 184.956  34.260 119.296
  228   2H5*    C  21          H5''        C  21 184.883  32.974 120.527
  229    H4*    C  21           H4'        C  21 185.567  32.137 118.304
  230    H3*    C  21           H3'        C  21 186.801  31.590 120.704
  231    H1*    C  21           H1'        C  21 188.941  32.577 117.556
  232   1H4     C  21          H41         C  21 191.276  38.373 119.803
  233   2H4     C  21          H42         C  21 192.399  37.798 118.587
  234    H5     C  21           H5         C  21 189.282  37.173 120.429
  235    H6     C  21           H6         C  21 187.956  35.146 120.043
  236   2H2*    C  21          H2''        C  21 189.310  31.539 119.580
  237   1H2*    C  21          H2'         C  21 188.678  32.943 120.526
  238   1H5*    G  22          H5'         G  22 189.342  29.595 117.039
  239   2H5*    G  22          H5''        G  22 189.362  27.911 117.626
  240    H4*    G  22           H4'        G  22 191.463  28.492 116.527
  241    H3*    G  22           H3'        G  22 191.264  27.502 119.162
  242    H1*    G  22           H1'        G  22 193.839  30.012 117.861
  243    H8     G  22           H8         G  22 191.547  31.486 120.619
  244    H1     G  22           H1         G  22 196.267  35.302 118.691
  245   1H2     G  22          H21         G  22 196.938  32.773 116.393
  246   2H2     G  22          H22         G  22 197.377  34.344 117.027
  247   2H2*    G  22          H2''        G  22 193.691  28.667 119.769
  248   1H2*    G  22          H2'         G  22 192.100  29.382 120.261
  249   1H5*    C  23          H5'         C  23 195.306  27.620 116.372
  250   2H5*    C  23          H5''        C  23 195.957  26.003 116.751
  251    H4*    C  23           H4'        C  23 197.679  27.595 115.950
  252    H3*    C  23           H3'        C  23 197.863  25.940 118.161
  253    H1*    C  23           H1'        C  23 198.990  29.697 118.340
  254   1H4     C  23          H41         C  23 195.727  33.216 122.463
  255   2H4     C  23          H42         C  23 194.534  31.957 122.705
  256    H5     C  23           H5         C  23 194.600  29.840 121.542
  257    H6     C  23           H6         C  23 195.823  28.488 119.904
  258   2H2*    C  23          H2''        C  23 199.407  27.776 119.531
  259   1H2*    C  23          H2'         C  23 197.653  27.490 119.873
  260   1H5*    G  24          H5'         G  24 201.929  28.742 117.187
  261   2H5*    G  24          H5''        G  24 203.166  27.482 117.450
  262    H4*    G  24           H4'        G  24 203.904  29.726 118.182
  263    H3*    G  24           H3'        G  24 204.097  27.381 119.652
  264    H1*    G  24           H1'        G  24 203.152  30.744 121.180
  265    H8     G  24           H8         G  24 200.223  28.215 121.291
  266    H1     G  24           H1         G  24 199.099  33.784 124.176
  267   1H2     G  24          H21         G  24 202.236  34.675 122.952
  268   2H2     G  24          H22         G  24 200.825  35.147 123.872
  269    H3T    G  24           H3T        G  24 205.761  28.483 120.716
  270   2H2*    G  24          H2''        G  24 203.709  28.636 122.042
  271   1H2*    G  24          H2'         G  24 202.348  27.820 121.159
  272   1H5*  RIB  25          H5R         T   8 175.410  42.596 108.785
  273   2H5*  RIB  25          H5'R        T   8 175.845  40.866 108.786
  274    H4*  RIB  25           H4R        T   8 174.820  41.441 110.913
  275    H3*  RIB  25           H3R        T   8 176.704  43.705 110.557
  276   *HO3  RIB  25          H3'R        T   8 174.663  43.426 112.512
  277    H2*  RIB  25           H2R        T   8 177.771  43.585 112.631
  278   *HO2  RIB  25          H2'R        T   8 176.814  42.350 114.382
  279    H1*  RIB  25           H1R        T   8 177.915  40.926 113.004
  280   1H5*  RIB  26          H5R         T  20 183.987  34.981 123.857
  281   2H5*  RIB  26          H5'R        T  20 183.849  36.743 123.630
  282    H4*  RIB  26           H4R        T  20 181.711  35.707 123.141
  283    H3*  RIB  26           H3R        T  20 183.557  33.884 121.710
  284   *HO3  RIB  26          H3'R        T  20 180.777  33.559 122.216
  285    H2*  RIB  26           H2R        T  20 182.526  33.912 119.620
  286   *HO2  RIB  26          H2'R        T  20 180.318  34.663 119.395
  287    H1*  RIB  26           H1R        T  20 181.686  36.470 119.455